CN103238921B - The production method of reconstituted tobacoo - Google Patents
The production method of reconstituted tobacoo Download PDFInfo
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- CN103238921B CN103238921B CN201310188165.1A CN201310188165A CN103238921B CN 103238921 B CN103238921 B CN 103238921B CN 201310188165 A CN201310188165 A CN 201310188165A CN 103238921 B CN103238921 B CN 103238921B
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Abstract
The invention provides a kind of production method of reconstituted tobacoo, comprise the following steps: offal, offal and water are mixed rear heating extraction 2 ~ 3 times by (1), after filter, obtain filtrate and filter residue, merging filtrate, concentrates filtrate, obtains concentrate; (2) in concentrate, add Chinese toon medicinal extract, giant knotweed medicinal extract, combination of enzyme preparations thing, carry out enzyme digestion reaction, heat the enzyme that goes out afterwards, form coating fluid; (3) in filter residue, add slurry, mix, making beating, after add auxiliary agent, obtain mixed slurry; And (4) adopt paper process, paper substrate that mixed slurry is laminated, after by coating solution on sheet paper base, then drying, makes reconstituted tobacoo.The preparation method of above-mentioned reconstituted tobacco, the treatment process adopting combination of enzyme preparations thing to combine with auxiliary agent, can reduce the content of lignin, improves and sucks effect.
Description
Technical field
The present invention relates to tobacco processing procedure, particularly relate to a kind of production method of reconstituted tobacoo.
Background technology
China's tobacco planting area 2,000 ten thousand mu, annual yield of tobacco 450-500 ten thousand tons, all occupies first place in the world.The tobacco of domestic and international plantation is mainly used as cigarette, and it is raw material that cigarette industry gets sound tobacco more, wherein about has the leftover bits and pieces such as the tobacco leaf of nearly 25%, offal to go out of use, will cause the pollution of environment as thrown aside or dealing with improperly." resource " of these tobacco wastes is utilized, not only can obtain various useful product, provide the opportunity of sustainable development for enterprise taps the potential and upgrade technologically, also can alleviate the pollution of soil property that tobacco waste brings and soil, avoid harmful components to the pollution of underground water.Therefore, the recycling strengthening tobacco waste not only can make this part refuse become resource, and can improve income, meets the policy of country to " minimizing ", " resource " and " innoxious " of solid waste.
The domestic processing method to reconstituted tobacoo mainly contains: 1, physical treatment method, mainly uses the process of the method such as microwave, steam blasting.Physical treatment method process intensity is large, comparatively large to aroma component loss in offal, affects the sucking quality of cigarette, can not change its intrinsic microstructure simultaneously, be difficult to nano material is effectively adsorbed.2, chemical treatment method, mainly using the process such as diluted acid, alkali, ozone, organic solvent and oxidation, there is chemical substance later stage reluctant problem in chemical treatment method aborning.3, bioremediation, the cell wall constituent to offal mainly through simple biology enzyme or bacterium of carrying out a biological disposal upon is degraded, alone cellulase treatment offal produces reconstituted tobacoo, due to the natural protective barrier that plant cell wall is plant, often not thorough with ferment treatment, part of can only degrading cell wall constituent; Alone bacterium processing time longer meeting causes the thorough avalanche of cell membrane, affect the quality of reconstituted tobacoo, and the time is short and can not achieve the goal.
Summary of the invention
Based on this, be necessary the production method that the good reconstituted tobacoo of a kind of smoking property of cigarette quality is provided.
A production method for reconstituted tobacoo, comprises the following steps:
(1) offal, offal and water are mixed rear heating extraction 2 ~ 3 times, after filter, obtain filtrate and filter residue, merging filtrate, described filtrate is concentrated, obtain concentrate, wherein, the mass ratio of offal, offal, water is offal: offal: water=1 ~ 3: 4 ~ 6: 20 ~ 54;
(2) in described concentrate, Chinese toon medicinal extract, giant knotweed medicinal extract, combination of enzyme preparations thing is added, carry out enzyme digestion reaction, heat the enzyme that goes out afterwards, form coating fluid, wherein, described combination of enzyme preparations thing is made up of each component of following mass percent: the pectase of 10 ~ 30%, the protease of 5 ~ 10%, 5 ~ 20% amylase, 10 ~ 20% cellulase, the trehalose of 10 ~ 30%, the polyacrylamide of 2 ~ 8% and 3 ~ 10% tannic acid;
(3) in described filter residue, slurry is added, mix, making beating, after add auxiliary agent, obtain mixed slurry, wherein, described slurry is the mixture of one or more in bamboo pulp, Chinese alpine rush slurry, and described auxiliary agent is grouped into by the one-tenth of following mass percent: the alkylamide imidazoline of 10 ~ 20%, the alkyl betaine of 5 ~ 20%, the oxirane of 20 ~ 40%, the stearic acid of 10 ~ 30%; And
(4) adopt paper process, paper substrate of being laminated by described mixed slurry, after by described coating solution on described sheet paper base, then drying, makes reconstituted tobacoo.
Wherein in an embodiment, the length of described offal is 10 ~ 15mm.
Wherein in an embodiment, in step (1), filter with filter membrane, the aperture of described filter membrane is 1 ~ 3 μm, and the density of concentrate is 1.17 ~ 1.22g/mL.
Wherein in an embodiment, in step (2), described combination of enzyme preparations thing is made up of each component of following mass percent: the pectase of 30%, the protease of 10%, 20% amylase, 10% cellulase, the trehalose of 15%, the polyacrylamide of 5% and 10% tannic acid.
Wherein in an embodiment, in step (2), the condition heating the enzyme that goes out is: heating-up temperature is 90 ~ 100 DEG C, and the heat time is 10 ~ 15min.
Wherein in an embodiment, described auxiliary agent is grouped into by the one-tenth of following mass percent: the alkylamide imidazoline of 20%, the alkyl betaine of 20%, the oxirane of 40%, the stearic acid of 20%.
Wherein in an embodiment, the quality of described combination of enzyme preparations thing is 0.5 ~ 2 ‰ of offal and offal total amount; The quality of described Chinese toon medicinal extract is 0.1 ~ 0.5% of solid content dry weight in concentrate, and the quality of described giant knotweed medicinal extract is 0.2 ~ 0.6% of solid content dry weight in concentrate; The condition of enzyme digestion reaction is: pH=4.0 ~ 7.0, hydrolysis temperature are 20 ~ 60 DEG C, enzymolysis time is 0.5 ~ 2h.
Wherein in an embodiment, the quality of described auxiliary agent is 0.2 ~ 0.6 ‰ of offal and offal total amount.
Wherein in an embodiment, described slurry is the mixture of bamboo pulp, Chinese alpine rush slurry, and wherein, the quality of bamboo pulp is 3 ~ 6% of filter residue dry weight, and the quality of Chinese alpine rush slurry is 4 ~ 7% of filter residue dry weight.
The production method of above-mentioned reconstituted tobacoo, adopt the treatment process that combination of enzyme preparations thing combines with auxiliary agent, working condition is gentle, efficiency is high, pollutes little, and enzyme used, auxiliary agent, slurry are the conventional commercialization material of food service industry, purity is high, price is low, be easy to obtain and working condition is easily grasped and controlled, combination of enzyme preparations thing, between slurry and auxiliary agent exist synergy, obviously can reduce the content of lignin, improve suck effect; The coating fluid utilizing the present invention to obtain and paper substrate manufacture reconstituted tobacoo, have excellent stability and repeatability, and have more significantly flavouring effect and unique style and features.This method production technology is simple, and production cost is low, is easy to realize suitability for industrialized production.
Accompanying drawing explanation
Fig. 1 is the production method flow chart of the reconstituted tobacoo of an embodiment.
Detailed description of the invention
For enabling above-mentioned purpose of the present invention, feature and advantage become apparent more, are described in detail below to the specific embodiment of the present invention.Set forth a lot of detail in the following description so that fully understand the present invention.But the present invention can be much different from alternate manner described here to implement, those skilled in the art can when without prejudice to doing similar improvement when intension of the present invention, therefore the present invention is by the restriction of following public concrete enforcement.
Refer to Fig. 1, the production method of the reconstituted tobacoo of an embodiment, comprises the following steps:
Step S100, offal, offal and water are mixed rear heating extraction 2 ~ 3 times, after filter, obtain filtrate and filter residue, merging filtrate, filtrate concentrated, obtain concentrate.
Adopt mechanical crushing method, offal being crushed to length is 10 ~ 15mm.Filter with filter membrane, the aperture of filter membrane is 1 ~ 3 μm, and the density of concentrate is 1.15 ~ 1.25g/mL.
Step S200, in concentrate, add Chinese toon medicinal extract, giant knotweed medicinal extract, combination of enzyme preparations thing, carry out enzyme digestion reaction, heat the enzyme that goes out afterwards, form coating fluid, wherein, combination of enzyme preparations thing is made up of each component of following mass percent: the pectase of 10 ~ 30%, the protease of 5 ~ 10%, 5 ~ 20% amylase, 10 ~ 20% cellulase, the trehalose of 10 ~ 30%, the polyacrylamide of 2 ~ 8% and 3 ~ 10% tannic acid.
Wherein, the quality of combination of enzyme preparations thing is 0.5 ~ 2 ‰ of offal and offal total amount.The quality of Chinese toon medicinal extract is 0.1 ~ 0.5% of solid content dry weight in concentrate.The quality of giant knotweed medicinal extract is 0.2 ~ 0.6% of solid content dry weight in concentrate.The condition of enzyme digestion reaction is: pH=4.0 ~ 7.0, hydrolysis temperature are 20 ~ 60 DEG C, enzymolysis time is 0.5 ~ 2h.
The condition heating the enzyme that goes out is: heating-up temperature is 90 ~ 100 DEG C, and the heat time is 10 ~ 15min.
Preferably, combination of enzyme preparations thing is made up of each component of following mass percent: the pectase of 30%, the protease of 10%, 20% amylase, 10% cellulase, the trehalose of 15%, the polyacrylamide of 5% and 10% tannic acid.
Add combination of enzyme preparations thing and can reach following beneficial effect: first, pectase, protease, amylase, cellulase can reduce the macromolecular substances content in concentrate targetedly, be hydrolyzed into galacturonic acid, amino acid, polypeptide,, can there is Maillard reaction in the small-molecule substances such as glucose, improve flavor matter content in follow-up enzyme pyroprocess of going out; Secondly, cellulase can saponin(e in Chinese toon medicinal extract and giant knotweed medicinal extract and flavonoid glycoside substance, and generate aglycon, aglycon class material has good health-care effect to human body, and this kind of aglycon material has natural aroma component; Again, trehalose can be used as the stabilizing agent of combination of enzyme preparations thing, after adding trehalose, liquid enzyme formulation composition can preserve more than 1 year at normal temperatures, join in concentrate, can increase the stability of concentrate, and trehalose is natural polysaccharide, for having good health-care effect in reconstituted tobacoo; Finally, polyacrylamide and tannic acid, on the one hand as surfactant, can reduce surface tension, be conducive to biology enzyme and better contact with substrate, improve enzymolysis efficiency, reduce the consumption of enzyme.Also can be used as flocculant on the other hand, combination of enzyme preparations thing is coordinated to be used in concentrate, can by unhydrolyzable for enzyme preparation macromolecule some special pectin more than 100,000, albumen, starch etc. carry out flocculation removing, the above enzyme preparation molecular weight that we select is below 30,000, so polyacrylamide and tannic acid can not flocculate to enzyme preparation.
Add Chinese toon medicinal extract and can reach following beneficial effect: Chinese toon medicinal extract is rich in the multiple bioactive ingredients such as amino acid, volatile oil and flavones, saponin(e, alkaloid, can add in tobacco concentrate and make reconstituted tobacoo, the flavor matter of thin slice can be significantly improved, and the amino acid that Chinese toon medicinal extract contains, volatilization wet goods composition can cover assorted gas and the stimulation of thin slice.
Add giant knotweed medicinal extract and can reach following beneficial effect: polygonin and archen are the main functional component in giant knotweed medicinal extract.Gentrin Knotweed P.E and combination of enzyme preparations thing add simultaneously, and the cellulase hydrolyzable polygonin in combination of enzyme preparations thing is resveratrol.Research display resveratrol and archen show anti-oxidation characteristics widely, as LDL-C oxidation and peroxidatic reaction of lipid.Resveratrol demonstrates simultaneously and contributes to cardiovascular health and invigorate blood circulation, and ease the pain, clearing heat and removing internal wetness, detoxification removes phlegm.Other composition comprises red anthrone, and Physcion and Rhein all have anti-inflammatory, arthritis of dispelling and antimicrobial acivity.Add to after reconstituted tobacoo with the synergy of Chinese toon medicinal extract, both can play a role in health care, the bad stimulation of reconstituted tobacoo and assorted gas can be covered again.
Step S300, in filter residue, add slurry, mix, making beating, after add auxiliary agent, obtain mixed slurry, wherein, slurry is the mixture of one or more in bamboo pulp, Chinese alpine rush slurry, and auxiliary agent is grouped into by the one-tenth of following mass percent: the alkylamide imidazoline of 10 ~ 20%, the alkyl betaine of 5 ~ 20%, the oxirane of 20 ~ 40%, the stearic acid of 10 ~ 30%.
The quality of auxiliary agent is 0.2 ~ 0.6% of solid content dry weight in concentrate.Preferably, auxiliary agent is grouped into by the one-tenth of following mass percent: the alkylamide imidazoline of 20%, the alkyl betaine of 20%, the oxirane of 40%, the stearic acid of 20%.
Add auxiliary agent and can reach following beneficial effect: the quality that 1. can improve paper, improve de-watering of slurries performance, improve the retention of fiber fines and filler, reduce raw-material consumption and the pollution etc. to environment; 2. improve the filter of paper pulp, increase dry paper intensity, improve the retention of fiber and filler; 3. can reduce plain boiled water solid content, improve the efficiency of raw material yield and recovery system, and can spreading rate be significantly improved, improve paper pliability; 4. selected alkylamide imidazoline, alkyl betaine, oxirane, stearic acid have very strong flocculation to the high molecular weight protein in slurry, pectin, starch, polysaccharide etc., reduce the content of non-fiber part in paper substrate, reduce paper brittleness, improve spreading rate and the pliability of paper substrate, and non-caked between thin slice in FINISHED packing extrusion process, be beneficial to chopping.
Preferably, the quality of slurry is 3 ~ 7% of filter residue dry weight.Slurry is the mixture of bamboo pulp, Chinese alpine rush slurry, and wherein, the quality of bamboo pulp is 3 ~ 6% of filter residue dry weight, and the quality of Chinese alpine rush slurry is 4 ~ 7% of filter residue dry weight.
Add bamboo pulp and Chinese alpine rush slurry can reach following beneficial effect: the fiber content that can supplement on the one hand offal itself is low, and fiber is short, paper substrate toughness and insufficient strength after the papermaking caused; Bamboo pulp, Chinese alpine rush slurry and the fiber of bamboo pulp own are longer on the other hand, the component contents such as the lignin in fiber are low, both toughness and the intensity of fiber can have been improved, the spreading rate of paper substrate can be increased again, and itself there is natural light fragrance, stimulation and assorted gas that in offal, macromolecular substances causes can be covered, effectively promote the quality of reconstituted tobacoo.
Step S400, adopt paper process, paper substrate of being laminated by mixed slurry, after by coating solution on sheet paper base, then drying, makes reconstituted tobacoo.
The production method of above-mentioned reconstituted tobacoo, adopt the treatment process that combination of enzyme preparations thing combines with auxiliary agent, working condition is gentle, efficiency is high, pollutes little, and enzyme used, auxiliary agent, slurry are conventional commercialization material, purity is high, price is low, be easy to obtain and working condition is easily grasped and controlled, combination of enzyme preparations thing, between slurry and auxiliary agent exist synergy, obviously can reduce the content of lignin, improve suck effect; The coating fluid utilizing the present invention to obtain and paper substrate manufacture reconstituted tobacoo, have excellent stability and repeatability, and have more significantly flavouring effect and unique style and features.This method production technology is simple, and production cost is low, is easy to realize suitability for industrialized production.
Below in conjunction with specific embodiment, the invention will be further elaborated.
Embodiment 1
A production method for reconstituted tobacoo, comprises the following steps:
(1) be 10mm by offal Mechanical Crushing to length, the water of the offal of 500g, the offal of 2500g and 25000g mixed rear heating extraction 3 times, after filter; obtain filtrate and filter residue; merging filtrate, concentrates filtrate, obtains the concentrate that density is 1.16g/mL.
Filtering required filter sizes is 1 μm.
(2) in concentrate, add Chinese toon medicinal extract, giant knotweed medicinal extract, combination of enzyme preparations thing, carry out enzyme digestion reaction, be heated to 90 DEG C of enzyme 10min that go out afterwards, form coating fluid.
Wherein, combination of enzyme preparations thing is made up of each component of following mass percent: the pectase of 30%, the protease of 10%, 20% amylase, 10% cellulase, the trehalose of 15%, the polyacrylamide of 5% and 10% tannic acid.The quality of combination of enzyme preparations thing is 1 ‰ of offal and offal total amount.The quality of Chinese toon medicinal extract is 0.2% of solid content dry weight in concentrate.The quality of giant knotweed medicinal extract is 0.2% of solid content dry weight in concentrate.The condition of enzyme digestion reaction is: pH=4.5, hydrolysis temperature are 60 DEG C, enzymolysis time is 0.5h.
(3) in filter residue, add slurry, mix, making beating, after add auxiliary agent, obtain mixed slurry.
Wherein, slurry is the mixture in bamboo pulp, Chinese alpine rush slurry, and the quality of bamboo pulp is 4% of filter residue dry weight, and the quality of Chinese alpine rush slurry is 6% of filter residue dry weight.The quality of auxiliary agent is 0.3% of solid content dry weight in concentrate.Auxiliary agent is grouped into by the one-tenth of following mass percent: the alkylamide imidazoline of 20%, the alkyl betaine of 20%, the oxirane of 40%, the stearic acid of 20%.
(4) adopt paper process, paper substrate of being laminated by mixed slurry, after by coating solution on sheet paper base, then drying, makes reconstituted tobacoo.
Embodiment 2
A production method for reconstituted tobacoo, comprises the following steps:
(1) be 12mm by offal Mechanical Crushing to length, the water of the offal of 600g, the offal of 800g and 6000g mixed rear heating extraction 2 times, after filter; obtain filtrate and filter residue; merging filtrate, concentrates filtrate, obtains the concentrate that density is 1.21g/mL.
Filtering required filter sizes is 3 μm.
(2) in concentrate, add Chinese toon medicinal extract, giant knotweed medicinal extract, combination of enzyme preparations thing, carry out enzyme digestion reaction, be heated to 90 DEG C of enzyme 10min that go out afterwards, formed coating fluid.
Wherein, combination of enzyme preparations thing is made up of each component of following mass percent: the pectase of 20%, the protease of 10%, 15% amylase, 15% cellulase, the trehalose of 25%, the polyacrylamide of 5% and 10% tannic acid.The quality of combination of enzyme preparations thing is 1.2 ‰ of offal and offal total amount.The quality of Chinese toon medicinal extract is 0.4% of solid content dry weight in concentrate.The quality of giant knotweed medicinal extract is 0.5% of solid content dry weight in concentrate.The condition of enzyme digestion reaction is: pH=5.0, hydrolysis temperature are 45 DEG C, enzymolysis time is 1.5h.
(3) in filter residue, add slurry, mix, making beating, after add auxiliary agent, obtain mixed slurry.
Wherein, slurry is the mixture in bamboo pulp, Chinese alpine rush slurry, and the quality of bamboo pulp is 4.5% of filter residue dry weight, and the quality of Chinese alpine rush slurry is 5.5% of filter residue dry weight.The quality of auxiliary agent is 0.4% of solid content dry weight in concentrate.Auxiliary agent is grouped into by the one-tenth of following mass percent: the alkylamide imidazoline of 10%, the alkyl betaine of 20%, the oxirane of 40%, the stearic acid of 30%.
(4) adopt paper process, paper substrate of being laminated by mixed slurry, after by coating solution on sheet paper base, then drying, makes reconstituted tobacoo.
Embodiment 3
A production method for reconstituted tobacoo, comprises the following steps:
(1) be 15mm by offal Mechanical Crushing to length, the water of the offal of 400g, the offal of 1000g and 10800g mixed rear heating extraction 2 times, after filter; obtain filtrate and filter residue; merging filtrate, concentrates filtrate, obtains the concentrate that density is 1.25g/mL.
Filtering required filter sizes is 3 μm.
(2) in concentrate, add Chinese toon medicinal extract, giant knotweed medicinal extract, combination of enzyme preparations thing, carry out enzyme digestion reaction, be heated to 90 DEG C of enzyme 10min that go out afterwards, form coating fluid.
Wherein, combination of enzyme preparations thing is made up of each component of following mass percent: the pectase of 25%, the protease of 10%, 15% amylase, 20% cellulase, the trehalose of 20%, the polyacrylamide of 5% and 5% tannic acid.The quality of combination of enzyme preparations thing is 1.0 ‰ of offal and offal total amount.The quality of Chinese toon medicinal extract is 0.5% of solid content dry weight in concentrate.The quality of giant knotweed medicinal extract is 0.5% of solid content dry weight in concentrate.The condition of enzyme digestion reaction is: pH=6, hydrolysis temperature are 30 DEG C, enzymolysis time is 2h.
(3) in filter residue, add slurry, mix, making beating, after add auxiliary agent, obtain mixed slurry.
Wherein, slurry is the mixture in bamboo pulp, Chinese alpine rush slurry, and the quality of bamboo pulp is 3.6% of filter residue dry weight, and the quality of Chinese alpine rush slurry is 6.4% of filter residue dry weight.The quality of auxiliary agent is 0.6% of solid content dry weight in concentrate.Auxiliary agent is grouped into by the one-tenth of following mass percent: the alkylamide imidazoline of 20%, the alkyl betaine of 20%, the oxirane of 30%, the stearic acid of 30%.
(4) adopt paper process, paper substrate of being laminated by mixed slurry, after by coating solution on sheet paper base, then drying, makes reconstituted tobacoo.
Embodiment 4
A production method for reconstituted tobacoo, comprises the following steps:
(1) be 13mm by offal Mechanical Crushing to length, the water of the offal of 500g, the offal of 2500g and 10000g mixed rear heating extraction 3 times, after filter; obtain filtrate and filter residue; merging filtrate, concentrates filtrate, obtains the concentrate that density is 1.20g/mL.
Filtering required filter sizes is 1 μm.
(2) in concentrate, add Chinese toon medicinal extract, giant knotweed medicinal extract, combination of enzyme preparations thing, carry out enzyme digestion reaction, be heated to 90 DEG C of enzyme 10min that go out afterwards, form coating fluid.
Wherein, combination of enzyme preparations thing is made up of each component of following mass percent: the pectase of 20%, the protease of 8%, 18% amylase, 20% cellulase, the trehalose of 24%, the polyacrylamide of 3% and 7% tannic acid.The quality of combination of enzyme preparations thing is 1.5 ‰ of offal and offal total amount.The quality of Chinese toon medicinal extract is 0.1% of solid content dry weight in concentrate.The quality of giant knotweed medicinal extract is 0.6% of solid content dry weight in concentrate.The condition of enzyme digestion reaction is: pH=7.0, hydrolysis temperature are 25 DEG C, enzymolysis time is 2h.
(3) in filter residue, add slurry, mix, making beating, after add auxiliary agent, obtain mixed slurry.
Wherein, slurry is the mixture in bamboo pulp, Chinese alpine rush slurry, and the quality of bamboo pulp is 5% of filter residue dry weight, and the quality of Chinese alpine rush slurry is 5% of filter residue dry weight.The quality of auxiliary agent is 0.3% of solid content dry weight in concentrate.The one-tenth of the following mass percent of auxiliary agent is grouped into: the alkylamide imidazoline of 15%, the alkyl betaine of 20%, the oxirane of 40%, the stearic acid of 25%.
(4) adopt paper process, paper substrate of being laminated by mixed slurry, after by coating solution on sheet paper base, then drying, makes reconstituted tobacoo.
Comparative example 1
A production method for reconstituted tobacoo, comprises the following steps:
(1) be 10mm by offal Mechanical Crushing to length, the water of the offal of 500g, the offal of 2500g and 25000g mixed rear heating extraction 3 times, after filter; obtain filtrate and filter residue; merging filtrate, concentrates filtrate, obtains the concentrate that density is 1.16g/mL.
Filtering required filter sizes is 1 μm.
(2) in concentrate, add combination of enzyme preparations thing, carry out enzyme digestion reaction, be heated to 90 DEG C of enzyme 10min that go out afterwards, form coating fluid.
Wherein, combination of enzyme preparations thing is made up of each component of following mass percent: the pectase of 30%, the protease of 10%, 20% amylase, 10% cellulase, the trehalose of 15%, the polyacrylamide of 5% and 10% tannic acid.The quality of combination of enzyme preparations thing is 1 ‰ of offal and offal total amount.The condition of enzyme digestion reaction is: pH=4.5, hydrolysis temperature are 60 DEG C, enzymolysis time is 0.5h.
(3) adopt paper process, paper substrate of being laminated by filter residue, after by coating solution on sheet paper base, then drying, makes reconstituted tobacoo.
Comparative example 2
A production method for reconstituted tobacoo, comprises the following steps:
(1) be 10mm by offal Mechanical Crushing to length, the water of the offal of 500g, the offal of 2500g and 25000g mixed rear heating extraction 3 times, after filter; obtain filtrate and filter residue; merging filtrate, concentrates filtrate, obtains the concentrate that density is 1.16g/mL.
Filtering required filter sizes is 1 μm.
(2) in concentrate, add Chinese toon medicinal extract, giant knotweed medicinal extract, combination of enzyme preparations thing, carry out enzyme digestion reaction, be heated to 90 DEG C of enzyme 10min that go out afterwards, form coating fluid.
Wherein, combination of enzyme preparations thing is made up of each component of following mass percent: the pectase of 30%, the protease of 10%, 20% amylase, 10% cellulase, the trehalose of 15%, the polyacrylamide of 5% and 10% tannic acid.The quality of combination of enzyme preparations thing is 1 ‰ of offal and offal total amount.The quality of Chinese toon medicinal extract is 0.2% of solid content dry weight in concentrate.The quality of giant knotweed medicinal extract is 0.2% of solid content dry weight in concentrate.The condition of enzyme digestion reaction is: pH=4.5, hydrolysis temperature are 60 DEG C, enzymolysis time is 0.5h.
(3) adopt paper process, paper substrate of being laminated by filter residue, after by coating solution on sheet paper base, then drying, makes reconstituted tobacoo.
Comparative example 3
A production method for reconstituted tobacoo, comprises the following steps:
(1) be 10mm by offal Mechanical Crushing to length, the water of the offal of 500g, the offal of 2500g and 25000g mixed rear heating extraction 2 times, after filter; obtain filtrate and filter residue; merging filtrate, concentrates filtrate, obtains the concentrate that density is 1.16g/mL.
Filtering required filter sizes is 1 μm.
(2) to filter residue making beating, after add auxiliary agent, obtain mixed slurry.
Wherein, the quality of auxiliary agent is 0.3% of solid content dry weight in concentrate.Auxiliary agent is grouped into by the one-tenth of following mass percent: the alkylamide imidazoline of 20%, the alkyl betaine of 20%, the oxirane of 40%, the stearic acid of 20%.
(4) adopt paper process, paper substrate of being laminated by mixed slurry, after concentrate is applied on sheet paper base, then drying, makes reconstituted tobacoo.
Comparative example 4
A production method for reconstituted tobacoo, comprises the following steps:
(1) be 10mm by offal Mechanical Crushing to length, the water of the offal of 500g, the offal of 2500g and 25000g mixed rear heating extraction 3 times, after filter; obtain filtrate and filter residue; merging filtrate, concentrates filtrate, obtains the concentrate that density is 1.16g/mL.
Filtering required filter sizes is 1 μm.
(2) in filter residue, add slurry, mix, making beating, after add auxiliary agent, obtain mixed slurry.
Wherein, slurry is the mixture in bamboo pulp, Chinese alpine rush slurry, and the quality of bamboo pulp is 4% of filter residue dry weight, and the quality of Chinese alpine rush slurry is 6% of filter residue dry weight.The quality of auxiliary agent is 0.3% of solid content dry weight in concentrate.Auxiliary agent is grouped into by the one-tenth of following mass percent: the alkylamide imidazoline of 20%, the alkyl betaine of 20%, the oxirane of 40%, the stearic acid of 20%.
(4) adopt paper process, paper substrate of being laminated by mixed slurry, after concentrate is applied on sheet paper base, then drying, makes reconstituted tobacoo.
Result of the test
Choose current existing reconstituted tobacoo production technology as blank group, the reconstituted tobacoo of reconstituted tobacoo obtained for embodiment 1 ~ 4 and comparative example 1 ~ 4 is compared, draws following data after testing.
Table 1 smoking result
As shown in Table 1, comparative example 1 ~ 4, embodiment 1 ~ 4 are compared with blank group, the aroma quality of embodiment 1 ~ 4, assorted gas, excitant and pleasant impression have and largely improve, aroma quality has very large lifting, and assorted gas, excitant and pleasant impression have reduction, combination of enzyme preparations thing is described, there is synergy between slurry and auxiliary agent, obviously can reduce the content of lignin, improve and suck effect; The coating fluid utilizing the present invention to obtain and paper substrate manufacture reconstituted tobacoo, have excellent stability and repeatability, and have more significantly flavouring effect and unique style and features.This method production technology is simple, and production cost is low, is easy to realize suitability for industrialized production.
The above embodiment only have expressed several embodiment of the present invention, and it describes comparatively concrete and detailed, but therefore can not be interpreted as the restriction to the scope of the claims of the present invention.It should be pointed out that for the person of ordinary skill of the art, without departing from the inventive concept of the premise, can also make some distortion and improvement, these all belong to protection scope of the present invention.Therefore, the protection domain of patent of the present invention should be as the criterion with claims.
Claims (8)
1. a production method for reconstituted tobacoo, is characterized in that, comprises the following steps:
(1) offal, offal and water are mixed rear heating extraction 2 ~ 3 times, after filter, obtain filtrate and filter residue, merging filtrate, described filtrate is concentrated, obtain concentrate, wherein, the mass ratio of offal, offal, water is offal: offal: water=1 ~ 3: 4 ~ 6: 20 ~ 54;
(2) in described concentrate, Chinese toon medicinal extract, giant knotweed medicinal extract, combination of enzyme preparations thing is added, carry out enzyme digestion reaction, heat the enzyme that goes out afterwards, form coating fluid, wherein, described combination of enzyme preparations thing is made up of each component of following mass percent: the pectase of 10 ~ 30%, the protease of 5 ~ 10%, 5 ~ 20% amylase, 10 ~ 20% cellulase, the trehalose of 10 ~ 30%, the polyacrylamide of 2 ~ 8% and 3 ~ 10% tannic acid;
(3) in described filter residue, slurry is added, mix, making beating, after add auxiliary agent, obtain mixed slurry, wherein, described slurry is the mixture of one or more in bamboo pulp, Chinese alpine rush slurry, and described auxiliary agent is grouped into by the one-tenth of following mass percent: the alkylamide imidazoline of 20%, the alkyl betaine of 20%, the oxirane of 40%, the stearic acid of 20%; Or described auxiliary agent is grouped into by the one-tenth of following mass percent: the alkylamide imidazoline of 10%, the alkyl betaine of 20%, the oxirane of 40%, the stearic acid of 30%; Or described auxiliary agent is grouped into by the one-tenth of following mass percent: the alkylamide imidazoline of 20%, the alkyl betaine of 20%, the oxirane of 30%, the stearic acid of 30%; Or described auxiliary agent is grouped into by the one-tenth of following mass percent: the alkylamide imidazoline of 15%, the alkyl betaine of 20%, the oxirane of 40%, the stearic acid of 25%; And
(4) adopt paper process, paper substrate of being laminated by described mixed slurry, after by described coating solution on described sheet paper base, then drying, makes reconstituted tobacoo.
2. the production method of reconstituted tobacoo according to claim 1, is characterized in that, the length of described offal is 10 ~ 15mm.
3. the production method of reconstituted tobacoo according to claim 1, is characterized in that, in step (1), filters with filter membrane, and the aperture of described filter membrane is 1 ~ 3 μm, and the density of concentrate is 1.17 ~ 1.22g/mL.
4. the production method of reconstituted tobacoo according to claim 1, it is characterized in that, in step (2), described combination of enzyme preparations thing is made up of each component of following mass percent: the pectase of 30%, the protease of 10%, 20% amylase, 10% cellulase, the trehalose of 15%, the polyacrylamide of 5% and 10% tannic acid.
5. the production method of reconstituted tobacoo according to claim 1, is characterized in that, in step (2), the condition heating the enzyme that goes out is: heating-up temperature is 90 ~ 100 DEG C, and the heat time is 10 ~ 15min.
6. the production method of reconstituted tobacoo according to claim 1, is characterized in that, described auxiliary agent is grouped into by the one-tenth of following mass percent: the alkylamide imidazoline of 20%, the alkyl betaine of 20%, the oxirane of 40%, the stearic acid of 20%.
7. the production method of reconstituted tobacoo according to claim 1, is characterized in that, the quality of described combination of enzyme preparations thing is 0.5 ~ 2 ‰ of offal and offal total amount; The quality of described Chinese toon medicinal extract is 0.1 ~ 0.5% of solid content dry weight in concentrate, and the quality of described giant knotweed medicinal extract is 0.2 ~ 0.6% of solid content dry weight in concentrate; The condition of enzyme digestion reaction is: pH=4.0 ~ 7.0, hydrolysis temperature are 20 ~ 60 DEG C, enzymolysis time is 0.5 ~ 2h.
8. the production method of reconstituted tobacoo according to claim 1, is characterized in that, described slurry is the mixture of bamboo pulp, Chinese alpine rush slurry, and wherein, the quality of bamboo pulp is 3 ~ 6% of filter residue dry weight, and the quality of Chinese alpine rush slurry is 4 ~ 7% of filter residue dry weight.
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| CN108652068A (en) * | 2018-06-08 | 2018-10-16 | 湖北中烟工业有限责任公司 | Low stimulation papermaking-method reconstituted tobaccos product of one kind and preparation method thereof |
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| CN112471587A (en) * | 2020-12-10 | 2021-03-12 | 云南中烟再造烟叶有限责任公司 | Method for increasing length of tobacco stalk fiber and adjusting chemical components of coating liquid |
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