CN1203789C - Menthol microemulsion used for filter-tip of cigarette - Google Patents
Menthol microemulsion used for filter-tip of cigarette Download PDFInfo
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- CN1203789C CN1203789C CN 03146748 CN03146748A CN1203789C CN 1203789 C CN1203789 C CN 1203789C CN 03146748 CN03146748 CN 03146748 CN 03146748 A CN03146748 A CN 03146748A CN 1203789 C CN1203789 C CN 1203789C
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- menthol
- agent
- cigarettes
- cigarette
- microemulsion liquid
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Abstract
The present invention relates to a menthol micro emulsion used for filter tips of cigarettes, which is composed of a cool-taste agent, an emulsifying agent, a stabilizing agent, a preservative agent, an oxidation inhibitor and water, wherein menthol is used as the cool-taste agent; polyethylene glycol dehydrated sorbitol stearin, polyethylene glycol dehydrated sorbitol oleate, tween, etc., are used as the emulsifying agent; pectin, gum arabic, gelatine, glycerin, etc., are used as the stabilizing agent; sorbic acid, citric acid, etc., are used as the preservative agent; VC, VE, etc., are used as the oxidation inhibitor. The micro emulsion used for industrial production has the advantages that the cost can be lowered, the pollution on the environment and equipment during processing is reduced, cigarettes produced by the micro emulsion have no impurity odor or foreign taste, the cigarettes can be stored more than one year at room temperature, and the menthol flavor is uniformly and moderately released when the cigarettes are smoked.
Description
Technical field the present invention relates to a kind of menthol microemulsion liquid, and this microemulsion is used for the igniting and sucking quality that cigarette industry can effectively be improved the mint type cigarette goods, overcomes to add the man-hour menthol to the adverse effect of environment.
The peppermint cigarette production technology that background technology is traditional, complicated operation, loaded down with trivial details.Normally menthol is dissolved in the absolute alcohol, makes the menthol alcoholic solution of debita spissitudo, be sprayed onto in the pipe tobacco equably in proportion again and go.Mentholated pipe tobacco rolls into cigarette again and props up after the sealing of some time is stored, and need pack involution immediately subsequently, in order to avoid mint flavored volatilization naturally.
Menthol has strong volatilization character, and penetration is strong.The menthol volatilization gas of high concentration has strong impulse and corrosion function to people's skin and mucous membrane, therefore in the process of making processing peppermint cigarette, operating personnel are difficult to avoid the smoked of peppermint gas and endure, and all equipment that contact with mentholated pipe tobacco and surrounding environment all can be subjected to certain pollution.The menthol uniformity is relatively poor when producing the peppermint cigarette according to a conventional method, and product quality is difficult to guarantee that the storage life of product is short, and dense back was light before the peppermint cold was distinguished the flavor of when suction.
European patent EP 0486212 proposes with menthol-glucose mixed carbonate as the cold releasing agent of distinguishing the flavor of, and this method is that mixed carbonate ester is added in the tobacco, and the burning by tobacco impels the release menthol.Chinese patent CN1193901 has disclosed a kind of coolant compositions that contains thin lotus alcohol radical succinate, and this composition can be used for aspects such as the filter tip, cigarette paper of tobacco product, and refrigerant, the pure and fresh sense of taste is provided.Chinese patent CN1394591 has disclosed menthol and menthanol lactic acid ester preparation of compositions methods and applications, proposes the mixture of menthol and menthanol lactic acid ester formation is used for tobacco product, fields such as toothpaste.Chinese patent CN1099957 has disclosed a kind of adsorbent of cigarette filter, this adsorbent is the unformed manosil AS or the unformed aluminosilicate of certain specification, point out that this adsorbent has the ability of strong absorption and release spices, can be used as the adsorbent of menthol in the cigarette filter.
The derivative of employing menthol such as menthyl ester etc. are made cool flavor releasing agent, can reduce volatilization to a certain extent, but cost is increased owing to carrying out derivatization to menthol, these derivatives are added in the tobacco, addition is bigger, some menthol derivative is used for tobacco product also can bring peculiar smell and assorted gas into, thereby production brings negative effect to cigarette industry.Adopting the filter tip of menthol adsorbent production is composite filter tip, its process conditions complexity, and cost is higher, needs with expensive composite tip stick make-up machine.Therefore, must be improved, could be satisfied demand of practical production existing peppermint cigarette production technology.
Summary of the invention the purpose of this invention is to provide a kind of method of producing mint type mouth rod with the menthol emulsifying technology.Use mouth rod of the present invention, can produce various mint type cigarettes easily, it is with low cost, and can make the mint type cigarette of production keep its distinctive cool flavor and fragrance, long shelf-life, and mint flavored discharges evenly when suction, free from extraneous odour and assorted gas.
Menthol microemulsion liquid of the present invention is to be coolant agent (5%-30%) with menthol; Polyoxyethylene sorbitan stearate, polyoxyethylene sorbitan oleate, tween etc. are as emulsifying agent (0.1%-15%); Pectin, gum arabic, gelatin, glycerine etc. are as stabilizing agent (0.1%-15%); Sorbic acid, citric acid etc. are as anticorrisive agent (0-5%); VC, VE etc. form menthol microemulsion liquid as antioxidant (0-5%) and water (55%-90%) through adding the thermal agitation supervisor.The microemulsion that obtains adds in the mouth rod when the moulding of mouth rod.
Use menthol microemulsion liquid of the present invention to have the following advantages: 1. in the process of preparation microemulsion, formed oil-in-water molecule after the menthol dissolving, this molecule that contains menthol, owing to the existence of emulsifying agent, stabilizing agent etc. forms the metastable system of deciding, thereby the volatility of menthol is greatly reduced.2. the used coolant agent of the present invention does not need menthyl ester, does not need to add in addition adsorbent yet, only needs low price, the menthol of wide material sources.3. the mentholated cigarette that uses mouth rod of the present invention to produce, the resting period is long, deposits at ambient temperature more than 1 year, still has denseer mint flavored, and mint flavored discharges evenly when suction, does not have peculiar smell and assorted gas.4. resulting menthol microemulsion liquid directly adds in the tow of mouth rod and goes, and only needs a less addition just can reach technological requirement, and cost is lower, and every case cigarette (50,000) increase cost is no more than 20 yuan, and its operation is also very simple.
Specific embodiment embodiment 1: 0.5g polyoxyethylene sorbitan stearate and 0.5g pectolysis in 100g hot water, are added the VC of 0.05g again, and stirring condition slowly adds the 10g menthol down, continue to stir menthol microemulsion liquid.Add gained menthol microemulsion liquid in the tow (adding proportion: menthol/tow=0.0025, mass ratio), moulding gets peppermint mouth rod.
Embodiment 2: 0.6g polyoxyethylene sorbitan stearate and 0.6g gum arabic are dissolved in the 100g hot water, add the 0.06g sorbic acid again, stirring condition adds down slowly the 12g menthol, continue to stir menthol microemulsion liquid.Add gained menthol microemulsion liquid in the tow (adding proportion: menthol/tow=0.0025, mass ratio), moulding gets peppermint mouth rod.
Embodiment 3: 0.8g polyoxyethylene sorbitan oleate and 0.8g gum arabic are dissolved in the 100g hot water, add the citric acid of 0.08g again, stirring condition adds down slowly the 15g menthol, continue to stir menthol microemulsion liquid.Add gained menthol microemulsion liquid in the tow (adding proportion: menthol/tow=0.0025, mass ratio), moulding gets peppermint mouth rod.
Claims (5)
1. menthol microemulsion liquid that is used for cigarette filter, contain menthol and water, it is characterized in that also containing emulsifying agent, stabilizing agent, anticorrisive agent, antioxidant, its weight ratio is: menthol is 5%-30%, emulsifying agent is 0.1%-15%, and stabilizing agent is 0.1%-15%, and anticorrisive agent is 0-5%, antioxidant is 0-5%, and water is 55%-90%.
2. according to right 1 described menthol microemulsion liquid, it is characterized in that its described emulsifying agent is polyoxyethylene sorbitan stearate, polyoxyethylene sorbitan oleate, tween.
3. according to right 1 described menthol microemulsion liquid, it is characterized in that its described stabilizing agent is pectin, gum arabic, gelatin, glycerine.
4. according to right 1 described menthol microemulsion liquid, it is characterized in that its described anticorrisive agent is sorbic acid, citric acid.
5. according to right 1 described menthol microemulsion liquid, it is characterized in that its described antioxidant is VC and VE.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 03146748 CN1203789C (en) | 2003-06-23 | 2003-06-23 | Menthol microemulsion used for filter-tip of cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 03146748 CN1203789C (en) | 2003-06-23 | 2003-06-23 | Menthol microemulsion used for filter-tip of cigarette |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1480075A CN1480075A (en) | 2004-03-10 |
| CN1203789C true CN1203789C (en) | 2005-06-01 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 03146748 Expired - Fee Related CN1203789C (en) | 2003-06-23 | 2003-06-23 | Menthol microemulsion used for filter-tip of cigarette |
Country Status (1)
| Country | Link |
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| CN (1) | CN1203789C (en) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100409777C (en) * | 2004-07-06 | 2008-08-13 | 樊金生 | Method for reducing cigarette tar content |
| CN101002827B (en) * | 2006-12-15 | 2011-01-26 | 江南大学 | Micro-emulsion of mint oil with slow-releasing property, and its preparing method |
| CN101390657B (en) * | 2007-09-21 | 2011-05-25 | 武汉烟草(集团)有限公司 | Cigarette filter tip rod capable of sustained releasing mint and production technique thereof |
| CN101797071B (en) * | 2010-01-28 | 2012-08-22 | 川渝中烟工业有限责任公司 | Cigar mildewproof additive and using method thereof |
| CN102273733B (en) * | 2010-06-08 | 2014-01-29 | 湖北中烟工业有限责任公司 | Sustained-release pellet capsule of sweet cooling agent for cigarette with filter plug |
| CN105029667A (en) * | 2015-07-31 | 2015-11-11 | 湖北中烟工业有限责任公司 | Water-soluble anise oil microemulsion for cigarettes and preparation method and application thereof |
| CN105124752A (en) * | 2015-08-18 | 2015-12-09 | 湖北中烟工业有限责任公司 | Peppermint oil based nano-emulsion for cigarettes and preparation method and application of peppermint oil based nano-emulsion |
| CN111100756A (en) * | 2019-12-31 | 2020-05-05 | 广州华芳烟用香精有限公司 | Micro-emulsified mint essence for cigarette paper, and preparation method and application thereof |
-
2003
- 2003-06-23 CN CN 03146748 patent/CN1203789C/en not_active Expired - Fee Related
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| Publication number | Publication date |
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| CN1480075A (en) | 2004-03-10 |
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