CN107173848A - A kind of temperature becomes sustained release gel complex material and its application in cigarette filter rod - Google Patents
A kind of temperature becomes sustained release gel complex material and its application in cigarette filter rod Download PDFInfo
- Publication number
- CN107173848A CN107173848A CN201710521792.0A CN201710521792A CN107173848A CN 107173848 A CN107173848 A CN 107173848A CN 201710521792 A CN201710521792 A CN 201710521792A CN 107173848 A CN107173848 A CN 107173848A
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- Prior art keywords
- gel
- sustained release
- temperature
- complex material
- filter stick
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
Become sustained release gel complex material and its application in cigarette filter rod the invention provides a kind of temperature, belong to the manufacturing technology field of cigarette holder, preparation method includes gel heating and melting;It is then sent in the immersion slot with heat insulation function;Guide to immersion slot, and be dipped in liquid gel after common flavouring cored wire is unreeled by unreeling structure, adjust the concentration of liquid gel, so that the thickness for being attached to the gel layer on flavouring cored wire surface is more than or equal to the diameter of flavouring cored wire;The flavouring cored wire after infiltration is subjected to cool drying afterwards, gel sets are that solid is attached to flavouring cored wire surface, obtain temperature and become sustained release gel complex material.Composite and the filter stick of preparation prepared by gel of the present invention, the scheduling of production of filter stick is also convenient for while forming degree and the good fragrant effect of lock, products obtained therefrom is compared with horn of plenty, the simple gel being applied in filter stick can be slowed down quickly to volatilize in suction, whole branch smoking set is had more mouthfeel in a balanced way.
Description
Technical field
The present invention relates to the manufacturing technology field of cigarette holder, and in particular to a kind of temperature becomes sustained release gel complex material, manufacturer
Method and its application in cigarette filter rod.
Background technology
With the development of current cigarette technology, the hot volatile content in cigarette is greatly reduced, but also causes it
Inhale taste and receive considerable influence, therefore, introduce perfuming technology into current cigarette industry the only way which must be passed, by add cause fragrant composition with
Smoke concentration is supplemented, while not increasing nuisance content, the essence allocated on the basis of scientific research, its Main Ingredients and Appearance has changed
Become the past with the tobacco of nature material and synthesis contained flavor matter in itself, thus act on it is larger will not also produce it is different
Taste, chemical analysis the shortcomings of to producing miscellaneous taste, excitant, it would however also be possible to employ the corresponding compound of addition is solved.
And conventional perfuming mode is perfuming cigarette and filter stick perfuming, so-called perfuming cigarette is that spices is directly appended into cigarette
In silk, but the service efficiency of spices is low, and the security after the pipe tobacco burning of spices UNICOM is difficult to assess；Filter stick perfuming is by flavouring
Material is added in filter stick, is eluted by the temperature of flue gas during cigarette burning and discharges fragrance, the use effect of which spices
Rate is high, and the composition added, without high-temp combustion and cracking, security is more preferable.
Filter stick perfuming is that addition is stained with the fragrant line of spices and added in filter stick in filter stick using wide mode
Microcapsules or quick-fried pearl, two ways are each advantageous, but there is also respective weak point.
Also a kind of filter stick perfuming mode, i.e., add flavouring gel in filter stick, good using long lasting quality under gel normal temperature,
Volatilized in suction under flue-gas temperature effect the characteristic of release, and adding technology is also relatively easy, a kind of such as " plural gel
Fragrance slow-release particle and preparation method thereof and its .3 of purposes 201610764049 ", its preparation method is mixed including preparation raw material
Thing solution, plural gel and the addition step such as spices are prepared, with compounded gels such as polyethylene glycol and beta-schardinger dextrin, gelatin
As particle made from material, particle filter stick perfuming amount, perfuming uniformity, controllability and stability can be effectively increased；And
" a kind of purposes of the wire plural gel fragrance slow-release filter stick and preparation method thereof with it, 201610064101.4 ", are related to one kind
Purposes of the wire plural gel fragrance slow-release filter stick and preparation method thereof with it, it is not necessary to traditional cotton thread or synthetic fibers system
Into fragrant line as carrier, it is fragrant with polyethylene glycol and the compounded gel thread simulation tradition of chitosan sodium carboxymethylcellulose
Line, but this mode is when wire-beam forming is squeezed, gel easily filter stick axially or radially in the range of flee, or even filter of emerging
Rod termination, the shaping of final influence filter stick, also has an impact the overall perception of filter stick while reduction aroma retaining effect；And this side
Formula when preparing filter stick can only online production, i.e. gel apply and wire-beam forming must be carried out simultaneously, products obtained therefrom is more single, nothing
Method carries out the production of the gel filter stick of diversified forms according to demand；Further, because its gel is directly combined with tow, in suction
When, the thawing of gel and volatilize all more directly and quick, it is stronger fragrance during early stage suction often occur, to stage taste
It is thin, cause the suction taste big rise and fall of whole cigarette.
The content of the invention
To solve problem present in background technology, the invention provides a kind of temperature become sustained release gel complex material and its
Application in cigarette filter rod.
Become sustained release gel complex material and preparation method thereof present invention firstly provides a kind of temperature, using following technical side
Case：
A kind of temperature becomes sustained release gel complex material, it is characterised in that by being coated on the gel layer of periphery, being arranged on the flavouring of core
Cored wire and gel positioned there between-cored wire soakage layer composition.
The raw material of the gel includes polyethylene glycol, octadecane, 18 carbonic acid, propane diols, glycerin monostearate, will be with
Upper raw material is blended under the conditions of 70 DEG C in proportion with essence, and transparency liquid is obtained after heating water bath 3h；Pour into and 25-30 is placed in container
Solid is congealed into after 8-12h in DEG C environment, gel is made.
The temperature becomes the preparation method of sustained release gel complex material, comprises the following steps：
The gel prepared is inserted in water-bath first, 70-80 DEG C is heated to and is melted;
Then it is transported to by heat preserving conduit pipe, delicate flow pump in the immersion slot with heat insulation function;
Guide to immersion slot, and be dipped in liquid gel after common flavouring cored wire is unreeled by unreeling structure, adjust liquid
The concentration of state gel, so that the thickness for being attached to the gel layer on flavouring cored wire surface is more than or equal to the diameter of flavouring cored wire;
The flavouring cored wire after infiltration is subjected to cool drying afterwards, gel sets are that solid is attached to flavouring cored wire surface, are obtained
Temperature becomes sustained release gel complex material.
Become application of the sustained release gel complex material in cigarette filter rod present invention also offers a kind of temperature, it is characterised in that
The temperature is become to be made by filter stick formation equipment after sustained release gel complex material is combined with filter stick tow and slowed down containing wire temperature
The filter stick of gel complex material is released, including acetate silk, the temperature through acetate silk become sustained release gel complex material,
And parcel acetate silk and temperature become the interior integument of sustained release gel complex material.
It is preferred that, it is described to become the filter stick for being sustained gel complex material using pipe tobacco section junction as starting point containing wire temperature, according to
It is secondary to set two or more, the wire temperature change sustained release respectively prepared by the gel comprising different colours, fragrance and volatilization temperature solidifying
Glue composite.
Become application of the sustained release gel complex material in cigarette filter rod present invention also offers a kind of temperature, it is characterised in that
Carry out offline production temperature and become sustained release gel complex material, and be prepared into the graininess of cylinder, it is then multiple with filter stick tow
It is made after conjunction by filter stick formation equipment and becomes the filter stick for being sustained gel complex material containing graininess temperature.
It is preferred that, filter stick is set to more than two sections of structure, according to apart from the far and near respectively in correspondence filter core of pipe tobacco section
Different colours, diverse fragrant flavour are set in section, but the consistent graininess temperature of volatilization temperature becomes sustained release gel complex material, flue-gas temperature
It is directly proportional to apart from the distance of pipe tobacco burning zone, becoming sustained release gel complex material apart near graininess temperature first volatilizees, and distance is remote
Rear volatilization, flue gas is obtained with this and inhales the polynary filter stick that can be changed according to suction time length of taste.
Beneficial effects of the present invention：
Gel of the present invention can effectively dissolve each other with PG, GL, phenomenon of osmosis after no layering, solidification, can subtract as far as possible
Few consumption；And gel is without obvious peculiar smell, do not influence moisture content in the style and features of spices, thermal inductance gel few, it is to avoid cigarette
Make moist pollution.
The composite and the filter stick of preparation prepared using gel of the present invention is good in forming degree and the fragrant effect of lock
The scheduling of production of filter stick is also convenient for simultaneously, and products obtained therefrom can carry out the gel filter stick of diversified forms according to demand compared with horn of plenty
Production；By the combination of gel and flavouring cored wire, the simple gel being applied in filter stick can be slowed down quick in suction
Volatilization, it is to avoid the deficiency that differs greatly of taste before and after suction occur, makes whole branch smoking set have more mouthfeel in a balanced way.
Embodiment
Embodiment 1
Peppermint temperature becomes the preparation of sustained release gel complex material and filter stick, and the raw material of gel includes polyethylene glycol, octadecane, 18 carbon
Acid, propane diols, glycerin monostearate, above raw material and menthol are blended under the conditions of 70 DEG C in proportion, heating water bath 3h
Transparency liquid is obtained afterwards；Pour into container to be placed in 25-30 DEG C of environment and congeal into solid after 8-12h, gel is made.
The temperature becomes the preparation method of sustained release gel complex material, comprises the following steps：
The gel prepared is inserted in water-bath first, 70-80 DEG C is heated to and is melted;
Then it is transported to by heat preserving conduit pipe, delicate flow pump in the immersion slot with heat insulation function;
Guide to immersion slot, and be dipped in liquid gel after common flavouring cored wire is unreeled by unreeling structure, adjust liquid
The concentration of state gel, so that the thickness for being attached to the gel layer on flavouring cored wire surface is more than or equal to the diameter of flavouring cored wire;
The flavouring cored wire after infiltration is subjected to cool drying afterwards, gel sets are that solid is attached to flavouring cored wire surface, are obtained
Temperature becomes sustained release gel complex material.
The temperature is become after sustained release gel complex material is combined with filter stick tow and is made by filter stick formation equipment containing wired
Shape temperature becomes the filter stick of sustained release gel complex material.
Peppermint temperature becomes sustained-release gel composite filter storage weight change situation（120mm 60mg/ branch）.
| Sample | Blank peppermint filter stick 20 | Gel peppermint filter stick 20 |
| Opening storage 0d | 16.142g | 16.228g |
| Opening storage 3d | 15.821g | 16.089g |
| Opening storage 6d | 15.738g | 15.991g |
| Opening storage 10d | 15.742g | 15.978g |
After the storage of peppermint filter stick in filter stick menthol content change（120mm 60mg/ branch）
Menthol（GC/MS）Inspection data
Embodiment 2
Aroma temperature becomes the preparation of sustained release gel complex material and filter stick, and method and embodiment 1 are basically identical, and difference is in gel
The spices of addition is white wine；Other difference is that the aroma temperature becomes sustained release gel complex material and uses offline processing mode
Graininess is made, is worth aroma filter stick with tow composite molding afterwards.
Aroma filter stick aspirates evaluation situation（120mm 180mg/ branch）
| Sample | Compare aroma cigarette | Use 9mg/ branch aroma gel filter sticks Aroma cigarette | Use 18mg/ branch aroma gel filter sticks Aroma cigarette |
| Bag is opened to comment Suction situation | Flue gas is finer and smoother, coordinate, But aroma fragrance is weaker, First two mouthfuls have, rear end performance It is unobvious | Tobacco aroma is finer and smoother, coordinates, but Hair property is slightly weak thoroughly, and aroma is relatively compareed Sample is obvious, | Tobacco aroma is finer and smoother, coordinates, but hair thoroughly Property it is slightly weak, aroma substantially, front and rear section has Aroma |
| Opening is put Put 1 day After smoke panel test Situation | Flue gas is finer and smoother, coordinate, But aroma fragrance is weaker, entirely Aspiration procedure is experienced substantially Less than | Tobacco aroma is finer and smoother, coordinates, but Hair property is slightly weak thoroughly, and aroma is relatively compareed Substantially, overall density is reduced not sample Substantially | Tobacco aroma is finer and smoother, coordinates, but hair thoroughly Property is slightly weak, and aroma is more apparent, and front and rear section is all There is aroma obvious |
| Opening is put Put 2 days After smoke panel test Situation | Flue gas is finer and smoother, coordinate, But aroma fragrance is weaker, entirely Aspiration procedure is experienced substantially Less than | Tobacco aroma is finer and smoother, coordinates, but Hair property is slightly weak thoroughly, and aroma is compared with first Its sample has obvious reduction | Tobacco aroma is finer and smoother, coordinates, but hair thoroughly Property is slightly weak, and aroma is more apparent, and front and rear section is all There is aroma obvious |
| Opening is put Put 3 days After smoke panel test Situation | Flue gas is finer and smoother, coordinate, But aroma fragrance is weaker, entirely Aspiration procedure is experienced substantially Less than | Tobacco aroma is finer and smoother, coordinates, but Hair property is slightly weak thoroughly, and aroma is compared with first Its sample has obvious reduction, taste It is not notable | Tobacco aroma is finer and smoother, coordinates, but hair thoroughly Property is slightly weak, and aroma decreases, front end wine Perfume (or spice) decreases, and opposed rear end is more apparent |
| Opening is put Put 5 days After smoke panel test Situation | Flue gas is finer and smoother, coordinate, But aroma fragrance is weaker, entirely Aspiration procedure is experienced substantially Less than | Tobacco aroma is finer and smoother, coordinates, but Hair property is slightly weak thoroughly, and aroma is not obvious | Tobacco aroma is finer and smoother, coordinates, but hair thoroughly Property is slightly weak, and aroma has obvious reduction, in cigarette End group of supporting the front originally is not felt by, and rear end has Certain aroma |
Aroma filter stick deposits weight change situation（120mm 180mg/ branch）
| The open resting period | The aroma filter stick of common perfuming（20）90mg/ branch |
| 0d | 21.653 |
| 1d | 21.689 |
| 2d | 21.652 |
| 3d | 21.670 |
| 4d | 21.700 |
| 5d | 21.669 |
| 6d | 21.703 |
| 7d | 21.678 |
| 8d | 21.672 |
| 9d | 21.689 |
| 10d | 21.678 |
Claims (7)
1. a kind of temperature becomes sustained release gel complex material, it is characterised in that by being coated on the gel layer of periphery, being arranged on the increasing of core
Fragrant cored wire and gel positioned there between-cored wire soakage layer composition.
2. a kind of temperature according to claim 1 becomes sustained release gel complex material, it is characterised in that the raw material bag of the gel
Polyethylene glycol, octadecane, 18 carbonic acid, propane diols, glycerin monostearate are included, the raw material is blended in proportion with essence
Under the conditions of 70 DEG C, transparency liquid is obtained after heating water bath 3h；Pour into container to be placed in 25-30 DEG C of environment and congeal into solid after 8-12h,
Gel is made.
3. a kind of temperature becomes the preparation method of sustained release gel complex material, it is characterised in that comprise the following steps：
The gel prepared is inserted in water-bath first, 70-80 DEG C is heated to and is melted;
Then it is transported to by heat preserving conduit pipe, delicate flow pump in the immersion slot with heat insulation function;
Guide to immersion slot, and be dipped in liquid gel after common flavouring cored wire is unreeled by unreeling structure, adjust liquid
The concentration of state gel, so that the thickness for being attached to the gel layer on flavouring cored wire surface is more than or equal to the diameter of flavouring cored wire;
The flavouring cored wire after infiltration is subjected to cool drying afterwards, gel sets are that solid is attached to flavouring cored wire surface, are obtained
Temperature becomes sustained release gel complex material.
4. a kind of temperature becomes application of the sustained release gel complex material in cigarette filter rod, it is characterised in that it is solidifying that the temperature is become into sustained release
After glue composite is combined with filter stick tow, it is made by filter stick formation equipment and becomes sustained release gel complex material containing wire temperature
Filter stick, the filter stick includes acetate silk, the temperature through acetate silk and becomes sustained release gel complex material, and parcel vinegar
Sour fibre bundle and temperature become the interior integument of sustained release gel complex material.
5. a kind of temperature according to claim 4 becomes application of the sustained release gel complex material in cigarette filter rod, its feature exists
In, it is described containing wire temperature become sustained release gel complex material filter stick using pipe tobacco section junction as starting point, set gradually two with
Wire temperature upper, respectively prepared by the gel comprising different colours, fragrance and volatilization temperature becomes sustained release gel complex material.
6. a kind of temperature becomes application of the sustained release gel complex material in cigarette filter rod, it is characterised in that offline production prepares temperature and become
Sustained-release gel composite, and the graininess of cylinder is made into, set after being then combined with filter stick tow by filter stick formation
The filter stick of sustained release gel complex material must be become containing graininess temperature by preparing.
7. a kind of temperature according to claim 6 becomes application of the sustained release gel complex material in cigarette filter rod, its feature exists
In filter stick to be set to more than two sections of structure, sets different in correspondence filter rod segments respectively according to apart from the far and near of pipe tobacco section
Color, diverse fragrant flavour, but the consistent graininess temperature of volatilization temperature becomes sustained release gel complex material, and flue-gas temperature apart from pipe tobacco with firing
The distance for burning section is directly proportional, and becoming sustained release gel complex material apart near graininess temperature first volatilizees, the remote rear volatilization of distance, with this
Obtain flue gas and inhale the polynary filter stick that taste can change according to suction time length.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710521792.0A CN107173848A (en) | 2017-06-30 | 2017-06-30 | A kind of temperature becomes sustained release gel complex material and its application in cigarette filter rod |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710521792.0A CN107173848A (en) | 2017-06-30 | 2017-06-30 | A kind of temperature becomes sustained release gel complex material and its application in cigarette filter rod |
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| CN107173848A true CN107173848A (en) | 2017-09-19 |
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| CN201710521792.0A Pending CN107173848A (en) | 2017-06-30 | 2017-06-30 | A kind of temperature becomes sustained release gel complex material and its application in cigarette filter rod |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107802032A (en) * | 2017-11-10 | 2018-03-16 | 云南中烟新材料科技有限公司 | A kind of discontinuous temperature causes production method and the application of the fragrant filter stick of phase change gel load |
| CN108041681A (en) * | 2018-02-12 | 2018-05-18 | 云南芯韵科技开发有限公司 | aloe gel composite material and its preparation method and application |
| CN108523216A (en) * | 2018-04-19 | 2018-09-14 | 云南巴菰生物科技有限公司 | A kind of preparation method for reducing the low resistance to suction polylactic acid fiber tow filter rods of flue-gas temperature |
| CN109588771A (en) * | 2018-12-26 | 2019-04-09 | 湖南中烟工业有限责任公司 | A kind of cooling mouth stick, smoking article and application |
| CN109588775A (en) * | 2018-12-12 | 2019-04-09 | 重庆中烟工业有限责任公司 | A kind of heating with cooling function is not burnt cigarette filter rod |
| CN109820243A (en) * | 2019-03-15 | 2019-05-31 | 湖北中烟工业有限责任公司 | Have effects that the scented gel of sustained release and its preparation and the application in cigarette |
| CN110447956A (en) * | 2019-08-12 | 2019-11-15 | 深圳市科伊斯科技有限公司 | A kind of non-tobacco composition, variable amount of smoke cigarette stick and its methods for making and using same |
| CN110946324A (en) * | 2019-12-26 | 2020-04-03 | 王传涛 | Production method of ginsenoside gel filter stick |
| CN111150111A (en) * | 2020-03-09 | 2020-05-15 | 云南喜科科技有限公司 | Fragrance slow-release cooling unit and heating type aerosol generating product comprising same |
| CN111713738A (en) * | 2020-06-29 | 2020-09-29 | 云南恩典科技产业发展有限公司 | Fragrance-carrying non-woven fabric and application thereof in cigarette filter stick material |
| CN111759002A (en) * | 2020-07-11 | 2020-10-13 | 云南中烟新材料科技有限公司 | Composite aroma-carrying core line for cigarettes |
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| CN106174694A (en) * | 2016-08-30 | 2016-12-07 | 云南芯韵科技开发有限公司 | A kind of pluralgel fragrance slow-release granule and preparation method thereof and its purposes |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107802032A (en) * | 2017-11-10 | 2018-03-16 | 云南中烟新材料科技有限公司 | A kind of discontinuous temperature causes production method and the application of the fragrant filter stick of phase change gel load |
| CN107802032B (en) * | 2017-11-10 | 2021-02-09 | 云南中烟新材料科技有限公司 | Production method and application of discontinuous temperature-induced phase change gel aroma-carrying filter stick |
| CN108041681A (en) * | 2018-02-12 | 2018-05-18 | 云南芯韵科技开发有限公司 | aloe gel composite material and its preparation method and application |
| CN108523216A (en) * | 2018-04-19 | 2018-09-14 | 云南巴菰生物科技有限公司 | A kind of preparation method for reducing the low resistance to suction polylactic acid fiber tow filter rods of flue-gas temperature |
| CN109588775A (en) * | 2018-12-12 | 2019-04-09 | 重庆中烟工业有限责任公司 | A kind of heating with cooling function is not burnt cigarette filter rod |
| CN109588771B (en) * | 2018-12-26 | 2020-09-11 | 湖南中烟工业有限责任公司 | Cooling filter tip, smoking article and application |
| CN109588771A (en) * | 2018-12-26 | 2019-04-09 | 湖南中烟工业有限责任公司 | A kind of cooling mouth stick, smoking article and application |
| CN109820243A (en) * | 2019-03-15 | 2019-05-31 | 湖北中烟工业有限责任公司 | Have effects that the scented gel of sustained release and its preparation and the application in cigarette |
| CN110447956A (en) * | 2019-08-12 | 2019-11-15 | 深圳市科伊斯科技有限公司 | A kind of non-tobacco composition, variable amount of smoke cigarette stick and its methods for making and using same |
| CN110946324A (en) * | 2019-12-26 | 2020-04-03 | 王传涛 | Production method of ginsenoside gel filter stick |
| CN111150111A (en) * | 2020-03-09 | 2020-05-15 | 云南喜科科技有限公司 | Fragrance slow-release cooling unit and heating type aerosol generating product comprising same |
| CN111713738A (en) * | 2020-06-29 | 2020-09-29 | 云南恩典科技产业发展有限公司 | Fragrance-carrying non-woven fabric and application thereof in cigarette filter stick material |
| CN111759002A (en) * | 2020-07-11 | 2020-10-13 | 云南中烟新材料科技有限公司 | Composite aroma-carrying core line for cigarettes |
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Application publication date: 20170919 |
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