CN109820243A - Have effects that the scented gel of sustained release and its preparation and the application in cigarette - Google Patents
Have effects that the scented gel of sustained release and its preparation and the application in cigarette Download PDFInfo
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- CN109820243A CN109820243A CN201910196885.XA CN201910196885A CN109820243A CN 109820243 A CN109820243 A CN 109820243A CN 201910196885 A CN201910196885 A CN 201910196885A CN 109820243 A CN109820243 A CN 109820243A
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- Prior art keywords
- gel
- cigarette
- sustained release
- fragrance
- scented
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- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 60
- 238000013268 sustained release Methods 0.000 title claims abstract description 34
- 239000012730 sustained-release form Substances 0.000 title claims abstract description 34
- 238000002360 preparation method Methods 0.000 title claims abstract description 17
- 230000000694 effects Effects 0.000 title claims description 17
- 239000003205 fragrance Substances 0.000 claims abstract description 46
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 30
- 241000208125 Nicotiana Species 0.000 claims abstract description 20
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims abstract description 18
- 238000000034 method Methods 0.000 claims abstract description 14
- 239000011365 complex material Substances 0.000 claims abstract description 13
- 229920001282 polysaccharide Polymers 0.000 claims abstract description 12
- 239000005017 polysaccharide Substances 0.000 claims abstract description 12
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims abstract description 10
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 10
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000008103 glucose Substances 0.000 claims abstract description 10
- 239000001630 malic acid Substances 0.000 claims abstract description 10
- 235000011090 malic acid Nutrition 0.000 claims abstract description 10
- IXPNQXFRVYWDDI-UHFFFAOYSA-N 1-methyl-2,4-dioxo-1,3-diazinane-5-carboximidamide Chemical compound CN1CC(C(N)=N)C(=O)NC1=O IXPNQXFRVYWDDI-UHFFFAOYSA-N 0.000 claims abstract description 9
- 239000002202 Polyethylene glycol Substances 0.000 claims abstract description 9
- 235000021355 Stearic acid Nutrition 0.000 claims abstract description 9
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 claims abstract description 9
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229920001223 polyethylene glycol Polymers 0.000 claims abstract description 9
- 239000000661 sodium alginate Substances 0.000 claims abstract description 9
- 235000010413 sodium alginate Nutrition 0.000 claims abstract description 9
- 229940005550 sodium alginate Drugs 0.000 claims abstract description 9
- 239000008117 stearic acid Substances 0.000 claims abstract description 9
- 238000002156 mixing Methods 0.000 claims abstract description 8
- 238000004090 dissolution Methods 0.000 claims abstract description 7
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 230000035807 sensation Effects 0.000 claims abstract description 7
- 235000019615 sensations Nutrition 0.000 claims abstract description 7
- 230000015572 biosynthetic process Effects 0.000 claims abstract description 4
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims abstract description 3
- 235000001727 glucose Nutrition 0.000 claims abstract description 3
- 150000004676 glycans Chemical class 0.000 claims abstract 3
- 235000006679 Mentha X verticillata Nutrition 0.000 claims description 24
- 235000002899 Mentha suaveolens Nutrition 0.000 claims description 24
- 235000001636 Mentha x rotundifolia Nutrition 0.000 claims description 24
- 239000000463 material Substances 0.000 claims description 18
- 239000002994 raw material Substances 0.000 claims description 14
- 238000003756 stirring Methods 0.000 claims description 10
- 235000013373 food additive Nutrition 0.000 claims description 9
- 239000002778 food additive Substances 0.000 claims description 9
- 235000005979 Citrus limon Nutrition 0.000 claims description 4
- 244000131522 Citrus pyriformis Species 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 claims description 4
- XMGQYMWWDOXHJM-UHFFFAOYSA-N limonene Chemical compound CC(=C)C1CCC(C)=CC1 XMGQYMWWDOXHJM-UHFFFAOYSA-N 0.000 claims description 4
- 239000007968 orange flavor Substances 0.000 claims description 4
- 239000002131 composite material Substances 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 2
- 239000000203 mixture Substances 0.000 claims description 2
- 238000005096 rolling process Methods 0.000 claims description 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims 3
- 239000000796 flavoring agent Substances 0.000 abstract description 9
- 235000019634 flavors Nutrition 0.000 abstract description 9
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 238000003860 storage Methods 0.000 abstract description 3
- 244000283207 Indigofera tinctoria Species 0.000 abstract description 2
- 239000000047 product Substances 0.000 description 12
- 150000004804 polysaccharides Chemical class 0.000 description 8
- 239000000654 additive Substances 0.000 description 7
- 230000000996 additive effect Effects 0.000 description 7
- 238000011156 evaluation Methods 0.000 description 6
- 238000012545 processing Methods 0.000 description 6
- 230000001953 sensory effect Effects 0.000 description 5
- 230000000391 smoking effect Effects 0.000 description 5
- 239000002904 solvent Substances 0.000 description 5
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 4
- 244000246386 Mentha pulegium Species 0.000 description 4
- 235000016257 Mentha pulegium Nutrition 0.000 description 4
- 235000004357 Mentha x piperita Nutrition 0.000 description 4
- 239000003814 drug Substances 0.000 description 4
- 235000001050 hortel pimenta Nutrition 0.000 description 4
- 230000002045 lasting effect Effects 0.000 description 4
- 239000002304 perfume Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 238000005303 weighing Methods 0.000 description 4
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 description 3
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 description 3
- 230000007812 deficiency Effects 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 229940041616 menthol Drugs 0.000 description 3
- 231100000614 poison Toxicity 0.000 description 3
- 230000007096 poisonous effect Effects 0.000 description 3
- 238000013461 design Methods 0.000 description 2
- 235000013399 edible fruits Nutrition 0.000 description 2
- 235000013599 spices Nutrition 0.000 description 2
- 230000002459 sustained effect Effects 0.000 description 2
- 239000002562 thickening agent Substances 0.000 description 2
- RSWGJHLUYNHPMX-UHFFFAOYSA-N 1,4a-dimethyl-7-propan-2-yl-2,3,4,4b,5,6,10,10a-octahydrophenanthrene-1-carboxylic acid Chemical compound C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 description 1
- 229920000742 Cotton Polymers 0.000 description 1
- 108010022355 Fibroins Proteins 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- -1 Propiram Polysaccharide Chemical class 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 235000010443 alginic acid Nutrition 0.000 description 1
- 239000000783 alginic acid Substances 0.000 description 1
- 229960001126 alginic acid Drugs 0.000 description 1
- 229920000615 alginic acid Polymers 0.000 description 1
- 150000004781 alginic acids Chemical class 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 125000003118 aryl group Chemical group 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 239000002537 cosmetic Substances 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000006870 function Effects 0.000 description 1
- 238000002290 gas chromatography-mass spectrometry Methods 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 239000003906 humectant Substances 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- 230000007794 irritation Effects 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 150000002885 octadecanoids Chemical class 0.000 description 1
- 239000013618 particulate matter Substances 0.000 description 1
- 239000004014 plasticizer Substances 0.000 description 1
- 229950003779 propiram Drugs 0.000 description 1
- 238000012797 qualification Methods 0.000 description 1
- 239000003507 refrigerant Substances 0.000 description 1
- 238000005070 sampling Methods 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 230000003313 weakening effect Effects 0.000 description 1
Abstract
Application the present invention provides a kind of scented gel with sustained release and preparation method thereof and in cigarette.The scented gel is after mixing propylene glycol, polyethylene glycol, stearic acid, malic acid, glucose, pulullan polysaccharide, sodium alginate according to certain proportion, merging is in the heating tank of agitating device, dissolution process is up to gel complex material, then the fragrance of mass ratio 10-50% is added, up to the scented gel with sustained release after mixing.Scented gel is applied to preparation thermal sensation slow-release fragrance filter stick in tow online during filter stick formation, is then carrying out cigarette trial-production on high-speed cigarette machine, pipe tobacco used is Yellow Crane Tower " soft indigo plant " blank pipe tobacco.Sustained-release gel of the present invention enters cigarette filter rod after mixing with fragrance, be solid-state under room temperature, solidify flavor component, reduce the fragrance loss during cigarette storage, preparation method is simple, economical and practical.
Description
Technical field
The present invention relates to cigarette flavors field, specifically a kind of scented gel with sustained release and its system
The standby and application in cigarette.
Background technique
Current National cigarette industry situation day is becoming tight, and the competition of cigarette product is fiercer, it means that produces to cigarette
The technology content requirement of product is higher, and the suction taste feature of cigarette needs further rich and variedization.With the innovation of production technology,
Cigarette scientific and technical personnel are developed using filter tip as the carrier of supplement main flume aromatic odor, apply essence in filter tip material
Fragrance prepares the cigarette of personalized note.For example, on filter tip rod forming machine will be impregnated with fragrance cotton thread insertion tow in or
Fragrance is dissolved in plasticizer to be applied in tow by person is made fragrance mouth stick.However, the cigarette prepared by the above method,
Distinctive fragrance is aspirating former mouthfuls of intensity abundances, and then several mouthfuls of intensity deficiencies, when burning and sucking cigarette end, fragrance is non-
It is often thin.Meanwhile during cigarette storage, some fragrance such as peppermint are readily volatilized, and residence time is shorter, shorten production
The shelf-life of product significantly limits application of the part fragrance in cigarette filter rod.It is therefore desirable to find efficient, reasonable add
Fragrant mode solves the above technological deficiency.
Gel rubber material has good absorption property and sustained release performance, through controlling essence frequently as sustained release agent and stabilizer
Release of the fragrance under specific occasion expands the application range of flavors and fragrances to effectively extend fragrance remaining time.
The characteristics of novel perfuming technology for exploration suitable for cigarette, loss volatile for part fragrance, purport of the present invention
A simple, practical, convenient approach is being found, is being as basic material, by adding feature flavors and fragrances using gel rubber material
Preparation has effects that the scented gel of sustained release, then gel products is added in cigarette filter rod, thermal sensation slow-release fragrance filter stick is made,
Guaranteeing that good flowing properties, cementability be strong and rate of drying is fastly to realizing its application in cigarette.
Summary of the invention
The purpose of the present invention is in view of the deficiencies of the prior art, provide it is a kind of have effects that sustained release scented gel and its system
Standby and the application in cigarette, the gel are strong to the carrying capacity of fragrance, and limit fragrance content reaches 50%, and the present invention
The material used is food-grade, will not introduce poisonous and harmful substance, is had easy to operate, economical and practical.
A kind of technical solution provided by the invention: scented gel with sustained release, it is characterised in that: the perfume (or spice)
Taste gel is that the fragrance of its quality 10~50% is added in composite gel material to obtain after mixing, wherein described compound solidifying
Glue material is by the material composition of following mass percent:
The present invention preferably technical solution: the propylene glycol, polyethylene glycol, stearic acid, malic acid, glucose, Propiram
Polysaccharide and sodium alginate are all made of GB2760 and are permitted workable food additives.
The present invention preferably technical solution: the essence is volatile flavouring essence for tobacco, including Mint Essence, Rum perfume
Essence, lemon extract, any one or a few in orange flavor.
The preparation method of a kind of scented gel with sustained release provided by the invention, it is characterised in that specific steps are such as
Under:
(1) prepare raw material: propylene glycol 40-60%, polyethylene glycol 10-20% according to the formula of following mass percent, firmly
Resin acid 10-20%, malic acid 0.1-1%, glucose 0.1-1%, pulullan polysaccharide 5-10%, sodium alginate 5-10%；
(2) raw material in strong step (1) is uniformly mixed merging in the heating tank of agitating device according to the proportion, 50~
3~5h of dissolution is carried out under the conditions of 70 DEG C while stirring and waits for that each raw material is completely dissolved to form gel complex material；
(3) have to obtain the final product after adding the fragrance mixing of its quality 10~50% in the gel complex material in step (2)
It is sustained the scented gel of effect.
The present invention preferably technical solution: in the step (3) essence be Mint Essence, rum essence, lemon extract,
The volatile flavouring essence for tobacco of any one or a few in orange flavor.
A kind of application of the scented gel with sustained release provided by the invention in cigarette filter tip, it is characterised in that:
The above-mentioned scented gel with sustained release is applied to preparation thermal sensation slow-release fragrance in tow online during filter stick formation
Then filter stick is rolling into cigarette on high-speed cigarette machine, wherein the additional amount of the scented gel with sustained release is
0.5~1.5mg/mm filter stick.
Propylene glycol is that GB2760 is permitted workable food additives, and is permitted workable additive, tool for tobacco business
Have good safety, can skin contact, oral, be usually used in tobacco humectant and perfume solvent.
Polyethylene glycol is that GB2760 license uses food additives, has good safety, can skin contact, oral,
Application in cosmetics industry and pharmaceuticals industry is very wide.
Stearic acid also known as octadecanoid acid are permitted workable food additives for GB2760, have good safety, can skin
It is skin contact, oral, it is cured tobacco leaf, burley tobaccos tobacco leaf, can be detected in Turkish tobaccos tobacco leaf, can be used as fruit glaze agent for day
With in chemical products and food.
Malic acid is that GB2760 is permitted workable food additives, and is permitted workable additive, tool for tobacco business
Have good safety, can skin contact, oral, in candy making industry, field of medicaments and tobacco business extensive application,
It can increase the acidity of tobacco to a certain extent, improve jealous, reduction irritation and miscellaneous gas.
Glucose is that GB2760 is permitted workable food additives, and is permitted workable additive, tool for tobacco business
Have good safety, can skin contact, oral, for the moisture retention of product can be improved in cigarette, can do corrigent be flue-cured tobacco,
Self-service cigarette processing charging.
Pulullan polysaccharide is that GB2760 is permitted workable food additives, has good safety, can skin contact, mouth
Clothes, are commonly used as fruit glaze agent and thickener is widely used in medicine and field of food.Dry sensation can be reduced by being added in cigarette,
Have the function of that extending cigarette dries out the phase.In addition, pulullan polysaccharide also has certain bacteriostasis property.
Sodium alginate is a kind of natural polysaccharide, is permitted workable food additives for GB2760, has good safety,
Can skin contact, oral, be used widely in food industry and field of medicaments as thickener.
Sustained-release gel of the present invention enters cigarette filter rod after mixing with fragrance, be solid-state under room temperature, solidify flavor component, reduce
Fragrance loss during cigarette storage；When cigarette is burnt and sucked, main flume is acted on by filter stick in the hot stream temperature of aerosol
Under, heated melt of gel is liquid, and fragrance component is released by diffusion, and gel rubber material controls fragrance as slow-release material
Release of the essence in filter stick effectively extends fragrance remaining time so that reaching fragrance discharges uniform purpose.
Beneficial effects of the present invention:
(1) gel of the present invention is strong to the carrying capacity of fragrance, and limit fragrance content reaches 50%, and the present invention makes
Material is food-grade, will not introduce poisonous and harmful substance, is had many advantages, such as easy to operate, economical and practical；
(2) gel perfuming effect of the invention is stablized, and lasting is lasting, avoids flavor component and participates in cigarette burning, guarantees
Effective stabilizations of tobacco aromaticss, uniformly, fragrance is very sufficient when during cigarette being burnt and sucked without occurring just starting for fragrance release
And back segment time fragrance the phenomenon that obviously weakening, further promote application effect of the tobacco aromaticss in cigarette；
(3) gel filing provision can be used in the scented gel prepared by the present invention, is added online by the additive amount of design
Into filter stick, thermal sensation slow-release fragrance filter stick is made, can effectively ensure that the controllability and homogeneity of flavors and fragrances additive amount, have
Very strong practicability.
Method of the invention has many advantages, such as easy to operate, economical and practical, and the material used is food-grade, will not be introduced
Poisonous and harmful substance, preparation properties of product stablize, gel rubber material to the pumped mass of cigarette product without negative effect, with volume
Cigarette compatibility is good, strong to the delivered payload capability of fragrance, and limit fragrance content reaches 50%.
Specific embodiment
Below with reference to embodiment, the present invention is further described.
A kind of scented gel with sustained release that embodiment 1 provides, preparation process are as follows:
(1) after weighing raw material according to certain formula rate, merging is had in the heating tank of agitating device, 50
It is dissolved while stirring under the conditions of DEG C, the processing time is 5h, and dissolution process is up to gel complex material；The proportion of its raw material
Are as follows: propylene glycol 60%, polyethylene glycol 10%, stearic acid 10%, malic acid 0.5%, glucose 0.5%, pulullan polysaccharide 9%,
Sodium alginate 10%.
(2) in the gel complex material in step (1) addition 25% Mint Essence, the solvent of Mint Essence is the third two
Alcohol stirs and evenly mixs rear up to the mint flavored gel with sustained release.
A kind of scented gel with sustained release that embodiment 2 provides, preparation process are as follows:
(1) after weighing raw material according to certain formula rate, merging is had in the heating tank of agitating device, 70
It is dissolved while stirring under the conditions of DEG C, the processing time is 3h, and dissolution process is up to gel complex material.The proportion of raw material are as follows:
Propylene glycol 40%, polyethylene glycol 19%, stearic acid 19%, malic acid 1%, glucose 1%, pulullan polysaccharide 10%, alginic acid
Sodium 10%.
(2) in the gel complex material in step (1) addition 50% Mint Essence, the solvent of Mint Essence is the third two
Alcohol stirs and evenly mixs rear up to the mint flavored gel with sustained release.
Embodiment 3 provides a kind of scented gel with sustained release, and preparation process is as follows:
(1) after weighing raw material according to certain formula rate, merging is had in the heating tank of agitating device, 60
It is dissolved while stirring under the conditions of DEG C, the processing time is 4h, and dissolution process is up to gel complex material.The proportion of raw material are as follows:
Propylene glycol 50%, polyethylene glycol 16%, stearic acid 16%, malic acid 1%, glucose 1%, pulullan polysaccharide 8%, sodium alginate
8%.
(2) in the gel complex material in step (1) addition 20% Mint Essence, the solvent of Mint Essence is the third two
Alcohol stirs and evenly mixs rear up to the mint flavored gel with sustained release.
Embodiment 4 provides a kind of scented gel with sustained release, and preparation process is as follows: having effects that the perfume (or spice) of sustained release
Taste gel process for preparing is as follows:
(1) after weighing raw material according to certain formula rate, merging is had in the heating tank of agitating device, 65
It is dissolved while stirring under the conditions of DEG C, the processing time is 3.5h, and dissolution process is up to gel complex material.The proportion of raw material
Are as follows: propylene glycol 45%, polyethylene glycol 20%, stearic acid 15%, malic acid 0.5%, glucose 1%, pulullan polysaccharide 8.5%,
Sodium alginate 10%.
(2) in the gel complex material in step (1) addition 40% Mint Essence, the solvent of Mint Essence is the third two
Alcohol stirs and evenly mixs rear up to the mint flavored gel with sustained release.
Application examples: it is sustained application of the mint flavored gel of effect in cigarette filter rod
Using the gel filing provision of autonomous Design, by mint flavored gel prepared by embodiment 1-4 in filter stick formation
It is applied to preparation thermal sensation slow-release fragrance filter stick in tow online in the process, is then carrying out cigarette trial-production on high-speed cigarette machine,
Pipe tobacco used is Yellow Crane Tower " soft indigo plant " blank pipe tobacco.To guarantee that the essence content in each filter stick is consistent, peppermint described in embodiment 1-4
The additional amount of scented gel is respectively 1.0mg/mm filter stick, 0.5mg/mm filter stick, 1.25mg/mm filter stick, 0.625mg/mm filter stick.
Trial-production cigarette is evaluated referring to State Bureau's evaluation standard, group of smokeing panel test is by 13 cigarette sensory evaluation expert groups
At using secretly commenting mode to carry out sensory evaluation and giving a mark, Analyses Methods for Sensory Evaluation Results is as shown in table 1.Blank is straight in filter stick fibroin
The addition made cigarette of Mint Essence is connect, essence adding proportion is 0.25mg/mm filter stick.
1 cigarette sensory effects evaluation result of table
| Sample | Blank | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 |
| Mean scores | 72.5 | 84.5 | 85.5 | 84.9 | 85.0 |
The result shows that:
(1) the essence maximum additive amount of scented gel of the present invention up to 50%, stablize by the online molding effect of filter stick,
Product qualification rate reaches 95% or more, does not make significant difference to indexs such as filter stick hardness, seam brokens.
(2) gel rubber material is to the pumped mass of cigarette product without negative effect, the cigarette manufactured experimently good with cigarette compatibility
Product is after sensory evaluating smoking, and evaluation score significantly improves, and application effect is more significant, and lasting is lasting, has in aspiration procedure
The refrigerant feature of apparent peppermint, comfortable taste are pure；And the release of its fragrance is uniformly, when in aspiration procedure without occurring just starting
Mint flavored is very sufficient and the phenomenon that back segment time fragrance obviously weakens, there is preferable slow release effect.
In order to further verify the uniformity and stability of mint flavored release when cigarette is burnt and sucked, using smoking machine to peppermint
Fragrant uniformity of releasing during cigarette smoking is studied.It takes and uses in embodiment 1-4 sample cigarette 40 made of scented gel,
Two groups are equally divided into, is detected on smoking machine by certain puff number respectively.First group of two groups of cigarette is at the 4th mouthful
Place is artificial to extinguish, and second group of artificial extinguishing at the 7th mouthful traps total particulate matter in mainstream smoke with cambridge filter, then at
Reason, sampling carries out GC-MS analysis, wherein the peak area ratio of menthol is more as shown in table 2 in two groups of sample cigarette main flumes.
The slow release effect of Mint Essence during 2 cigarette smoking of table
Fragrant effect is released compared in aspiration procedure according to the peak area ratio of menthol in two groups of sample cigarette main flumes.Through data
Processing it is found that said sample cigarette aspirate in four mouthfuls and seven mouthfuls of main flumes the ratio between menthol content respectively 4.10/7,4.07/7,
4.06/7,4.09/7, this further explanation is released in combustion using sample cigarette made of scented gel in embodiment 1-4
It is fragrant uniform.
The present invention is of the present invention to add in gel rubber material only using Mint Essence as additive as demonstration
Flavors and fragrances be not limited to Mint Essence, the low flavors and fragrances product of other volatile, low boiling points, threshold value can be extended to
Kind.
Claims (6)
1. a kind of scented gel with sustained release, it is characterised in that: the scented gel is added in composite gel material
The fragrance for entering its quality 10~50% obtains after mixing, wherein the composite gel material is by following mass percent
Material composition:
2. a kind of scented gel with sustained release according to claim 1, it is characterised in that: the propylene glycol is gathered
Ethylene glycol, stearic acid, malic acid, glucose, pulullan polysaccharide and sodium alginate are all made of GB2760 and are permitted workable food additive
Add agent.
3. a kind of scented gel with sustained release according to claim 1, it is characterised in that: the essence is easily to wave
The flavouring essence for tobacco of hair, including any one or a few in Mint Essence, rum essence, lemon extract, orange flavor.
4. a kind of preparation method of the scented gel with sustained release described in claim 1, it is characterised in that specific steps
It is as follows:
(1) prepare raw material: propylene glycol 40-60%, polyethylene glycol 10-20%, stearic acid according to the formula of following mass percent
10-20%, malic acid 0.1-1%, glucose 0.1-1%, pulullan polysaccharide 5-10%, sodium alginate 5-10%；
(2) raw material in strong step (1) is uniformly mixed merging according to the proportion and has in the heating tank of agitating device, at 50~70 DEG C
Under the conditions of carry out 3~5h of dissolution while stirring and wait for that each raw material is completely dissolved to form gel complex material；
(3) there is sustained release to obtain the final product after adding the fragrance mixing of its quality 10~50% in the gel complex material in step (2)
The scented gel of effect.
5. a kind of preparation method of scented gel with sustained release according to claim 4, it is characterised in that: described
Essence is that Mint Essence, rum essence, lemon extract, any one or a few in orange flavor are volatile in step (3)
Flavouring essence for tobacco.
6. a kind of application according to the scented gel with sustained release of the method preparation in claim 4 in cigarette,
It is characterized in that: the above-mentioned scented gel with sustained release being applied in tow online during filter stick formation and prepares thermal sensation
Then slow-release fragrance filter stick is rolling into cigarette on high-speed cigarette machine, wherein the scented gel with sustained release
Additional amount is 0.5~1.5mg/mm filter stick.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
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| CN110537729A (en) * | 2019-09-20 | 2019-12-06 | 安徽坤大生物工程技术有限公司 | Instant cigarette blasting bead |
| CN110754687A (en) * | 2019-10-31 | 2020-02-07 | 湖北中烟工业有限责任公司 | Preparation method of magnolia officinalis flavored cigarette filter |
| CN111000288A (en) * | 2019-12-30 | 2020-04-14 | 福建中烟工业有限责任公司 | Gel for cigarettes and tobacco products |
| CN111035061A (en) * | 2019-12-30 | 2020-04-21 | 福建中烟工业有限责任公司 | Composition for cigarettes, preparation method and application thereof |
| CN111117768A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Composition for cigarette, preparation method thereof and application of composition in tobacco products |
| CN111109654A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Composition for cigarettes, preparation method and application thereof, and cigarette filter stick |
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| CN111109653A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Gel for cigarettes and tobacco products |
| CN111213903A (en) * | 2020-02-20 | 2020-06-02 | 云南氪莱铂科技有限公司 | High-fuming particle for heating non-combustible product and preparation method and application thereof |
| CN112075662A (en) * | 2020-10-19 | 2020-12-15 | 甘肃烟草工业有限责任公司 | Preparation method of natural ylang-rosea flavor-carrying gel filter stick and application of natural ylang-rosea flavor-carrying gel filter stick in cigarettes |
| CN115151145A (en) * | 2019-11-29 | 2022-10-04 | 尼科创业贸易有限公司 | Aerosol generation |
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| CN110537729A (en) * | 2019-09-20 | 2019-12-06 | 安徽坤大生物工程技术有限公司 | Instant cigarette blasting bead |
| CN110754687A (en) * | 2019-10-31 | 2020-02-07 | 湖北中烟工业有限责任公司 | Preparation method of magnolia officinalis flavored cigarette filter |
| CN110754687B (en) * | 2019-10-31 | 2022-03-04 | 湖北中烟工业有限责任公司 | Preparation method of magnolia officinalis flavored cigarette filter |
| CN115151145B (en) * | 2019-11-29 | 2024-01-26 | 尼科创业贸易有限公司 | Aerosol generation |
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| CN111117767A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Gel for cigarettes and tobacco products |
| CN111109654A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Composition for cigarettes, preparation method and application thereof, and cigarette filter stick |
| CN111109653A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Gel for cigarettes and tobacco products |
| CN111117768A (en) * | 2019-12-30 | 2020-05-08 | 福建中烟工业有限责任公司 | Composition for cigarette, preparation method thereof and application of composition in tobacco products |
| CN111035061A (en) * | 2019-12-30 | 2020-04-21 | 福建中烟工业有限责任公司 | Composition for cigarettes, preparation method and application thereof |
| CN111000288A (en) * | 2019-12-30 | 2020-04-14 | 福建中烟工业有限责任公司 | Gel for cigarettes and tobacco products |
| CN111213903A (en) * | 2020-02-20 | 2020-06-02 | 云南氪莱铂科技有限公司 | High-fuming particle for heating non-combustible product and preparation method and application thereof |
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| CN112075662A (en) * | 2020-10-19 | 2020-12-15 | 甘肃烟草工业有限责任公司 | Preparation method of natural ylang-rosea flavor-carrying gel filter stick and application of natural ylang-rosea flavor-carrying gel filter stick in cigarettes |
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