CN103351949A - Anti-bacterium essence for cigarettes and yew paper containing same for cigarettes - Google Patents

Anti-bacterium essence for cigarettes and yew paper containing same for cigarettes Download PDF

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Publication number
CN103351949A
CN103351949A CN2013102683766A CN201310268376A CN103351949A CN 103351949 A CN103351949 A CN 103351949A CN 2013102683766 A CN2013102683766 A CN 2013102683766A CN 201310268376 A CN201310268376 A CN 201310268376A CN 103351949 A CN103351949 A CN 103351949A
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oil
essence
cigarettes
tobacco
cigarette
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CN2013102683766A
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CN103351949B (en
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祃志明
陈�胜
熊国玺
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China Tobacco Hunan Industrial Co Ltd
Wuhan Huanghelou Science and Technology Park Co Ltd
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China Tobacco Hunan Industrial Co Ltd
Wuhan Huanghelou Science and Technology Park Co Ltd
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Abstract

The invention provides an anti-bacterium essence for cigarettes. The essence is composed of following components in percentage by weight: 0.6 to 0.8% of sweet orange oil, 0.3 to 0.8% of California lemon oil, 1 to 1.4% of rose essential oil, 0.5 to 1% of lavender oil, 0.1 to 0.3% of clove oil, 0.2 to 0.5% of peppermint oil, 0.1 to 0.4% of celery seed oil, 0.4 to 0.6% of coriander oil, 0.8 to 1.2% of common fennel fruit oil, 0.6 to 1.2% of Shennong Chinese crossostepium leaf essential oil, 0.5 to 1.1% of patchouly oil, 0.2 to 0.4% of cedarwood oil, 0.6 to 1.4% of vanillin, 20 to 25% of honey, and the rest is mixed solution of propylene glycol and ethanol. The invention also discloses a yew paper containing the essence for cigarettes and a preparation method thereof. The yew paper added with the anti-bacterium essence for cigarettes, not only improves the smoking effect of cigarettes, but also inhibits the bacterium in the cigarette holders.

Description

Flavouring essence for tobacco and the cigarette cork paper that contains this essence with bacteriostatic action
Technical field
The invention belongs to field of cigarette producing technology, be specifically related to a kind of cigarette cork paper that has the flavouring essence for tobacco of bacteriostatic action and contain this essence.
Background technology
In the process of smoking, hand can touch the mouth rod of cigarette unavoidably, and bacterium on hand is easy to enter the mouth by cigarette holder, particularly cigarette in transmittance process, easier communicate illness.For example, streptococcus aureus and suis often are present in skin surface, nasal cavity and do not cause disease, but can potentially cause skin infections, pneumonia, meningitis, septicemia.
Research finds, many plants essential oils have stronger bacteriostatic activity, and to compare toxic side effect less with chemical fungistat, and security is higher.Various plants essential oils with fungistatic effect are united use, not only can be to the antibacterial synergies that plays of bacterium, and can greatly reduce its effective level, thus reduce plants essential oil to the detrimentally affect of tobacco local flavor, enlarge its use range.
Summary of the invention
The purpose of this invention is to provide a kind of flavouring essence for tobacco with bacteriostatic action, this flavouring essence for tobacco can not only improve the effect of smokeing panel test of cigarette, can also suppress the bacterium on the cigarette holder simultaneously.Another object of the present invention provides a kind of cigarette cork paper that contains this essence.
Above-mentioned purpose is achieved through the following technical solutions:
A kind of flavouring essence for tobacco with bacteriostatic action, it is comprised of the component of following weight per-cent meter: sweet orange oil 0.6 ~ 0.8%, California lemon oil 0.3 ~ 0.8%, Flos Rosae Rugosae quintessence oil 1 ~ 1.4%, Oleum lavandula angustifolia 0.5 ~ 1%, Syzygium aromaticum stem oil 0.1 ~ 0.3%, mentha piperita oil 0.2 ~ 0.5%, seed oil of Herba Apii graveolentis 0.1 ~ 0.4%, Fructus Coriandri oil 0.4 ~ 0.6%, Sweet fennel oil 0.8 ~ 1.2%, Dendranthema indicum essential oil 0.6 ~ 1.2%, patchouli oil 0.5 ~ 1.1%, cedar(wood)oil 0.2 ~ 0.4%, vanillin food grade,1000.000000ine mesh 0.6 ~ 1.4%, honey 20 ~ 25%, surplus are the mixing solutions of propylene glycol and ethanol.
Preferred scheme is, described flavouring essence for tobacco is comprised of the component of following weight per-cent meter: sweet orange oil 0.7%, California lemon oil 0.6%, Flos Rosae Rugosae quintessence oil 1.2%, Oleum lavandula angustifolia 0.8%, Syzygium aromaticum stem oil 0.2%, mentha piperita oil 0.4%, seed oil of Herba Apii graveolentis 0.3%, Fructus Coriandri oil 0.5%, Sweet fennel oil 1%, Dendranthema indicum essential oil 0.9%, patchouli oil 0.8%, cedar(wood)oil 0.3%, vanillin food grade,1000.000000ine mesh 1%, honey 23%, surplus are the mixing solutions of propylene glycol and ethanol.
Preferably, in the mixing solutions of described propylene glycol and ethanol, the mass ratio of propylene glycol and ethanol is 2:1.
A kind of cigarette cork paper, described cigarette is with containing above-mentioned flavouring essence for tobacco in the cork paper.
Experimental results show that: flavouring essence for tobacco of the present invention is in extracorporeal bacteria inhibitor test, streptococcus aureus, intestinal bacteria, subtilis all there is certain fungistatic effect, the staphylococcic bacteriostatic diameter of golden yellow grape is reached 20mm, its minimum inhibitory concentration (MIC) is 25mg/ml, shows the effect with stronger antibacterial growth.The present invention joins in the cigarette tipping paper, and each component is to the antibacterial synergy that plays of bacterium, and its effective level is significantly less than the effective level of independent each component of use, therefore can effectively reduce plants essential oil to the detrimentally affect of tobacco local flavor.
Sensory evaluating smoking's test-results shows, the cigarette that makes with the cork paper that contains flavouring essence for tobacco of the present invention, its perfumed ribbon has fruital and fragrance of a flower note, body note is with hot perfume, herbal and delicate fragrance note, and bottom note has the banksia rose, beans are fragrant and fragrant and sweet note, and fragrance is coordinated, the sweet sense of flue gas improves, the oral cavity is with returning sweet sense and refrigerant sense, and pleasant impression is totally comfortable, and cigarette is whole inhales flavor better.
Embodiment
The present invention is described in detail below in conjunction with embodiment.
Embodiment 1
A kind of flavouring essence for tobacco with bacteriostatic action, it is comprised of the component of following weight per-cent meter: sweet orange oil 0.6%, California lemon oil 0.3%, Flos Rosae Rugosae quintessence oil 1%, Oleum lavandula angustifolia 0.5%, Syzygium aromaticum stem oil 0.1%, mentha piperita oil 0.2%, seed oil of Herba Apii graveolentis 0.1%, Fructus Coriandri oil 0.4%, Sweet fennel oil 0.8%, Dendranthema indicum essential oil 0.6%, patchouli oil 0.5%, cedar(wood)oil 0.2%, vanillin food grade,1000.000000ine mesh 0.6%, honey 20%, surplus are the mixing solutions of propylene glycol and ethanol, in the described mixing solutions, the mass ratio of propylene glycol and ethanol is 10:1.
The preparation method of above-mentioned flavouring essence for tobacco is that with magnetic agitation 25 ~ 70min, the rotating speed of stirring was 200 ~ 250rpm after each component was mixed.
A kind of cigarette cork paper, described cigarette is with containing above-mentioned flavouring essence for tobacco in the cork paper.
This cigarette with the preparation method of cork paper is: above-mentioned flavouring essence for tobacco is sprayed to the tow sides of cork paper according to routine dose, then make solvent evaporates and dry under cold condition.
Make cigarette with the soft blue smoke leaf of Yellow Crane Tower.The sensory evaluating smoking result of this cigarette shows: the sweet sense of flue gas improves, and the oral cavity is with returning sweet sense and refrigerant sense, and totally the whole suction flavor of comfortable, cigarette is better for pleasant impression.
Embodiment 2
A kind of flavouring essence for tobacco with bacteriostatic action, it is comprised of the component of following weight per-cent meter: sweet orange oil 0.8%, California lemon oil 0.8%, Flos Rosae Rugosae quintessence oil 1.4%, Oleum lavandula angustifolia 1%, Syzygium aromaticum stem oil 0.3%, mentha piperita oil 0.5%, seed oil of Herba Apii graveolentis 0.4%, Fructus Coriandri oil 0.6%, Sweet fennel oil 1.2%, Dendranthema indicum essential oil 1.2%, patchouli oil 1.1%, cedar(wood)oil 0.4%, vanillin food grade,1000.000000ine mesh 1.4%, honey 25%, surplus are the mixing solutions of propylene glycol and ethanol, in the described mixing solutions, the mass ratio of propylene glycol and ethanol is 2:1.
The preparation method of flavouring essence for tobacco, cork paper and cigarette is identical with embodiment 1.
Sensory evaluating smoking result is identical with embodiment 1.
Embodiment 3
A kind of flavouring essence for tobacco with bacteriostatic action, it is comprised of the component of following weight per-cent meter: sweet orange oil 0.7%, California lemon oil 0.6%, Flos Rosae Rugosae quintessence oil 1.2%, Oleum lavandula angustifolia 0.8%, Syzygium aromaticum stem oil 0.2%, mentha piperita oil 0.4%, seed oil of Herba Apii graveolentis 0.3%, Fructus Coriandri oil 0.5%, Sweet fennel oil 1%, Dendranthema indicum essential oil 0.9%, patchouli oil 0.8%, cedar(wood)oil 0.3%, vanillin food grade,1000.000000ine mesh 1%, honey 23%, surplus are the mixing solutions of propylene glycol and ethanol, in the described mixing solutions, the mass ratio of propylene glycol and ethanol is 2:1.
The preparation method of flavouring essence for tobacco, cork paper and cigarette is identical with embodiment 1.
Sensory evaluating smoking result is identical with embodiment 1.
Embodiment 4
Flavouring essence for tobacco among the embodiment 1 ~ 3 is carried out extracorporeal bacteria inhibitor test
1) selecting of bacterial classification: streptococcus aureus, intestinal bacteria, subtilis.
2) selection of substratum: beef-protein medium
3) mensuration of essential oil bacteriostatic activity
The employing disk diffusion method is measured. take by weighing a certain amount of essence, the adding acetone diluted becomes the sample solution that supplies of 5% (volume fraction), under the aseptic condition, to justify filter paper (diameter 6mm) immerses in the sample acetone solution that has prepared, be attached to after draining on the culture medium flat plate of smearing the suitable concentration bacteria suspension, 4 in every ware (diameter 9cm), each test liquid repeats for 3 times, in 3 culture dish, finish respectively, every ware central authorities compare with acetone. cultivate (37 ℃ on bacterium in the darkroom for the examination bacterium, 24h, 28 ℃ of fungies, 48h), adopt the right-angled intersection method to measure antibacterial circle diameter, get its mean value as test-results.
4) mensuration of essential oil minimum inhibitory concentration (MIC)
The employing serial dilution is measured. take acetone as solvent, prepare the solution of a series of gradient mass concentrations, this gradient mass concentration solution is fallen the people have been melted in the good substratum, mix, make that the mass concentration of essence is respectively 1.0000 in the substratum, 0.5000,0.2500,0.1250,0.0625,0.0312,0.0156mg/ml after the substratum cooled and solidified, the plate streaking inoculation, cultivate by aforementioned condition, observations. do 3 groups of parallel tests, compare with control group (colony growth is normal), it is without bacteriostatic action that the visible colony growth person of naked eyes is arranged, take the minimum essential oil mass concentration that do not have colony growth fully as its MIC. with acetone, sterile distilled water compares, and records respectively essence to the MIC. of several bacterium
Whole experimental result shows, this flavouring essence for tobacco has significantly bacteriostatic action to bacterium.
The In Vitro Bacteriostasis experimental result of table 1 flavouring essence for tobacco
Bacterial classification Antibacterial circle diameter Minimal inhibitory concentration (mg/ml)
Streptococcus aureus +++ 25
Intestinal bacteria +++ 25
Subtilis ++ 50
+ represent slight fungistatic effect, sample bacteriostatic diameter 1 ~ 3mm〉the solvent bacteriostatic diameter
++ represent medium fungistatic effect, sample bacteriostatic diameter 3 ~ 4mm〉the solvent bacteriostatic diameter
The obvious fungistatic effect of +++represent, sample bacteriostatic diameter 4 ~ 10mm〉the solvent bacteriostatic diameter
The impact that embodiment 5 essence are jealous on cigarette
For checking the practical application of the present invention impact jealous on cigarette, in the situation that outward appearance, starting material are consistent, embodiment 1 ~ 3 cigarette of making and the blank cigarette that does not add essence are contrasted.By 90 people's survey, the person's of smokeing panel test test result such as following table 2.
Table 2 cigarette odor-absorbing investigation summary sheet
Figure BDA0000343342341
Draw to draw a conclusion by above-mentioned test:
1) the sweet acceptance level in cigarette oral cavity behind the cork paper adding essence, suction flavor overall evaluation integral body are better.
2) the odor type style of two groups of cigarette is basically identical.

Claims (4)

1. flavouring essence for tobacco with bacteriostatic action, it is characterized in that what it was comprised of the component of following weight per-cent meter: sweet orange oil 0.6 ~ 0.8%, California lemon oil 0.3 ~ 0.8%, Flos Rosae Rugosae quintessence oil 1 ~ 1.4%, Oleum lavandula angustifolia 0.5 ~ 1%, Syzygium aromaticum stem oil 0.1 ~ 0.3%, mentha piperita oil 0.2 ~ 0.5%, seed oil of Herba Apii graveolentis 0.1 ~ 0.4%, Fructus Coriandri oil 0.4 ~ 0.6%, Sweet fennel oil 0.8 ~ 1.2%, Dendranthema indicum essential oil 0.6 ~ 1.2%, patchouli oil 0.5 ~ 1.1%, cedar(wood)oil 0.2 ~ 0.4%, vanillin food grade,1000.000000ine mesh 0.6 ~ 1.4%, honey 20 ~ 25%, surplus are the mixing solutions of propylene glycol and ethanol.
2. the flavouring essence for tobacco with bacteriostatic action according to claim 1, it is characterized in that what it was comprised of the component of following weight per-cent meter: sweet orange oil 0.7%, California lemon oil 0.6%, Flos Rosae Rugosae quintessence oil 1.2%, Oleum lavandula angustifolia 0.8%, Syzygium aromaticum stem oil 0.2%, mentha piperita oil 0.4%, seed oil of Herba Apii graveolentis 0.3%, Fructus Coriandri oil 0.5%, Sweet fennel oil 1%, Dendranthema indicum essential oil 0.9%, patchouli oil 0.8%, cedar(wood)oil 0.3%, vanillin food grade,1000.000000ine mesh 1%, honey 23%, surplus are the mixing solutions of propylene glycol and ethanol.
3. the flavouring essence for tobacco with bacteriostatic action according to claim 1 and 2, it is characterized in that: in the described mixing solutions, the mass ratio of propylene glycol and ethanol is 2:1.
4. cigarette cork paper, it is characterized in that: described cigarette is with containing claim 1 or 2 described flavouring essence for tobaccos in the cork paper.
CN201310268376.6A 2013-06-28 2013-06-28 Anti-bacterium essence for cigarettes and yew paper containing same for cigarettes Active CN103351949B (en)

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Cited By (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103666764A (en) * 2013-12-30 2014-03-26 湖南中烟工业有限责任公司 Cooling peppermint tobacco flavor composition
CN103741552A (en) * 2013-12-16 2014-04-23 滁州卷烟材料厂 Antibacterial tipping paper and production method thereof
CN103741554A (en) * 2013-12-16 2014-04-23 滁州卷烟材料厂 Osmanthus-fragrans-fragrance tipping paper and production method thereof
CN104005288A (en) * 2014-05-30 2014-08-27 滁州卷烟材料厂 Health-care tipping paper capable of reducing harm of cigarettes to human body and preparation method of health-care tipping paper
CN104005252A (en) * 2014-05-30 2014-08-27 滁州卷烟材料厂 Multi-flavor health care tipping paper and preparation method thereof
CN104178338A (en) * 2014-07-28 2014-12-03 湖北中烟工业有限责任公司 Preparation method of sweet-taste tipping paper
CN104928029A (en) * 2015-06-18 2015-09-23 湖北中烟工业有限责任公司 Pineapple type tipping paper essence for cigarettes
CN104962393A (en) * 2015-06-18 2015-10-07 湖北中烟工业有限责任公司 Strawberry type tipping paper essence for cigarettes
CN106012672A (en) * 2016-05-28 2016-10-12 长葛市大阳纸业有限公司 Tipping paper coating agent and tipping paper
CN106283846A (en) * 2016-10-10 2017-01-04 四川兴睿龙实业有限公司 A kind of antibacterial Chinese medicine compound volatile oil and Chinese medicine paper thereof with and preparation method thereof
CN106590914A (en) * 2016-11-30 2017-04-26 湖北中烟工业有限责任公司 Natural spicy essence as well as preparation method and application thereof
CN107603739A (en) * 2017-10-24 2018-01-19 湖北中烟工业有限责任公司 It is a kind of to be used for cigarette blue or green lemon essence of mouth rod and its preparation method and application
CN108179063A (en) * 2018-01-16 2018-06-19 武汉黄鹤楼香精香料有限公司 Cool savory essence for mint type cigarette cork paper and its preparation method and application
CN112220025A (en) * 2020-09-14 2021-01-15 丽水市天博生物科技有限公司 Lemon essence with antibacterial effect and preparation method thereof
CN115428980A (en) * 2022-10-12 2022-12-06 茂名华美实业有限公司 Tobacco essence suitable for heating non-combustion tobacco products

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Cited By (20)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103741552A (en) * 2013-12-16 2014-04-23 滁州卷烟材料厂 Antibacterial tipping paper and production method thereof
CN103741554A (en) * 2013-12-16 2014-04-23 滁州卷烟材料厂 Osmanthus-fragrans-fragrance tipping paper and production method thereof
CN103666764A (en) * 2013-12-30 2014-03-26 湖南中烟工业有限责任公司 Cooling peppermint tobacco flavor composition
CN104005288A (en) * 2014-05-30 2014-08-27 滁州卷烟材料厂 Health-care tipping paper capable of reducing harm of cigarettes to human body and preparation method of health-care tipping paper
CN104005252A (en) * 2014-05-30 2014-08-27 滁州卷烟材料厂 Multi-flavor health care tipping paper and preparation method thereof
CN104178338A (en) * 2014-07-28 2014-12-03 湖北中烟工业有限责任公司 Preparation method of sweet-taste tipping paper
CN104962393B (en) * 2015-06-18 2018-07-03 湖北中烟工业有限责任公司 Cigarette strawberry type cork paper essence
CN104928029A (en) * 2015-06-18 2015-09-23 湖北中烟工业有限责任公司 Pineapple type tipping paper essence for cigarettes
CN104962393A (en) * 2015-06-18 2015-10-07 湖北中烟工业有限责任公司 Strawberry type tipping paper essence for cigarettes
CN104928029B (en) * 2015-06-18 2018-08-28 湖北中烟工业有限责任公司 Cigarette pineapple type cork paper essence
CN106012672A (en) * 2016-05-28 2016-10-12 长葛市大阳纸业有限公司 Tipping paper coating agent and tipping paper
CN106283846A (en) * 2016-10-10 2017-01-04 四川兴睿龙实业有限公司 A kind of antibacterial Chinese medicine compound volatile oil and Chinese medicine paper thereof with and preparation method thereof
CN106590914A (en) * 2016-11-30 2017-04-26 湖北中烟工业有限责任公司 Natural spicy essence as well as preparation method and application thereof
CN106590914B (en) * 2016-11-30 2020-06-23 湖北中烟工业有限责任公司 Natural spicy essence and preparation method and application thereof
CN107603739A (en) * 2017-10-24 2018-01-19 湖北中烟工业有限责任公司 It is a kind of to be used for cigarette blue or green lemon essence of mouth rod and its preparation method and application
CN108179063A (en) * 2018-01-16 2018-06-19 武汉黄鹤楼香精香料有限公司 Cool savory essence for mint type cigarette cork paper and its preparation method and application
CN108179063B (en) * 2018-01-16 2020-11-03 武汉黄鹤楼香精香料有限公司 Cool essence for mint type cigarette tipping paper and preparation method and application thereof
CN112220025A (en) * 2020-09-14 2021-01-15 丽水市天博生物科技有限公司 Lemon essence with antibacterial effect and preparation method thereof
CN115428980A (en) * 2022-10-12 2022-12-06 茂名华美实业有限公司 Tobacco essence suitable for heating non-combustion tobacco products
CN115428980B (en) * 2022-10-12 2023-05-09 茂名华美实业有限公司 Tobacco essence suitable for heating non-combustible tobacco products

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