CN103666764A - Cooling peppermint tobacco flavor composition - Google Patents
Cooling peppermint tobacco flavor composition Download PDFInfo
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- CN103666764A CN103666764A CN201310744007.XA CN201310744007A CN103666764A CN 103666764 A CN103666764 A CN 103666764A CN 201310744007 A CN201310744007 A CN 201310744007A CN 103666764 A CN103666764 A CN 103666764A
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- peppermint
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Abstract
The invention relates to a cooling peppermint tobacco flavor composition. A conventional tobacco cooling agent adopting conventional peppermint is easy to volatilize, and a conventional tobacco cooling agent adopting a peppermint derivative is distasteful. The cooling peppermint tobacco flavor composition comprises the following components at weight ratio: 65 to 85 grams of tri-peppermint monoethyl titanate, 1 to 3 grams of methyl salicylate, 0 to 0.5 gram of lemon oil, 0.2 to 0.3 gram of peppermint oil and 6 to 11 grams of flavor. According to the flavor composition, the problems of cross contamination and environmental contamination, which are caused the sublimation of peppermint, in a process of producing peppermint tobacco from the flavor composition are solved; the condition that the cool sense of the peppermint is reduced due to excessively high temperature and excessively long time in transportation and storage processes is avoided; the cool sense is persistent and uniform in a smoking process, and the plant note of the peppermint is maintained.
Description
Technical field
The present invention relates to a kind of cool taste type cigarette flavoring essence, particularly a kind of mint type cigarette essence.
Background technology
Existing mint type cigarette essence main component is menthol, or the chemical derivative of menthol, and these mint type cigarette essence exist some defects, mainly:
1, in production process, peppermint distillation causes crossed contamination and problem of environmental pollution.Menthol has strong volatilization character, and seepage force is extremely strong, and the menthol volatilization gas of high density has strong impulse and erosion action to people's skin and mucous membrane, pollutes cigarette production line and Working environment;
2, adopt that the cigarette products igniting and sucking quality of menthol perfuming is poor and shelf-lives is short.The simple cigarette products that adopts menthol perfuming, minty note when burning and sucking (cool) taste weakens rapidly with the increase of puff number, arrived cigarette end, minty note (cool) taste is very thin, can not obtain the suction sensation that minty note (cool) taste evenly discharges, exist great igniting and sucking quality defect; And the shelf-lives of cigarette is relatively short, the shelf-time is long to cause menthol volatilization and affects its stability
3,, in order to overcome the defect of above-mentioned menthol flavored cigarette product, the applicant discloses a kind of metatitanic acid three peppermint one ethyl esters (CN102321116A).This menthol derivative can well keep cool taste, but adopts the cigarette products of menthol derivative perfuming when sucking, and it is not enough that the distinctive plant note of menthol is slightly felt.Although menthol derivative can increase the stability of mentholated cigarette, extend the cigarette shelf-time, aspirating the time has cool feeling, has lost the distinctive plant note of menthol.
Summary of the invention
The object of the present invention is to provide a kind of cool taste essence of mint type cigarette, solve the above-mentioned defect of existing mint type cigarette, can make the cool taste of mentholated cigarette even lastingly, the shelf-time is long, and when suction retains the distinctive plant note of menthol.
For achieving the above object, the present invention has taked following technical scheme:
The cool taste essence of a kind of mint type cigarette of the present invention, it comprise following composition and weight ratio as follows:
Metatitanic acid three peppermint one ethyl ester 65--85;
Wintergreen oil 1--3;
Peppermint Oil 0.2-0.3;
Essence 6-11.
In above-mentioned cold taste essence for peppermint type cigarette composition provided by the invention, can also add protective material, with the weight ratio of other components be 1-4.Described protective material is low-carbon alcohol.Protectant effect is to prevent in titanic acid ester technological process, absorbs airborne moisture and decomposes, and discharges solid-state peppermint, like this, can cause the obstruction of spray gun when giving tobacco flavoring.Preferred alcohol in the present invention is or/and propylene glycol.
While adopting the cool taste essence of a kind of mint type cigarette of the present invention to prepare cigarette; after weighing by above-mentioned weight percent; metatitanic acid three peppermint one ethyl esters, Peppermint Oil, spearmint base, wintergreen oil, lemon oil, perfume base raw material are added in container; and add protective material, stir and obtain the cool taste essence of the present invention solution.Then described cool taste essence solution is evenly sprayed in pipe tobacco, then pipe tobacco is made to cigarette, make mint type cigarette.
The preferred spearmint base of described essence is or/and perfume base.
The cool taste essence of a kind of mint type cigarette of the present invention compared with prior art, possesses following advantage:
1, the cool taste essence preparation technology of a kind of mint type cigarette of the present invention is simple, and in preparation process, menthol volatilization is few, on production operation personnel and production of cigarettes environment without impact.While producing mint type cigarette, the crossed contamination and the problem of environmental pollution that because of peppermint distillation, do not cause.
2, the cool taste essence of a kind of mint type cigarette of the present invention, main component is metatitanic acid three peppermint one ethyl esters, utilize active hydroxyl in menthol, method by chamical binding is fixed on menthol on inorganic group, form metastable peppermint derivative, when cigarette is burnt, peppermint derivative decomposes, thereby discharges menthol equably.When the cigarette made from the present invention is deposited at 50 ℃ of high temperature, the menthol transformation period is about 130 days, is the more than 2 times of traditional pure menthol cigarette transformation period; Deposit under normal operation, the transformation period surpasses 8 months, and traditional pure menthol cigarette is 2 months.Adopt in the mint type cigarette transportation and storage process of essence of the present invention, can not cause the decline of peppermint cool feeling because of excess Temperature, overlong time.
3, the cool taste essence of a kind of mint type cigarette of the present invention, in composition, also include wintergreen oil, lemon oil, perfume base, Peppermint Oil, spearmint base, made up simple employing metatitanic acid three peppermint one ethyl esters and as the cigarette products of essence, lacked the defect of menthol endemic plant note.By to main component metatitanic acid three peppermint one ethyl esters and ancillary component wintergreen oil, lemon oil, essence, Peppermint Oil and protectant distributing rationally, make cool taste essence of the present invention.The cigarette products that adopts essence of the present invention to make, during suction, cool taste is evenly lasting, and has the plant note of pleasant.
Accompanying drawing explanation
Fig. 1 prepares the cigarette essence extinction curve after cold taste essence for peppermint type cigarette compositions-treated by the embodiment of the present invention.
Illustrate: A is the embodiment of the present invention 2 formula mentholated cigarette samples, and B is conventional formulation mentholated cigarette sample, two samples are all that two samples were the not capsule packing in Kaifeng 50 ℃ of oven-baked 5,12,24,32,40 days.
Embodiment
In container, add metatitanic acid three peppermint one ethyl ester 65g, wintergreen oil 3g, Peppermint Oil 0.2g, lemon oil 0.5g, ethanol 4g, perfume base 10g, spearmint base 0.8g, stir, be then evenly sprayed in 10Kg pipe tobacco, make light mint flavor cigarette.
Embodiment 2
In container, add metatitanic acid three peppermint one ethyl ester 85g, wintergreen oil 1g, Peppermint Oil 0.3g, propylene glycol 1g, perfume base 5g, spearmint base 1g, stir, be then evenly sprayed in 10Kg pipe tobacco, make dense mint flavor cigarette.
Embodiment 3
The mentholated cigarette that adopts essence combination of the present invention (composition of embodiment 2) to make and conventional formulation mentholated cigarette are put into 50 ℃ of oven-baked, the decrement of test essence.Draw essence extinction curve as shown in Figure 1.
According to Fig. 1, estimation is deposited at 50 ℃ of temperature, and the transformation period of conventional formulation mentholated cigarette Mint Essence is approximately 50 days, and the transformation period of this patent formula mentholated cigarette Mint Essence is approximately 130 days.
Embodiment 4:
On October 15th, 2009, the present patent application people engages some tobacco industry sensory evaluating smoking experts that the mentholated cigarette that adopts the essence combination of the embodiment of the present invention 1 and make and conventional formulation mentholated cigarette are contrasted and smoked panel test.
Expert's the conclusion of smokeing panel test is as follows:
Wherein 1# is traditional Mint Essence cigarette, and 2# is for adding the cigarette of essence of the present invention.
The sucking of the cool taste perfume formulation that the applicant also provides existing coolant agent and the application, preparation and security are appraised through comparison, and result is as following table:
Claims (5)
1. a cold taste essence for peppermint type cigarette composition, is characterized in that it comprises following ingredients and weight ratio:
Metatitanic acid three peppermint one ethyl ester 65--85;
Wintergreen oil 1--3;
Lemon oil 0--0.5;
Peppermint Oil 0.2-0.3;
Essence 6-11.
2. cold taste essence for peppermint type cigarette composition according to claim 1, characterized by further comprising the protective material that weight ratio is 1-4, and described protective material is selected low-carbon alcohol.
3. cold taste essence for peppermint type cigarette composition according to claim 2, it is characterized in that described low-carbon alcohol be ethanol or/propylene glycol.
According to described in claim 2 or 3 cold taste essence for peppermint type cigarette composition, it is characterized in that
Metatitanic acid three peppermint one ethyl esters 65;
Wintergreen oil 3;
Lemon oil 0.5;
Peppermint Oil 0.2;
Essence 6-11.
According to described in claim 2 or 3 cold taste essence for peppermint type cigarette composition, it is characterized in that:
Metatitanic acid three peppermint one ethyl esters 85;
Wintergreen oil 1;
Peppermint Oil 0.3;
Essence 6-11.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310744007.XA CN103666764B (en) | 2013-12-30 | 2013-12-30 | A kind of cold taste essence for peppermint type cigarette composition |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310744007.XA CN103666764B (en) | 2013-12-30 | 2013-12-30 | A kind of cold taste essence for peppermint type cigarette composition |
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| CN103666764A true CN103666764A (en) | 2014-03-26 |
| CN103666764B CN103666764B (en) | 2016-01-20 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104161303A (en) * | 2014-07-16 | 2014-11-26 | 广西中烟工业有限责任公司 | Preparation method of cooling mint type cigarette filter additive and application of cooling mint type cigarette filter additive |
| CN106753787A (en) * | 2016-11-29 | 2017-05-31 | 湖北中烟工业有限责任公司 | A kind of cigarette quick-fried pearl lemon-mint essential oil and its preparation method and application |
| CN110477440A (en) * | 2019-07-09 | 2019-11-22 | 河南中烟工业有限责任公司 | For heating the Mint Essence and reconstituted tobacoo and the cigarette that do not burn of the cigarette that do not burn |
| CN116376636A (en) * | 2023-04-27 | 2023-07-04 | 四川味欣食品科技有限公司 | Refreshing mint essence and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101808541A (en) * | 2007-06-08 | 2010-08-18 | 菲利普莫里斯生产公司 | Has the smoking article that controlled flavor discharges |
| CN102321116A (en) * | 2011-06-07 | 2012-01-18 | 湖南中烟工业有限责任公司 | Triple refined peppermint titanate-ethyl ester, and preparation and application methods thereof |
| CN103351949A (en) * | 2013-06-28 | 2013-10-16 | 湖北中烟工业有限责任公司 | Anti-bacterium essence for cigarettes and yew paper containing same for cigarettes |
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2013
- 2013-12-30 CN CN201310744007.XA patent/CN103666764B/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101808541A (en) * | 2007-06-08 | 2010-08-18 | 菲利普莫里斯生产公司 | Has the smoking article that controlled flavor discharges |
| CN102321116A (en) * | 2011-06-07 | 2012-01-18 | 湖南中烟工业有限责任公司 | Triple refined peppermint titanate-ethyl ester, and preparation and application methods thereof |
| CN103351949A (en) * | 2013-06-28 | 2013-10-16 | 湖北中烟工业有限责任公司 | Anti-bacterium essence for cigarettes and yew paper containing same for cigarettes |
Non-Patent Citations (1)
| Title |
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| 何智慧等: "薄荷卷烟研究进展", 《烟草科技》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104161303A (en) * | 2014-07-16 | 2014-11-26 | 广西中烟工业有限责任公司 | Preparation method of cooling mint type cigarette filter additive and application of cooling mint type cigarette filter additive |
| CN106753787A (en) * | 2016-11-29 | 2017-05-31 | 湖北中烟工业有限责任公司 | A kind of cigarette quick-fried pearl lemon-mint essential oil and its preparation method and application |
| CN110477440A (en) * | 2019-07-09 | 2019-11-22 | 河南中烟工业有限责任公司 | For heating the Mint Essence and reconstituted tobacoo and the cigarette that do not burn of the cigarette that do not burn |
| CN116376636A (en) * | 2023-04-27 | 2023-07-04 | 四川味欣食品科技有限公司 | Refreshing mint essence and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN103666764B (en) | 2016-01-20 |
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Inventor after: Luo Jia Inventor after: Ren Jianxin Inventor after: Lian Wenliu Inventor after: Li Yabai Inventor after: Liu Jinyun Inventor before: Guo Xiaoyi Inventor before: Zhong Kejun Inventor before: Dai Yuangang Inventor before: Du Wen Inventor before: Zhuo Ningye Inventor before: Lian Wenliu Inventor before: Han Xing |
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Free format text: CORRECT: INVENTOR; FROM: GUO XIAOYI ZHONG KEJUN DAI YUANGANG DU WEN ZHUO NINGYE LIAN WENLIU HAN XING TO: LUO JIA REN JIANXIN LIAN WENLIU LI YABAI LIU JINYUN |
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