CN111109654A - Composition for cigarettes, preparation method and application thereof, and cigarette filter stick - Google Patents
Composition for cigarettes, preparation method and application thereof, and cigarette filter stick Download PDFInfo
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- CN111109654A CN111109654A CN201911394370.7A CN201911394370A CN111109654A CN 111109654 A CN111109654 A CN 111109654A CN 201911394370 A CN201911394370 A CN 201911394370A CN 111109654 A CN111109654 A CN 111109654A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
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- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The invention belongs to the field of tobacco products, and particularly relates to a composition for cigarettes, which comprises the following components: 13-37 parts of polyethylene glycol 800, 35-76 parts of polyethylene glycol 1500, 15-41 parts of stearic acid, 0.5-11 parts of citric acid, 0.1-5 parts of malic acid and 0.1-4 parts of tea polyphenol. The invention also relates to a preparation method and application of the cigarette composition, and a cigarette filter stick. The composition for cigarettes is added into the cigarette filter stick, so that the release of essence fragrance is more obvious, the harmony of the essence fragrance and the cigarette fragrance is good, the smoking fragrance quality of the cigarettes is improved, the aftertaste comfort of the cigarettes is improved, the irritation and miscellaneous gas of smoke are reduced, and the sensory quality of the cigarettes is improved.
Description
Technical Field
The invention belongs to the field of tobacco products, and particularly relates to a tobacco composition, a preparation method and application of the tobacco composition, and a cigarette filter stick containing the tobacco composition.
Background
The cigarette belongs to a hobby product, the tar contained in the cigarette seriously harms human health, the tar content of the cigarette is greatly reduced along with the promotion of harm and tar reduction work, but the smoking quality of the cigarette is also influenced. How to greatly reduce tar while keeping the smoking taste of cigarettes has become a technical problem in the cigarette industry and also becomes a key factor for restricting the development of low-tar cigarettes at present.
The essence and the spice can cover the defects of the tobacco, improve the fragrance and the taste of the tobacco and improve the physical performance of the tobacco in the cigarette, can endow the cigarette with unique taste and style, and realize quality differentiation. The method has the advantages that the aroma quality of cigarette smoking is stabilized, the formation of the style and quality of cigarettes is greatly influenced, and the method is also the key for highlighting and propagating the style characteristics of cigarette brands and expanding and developing the cigarette brands. At present, essence and spice are mainly added into tobacco shreds, the cigarette fragrance is increased along with the combustion of the tobacco shreds in the smoking process, or solid particles or capsules loaded with essence are directly added into cigarette filter sticks to increase the fragrance, but the cigarette fragrance increasing methods generally have the defects of uneven fragrance release, short storage time, poor harmony of the fragrance and the smoke, heavy miscellaneous gas and the like, so that the fragrance improving effect is not ideal.
The gel is a good perfume-locking material, the melted glue solution is mixed with essence, and the gel can lock the essence after the normal temperature is recovered. The gel containing the essence is added into the cigarette filter stick, and when a consumer smokes the cigarette, the gel in the cigarette filter stick is melted into liquid under the influence of the smoke temperature, so that the aroma of the essence is released. However, researches find that the existing cigarette products generally have the problems of heavy oil smell during smoking, incongruity between essence aroma and tobacco aroma, poor smoking taste and the like.
At present, a tobacco composition which is added into a cigarette filter stick, can ensure that the fragrance of the essence is uniformly released, the fragrance and the tobacco fragrance are coordinated, the miscellaneous gas and the irritation are low, and the sensory quality of the cigarette is improved is needed.
Disclosure of Invention
The invention provides a composition for cigarettes, which is added into a cigarette filter stick, so that the release of essence fragrance is more obvious, the harmony of the essence fragrance and the cigarette fragrance is good, the smoking fragrance quality of the cigarettes is improved, the aftertaste comfort of the cigarettes is improved, the irritation and the miscellaneous gas of smoke are reduced, and the sensory quality of the cigarettes is improved. On the basis, the invention also provides a preparation method of the cigarette composition, application of the cigarette composition in tobacco products, and a cigarette filter stick containing the cigarette composition.
The invention relates to a composition for cigarettes, which comprises the following components:
polyethylene glycol 80013 to 37 parts by weight (e.g., 15 parts by weight, 17 parts by weight, 19 parts by weight, 20 parts by weight, 22 parts by weight, 24 parts by weight, 26 parts by weight, 28 parts by weight, 30 parts by weight, 31 parts by weight, 33 parts by weight, 35 parts by weight, 36 parts by weight)
150035 to 76 parts by weight of polyethylene glycol (e.g., 38 parts by weight, 39 parts by weight, 40 parts by weight, 42 parts by weight, 44 parts by weight, 46 parts by weight, 48 parts by weight, 50 parts by weight, 52 parts by weight, 54 parts by weight, 56 parts by weight, 58 parts by weight, 60 parts by weight, 62 parts by weight, 65 parts by weight, 67 parts by weight, 69 parts by weight, 70 parts by weight, 71 parts by weight, 73 parts by weight, 75 parts by weight, 76 parts by weight)
Stearic acid 15 to 41 parts by weight (for example, 18 parts by weight, 20 parts by weight, 22 parts by weight, 24 parts by weight, 26 parts by weight, 28 parts by weight, 30 parts by weight, 32 parts by weight, 34 parts by weight, 36 parts by weight, 38 parts by weight, 40 parts by weight, 41 parts by weight)
Citric acid 0.5 to 11 parts by weight (e.g., 0.8 part by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 4 parts by weight, 5 parts by weight, 6 parts by weight, 7 parts by weight, 9 parts by weight, 10 parts by weight)
Malic acid 0.1 to 5 parts by weight (e.g., 0.2 parts by weight, 0.5 parts by weight, 0.6 parts by weight, 0.8 parts by weight, 1 part by weight, 1.2 parts by weight, 1.5 parts by weight, 1.7 parts by weight, 2 parts by weight, 2.2 parts by weight, 2.5 parts by weight, 2.7 parts by weight, 2.8 parts by weight, 2.9 parts by weight, 3 parts by weight, 3.3 parts by weight, 3.6 parts by weight, 4 parts by weight, 4.2 parts by weight, 4.5 parts by weight, 4.8 parts by weight)
0.1 to 4 parts by weight (e.g., 0.3 part by weight, 0.5 part by weight, 0.7 part by weight, 0.9 part by weight, 1 part by weight, 1.1 part by weight, 1.2 parts by weight, 1.3 parts by weight, 1.4 parts by weight, 2 parts by weight, 2.3 parts by weight, 2.5 parts by weight, 2.7 parts by weight, 3 parts by weight, 3.2 parts by weight, 3.4 parts by weight, 3.6 parts by weight, 3.8 parts by weight) of tea polyphenol.
In some embodiments of the first aspect of the present invention, the tobacco composition further comprises a tobacco flavor.
In some embodiments of the first aspect of the present invention, the amount of the tobacco flavor is 0.1 to 130 parts by weight, for example, 0.5 parts by weight, 0.8 parts by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 5 parts by weight, 7 parts by weight, 10 parts by weight, 13 parts by weight, 15 parts by weight, 20 parts by weight, 25 parts by weight, 30 parts by weight, 35 parts by weight, 40 parts by weight, 45 parts by weight, 50 parts by weight, 60 parts by weight, 70 parts by weight, 80 parts by weight, 84 parts by weight, 86 parts by weight, 90 parts by weight, 95 parts by weight, 100 parts by weight, 104 parts by weight, 108 parts by weight, 110 parts by weight, 113 parts by weight, 116 parts by weight, 120 parts by weight, 124 parts by weight, 127 parts by weight, 130 parts by weight.
In some embodiments of the first aspect of the present invention, the tobacco flavor is selected from the group consisting of floral, fruity, and alcoholic flavors; floral essences include, but are not limited to, osmanthus-flavored essences, orchid-flavored essences, lily-flavored essences; fruit flavors include, but are not limited to, Hami melon flavor, passion fruit flavor, grape flavor; wine flavors include, but are not limited to, Maotai-flavor liquor flavors, red wine flavors, whisky flavors.
In some embodiments of the first aspect of the present invention, the tobacco flavor is selected from the group consisting of lily, grape, whiskey, osmanthus and passion fruit flavors.
In some embodiments of the first aspect of the present invention, the osmanthus-passion fruit-flavored essence is an essence that is a combination of osmanthus-flavored essence and passion fruit-flavored essence.
In some embodiments of the first aspect of the present invention, the osmanthus-passion fruit-flavored essence is an essence formed by mixing osmanthus-flavored essence and passion fruit-flavored essence.
In some embodiments of the first aspect of the present invention, the tobacco flavor comprises a solvent; preferably, the solvent is propylene glycol.
In some embodiments of the first aspect of the present invention, the content of the aroma component in the tobacco flavor is 1% (W/W) to 99% (W/W), for example, 10% (W/W), 20% (W/W), 30% (W/W), 40% (W/W), 50% (W/W), 60% (W/W), 70% (W/W), 80% (W/W), 90% (W/W).
In some embodiments of the first aspect of the present invention, the tobacco flavor may be a tobacco flavor that is conventional in the art and is available directly from the market.
In some embodiments of the first aspect of the present invention, the tobacco flavor is purchased from Balginia indica Biotech limited.
In some embodiments of the first aspect of the present invention, the smoking composition comprises the following components:
in some embodiments of the first aspect of the present invention, the smoking composition comprises the following components:
polyethylene glycol 80020 to 30 parts by weight (e.g., 21 parts by weight, 22 parts by weight, 23 parts by weight, 24 parts by weight, 25 parts by weight, 26 parts by weight, 27 parts by weight, 28 parts by weight, 29 parts by weight)
150040 to 65 parts by weight of polyethylene glycol (e.g., 42 parts by weight, 43 parts by weight, 44 parts by weight, 45 parts by weight, 46 parts by weight, 47 parts by weight, 48 parts by weight, 49 parts by weight, 50 parts by weight, 52 parts by weight, 55 parts by weight, 57 parts by weight, 60 parts by weight, 62 parts by weight, 64 parts by weight)
Stearic acid 20 to 40 parts by weight (for example, 22 parts by weight, 24 parts by weight, 25 parts by weight, 26 parts by weight, 28 parts by weight, 30 parts by weight, 32 parts by weight, 34 parts by weight, 35 parts by weight, 36 parts by weight, 37 parts by weight, 38 parts by weight)
1 to 6 parts by weight (e.g., 2 parts by weight, 3 parts by weight, 4 parts by weight, 5 parts by weight)
Malic acid 0.3 to 1 part by weight (e.g., 0.4 part by weight, 0.5 part by weight, 0.6 part by weight, 0.7 part by weight, 0.8 part by weight, 0.9 part by weight)
0.2 to 0.8 part by weight (e.g., 0.3 part by weight, 0.4 part by weight, 0.5 part by weight, 0.6 part by weight, 0.7 part by weight)
40-70 parts by weight of lily-flavored essence;
preferably, the content of the aroma component in the lily-flavored essence is 30% (W/W) to 60(W/W), such as 40% (W/W) and 50% (W/W);
preferably, the solvent in the lily-flavored essence is propylene glycol.
In some embodiments of the first aspect of the present invention, the smoking composition comprises the following components:
polyethylene glycol 80020 to 30 parts by weight (e.g., 21 parts by weight, 22 parts by weight, 23 parts by weight, 24 parts by weight, 25 parts by weight, 26 parts by weight, 27 parts by weight, 28 parts by weight, 29 parts by weight)
150040 to 65 parts by weight of polyethylene glycol (e.g., 42 parts by weight, 43 parts by weight, 44 parts by weight, 45 parts by weight, 46 parts by weight, 47 parts by weight, 48 parts by weight, 49 parts by weight, 50 parts by weight, 52 parts by weight, 55 parts by weight, 57 parts by weight, 60 parts by weight, 62 parts by weight, 64 parts by weight)
Stearic acid 20 to 40 parts by weight (for example, 22 parts by weight, 24 parts by weight, 25 parts by weight, 26 parts by weight, 28 parts by weight, 30 parts by weight, 32 parts by weight, 34 parts by weight, 35 parts by weight, 36 parts by weight, 37 parts by weight, 38 parts by weight)
1 to 6 parts by weight (e.g., 2 parts by weight, 3 parts by weight, 4 parts by weight, 5 parts by weight)
Malic acid 0.3 to 1 part by weight (e.g., 0.4 part by weight, 0.5 part by weight, 0.6 part by weight, 0.7 part by weight, 0.8 part by weight, 0.9 part by weight)
0.2 to 0.8 part by weight (e.g., 0.3 part by weight, 0.4 part by weight, 0.5 part by weight, 0.6 part by weight, 0.7 part by weight)
2-30 parts by weight of grape-flavored essence;
preferably, the content of the aroma component in the grape-flavor essence is 30% (W/W) to 60% (W/W), such as 40% (W/W) and 50% (W/W);
preferably, the solvent in the grape-flavored essence is propylene glycol.
In some embodiments of the first aspect of the present invention, the smoking composition comprises the following components:
polyethylene glycol 80020 to 30 parts by weight (e.g., 21 parts by weight, 22 parts by weight, 23 parts by weight, 24 parts by weight, 25 parts by weight, 26 parts by weight, 27 parts by weight, 28 parts by weight, 29 parts by weight)
150040 to 65 parts by weight of polyethylene glycol (e.g., 42 parts by weight, 43 parts by weight, 44 parts by weight, 45 parts by weight, 46 parts by weight, 47 parts by weight, 48 parts by weight, 49 parts by weight, 50 parts by weight, 52 parts by weight, 55 parts by weight, 57 parts by weight, 60 parts by weight, 62 parts by weight, 64 parts by weight)
Stearic acid 20 to 40 parts by weight (for example, 22 parts by weight, 24 parts by weight, 25 parts by weight, 26 parts by weight, 28 parts by weight, 30 parts by weight, 32 parts by weight, 34 parts by weight, 35 parts by weight, 36 parts by weight, 37 parts by weight, 38 parts by weight)
1 to 6 parts by weight (e.g., 2 parts by weight, 3 parts by weight, 4 parts by weight, 5 parts by weight)
Malic acid 0.3 to 1 part by weight (e.g., 0.4 part by weight, 0.5 part by weight, 0.6 part by weight, 0.7 part by weight, 0.8 part by weight, 0.9 part by weight)
0.2 to 0.8 part by weight (e.g., 0.3 part by weight, 0.4 part by weight, 0.5 part by weight, 0.6 part by weight, 0.7 part by weight)
80-120 parts by weight of whisky essence;
preferably, the content of the aroma component in the whisky flavour is 50% (W/W) to 80% (W/W), such as 60% (W/W) and 70% (W/W);
preferably, the solvent in the whisky flavour is propylene glycol.
In some embodiments of the first aspect of the present invention, the smoking composition comprises the following components:
polyethylene glycol 80020 to 30 parts by weight (e.g., 21 parts by weight, 22 parts by weight, 23 parts by weight, 24 parts by weight, 25 parts by weight, 26 parts by weight, 27 parts by weight, 28 parts by weight, 29 parts by weight)
150040 to 65 parts by weight of polyethylene glycol (e.g., 42 parts by weight, 43 parts by weight, 44 parts by weight, 45 parts by weight, 46 parts by weight, 47 parts by weight, 48 parts by weight, 49 parts by weight, 50 parts by weight, 52 parts by weight, 55 parts by weight, 57 parts by weight, 60 parts by weight, 62 parts by weight, 64 parts by weight)
Stearic acid 20 to 40 parts by weight (for example, 22 parts by weight, 24 parts by weight, 25 parts by weight, 26 parts by weight, 28 parts by weight, 30 parts by weight, 32 parts by weight, 34 parts by weight, 35 parts by weight, 36 parts by weight, 37 parts by weight, 38 parts by weight)
1 to 6 parts by weight (e.g., 2 parts by weight, 3 parts by weight, 4 parts by weight, 5 parts by weight)
Malic acid 0.3 to 1 part by weight (e.g., 0.4 part by weight, 0.5 part by weight, 0.6 part by weight, 0.7 part by weight, 0.8 part by weight, 0.9 part by weight)
0.2 to 0.8 part by weight (e.g., 0.3 part by weight, 0.4 part by weight, 0.5 part by weight, 0.6 part by weight, 0.7 part by weight)
90-120 parts by weight of osmanthus-passion fruit-flavored essence;
preferably, the content of the aroma component in the osmanthus-passion fruit flavor is 45% (W/W) to 75% (W/W), such as 50% (W/W), 55% (W/W), 60% (W/W), 65% (W/W) and 70% (W/W);
preferably, the solvent flavor propylene glycol in the osmanthus fragrans-passion fruit flavor.
In some embodiments of the first aspect of the present invention, the composition for tobacco is in the form of a gel under ambient conditions.
In a second aspect, the invention relates to a cigarette filter or filter comprising a composition for use in a cigarette according to the first aspect of the invention.
In some embodiments of the second aspect of the present invention, the amount of the smoking composition per cigarette filter rod or filter is 1 to 200mg, such as 5mg, 10mg, 15mg, 20mg, 25mg, 30mg, 35mg, 40mg, 45mg, 50mg, 60mg, 70mg, 80mg, 90mg, 100mg, 120mg, 140mg, 150mg, 160mg, 180mg, 190 mg.
In some embodiments of the second aspect of the present invention, the diameter of the cigarette filter stick or filter is 1 to 20mm, for example 2mm, 2.5mm, 3mm, 3.5mm, 4mm, 4.5mm, 5mm, 5.5mm, 6mm, 6.5mm, 7mm, 7.3mm, 7.7mm, 7.5mm, 8mm, 8.5mm, 9mm, 10mm, 11mm, 12mm, 13mm, 14mm, 15mm, 16mm, 17mm, 18mm, 19 mm.
In some embodiments of the second aspect of the present invention, the pressure drop of the cigarette filter rod or filter is 1000 to 8000Pa, such as 1100Pa, 1200Pa, 1300Pa, 1400Pa, 1500Pa, 1700Pa, 1800Pa, 2000Pa, 2200Pa, 2500Pa, 2700Pa, 3000Pa, 3200Pa, 3400Pa, 3600Pa, 3800Pa, 4000Pa, 4200Pa, 4400Pa, 4600Pa, 4800Pa, 5000Pa, 5200Pa, 5500Pa, 5700Pa, 5800Pa, 6000Pa, 6300Pa, 6500Pa, 6700Pa, 6800Pa, 7000Pa, 7200Pa, 7400Pa, 7600Pa, 7800 Pa.
In some embodiments of the second aspect of the present invention, the smoking composition in the cigarette filter rod or filter is in the form of a gel at ambient temperature.
In some embodiments of the second aspect of the present invention, the cross-section of the gelatinous smoking composition in the cigarette filter rod or filter is circular, pentagonal, or polygonal.
In some embodiments of the second aspect of the invention, the cross-sectional area of the gelatinous smoking composition comprises from 1% to 16%, for example 2%, 3%, 4%, 5%, 6%, 7%, 8%, 9%, 10%, 12%, 14%, 15% of the total cross-sectional area of the cigarette filter rod or filter.
In a third aspect, the invention relates to a cigarette comprising a smoking composition according to the first aspect of the invention, or comprising a cigarette filter rod or filter according to the second aspect of the invention.
In a fourth aspect, the present invention relates to a process for the preparation of a composition for use in cigarettes according to the first aspect of the invention, comprising the steps of:
(1) heating polyethylene glycol 800, polyethylene glycol 1500 and stearic acid to melt, and mixing to obtain a mixture;
(2) mixing the mixture, citric acid, malic acid, tea polyphenols and optional tobacco essence under sealed condition;
in certain embodiments of the fourth aspect of the present invention, in step (1), the temperature of heating and the temperature of mixing are not lower than the highest of the condensation point of polyethylene glycol 800, the condensation point of polyethylene glycol 1500 and the condensation point of stearic acid.
In certain embodiments of the fourth aspect of the present invention, the temperature of mixing in step (2) is not lower than the temperature of mixing in step (1).
In some embodiments of the fourth aspect of the present invention, the heating temperature in step (1) is not less than 62 ℃, preferably not less than 63 ℃, e.g., 65 ℃, 67 ℃, 69 ℃, 70 ℃, 72 ℃, 74 ℃, 75 ℃, 77 ℃, 78 ℃, 90 ℃, 92 ℃, 95 ℃, 97 ℃, 98 ℃, 100 ℃, 102 ℃, 105 ℃, 107 ℃, 110 ℃, 112 ℃, 115 ℃, 117 ℃, 120 ℃.
In some embodiments of the fourth aspect of the present invention, the temperature of mixing in step (1) is not less than 62 ℃, preferably not less than 63 ℃, e.g., 65 ℃, 67 ℃, 69 ℃, 70 ℃, 72 ℃, 74 ℃, 75 ℃, 77 ℃, 78 ℃, 90 ℃, 92 ℃, 95 ℃, 97 ℃, 98 ℃, 100 ℃, 102 ℃, 105 ℃, 107 ℃, 110 ℃, 112 ℃, 115 ℃, 117 ℃, 120 ℃.
In some embodiments of the fourth aspect of the present invention, the temperature of mixing in step (2) is not less than 62 ℃, preferably not less than 63 ℃, e.g., 65 ℃, 67 ℃, 69 ℃, 70 ℃, 72 ℃, 74 ℃, 75 ℃, 77 ℃, 78 ℃, 90 ℃, 92 ℃, 95 ℃, 97 ℃, 98 ℃, 100 ℃, 102 ℃, 105 ℃, 107 ℃, 110 ℃, 112 ℃, 115 ℃, 117 ℃, 120 ℃.
In some embodiments of the fourth aspect of the present invention, in step (2), citric acid, malic acid, tea polyphenol and optionally tobacco flavor are slowly added to the mixture under sealed conditions and mixed.
In some embodiments of the fourth aspect of the present invention, the weight ratio of polyethylene glycol 800, polyethylene glycol 1500, stearic acid, citric acid, malic acid, tea polyphenols and optionally tobacco flavour is as described in the first aspect of the present invention.
In some embodiments of the fourth aspect of the invention, the composition of the tobacco flavour is as described in the first aspect of the invention.
A fifth aspect of the invention relates to the use of a composition according to the first aspect of the invention for use in the manufacture of a cigarette filter, cigarette filter or cigarette.
The sixth aspect of the present invention relates to the use of the tobacco composition according to the first aspect of the present invention, or the cigarette filter stick or the cigarette filter according to the second aspect of the present invention, for improving the sensory quality of a cigarette.
In some embodiments of the sixth aspect of the present invention, the sensory quality of the cigarette is assessed by an indicator selected from the group consisting of aroma, harmony, aftertaste, irritation, and offensive odor.
In the invention, the polyethylene glycol 800 is white paste, the condensation point is 33-38 ℃, the average molecular weight is 750-850, the viscosity is 2.2-2.4, and the pH value is 5-7; the average molecular weight and viscosity were measured by the method of "polyethylene glycol 1500" in the fourth part of the pharmacopoeia 2015 of china.
In the present invention, polyethylene glycol 1500 complies with the specifications in the fourth part of the chinese pharmacopoeia 2015 edition.
In the present invention, stearic acid complies with the regulations in the four parts of the chinese pharmacopoeia 2015 edition.
In the invention, the citric acid meets the relevant national food and drug safety regulations, such as the GB1886.235-2016 food safety national standard food additive citric acid regulation.
In the invention, the malic acid meets the relevant regulations of national food and drug safety, such as the regulations of national standards GB1886.40-2015 and GB 25544-.
The tea polyphenol is a complex of more than 30 phenolic compounds separated and extracted from natural plant tea leaves, accounts for about 20-30% of the total dry matter of the tea leaves, and comprises flavanol, flavandiol, flavonoid and phenolic acid 4 substances. Flavanols are commonly referred to as catechins and constitute about 70% of the tea polyphenols. The catechin mainly comprises epigallocatechin gallate, epigallocatechin, epicatechin gallate, epicatechin, gallocatechin and catechin. The tea polyphenol in the invention conforms to the relevant regulations of national food and drug safety, for example, the tea polyphenol conforms to the regulations of GB 1886.211-2016 (national food safety standard) food additive tea polyphenol (vitamin polyphenol).
In the present invention, polyethylene glycol 800, polyethylene glycol 1500, stearic acid, citric acid, malic acid and tea polyphenol can be obtained from conventional purchase sources.
In the invention, the aroma injection equipment is usually an aroma and flavor injection machine and is mainly used for injecting aroma and flavor into cigarettes or cigarette filters.
In the present invention, the material of the cigarette filter stick is a common material, for example, selected from acetate fibers, polypropylene fibers, polylactic acid fibers and a composite material of any of the above.
The invention has the following beneficial effects:
the composition for cigarettes is added into a cigarette filter stick, so that the release of essence fragrance is more obvious, the harmony of the essence fragrance and the cigarette fragrance is good, the smoking fragrance quality of the cigarettes is improved, the aftertaste comfort of the cigarettes is improved, the irritation and the miscellaneous gas of smoke are reduced, and the sensory quality of the cigarettes is improved.
Detailed Description
Embodiments of the present invention will now be described more fully hereinafter with reference to the accompanying examples, in which some, but not all embodiments of the invention are shown. The following description of at least one exemplary embodiment is merely illustrative in nature and is in no way intended to limit the invention, its application, or uses. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The following examples and comparative examples used the following materials:
lily-flavored essence, grape-flavored essence, whisky-flavored essence and osmanthus-passion fruit-flavored essence are all purchased from Balanophora indica Biotech limited.
Example 1: preparation and application of composition 1 for cigarettes
Heating and melting 21 parts by weight of polyethylene glycol 800, 45 parts by weight of polyethylene glycol 1500 and 25 parts by weight of stearic acid at 67 ℃, mixing at 67 ℃, slowly adding 1 part by weight of citric acid, 0.7 part by weight of malic acid, 0.6 part by weight of tea polyphenol and 51.3 parts by weight of lily-flavored essence (the solvent is propylene glycol and the concentration is 47% (W/W)) into the mixture, and uniformly stirring the mixture under a sealed condition at 69 ℃ to obtain the cigarette composition 1.
The circular injection hole of the fragrance injection equipment is positioned at a bell mouth of a cigarette filter forming machine, the cigarette composition 1 is added into the fragrance injection equipment, in the process of forming loose acetate fibers into a bundle-shaped cigarette filter through the bell mouth, the cigarette composition 1 is injected into the cigarette filter through the fragrance injection equipment, the injection temperature is 69 ℃, the effective injection amount of a single filter rod is 8mg, after the temperature is reduced to the normal temperature, the cigarette composition 1 is in a gel state in the cigarette filter, the cross section area of the gel-shaped cigarette composition accounts for 5% of the total cross section area of the cigarette filter, and the cigarette filter 1 is obtained, the diameter of the cigarette filter is 5.50mm, and the pressure drop is 2890 Pa.
Example 2: preparation and application of composition 2 for cigarettes
Heating 25 parts by weight of polyethylene glycol 800, 49 parts by weight of polyethylene glycol 1500 and 29 parts by weight of stearic acid at 69 ℃ for melting, mixing at 67 ℃, then slowly adding 2 parts by weight of citric acid, 0.8 part by weight of malic acid, 0.5 part by weight of tea polyphenol and 16 parts by weight of grape-flavored essence (the solvent is propylene glycol, the concentration is 42% (W/W)), and uniformly stirring under sealed conditions at 71 ℃ to obtain the cigarette composition 2.
The circular injection hole of the fragrance injection equipment is positioned at a bell mouth of a cigarette filter forming machine, the cigarette composition 2 is added into the fragrance injection equipment, the cigarette composition 2 is injected into the cigarette filter through the fragrance injection equipment in the process that loose polypropylene fibers are formed into a bundle-shaped cigarette filter through the bell mouth, the injection temperature is 71 ℃, the effective injection amount of a single filter rod is 16mg, after the temperature is reduced to the normal temperature, the cigarette composition 2 is in a gel state in the cigarette filter rod, the cross section area of the gel-shaped cigarette composition accounts for 6% of the total cross section area of the cigarette filter rod, and the cigarette filter rod 2 is obtained, the diameter of the cigarette filter rod is 6.50mm, and the pressure drop is 3450 Pa.
Example 3: preparation and application of composition 3 for cigarettes
Heating and melting 23 parts by weight of polyethylene glycol 800, 60 parts by weight of polyethylene glycol 1500 and 34 parts by weight of stearic acid at 68 ℃, mixing at 68 ℃, slowly adding 3 parts by weight of citric acid, 0.3 part by weight of malic acid, 0.7 part by weight of tea polyphenol and 94.4 parts by weight of whiskey flavor essence (the solvent is propylene glycol, the concentration is 58% (W/W)), and uniformly stirring under sealed conditions at 70 ℃ to obtain the cigarette composition 3.
The circular injection hole of the aroma injection equipment is positioned at a bell mouth of a cigarette filter forming machine, the cigarette composition 3 is added into the aroma injection equipment, the cigarette composition 3 is injected into the cigarette filter through the aroma injection equipment in the process that loose polylactic acid fibers are formed into a bundle-shaped cigarette filter through the bell mouth, the injection temperature is 71 ℃, the effective injection amount of a single filter rod is 25mg, after the temperature is reduced to the normal temperature, the cigarette composition 3 is in a gel state in the cigarette filter, the cross section area of the gel-shaped cigarette composition accounts for 8% of the total cross section area of the cigarette filter, and the cigarette filter 3 is obtained, the diameter of the cigarette filter is 7.70mm, and the pressure drop is 3675 Pa.
Example 4: preparation and application of composition 4 for cigarettes
Heating and melting 22 parts by weight of polyethylene glycol 800, 64 parts by weight of polyethylene glycol 1500 and 38 parts by weight of stearic acid at 70 ℃, mixing at 70 ℃, then slowly adding 5 parts by weight of citric acid, 0.5 part by weight of malic acid, 0.3 part by weight of tea polyphenol and 101 parts by weight of osmanthus-passion fruit flavor essence (the solvent is propylene glycol, the concentration is 57% (W/W)), and uniformly stirring under sealed conditions and at 71 ℃ to obtain the cigarette composition 4.
The circular injection hole of the fragrance injection equipment is positioned at the bell mouth of the cigarette filter forming machine, the cigarette composition 4 is added into the fragrance injection equipment, the cigarette composition 4 is injected into the binary composite cigarette filter through the fragrance injection equipment in the process that loose acetate fibers and polylactic acid fibers are formed into a bundle-shaped cigarette filter through the bell mouth, the injection temperature is 71 ℃, the effective addition amount of a single filter rod is 25mg, after the temperature is reduced to the normal temperature, the cigarette composition 4 is in a gel state in the cigarette filter rod, the cross section area of the gel-shaped cigarette composition accounts for 4 percent of the total cross section area of the cigarette filter rod, and the cigarette filter rod 4 is obtained, the diameter of the cigarette filter rod 4 is 7.70mm, and the pressure drop is 3915 Pa.
Comparative example 1
The polyethylene glycol 800 was adjusted to 40 parts by weight, and the remainder was the same as in example 1, to obtain a tobacco composition a and a cigarette filter a. As a result, it was found that: the tobacco composition A in the cigarette filter stick A is not in a gel state at normal temperature, and the filter stick forming paper is soaked.
Comparative example 2
The polyethylene glycol 1500 was adjusted to 30 parts by weight, and the remainder was the same as in example 1, to obtain a tobacco composition B and a cigarette filter B. As a result, it was found that: the cigarette composition B in the cigarette filter stick B is in a soft gel state at normal temperature, so that the fragrance in the filter stick is quickly attenuated along with the prolonging of time.
Comparative example 3
The polyethylene glycol 1500 was adjusted to 83 parts by weight, and the remainder was the same as in example 1, to obtain a tobacco composition C and a cigarette filter stick C. During preparation, the polyethylene glycol 800, the polyethylene glycol 1500 and the stearic acid are not completely melted, and the uniformity of the tobacco composition C is poor.
Comparative example 4
The stearic acid was adjusted to 45 parts by weight, and the remainder was the same as in example 1, to obtain a tobacco composition D and a cigarette filter rod D. The cigarette composition D in the cigarette filter stick D is in a gel state with higher hardness at normal temperature, and the smoke is difficult to elute fragrance when the cigarette is smoked, so that the sensory quality of the cigarette is influenced.
Comparative example 5
The same procedures as in example 1 were repeated except for using 5 parts by weight of acetic acid, 0.8 part by weight of lactic acid, and 0.5 part by weight of catechin in place of citric acid, malic acid, and tea polyphenol to obtain a tobacco composition E and a cigarette filter rod E.
Test example
And rolling the cigarette filter sticks 1-4 and the cigarette filter sticks A-E into cigarettes by a cigarette making machine according to the same cigarette group formula by the same conventional method to obtain cigarettes 1-4 and cigarettes A-E. Referring to example 3, the addition of citric acid, malic acid and tea polyphenol components was omitted, and the rest was the same as in example 3, to obtain a cigarette filter stick, which was prepared into cigarettes as a control sample according to the conventional method using the above-described leaf group formulation.
The sensory quality evaluation of each cigarette was performed by 30 professionals for sensory evaluation of cigarettes according to national standard GB5606.4-2005, and the average results are listed in tables 1-2.
TABLE 1
TABLE 2
Tables 1-2 show that compared with cigarettes A-E and a control sample, the aroma release of the cigarette composition provided by the invention added into a cigarette filter stick is more obvious, the harmony of essence aroma and cigarette aroma is better, the smoking aroma quality of the cigarettes is improved, the aftertaste comfort of the cigarettes is improved, the irritation and miscellaneous gas of smoke are reduced, the cigarettes are free of oil smell during smoking, the sensory quality of the cigarettes is improved, and thus the psychological and physiological requirements of consumers are met.
It should be understood that the above examples are only for clarity of illustration and are not intended to limit the embodiments. Other variations and modifications will be apparent to persons skilled in the art in light of the above description. And are neither required nor exhaustive of all embodiments. And obvious variations or modifications therefrom are within the scope of the invention.
Claims (10)
1. A composition for tobacco comprising the following components:
2. the tobacco composition of claim 1, further comprising a tobacco flavor;
preferably, the weight part of the essence for tobacco is 0.1-130;
preferably, the tobacco flavor is selected from one or more of lily flower flavor, grape flavor, whisky flavor, sweet osmanthus flavor and passion fruit flavor;
preferably, the essence for tobacco contains a solvent;
more preferably, the solvent is propylene glycol.
3. The tobacco composition of claim 1 or 2, comprising the following components:
4. the composition for tobacco according to claim 1 or 2, wherein the composition for tobacco is in a gel state at normal temperature.
5. A cigarette filter rod or filter comprising the tobacco composition of any one of claims 1 to 4;
preferably, the content of the tobacco composition in each cigarette filter stick or each cigarette filter is 1-200 mg;
preferably, the diameter of the cigarette filter stick or the cigarette filter is 1-20 mm;
preferably, the pressure drop of the cigarette filter stick or the cigarette filter is 1000-8000 Pa.
6. A cigarette filter stick or filter according to claim 5 wherein the tobacco composition in the cigarette filter stick or filter is in the form of a gel at ambient temperature;
preferably, the cross-section of the gelatinous smoking composition in a cigarette filter rod or filter is circular, pentagonal, or polygonal;
preferably, the cross-sectional area of the gelatinous smoking composition is from 1% to 16% of the total cross-sectional area of the cigarette filter rod or filter.
7. A cigarette comprising the smoking composition of any one of claims 1 to 4, or comprising the cigarette filter rod or filter of claim 5 or 6.
8. A process for preparing a smoking composition according to any one of claims 1 to 4, comprising the steps of:
(1) heating polyethylene glycol 800, polyethylene glycol 1500 and stearic acid to melt, and mixing to obtain a mixture;
(2) mixing the mixture, citric acid, malic acid, tea polyphenols and optional tobacco essence under sealed condition;
preferably, in the step (1), the heating temperature is not lower than 62 ℃;
preferably, in the step (1), the temperature of mixing is not lower than 62 ℃;
preferably, in the step (2), the temperature of mixing is not lower than 62 ℃;
preferably, in step (2), citric acid, malic acid, tea polyphenol and optional tobacco flavor are slowly added to the mixture under sealed conditions for mixing.
9. Use of the composition for tobacco of any one of claims 1 to 4 in the manufacture of a cigarette filter, cigarette filter or cigarette.
10. Use of the tobacco composition of any one of claims 1 to 4, or the cigarette filter rod or filter of claim 5 or 6, for improving the sensory quality of a cigarette;
preferably, the evaluation index of the sensory quality of the cigarette is selected from the group consisting of aroma, harmony, aftertaste, irritation, and offensive odor.
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| CN205305981U (en) * | 2015-12-14 | 2016-06-15 | 张松波 | Tea polyphenol filter stick |
| CN109549249A (en) * | 2018-12-11 | 2019-04-02 | 云南巴菰生物科技有限公司 | A kind of preparation method of cigarette preservation antioxidation capsule |
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| CN110150742A (en) * | 2018-02-13 | 2019-08-23 | 湖南中烟工业有限责任公司 | A kind of packet capsule with diuresis promoting function and its one-step shaping preparation method and the application in cigarette |
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| CN205305981U (en) * | 2015-12-14 | 2016-06-15 | 张松波 | Tea polyphenol filter stick |
| CN110150742A (en) * | 2018-02-13 | 2019-08-23 | 湖南中烟工业有限责任公司 | A kind of packet capsule with diuresis promoting function and its one-step shaping preparation method and the application in cigarette |
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Application publication date: 20200508 |