CN115428980B - Tobacco essence suitable for heating non-combustible tobacco products - Google Patents
Tobacco essence suitable for heating non-combustible tobacco products Download PDFInfo
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- CN115428980B CN115428980B CN202211244847.5A CN202211244847A CN115428980B CN 115428980 B CN115428980 B CN 115428980B CN 202211244847 A CN202211244847 A CN 202211244847A CN 115428980 B CN115428980 B CN 115428980B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/022—Refining
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/025—Recovery by solvent extraction
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Abstract
The invention discloses a tobacco essence suitable for heating non-combustible tobacco products, which comprises the following raw materials in percentage by weight: 3 to 6 percent of Barbary dry tobacco extract, 3 to 5 percent of Quercus salicina wood chip extract, 3 to 5 percent of Virginia cedarwood oil, 3 to 5 percent of ku-ban-xiang oil, 3 to 5 percent of walnut shell extract, 2.4 to 3.6 percent of flavoring agent, 3 to 6 percent of sea cable oil, 2 to 6 percent of sensitive plant oil, 1 to 5 percent of yellow sunflower seed oil, 1 to 3 percent of Lv-kangcheng oil, 3 to 6 percent of German chamomile oil, 3 to 6 percent of Morocco jasmine extract and 45 to 60 percent of cosolvent. The tobacco essence can increase tobacco fragrance, has unique fragrance, has better harmony and permeability, improves comfort, and improves quality defects of insufficient fragrance, poor taste and the like of tobacco products in China, thereby having good practical production significance and economic value; the raw materials are easy to obtain, and the preparation process is simple.
Description
Technical Field
The invention relates to the technical field of essence and tobacco processing, in particular to a tobacco essence suitable for heating non-combustible tobacco products.
Background
At present, with the continuous improvement of the living standard of people, the requirements of consumers on the taste and style of cigarettes are continuously increased.
The tobacco essence is a mixture which is prepared from various spices, has a certain flavor type and can be directly used for flavoring tobacco. The traditional tobacco essence has the conditions of less pure tobacco aroma, insufficient aroma and insufficient alcohol in tobacco product application, is easy to leave dry and astringent taste feeling for consumers, and has unpleasant residual taste.
Disclosure of Invention
In order to overcome the defects in the prior art, the invention aims to provide a novel tobacco essence suitable for heating non-combustible tobacco products, which can increase tobacco fragrance, improve the sense of thickness of the tobacco fragrance and improve the taste of the tobacco products, and solves the problems of less pure tobacco fragrance, insufficient alcohol and taste to be improved of the tobacco products prepared by adopting the traditional tobacco essence.
In order to achieve the above purpose, the present invention adopts the following technical scheme:
the invention provides a tobacco essence suitable for heating non-combustible tobacco products, which comprises the following raw materials in percentage by weight:
according to the invention, a plurality of new raw materials which are not used in the tobacco essence are developed and used, so that the raw material selection of the tobacco essence is greatly broken through, and a proper proportioning amount is obtained through a large number of experiments, so that the tobacco essence with unique fragrance is obtained.
Bardry tobacco extract: endows unique bardry blended tobacco with fragrant smell and has better fragrance durability.
Quercus salicina wood chip extract: has unique and rich smell of Quercus salicina, and has very obvious effects of enriching the tobacco fragrance and improving the plumpness of cigarettes.
Virginia cedar oil: similar to the known red cypress oil or cedar oil, the cedar-wood oil has little cedar-wood alcohol but excellent air potential, is dry and sweet costustoot, is similar to the ethanol ionone, and has paste fragrance from cedar enol. The flavor is rich and mild, the fragrance is durable, the flavor is a better variety in cedar oil, the thickness sense of the tobacco fragrance can be well improved, and the tobacco fragrance is enriched.
Bitter compound balm oil: copaibabassam, a resin from kuibopa, is a viscous secretion produced by trees of the genus balsam grown in south america. The fragrance is sweet and woody, and has obvious effect of improving the intense sense of the fragrance; has anti-inflammatory and antiseptic properties, and is a natural anti-inflammatory agent; it also has sedative effect.
Hu Hetao shell extract: has unique and rich smell of walnut, and can improve the sense of thickness of the tobacco fragrance and enrich the tobacco fragrance.
Sea weed oil: is typically obtained by steam distillation of leaves and spikes of the labiate plant, seaweed (Hyssopus officinalis l.) which is mainly produced in south europe. The seaweed oil has the fragrance of herb and sweet taste, can effectively remove mucus and relieve bronchospasm in the aspect of helping to treat respiratory systems; it can also be used for treating bronchitis, asthma, influenza and cold, and also for promoting wound healing and dissipating bruises on the skin.
Mimosa oil: the mimosa oil has herbal fragrance, and can promote digestion and treat respiratory tract diseases; is also helpful for rejuvenating and delaying aging; has effects in tranquilizing mind, clearing away heat, promoting diuresis, eliminating phlegm, and relieving cough.
Okra seed oil: has musk fragrance, and contains farnesol, malvalactone, decanol, etc. The Huang Kuizi is considered by the traditional Chinese medicine to be suitable for treating heat clearing and detoxifying, pus discharging and granulation promoting, cooling, cough due to lung heat, cystitis, dysentery, constipation, postpartum galactostasis, varicose veins and the like.
Green health brewing oil: oil ofCognac Green it is a light green transparent flowing liquid, has fruit fragrance, herb fragrance and grape wine fragrance, has fresh natural smell, has strong fragrance and good diffusivity, and has good durability, and can be prepared by steam distilling grape paste or squeezing.
Germany chamomile oil: german chamomile, also known as Matricaria chamomilla (school name: matricaria chamomiluk/matricaria recutita), belongs to the class of Matricaria chamomilla, is distributed in Asia, europe and Xinjiang, etc. in China, and is produced in Egypt, french, germany and Morocco at present, and has a slightly sweet fragrance Xin Liaowei which is softer than that of Roma chamomile, and can be used for preparing perfume and essential oil. The essential oil is prepared by a steam distillation method, has dark blue appearance, has strong fragrance and sweetness, medium volatility and medium intensity. Clinical findings that it can prevent allergy, resist bacterial, fungal, viral infections; has antiinflammatory, sweating, pathogenic wind expelling, and spasmolytic effects, and can be used for treating inflammation and ulcer (especially ulcer of digestive system); the diluted essential oil has effects of promoting cell regeneration, promoting stem cell regeneration, sterilizing, reducing intestinal gas and inhibiting fungi, etc. for wound, herpes and infection; meanwhile, the health-care food has good effects in the aspects of improving sleep, eliminating pressure, relieving restlessness, relaxing mood and the like. Matricaria chamomilla has been regarded from ancient times as herb with excellent sedative and soothing effects.
Morocco jasmine extract: methyl anthranilate and indole are two major nitrogen-containing aromatic molecules important in jasmine of morocco. The jasmine extract prepared from the jasmine of morocco is fragrant and attractive, is beneficial to soothing nerves, can sooth emotion, can enhance self-confidence and has a special emotion regulating effect.
One preferable technical scheme provides a tobacco essence suitable for heating non-combustible tobacco products, which comprises the following raw materials in percentage by weight:
further, the tobacco essence suitable for heating non-combustible tobacco products is obtained by adopting the following preparation method:
(1) Weighing the raw materials according to the proportion;
(2) Firstly, adding the bardry tobacco extract, the Quercus salicina wood chip extract, the Virginia cypress oil, the copaiba balsam oil and the walnut shell extract into a stirring kettle, adding three fifths of cosolvent, and stirring and mixing for 15-20 min at a rotating speed of 300-500 r/min;
(3) Then adding the seaweed oil, the mimosa oil, the okra seed oil, the Lv-kang Ke oil, the German chamomile oil, the Morocco jasmine extract, the flavoring agent and the rest two fifths of cosolvent, and stirring and mixing for 25-30 min at the rotating speed of 400-600 r/min;
(4) Standing for 10-20 min at room temperature, taking out, packaging and storing.
As one of the technical schemes, hu Hetao shell extract is prepared by the following operations: selecting walnut shell, crushing and grinding the walnut shell to obtain walnut shell powder with the particle size of 1.2-1.5 mm, and then mixing the walnut shell powder with the particle size of 1:8, soaking the mixture in boiling water for 90-120 min by ultrasonic extraction with the ultrasonic frequency of 45-50 KHz, filtering the extract by a filter membrane with the aperture of 1.0 mu m after ultrasonic extraction to obtain filtrate, and concentrating the filtrate to obtain the concentrated solution of one tenth of the residues, namely the walnut shell extract.
One preferred technical scheme is that the flavoring agent is prepared from Spirachikungunya oil and Spirachikungunya oil according to a ratio of 2:1 weight ratio.
Spiransland cassia oil: has the same spicy and hot flavor as cinnamon and clove, and has the characteristics of strong and thick warm spicy flavor and strong lasting diffusion.
Spearmint oil of scotland: spearmint is a plant of the genus mentha, which is crossed by spearmint and spearmint (spearmint in the united states), and is commonly known in north america as spearmint. The aroma of spearmint oil can be described as strong, spicy, with some slight tea aroma.
The spearmint oil and the spearmint oil are added in a compounding mode according to a specific proportion, so that the smoke flavor can be well improved, the odor absorption can be corrected, and the fragrance is durable and lasting.
As one of the technical schemes, the morocco jasmine extractum is prepared by the following operations: firstly, cutting freshly picked jasmine flowers of Morocco into crushed materials, and then carrying out vacuum freeze drying on the crushed materials for 2-4 hours at the temperature of minus 30 ℃ to minus 10 ℃ and the vacuum degree of minus 0.06 to minus 0.08MPa to obtain frozen materials; grinding the frozen material to 5-10 meshes to obtain the jasmine flower powder of Morocco; then according to the powder ratio of 1: 5-8, adding an extractant into the jasmine powder material of morocco, standing and extracting for 12-24 hours at normal temperature, wherein the extraction pressure is 0.4MPa, and filtering to obtain an extract; and finally, concentrating the obtained extract liquid at low temperature under reduced pressure, and evaporating and recovering the extractant to obtain the jasmine extract of Morocco.
In one preferred embodiment, the extractant is an aqueous 95% ethanol solution.
One of the preferred technical schemes is that the conditions of reduced pressure and low temperature concentration are 0.06MPa and 25 ℃.
In one preferable technical scheme, the density of the jasmine extract in Morocco is 1.05-1.2.
As one of the technical schemes, the cosolvent is prepared from propylene glycol and edible ethanol according to the proportion of 3-7: 1. is prepared by the weight ratio of (1). Through the cosolvent with the special proportion, various raw materials can be fully dissolved, and the efficacy of the cosolvent can be better exerted.
One of the preferable technical proposal is that the cosolvent is prepared from propylene glycol and edible ethanol according to the proportion of 4: 1. is prepared by the weight ratio of (1).
Compared with the prior art, the invention provides the tobacco essence suitable for heating the non-combustible tobacco products, which has the following beneficial effects:
(1) According to the invention, the Quercus salicina wood chip extract, the Virginia cedarwood oil, the KU BA XIANG ZHI YOU, the Hu walnut shell extract and the Baer dry tobacco extract are compounded to be used as the bottom aroma to endow intense costustoot smell, so that the tobacco aroma is increased, the thick sense of the tobacco aroma is promoted, and the aroma is ensured to have better persistence.
(2) According to the invention, the sea weed oil, the mimosa oil and the okra seed oil are compounded to provide strong herbal fragrance as the top fragrance, so that the invention has a good fragrance enhancing effect, has the efficacy of treating respiratory diseases such as cough and the like, and is beneficial to relieving the symptoms of smokers such as cough patients.
(3) The added Lv kang brewing gram oil has fruit fragrance, herb fragrance and grape wine fragrance, has fresh natural smell, strong fragrance diffusivity, good durability; the German chamomile oil has strong aroma and sweetness, moderate volatility and medium intensity, and has better effects in the aspects of improving sleep, eliminating pressure, being uneasy, relaxing mood and the like; the jasmine extract of morocco is fragrant and attractive, is helpful for soothing nerves, enables emotion to be soothing, can enhance self-confidence, and has a special emotion regulating effect; the green health brewing oil, the German chamomile oil and the Morocco jasmine extract with specific proportions are added to give strong flower fragrance and fruit fragrance as surface fragrance, so that the tobacco fragrance can be improved, the natural sweet fragrance of tobacco can be increased, and the dry, astringent and bitter mouthfeel of consumers can be improved.
(4) The tobacco essence is prepared by setting various natural plant raw materials in reasonable proportion, the aroma quantity is increased when the tobacco essence is added into tobacco products for sucking, the tobacco essence has unique aroma, has good harmony and permeability, improves the comfort level, improves the quality defects of insufficient aroma, poor taste and the like of the tobacco products in China to a certain extent, and has good practical production significance and economic value.
(5) The tobacco essence has the advantages of easily obtained raw materials, easy preparation and processing, compliance with international and national laws and regulations and relevant regulations, and simple preparation process.
Detailed Description
The following description of the present invention will be made clearly and fully, and it is apparent that the embodiments described are only some, but not all, of the embodiments of the present invention. All other embodiments, which can be made by those skilled in the art based on the embodiments of the invention without making any inventive effort, are intended to be within the scope of the invention.
The invention provides a tobacco essence suitable for heating non-combustible tobacco products, which comprises the following raw materials in percentage by weight:
3 to 6 percent of Barbary dry tobacco extract, 3 to 5 percent of Quercus salicina wood chip extract, 3 to 5 percent of Virginia cedarwood oil, 3 to 5 percent of ku-ban-xiang oil, 3 to 5 percent of walnut shell extract, 2.4 to 3.6 percent of flavoring agent, 3 to 6 percent of sea cable oil, 2 to 6 percent of sensitive plant oil, 1 to 5 percent of yellow sunflower seed oil, 1 to 3 percent of Lv-kangcheng oil, 3 to 6 percent of German chamomile oil, 3 to 6 percent of Morocco jasmine extract and 45 to 60 percent of cosolvent.
The tobacco essence is prepared by the following steps:
(1) Weighing the raw materials according to the proportion;
(2) Firstly, adding the bardry tobacco extract, the Quercus salicina wood chip extract, the Virginia cypress oil, the copaiba balsam oil and the walnut shell extract into a stirring kettle, adding three fifths of cosolvent, and stirring and mixing for 15-20 min at a rotating speed of 300-500 r/min;
(3) Then adding the seaweed oil, the mimosa oil, the okra seed oil, the Lv-kang Ke oil, the German chamomile oil, the Morocco jasmine extract, the flavoring agent and the rest two fifths of cosolvent, and stirring and mixing for 25-30 min at the rotating speed of 400-600 r/min;
(4) Standing for 10-20 min at room temperature, taking out, packaging and storing.
Wherein the Hu Hetao shell extract is prepared by the following steps: selecting walnut shell, crushing and grinding the walnut shell to obtain walnut shell powder with the particle size of 1.2-1.5 mm, and then mixing the walnut shell powder with the particle size of 1:8, soaking the mixture in boiling water for 90-120 min by ultrasonic extraction with the ultrasonic frequency of 45-50 KHz, filtering the extract by a filter membrane with the aperture of 1.0 mu m after ultrasonic extraction to obtain filtrate, and concentrating the filtrate to obtain the concentrated solution of one tenth of the residues, namely the walnut shell extract.
The jasmine extract of Morocco is prepared by the following steps: firstly, cutting freshly picked jasmine flowers of Morocco into crushed materials, and then carrying out vacuum freeze drying on the crushed materials for 2-4 hours at the temperature of minus 30 ℃ to minus 10 ℃ and the vacuum degree of minus 0.06 to minus 0.08MPa to obtain frozen materials; grinding the frozen material to 5-10 meshes to obtain the jasmine flower powder of Morocco; then according to the powder ratio of 1: 5-8, adding an extractant into the morocco jasmine pollen material, wherein the extractant adopts an ethanol water solution with the concentration of 95 percent, and standing and extracting for 12-24 hours at normal temperature, and the extraction pressure is 0.4MPa; filtering to obtain extract; and finally, concentrating the obtained extract liquid at a low temperature under a reduced pressure, and evaporating and recovering the extractant to obtain the Morocco jasmine extract with the density of 1.05-1.2, wherein the condition of the low temperature concentration under the reduced pressure is 0.06MPa and the temperature is 25 ℃.
The flavoring agent is prepared from Spirac cassia bark oil and Scotland spearmint oil according to the weight ratio of 2:1 weight ratio. The spearmint oil and spearmint oil are commercially available.
The cosolvent is prepared from propylene glycol and edible ethanol according to the proportion of 3-7: 1 weight ratio. Propylene glycol and edible ethanol are commercially available.
Other raw materials not specifically described are commercially available.
The present invention will be described in further detail by the following examples.
Example 1
The embodiment provides a tobacco essence suitable for heating non-combustible tobacco products, which comprises the following raw materials in percentage by weight: 4% of Barbary dry tobacco extract, 4% of Quercus salicina wood chip extract, 4% of Virginia cedarwood oil, 4% of copaiba oil, 4% of walnut shell extract, 2% of Spearmint oil, 1% of Spearmint oil, 5% of sea cable herb oil, 4% of sensitive plant oil, 4% of yellow sunflower seed oil, 2% of Lvkangchen oil, 5% of German chamomile oil, 5% of Morocco jasmine extract, 41.6% of propylene glycol and 10.4% of edible ethanol.
Wherein the Hu Hetao shell extract is prepared by the following steps: selecting clean walnut shells, crushing and grinding the clean walnut shells to walnut shell powder with the particle size of 1.2-1.5 mm by using an ultrafine grinder, and then mixing the walnut shell powder with the particle size of 1:8, soaking the mixture in boiling water, performing ultrasonic extraction for 120min at an ultrasonic frequency of 45-50 KHz, filtering the extract with a filter membrane with a pore diameter of 1.0 μm to obtain a filtrate, and concentrating the filtrate to obtain a concentrate of one tenth of the residues, namely the walnut shell extract.
The jasmine extract of Morocco is prepared by the following steps: firstly, shearing freshly picked jasmine flowers of Morocco into crushed aggregates by using an aggregate crusher, and then vacuum freeze-drying the crushed aggregates for 3 hours by using a vacuum freeze dryer under the conditions of the temperature of minus 30 ℃ to minus 10 ℃ and the vacuum degree of minus 0.06 to minus 0.08MPa to obtain frozen materials; grinding the frozen material to 5-10 meshes by using an ultrafine grinder to obtain Morocco jasmine powder; then according to the powder ratio of 1:6, adding an extractant into the morocco jasmine powder, wherein the extractant adopts an ethanol water solution with the concentration of 95 percent, and standing and extracting for 18 hours in an extraction kettle at normal temperature, and the extraction pressure is 0.4MPa; filtering to obtain extract; and finally, concentrating the obtained extract liquid at a low temperature under a reduced pressure, and evaporating and recovering the extractant to obtain the Morocco jasmine extract with the density of 1.05-1.2, wherein the condition of the low temperature concentration under the reduced pressure is 0.06MPa and the temperature is 25 ℃.
The tobacco essence of the embodiment is obtained by adopting the following preparation method:
(1) Weighing the raw materials according to the proportion;
(2) Firstly, adding the bardry tobacco extract, the white oak chip extract, the virginia cypress oil, the copaiba balsam oil and the walnut shell extract into a stirring kettle, and adding three fifths of the components with the weight ratio of 4:1, propylene glycol and edible ethanol are mixed for 18min at a rotating speed of 400 r/min;
(3) Then adding the seaweed oil, the mimosa oil, the okra seed oil, the Lv-kang Ke oil, the German chamomile oil, the Morocco jasmine extract, the Spiranskia cinquefoil oil, the Spiranskia Spica oil and the rest two fifths of cosolvent, and stirring and mixing for 30min at a rotating speed of 500 r/min;
(4) Standing at room temperature for 15min, taking out, packaging, and storing.
Example 2
The embodiment provides a tobacco essence suitable for heating non-combustible tobacco products, which is different from embodiment 1 in that the tobacco essence comprises the following raw materials in percentage by weight: 4% of Barbary dry tobacco extract, 4% of Quercus salicina wood chip extract, 4% of Virginia cedarwood oil, 4% of copaiba oil, 4% of walnut shell extract, 2% of Spearmint oil, 1% of Spearmint oil, 6% of sea cable oil, 5% of mimosa oil, 1% of yellow sunflower seed oil, 2% of Lvkangchen oil, 5% of German chamomile oil, 5% of Morocco jasmine extract, 42.4% of propylene glycol and 10.6% of edible ethanol.
The preparation method of Hu Hetao shell extract, morocco jasmine extract and tobacco essence of this example is the same as that of example 1.
Example 3
The embodiment provides a tobacco essence suitable for heating non-combustible tobacco products, which is different from embodiment 1 in that the tobacco essence comprises the following raw materials in percentage by weight: 4% of Barbary dry tobacco extract, 4% of Quercus salicina wood chip extract, 4% of Virginia cedarwood oil, 4% of copaiba oil, 4% of walnut shell extract, 2% of Spearmint oil, 1% of Spearmint oil, 3% of sea cable oil, 2% of mimosa oil, 1% of yellow sunflower seed oil, 2% of Lvkangchen oil, 5% of German chamomile oil, 5% of Morocco jasmine extract, 47.2% of propylene glycol and 11.8% of edible ethanol.
The preparation method of Hu Hetao shell extract, morocco jasmine extract and tobacco essence of this example is the same as that of example 1.
Example 4
The embodiment provides a tobacco essence suitable for heating non-combustible tobacco products, which is different from embodiment 1 in that the tobacco essence comprises the following raw materials in percentage by weight: 6% of Barbary dry tobacco extract, 5% of Quercus salicina wood chip extract, 5% of Virginia cedarwood oil, 5% of copaiba oil, 5% of walnut shell extract, 2% of Spearmint oil, 1% of Spearmint oil, 5% of sea cable herb oil, 4% of sensitive plant oil, 4% of yellow sunflower seed oil, 2% of Lvkangchen oil, 5% of German chamomile oil, 5% of Morocco jasmine extract, 36.8% of propylene glycol and 9.2% of edible ethanol.
The preparation method of Hu Hetao shell extract, morocco jasmine extract and tobacco essence of this example is the same as that of example 1.
Example 5
The embodiment provides a tobacco essence suitable for heating non-combustible tobacco products, which is different from embodiment 1 in that the tobacco essence comprises the following raw materials in percentage by weight: 3% of Barbary dry tobacco extract, 3% of Quercus salicina wood chip extract, 3% of Virginia cedarwood oil, 3% of copaiba oil, 3% of walnut shell extract, 2% of Spearmint oil, 1% of Spearmint oil, 5% of sea cable herb oil, 4% of sensitive plant oil, 4% of yellow sunflower seed oil, 2% of Lvkangchen oil, 5% of German chamomile oil, 5% of Morocco jasmine extract, 45.6% of propylene glycol and 11.4% of edible ethanol.
The preparation method of Hu Hetao shell extract, morocco jasmine extract and tobacco essence of this example is the same as that of example 1.
Example 6
The embodiment provides a tobacco essence suitable for heating non-combustible tobacco products, which is different from embodiment 1 in that the tobacco essence comprises the following raw materials in percentage by weight: 3% of Balldry tobacco extract, 3% of Quercus salicina wood chip extract, 5% of Virginia cedarwood oil, 5% of copaiba oil, 3% of walnut shell extract, 1.6% of Spearmint oil, 0.8% of Spearmint oil, 4% of sea cable grass oil, 3% of mimosa oil, 5% of okra seed oil, 1% of Lvkangchen oil, 6% of German chamomile oil, 3% of Morocco jasmine extract, 42.45% of propylene glycol and 14.15% of edible ethanol.
The preparation method of Hu Hetao shell extract, morocco jasmine extract and tobacco essence of this example is the same as that of example 1.
Example 7
The embodiment provides a tobacco essence suitable for heating non-combustible tobacco products, which is different from embodiment 1 in that the tobacco essence comprises the following raw materials in percentage by weight: 6% of Balldry tobacco extract, 5% of Quercus salicina wood chip extract, 3% of Virginia cedarwood oil, 3% of copaiba oil, 5% of walnut shell extract, 2.4% of Spearmint oil, 1.2% of Scotch spearmint oil, 6% of sea cable grass oil, 6% of mimosa oil, 2% of okra seed oil, 3% of Lvkangchen oil, 3% of German chamomile oil, 6% of Morocco jasmine extract, 42.35% of propylene glycol and 6.05% of edible ethanol.
The preparation method of Hu Hetao shell extract, morocco jasmine extract and tobacco essence of this example is the same as that of example 1.
Comparative example 1
The comparative example provides essence for cigarettes, which comprises the following raw materials in percentage by weight: 4% of bardry tobacco extract, 4% of Quercus salicina wood chip extract, 4% of Virginia cedarwood oil, 4% of copaiba oil, 4% of walnut shell extract, 2% of Spearmint oil, 1% of Spearmint oil, 61.6% of propylene glycol and 15.4% of edible ethanol.
Wherein Hu Hetao shell extract was prepared in the same manner as in example 1.
The tobacco essence of the comparative example is obtained by adopting the following preparation method:
(1) Weighing the raw materials according to the proportion;
(2) Firstly, adding the bardry tobacco extract, the white oak chip extract, the virginia cypress oil, the copaiba balsam oil and the walnut shell extract into a stirring kettle, and adding three fifths of the components with the weight ratio of 4:1, propylene glycol and edible ethanol are mixed for 18min at a rotating speed of 400 r/min;
(3) Then adding Spirachica cassia bark oil, spirachica spearmint oil and the rest two fifths of cosolvent, stirring and mixing for 30min at a rotating speed of 500 r/min;
(4) Standing at room temperature for 15min, taking out, packaging, and storing.
Comparative example 2
The comparative example provides essence for cigarettes, which comprises the following raw materials in percentage by weight: 4% of Balldry tobacco extract, 4% of Quercus salicina wood chip extract, 4% of Virginia cedarwood oil, 4% of copaiba oil, 4% of walnut shell extract, 2% of Spearmint oil, 1% of Spearmint oil, 2% of Lvkangcheng oil, 5% of German chamomile oil, 5% of Morocco jasmine extract, 52% of propylene glycol and 13% of edible ethanol.
Wherein Hu Hetao shell extract and jasmine extract were prepared in the same manner as in example 1.
The tobacco essence of the comparative example is obtained by adopting the following preparation method:
(1) Weighing the raw materials according to the proportion;
(2) Firstly, adding the bardry tobacco extract, the white oak chip extract, the virginia cypress oil, the copaiba balsam oil and the walnut shell extract into a stirring kettle, and adding three fifths of the components with the weight ratio of 4:1, propylene glycol and edible ethanol are mixed for 18min at a rotating speed of 400 r/min;
(3) Then adding Lv kang niang oil, german chamomile oil, morocco jasmine extract, spirac cinnamon bark oil, scotch spearmint oil and the rest two-fifths of cosolvent, stirring and mixing for 30min at a rotation speed of 500 r/min;
(4) Standing at room temperature for 15min, taking out, packaging, and storing.
Comparative example 3
The comparative example provides essence for cigarettes, which comprises the following raw materials in percentage by weight: 4% of a bardry tobacco extract, 4% of a oak chip extract, 4% of virginia cedarwood oil, 4% of copaiba oil, 4% of a walnut shell extract, 2% of Spearmint oil, 1% of spearmint oil, 5% of sea cable oil, 4% of mimosa oil, 4% of okra seed oil, 51.2% of propylene glycol and 12.8% of edible ethanol.
Wherein Hu Hetao shell extract was prepared in the same manner as in example 1.
The tobacco essence of the comparative example is obtained by adopting the following preparation method:
(1) Weighing the raw materials according to the proportion;
(2) Firstly, adding the bardry tobacco extract, the white oak chip extract, the virginia cypress oil, the copaiba balsam oil and the walnut shell extract into a stirring kettle, and adding three fifths of the components with the weight ratio of 4:1, propylene glycol and edible ethanol are mixed for 18min at a rotating speed of 400 r/min;
(3) Then adding the seaweed oil, the mimosa oil, the okra seed oil, the Spirachica oil and the remaining two-fifths of cosolvent, and stirring and mixing for 30min at a rotating speed of 500 r/min;
(4) Standing at room temperature for 15min, taking out, packaging, and storing.
The tobacco flavors prepared in examples 1 to 7 and comparative examples 1 to 3 were added to cigarettes according to conventional addition ratios, and a blank control group (i.e., without tobacco flavor) was set, and cigarette smoking sensory quality assessment was performed by 21 professionals on randomly sampled cigarettes according to national standard GB5606.4-2005, sensory quality assessment criteria are shown in Table 1, and smoking results are shown in Table 2.
Table 1 sensory quality evaluation criteria for cigarettes
Table 2 evaluation results of suction
From the data in table 2, the novel tobacco essence suitable for heating non-combustible tobacco products provided by the invention can increase tobacco fragrance, has better harmony and permeability, improves the sense of thickness of the tobacco fragrance, improves comfort and improves the taste of the tobacco products by arranging various natural plant raw materials in proper proportions.
The foregoing description of the preferred embodiments of the invention is not intended to be limiting, but rather is intended to cover all modifications, equivalents, alternatives, and improvements that fall within the spirit and scope of the invention.
Furthermore, it should be understood that although the present disclosure describes embodiments in terms of embodiments, not every embodiment is provided with a separate technical solution, and this description is for clarity only, and those skilled in the art should consider the disclosure as a whole, and the technical solutions in the embodiments may be combined appropriately to form other embodiments that can be understood by those skilled in the art.
Claims (9)
1. The tobacco essence suitable for heating non-combustible tobacco products is characterized by comprising the following raw materials in percentage by weight:
3-6% of Balldry tobacco extract, 3-5% of Quercus salicina wood chip extract,
3-5% of Virginia cypress wood oil, 3-5% of bitter balm oil,
Hu Hetao shell extract 3-5%, flavoring agent 2.4-3.6%,
3-6% of seaweed oil, 2-6% of mimosa oil,
1-5% of okra seed oil, 1-3% of green brewing gram oil,
3-6% of German chamomile oil, 3-6% of Morocco jasmine extract,
45% -60% of cosolvent;
wherein the bardry tobacco extract imparts a tobacco-type flavor; the Quercus salicifolia wood chip extract endows Quercus salicifolia with smell; hu Hetao the shell extract was prepared by the following procedure: selecting walnut shell, crushing and grinding the walnut shell to obtain walnut shell powder with the particle size of 1.2-1.5 mm, and then mixing the walnut shell powder with the particle size of 1:8, soaking the mixture in boiling water for 90-120 min by adopting ultrasonic extraction, wherein the ultrasonic frequency is 45-50 KHz, filtering the extracting solution by adopting a filter membrane with the aperture of 1.0 mu m after ultrasonic extraction to obtain filtrate, and concentrating the filtrate to obtain the concentrated solution of one tenth of the residues, namely the walnut shell extract.
2. The tobacco flavor suitable for heating non-combustible tobacco products of claim 1, comprising the following raw materials in weight percent:
4% of Balldry tobacco extract, 4% of Quercus salicina wood chip extract,
4% of virginia cypress wood oil, 4% of bitter balm oil,
Hu Hetao shell extract 4%, corrigent 3%, and flavoring agent 3%,
5% of seaweed oil, 4% of mimosa oil,
4% of okra seed oil, 2% of green healthy brewing gram oil,
5% of German chamomile oil, 5% of Morocco jasmine extract, and,
And 52% of cosolvent.
3. Tobacco flavor suitable for heating non-combustible tobacco products according to claim 1 or 2, characterized in that the tobacco flavor is obtained by the following preparation method:
(1) Weighing the raw materials according to the proportion;
(2) Firstly, adding the bardry tobacco extract, the Quercus salicina wood chip extract, the Virginia cypress oil, the copaiba balsam oil and the walnut shell extract into a stirring kettle, adding three fifths of cosolvent, and stirring and mixing for 15-20 min at a rotating speed of 300-500 r/min;
(3) Then adding the seaweed oil, the mimosa oil, the okra seed oil, the Lv-kang Ke oil, the German chamomile oil, the Morocco jasmine extract, the flavoring agent and the rest two fifths of cosolvent, and stirring and mixing for 25-30 min at the rotating speed of 400-600 r/min;
(4) Standing for 10-20 min at room temperature, taking out, packaging and storing.
4. Tobacco flavor suitable for heating non-combustible tobacco products according to claim 1 or 2, characterized in that the flavoring agent consists of spearmint oil and spearmint oil in the ratio of 2:1 weight ratio.
5. Tobacco flavor suitable for heating non-combustible tobacco products according to claim 1 or 2, characterized in that the morocco jasmine extract is prepared by the following operations: firstly, cutting freshly picked jasmine flowers of Morocco into crushed materials, and then performing vacuum freeze drying on the crushed materials at-30 ℃ to-10 ℃ and-0.06 to-0.08 MPa under vacuum for 2-4 hours to obtain frozen materials; grinding the frozen material to 5-10 meshes to obtain Morocco jasmine flower powder; then according to the powder ratio of 1: 5-8, adding an extractant into the morocco jasmine powder, standing and extracting for 12-24 hours at normal temperature, wherein the extraction pressure is 0.4MPa, and filtering to obtain an extract; and finally, concentrating the obtained extract liquid at low temperature under reduced pressure, and evaporating and recovering the extractant to obtain the jasmine extract of Morocco.
6. The tobacco flavor for heating non-combustible tobacco products of claim 5 wherein the extractant is an aqueous 95% ethanol solution.
7. The tobacco flavor suitable for heating non-combustible tobacco products of claim 5 wherein the reduced pressure low temperature concentration is at 0.06mpa,25 ℃.
8. The tobacco flavor suitable for heating non-combustible tobacco products of claim 5, wherein the jasmine extract has a density of 1.05-1.2.
9. The tobacco flavor suitable for heating non-combustible tobacco products according to claim 1 or 2, wherein the cosolvent comprises propylene glycol and edible ethanol according to a ratio of 3-7: 1 weight ratio.
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