CN104687233B - The preparation method and orange flavor reconstituted tobacco of a kind of orange flavor reconstituted tobacco - Google Patents

The preparation method and orange flavor reconstituted tobacco of a kind of orange flavor reconstituted tobacco Download PDF

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Publication number
CN104687233B
CN104687233B CN201410839345.6A CN201410839345A CN104687233B CN 104687233 B CN104687233 B CN 104687233B CN 201410839345 A CN201410839345 A CN 201410839345A CN 104687233 B CN104687233 B CN 104687233B
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reconstituted tobacco
orange
cigarette
preparation
powder
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CN104687233A (en
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曾健
饶国华
刘熙
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China Tobacco Guangdong Industrial Co Ltd
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China Tobacco Guangdong Industrial Co Ltd
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/14Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products

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  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)
  • Manufacture Of Tobacco Products (AREA)

Abstract

The present invention provides the preparation method and orange flavor reconstituted tobacco of a kind of reconstituted tobacco of orange flavor, and the preparation method includes taking fresh orange peel immersion, drying, milling, orange peel powder is added into paper substrate in coating process, is coated with, the step such as drying.The present invention orange peel is made after the powder of suitable particulate to be organically combined with coating process, improve the properties of reconstituted tobacco, the more scientific preparation for being efficiently applied to reconstituted tobacco of the active ingredient of orange peel, the orange flavor reconstituted tobacco prepared is compared with being commonly not added with the reconstituted tobacco of tangerine peel powder, flue gas concentration is higher, fragrance texture is more preferable, note more enriches, play the note breath of fresh orange and the synergy of coating fluid active ingredient, the cigarette smoke exquisiteness prepared is long, smooth, and overall oral cavity comfort level is preferable.

Description

The preparation method and orange flavor reconstituted tobacco of a kind of orange flavor reconstituted tobacco
Technical field
The present invention relates to technical field of tobacco, more particularly, to a kind of preparation method of the reconstituted tobacco of orange flavor And orange flavor reconstituted tobacco.
Background technology
Reconstituted tobacco(Reconstituted Tobacco), also known as reconstituted tobacoo, homogeneous tobacco leaf or recombination tobacco leaf have Filling power is high, have good burning performance, the low characteristic of releasing content of coke tar, is substituted with reconstituted tobacco or part substitutes traditional pipe tobacco and prepared Cigarette is one of effective means of Tar.
The process for preparing reconstituted tobacco using paper process generally includes, to tobacco material immersion, extraction, extract to be concentrated Afterwards as coating fluid, slag charge after immersion carries out the defibrination step such as manufacture paper with pulp and is prepared into paper substrate, and coating solution is dried in paper substrate After obtain reconstituted tobacco.During the higher extraction of temperature and concentration etc., there be a part to inhaling taste and fragrance in tobacco material The material of contribution can volatilize, decomposes, convert, so that the reconstituted tobacco for causing paper process to prepare has fragrance shortcoming and pungent The defects such as sense aggravation, influence its sense organ suction quality.
Furthermore, the raw material used in reconstituted tobacco is typically the leftover bits and pieces produced during production of cigarettes, the leftover bits and pieces warp Multiple high-temperature process repeatedly in production process is crossed, raw material fragrance loss itself is big, and aesthetic quality is deteriorated.Therefore, enhancing reconstruction cigarette The tobacco aroma of leaf or other fragrance with tobacco aroma harmony, improve suction quality, are that reconstituted tobacco production field needs solution badly Technical problem certainly.
Orange(Orange)Skin is the epidermis of fruit orange, and consumer discards orange peel when edible orange.Orange The leatherware function such as have regulating qi-flowing for eliminating phlegm, stomach invigorating dehumidify, reduce blood pressure, is a kind of good Chinese medicine.Have no at present in tobacco leaf production The application in field.
The content of the invention
The technical problem to be solved in the present invention is to fill up the application technology deficiency of orange peel, while in order to overcome reconstruction cigarette Orange peel is effectively applied to reconstruction by the problem of leaf fragrance is not enough there is provided a kind of preparation method of orange flavor reconstituted tobacco The preparation of tobacco leaf.
Another technical problem to be solved by the present invention is that providing the orange flavor reconstruction cigarette that the preparation method is prepared Leaf.
The purpose of the present invention is achieved by the following technical programs:
A kind of preparation method of orange flavor reconstituted tobacco is provided, comprised the following steps:
S1. fresh orange peel is taken, 5~20s of hot-water soak is drained, drying to moisture is 10~15%;
S2. the orange peel progress handled S1 is crushed to particle diameter and is not more than 60 mesh, obtains tangerine peel powder.Orange peel powder Particle size, there is certain bad influence to sense organ, but particle diameter too big particle, uniformity when being mixed in coating fluid compared with Difference, easily causes reconstituted tobacco surface picking.So the present invention is less than the mesh powder of 60 mesh~120 from particle diameter.Most preferably use 60 mesh.
S3. tangerine peel powder is added in coating fluid, reconstituted tobacco paper substrate is coated, then at 100~110 DEG C It is 10~15% to be dried under temperature conditionss to moisture;The addition of the tangerine peel powder is true for 10~30% according to paper substrate quality It is fixed;
It is further preferable that S3 is that according to the 10%~30% of paper substrate quality tangerine peel powder uniformly is added into reconstituted tobacco paper substrate In, dry to moisture and produced for 10~15% under 100~110 DEG C of temperature conditionss after coated liquid coating, added using preferred Plus the method for orange peel powder can obtain organoleptic quality more excellent reconstituted tobacco.
It is further preferred that the addition of the tangerine peel powder is determined according to the 10~20% of paper substrate quality.
Preferably, the temperature of hot water described in S1 is 90~100 DEG C.
Preferably, drying temperature described in S1 is 30~50 DEG C.
Preferably, drying temperature described in S1 is 40 DEG C.
Preferably, immersion is to soak 10s at normal temperatures described in S1.
Preferably, S3 coating after reconstituted tobacco paper substrate in drying temperature be 100~110 DEG C.
Preferably, in S1 and S3 drying operation twice, it is 12% to dry to moisture.
Preferably, the coating weight being coated with described in S3 is 40~45%.
Present invention simultaneously provides the reconstituted tobacco that the preparation method is prepared.
The reconstituted tobacco can be advantageously applied to prepare cigarette, will be substituted after the reconstituted tobacco chopping or part is replaced Cigarette is prepared for pipe tobacco.
What coating fluid and reconstituted tobacco paper substrate of the present invention can be prepared using the existing conventional method in this area Coating fluid and reconstituted tobacco paper substrate.
Beneficial effects of the present invention:
The applicant's research finds that contained substantial amounts of vitamin C and essential oil in orange peel, its taste delicate fragrance add in right amount Coating fluid is added on, is made an addition in application step in reconstituted tobacco, the delicate fragrance of orange peel and the mutually auxiliary phase of the fragrance matter of tobacco material Into acquisition is a kind of with orange flavor, the reconstituted tobacco refreshed oneself, ventilated.
Orange peel makes an addition to reconstituted tobacco, there is number of ways in theory, and a kind of approach is by the extract of orange peel
As essence and flavoring agent existing conventional method is sprayed on to prepare in the pipe tobacco that gained reconstruction cigarette tobacco leaf is cut into, one kind be by Orange peel extraction together with tobacco material is handled, and leaching liquor is as coating fluid, and the slag charge after extraction carries out defibrination and manufactured paper with pulp preparation again Reconstituted tobacco, one kind is the inventive method, and orange peel is dried to suitable moisture and crushed, and strictly controls tangerine The particle diameter of sub- skin powder, orange peel powder is made an addition to and is coated on paper substrate after coating fluid together, reconstituted tobacco is prepared.By a large amount of Experimental study analysis and summary, the first approach addition orange peel, a large amount of essence oil substances, which can not be extracted, to be obtained, the perfuming of acquisition Effect is had a greatly reduced quality.The problem of processing method of second of approach equally exists extraction loss, tobacco is mixed into by orange peel slag charge Defibrination is manufactured paper with pulp the process conditions and effect that also have impact on original defibrination to a certain extent and manufacture paper with pulp together in raw material slag charge, is made The stability for obtaining paper substrate quality is difficult to be guaranteed.And the inventive method is used, because drying is suitable to moisture, it is ensured that crush Ease for operation and the loss of orange peel active ingredient is tried one's best attenuating, directly the orange peel powder of suitable particle diameter scope is added With coating fluid, contained fragrance matter and other beneficiating ingredients in orange peel are at utmost protected, and it is because scientifically and rationally strict Particle diameter and addition are controlled, harmful effect is not produced to the operating procedure and Painting effect of coating, on the contrary because with the addition of Appropriate orange peel powder so that some physical properties of reconstituted tobacco have obtained larger improvement.It the experiment proved that, using this Inventive method is applied to the preparation of reconstituted tobacco through orange peel, with being not added with tangerine peel powder, adopting foregoing other two approach addition tangerine The reconstituted tobacco of sub- skin is compared, and the flue gas concentration of present invention gained reconstituted tobacco effectively improves, and fragrance texture is more preferable, note It is more rich naturally, the note breath with fresh orange, flue gas is finer and smoother long, smooth, overall oral cavity comfort level is preferable.
The present invention provides a kind of new application for orange peel, using orange peel as the raw material for preparing reconstituted tobacco, While the sensory experience of abundant cigarette, the special component contained by tangerine peel can be brought newly by scientific disposal of the present invention for smoker Sensory experience.Fresh tangerine peel powder can not only assign reconstituted tobacco with orange flavor, increasingly deficient in reconstituted tobacco raw material In the case of, tangerine peel powder is also used as the manufacture raw material of reconstituted tobacco, is that reconstituted tobacco raw material makees more preferable supplement.
Embodiment
The present invention is further described with reference to specific embodiment, unless stated otherwise, the reagent that the present invention is used It is this area routinely reagent and raw material purchased in market with raw material.
Embodiment 1
S1. orange purchased in market, takes fresh orange peel, in boiling water(100℃)Middle immersion 10s, taking-up drains the water, in an oven, It is 12% that moisture is dried at 40 DEG C;
S2. using 200 grams of swing high speed Universal pulverizers(Model:DFY-200)Orange peel is crushed, tangerine is obtained Sub- powder;The particle diameter of powder is 60~120 mesh;
S3. orange powder is added in paper substrate, addition is the 20% of the quality of reconstituted tobacco paper substrate, to reconstituted tobacco Paper substrate is coated, and coating weight is 40%~45%, and the reconstituted tobacco after coating is placed under the conditions of 105 DEG C and dried to moisture For 12%.
Coating fluid is prepared using following raw material and preparation method:Difference Soakage extraction offal and offal.The offal The condition of Soakage extraction is solid-liquid ratio 1:7(Mass ratio), Extracting temperature be 60 DEG C, extraction time be 100 minutes(min);It is described The condition of offal Soakage extraction is that solid-liquid ratio is 1:10,70 DEG C of Extracting temperature, the min of extraction time 60;Obtained after impregnated processing Offal and offal extract solution according to 1:1 volume ratio mixing carries out conventional be concentrated by evaporation and obtains coating fluid;After impregnation process Offal, offal solid for defibrination use.
The paper substrate of reconstituted tobacco is preferably with reference to the applicant's China Patent No. with reference to existing routine Content disclosed in ZL201210062184.5 Chinese patent application file.
Table 1 adds the physical property of the last reconstituted tobacco paper substrate of orange meal
Detection project It is not added with tangerine peel powder Add tangerine peel powder 20%
Tensile index/Nmg-1 11.65 10.59
Tensile strength/kNm-1 0.78 0.72
Tear index/mNm2·g-1 1.14 1.08
Bulk/cm3·g -1 2.36 2.30
Tightness/gcm-3 0.42 0.41
Air permeability/μm Pa-1·s-1 2.34 2.18
From table 1, every intensity index has corresponding a little decline, and air permeability can decline slightly many, bulk and tightness Change is little
By the gained reconstituted tobacco of embodiment 1 according to existing conventional method chopping, roll after tipping acetate fiber filter tip be made Cigarette sample cigarette, using cigarette made from the reconstituted tobacco without orange peel powder as control cigarette, all samples cigarette rolls rule Lattice are consistent, carry out sensory evaluation by 10 professional members of smoking, compared to control cigarette, sample cigarette smoking result is as follows:Flue gas concentration Moderate, fragrance texture is good, and perfume quantity foot, the note of tangerine peel immersion oil is obvious, fragrance harmony, and flue gas is loose, soft silk floss, and smoke behavior is good Good, the stimulation in oral cavity, dry sensation are few, and time sweet tea is more apparent, and global comfort is fine.
Embodiment 2
S1. orange purchased in market, takes fresh orange peel, in boiling water(100℃)Middle immersion 10s, taking-up drains the water, in an oven, It is 12% that moisture is dried at 40 DEG C;
S2. using 200 grams of swing high speed Universal pulverizers(Model:DFY-200)Orange peel is crushed, tangerine is obtained Sub- powder;The particle diameter of powder is 60 mesh;
S3. orange powder is added in coating fluid, addition is the 20% of the quality of relative reconstituted tobacco paper substrate, to again Make tobacco leaf paper substrate to be coated, coating weight is 40%~45%, and the reconstituted tobacco after coating is placed under the conditions of 105 DEG C and dried to water It is 12% to divide content.
Coating fluid is prepared using following raw material and preparation method:Difference Soakage extraction offal and offal.The offal The condition of Soakage extraction is solid-liquid ratio 1:7(Mass ratio), Extracting temperature be 60 DEG C, extraction time be 100 minutes(min);It is described The condition of offal Soakage extraction is that solid-liquid ratio is 1:10,70 DEG C of Extracting temperature, the min of extraction time 60;Obtained after impregnated processing Offal and offal extract solution according to 1:1 volume ratio mixing carries out conventional be concentrated by evaporation and obtains coating fluid;After impregnation process Offal, offal solid for defibrination use.
The paper substrate of reconstituted tobacco is preferably with reference to the applicant's China Patent No. with reference to existing routine Content disclosed in ZL201210062184.5 Chinese patent application file.
By the gained reconstituted tobacco of embodiment 2 according to existing conventional method chopping, roll after tipping acetate fiber filter tip be made Cigarette sample cigarette, using cigarette made from the reconstituted tobacco without orange peel powder as control cigarette, all samples cigarette rolls rule Lattice are consistent, carry out sensory evaluation by 10 professional members of smoking, compared to control cigarette, sample cigarette smoking result is as follows:Flue gas concentration It is moderate, fragrance texture preferably, perfume quantity is more sufficient, and the note of tangerine peel immersion oil is more apparent, fragrance compared with harmony, flue gas loosely, soft silk floss, Preferably, the stimulation in oral cavity, dry sensation is micro- has for smoke behavior, returns that sweet tea is more apparent, and global comfort is preferable.
Embodiment 3
Other be the same as Examples 1, the difference is that orange powder is added in coating fluid by S3, addition is relative reconstituted tobacco The 10% of the quality of paper substrate, coating weight is 40%.
By the gained reconstituted tobacco of embodiment 3 according to existing conventional method chopping, roll after tipping acetate fiber filter tip be made Cigarette sample cigarette, using cigarette made from the reconstituted tobacco without orange peel powder as control cigarette, all samples cigarette rolls rule Lattice are consistent, carry out sensory evaluation by 10 professional members of smoking, compared to control cigarette, sample cigarette smoking result is as follows:Flue gas concentration Moderate, preferably, preferably, the saturating hair of fragrance has lifting to definition to fragrance texture compared with control sample, and perfume quantity is medium, tangerine peel immersion oil Note slightly, fragrance compared with harmony, flue gas loosely, it is long, smoke behavior preferably, global comfort is fine.
Embodiment 4
Other be the same as Examples 1, the difference is that orange powder is added in coating fluid by S3, addition is relative reconstituted tobacco The 15% of the quality of paper substrate, coating weight is 40%.
By the gained reconstituted tobacco of embodiment 4 according to existing conventional method chopping, roll after tipping acetate fiber filter tip be made Cigarette sample cigarette, using cigarette made from the reconstituted tobacco without orange peel powder as control cigarette, all samples cigarette rolls rule Lattice are consistent, carry out sensory evaluation by 10 professional members of smoking, compared to control cigarette, sample cigarette smoking result is as follows:Flue gas concentration Moderate, preferably, preferably, the saturating hair of fragrance has lifting to definition to fragrance texture compared with control sample, and perfume quantity is medium, tangerine peel immersion oil Note slightly, fragrance compared with harmony, flue gas loosely, it is long, smoke behavior preferably, global comfort is fine.
Embodiment 5
Other be the same as Examples 1, the difference is that orange powder is added in coating fluid by S3, addition is relative reconstituted tobacco The 30% of the quality of paper substrate, coating weight is 40%.
By the gained reconstituted tobacco of embodiment 5 according to existing conventional method chopping, roll after tipping acetate fiber filter tip be made Cigarette sample cigarette, using cigarette made from the reconstituted tobacco without orange peel powder as control cigarette, all samples cigarette rolls rule Lattice are consistent, carry out sensory evaluation by 10 professional members of smoking, compared to control cigarette, sample cigarette smoking result is as follows:Flue gas concentration Moderate, preferably, perfume quantity is more sufficient, and the note of tangerine peel immersion oil is more apparent for fragrance texture, and fragrance is compared with harmony, and smoke behavior is preferable, mouth Chamber and nasal cavity slightly have dry, excitement, and global comfort is preferable.
Comparative example 1
Other be the same as Examples 1, the difference is that orange powder is added in coating fluid by S3, addition is relative reconstituted tobacco The 5% of the quality of paper substrate, coating weight is 40%.
By the gained reconstituted tobacco of comparative example 1 according to existing conventional method chopping, roll after tipping acetate fiber filter tip be made Cigarette sample cigarette, using cigarette made from the reconstituted tobacco without orange peel powder as control cigarette, all samples cigarette rolls rule Lattice are consistent, carry out sensory evaluation by 10 professional members of smoking, compared to control cigarette, sample cigarette smoking result is as follows:Flue gas concentration Moderate, still, still, the note of tangerine peel immersion oil is micro- to be had perfume quantity fragrance texture, and flue gas is softer continuous, fine and smooth, the drying in oral cavity, thorn Swash slightly, global comfort is fine.
Comparative example 2
Other be the same as Examples 1, the difference is that orange powder is added in coating fluid by S3, addition is relative reconstituted tobacco The 32%~35% of the quality of paper substrate, coating weight is 40%.
By the gained reconstituted tobacco of comparative example 2 according to existing conventional method chopping, roll after tipping acetate fiber filter tip be made Cigarette sample cigarette, to add orange peel amount of powder cigarette made from 10~20% reconstituted tobacco as control cigarette, all samples cigarette To roll specification consistent, carry out sensory evaluations by 10 professional members of smoking, compared to control cigarette, this comparative example cigarette is smoked panel test knot Fruit is as follows:Orange powder addition increases above 30%, and the note of tangerine peel immersion oil strengthens, but the stimulation in oral cavity, dry meeting are Increase, global comfort is not as good as the sample cigarette that addition is 10~20%.
Comparative example 3
S1. flavoring orange essence purchased in market, flavoring orange essence is added in coating fluid, and addition is relative reconstituted tobacco paper substrate quality 10%;
S2. the coating fluid that flavoring orange essence is with the addition of with S1 is coated to the paper substrate of reconstituted tobacco, and the paper substrate after coating is existed It is 12% to be dried under the conditions of 105 DEG C to moisture.
By the gained reconstituted tobacco of comparative example 3 according to existing conventional method chopping, roll after tipping acetate fiber filter tip be made Cigarette sample cigarette, control cigarette, the volume of all samples cigarette are used as using cigarette made from the reconstituted tobacco of present invention addition orange peel powder Specification processed is consistent, carries out sensory evaluation by 10 professional members of smoking, compared to control cigarette, this comparative example cigarette smoking result is such as Under:Flavoring orange essence addition after, feel be outer perfuming note it is obvious, hamony is poor.
Comparative example 4
S1. orange purchased in market, takes fresh orange peel, in boiling water(100℃)Middle immersion 1min, taking-up drains the water, in an oven, It is 12% that moisture is dried at 40 DEG C;
Other be the same as Examples 1.
By the gained reconstituted tobacco of comparative example 4 according to existing conventional method chopping, roll after tipping acetate fiber filter tip be made Cigarette sample cigarette, cigarette made from the reconstituted tobacco of orange peel powder is added as control cigarette, all samples using the embodiment of the present invention 1,2 Product cigarette to roll specification consistent, carry out sensory evaluations by 10 professional members of smoking, compared to control cigarette, this comparative example cigarette is commented Inhale result as follows:This comparative example cigarette has more life green gas breath, and after coating fluid mixing, the miscellaneous gas in obtained reconstituted tobacco Substantially, green gas breath is particularly given birth to.

Claims (4)

1. a kind of preparation method of orange flavor reconstituted tobacco, it is characterised in that comprise the following steps:
S1. fresh orange peel is taken, 5~20s of hot-water soak is drained, drying to moisture is 10~15%;
S2. the orange peel to step S1 processing is crushed, and obtains tangerine peel powder;
S3. tangerine peel powder is uniformly added in reconstituted tobacco paper substrate according to the 10%~20% of paper substrate quality, coated liquid is applied Dry to moisture and produced for 10~15% under 100~110 DEG C of temperature conditionss after cloth;
The temperature of hot water described in step S1 is 90~100 DEG C;
Drying temperature described in step S1 is 30~50 DEG C.
2. a kind of preparation method of orange flavor reconstituted tobacco according to claim 1, it is characterised in that step S1 and step It is 12% that S3 is dried in drying operation, to moisture twice.
3. the reconstituted tobacco that preparation method described in claim 1 or 2 is prepared.
4. the application of reconstituted tobacco described in claim 3, it is characterised in that be applied to the reconstituted tobacco to prepare cigarette cigarette Silk.
CN201410839345.6A 2014-12-30 2014-12-30 The preparation method and orange flavor reconstituted tobacco of a kind of orange flavor reconstituted tobacco Active CN104687233B (en)

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CN106387987B (en) * 2016-09-28 2018-03-13 湖北中烟工业有限责任公司 A kind of preparation method and applications of red tangerine extract
CN106433987A (en) * 2016-10-31 2017-02-22 湖北中烟工业有限责任公司 Preparation method of refined sweet-orange spice and application thereof
CN107232639A (en) * 2017-06-22 2017-10-10 中烟施伟策(云南)再造烟叶有限公司 A kind of reconstituted tobacco of the powder of plum containing ultra micro and preparation method thereof
CN109363226A (en) * 2018-10-26 2019-02-22 云南中烟工业有限责任公司 A kind of low-intensity fumigates the reconstituted tobacco and preparation method thereof of flavoring extension fragrance remaining time
CN109730351B (en) * 2019-03-05 2021-06-15 湖北中烟工业有限责任公司 Preparation method of mixed fruity reconstituted tobacco
CN110150727B (en) * 2019-05-05 2023-07-21 贵州中烟工业有限责任公司 Preparation method of dried orange peel-flavor plant aroma-producing sheet suitable for heating non-combustible cigarettes
CN111000276A (en) * 2019-11-06 2020-04-14 湖北中烟工业有限责任公司 Preparation method of sandalwood-flavored paper-making reconstituted tobacco
CN112471584A (en) * 2020-11-18 2021-03-12 云南恒罡科技有限公司 Preparation method and application of mixed coating liquid of fungus-type tobacco

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