CN105146741B - A kind of natural herbal enzymolysis liquid and preparation method thereof and the application in cigarette - Google Patents
A kind of natural herbal enzymolysis liquid and preparation method thereof and the application in cigarette Download PDFInfo
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- CN105146741B CN105146741B CN201510531220.1A CN201510531220A CN105146741B CN 105146741 B CN105146741 B CN 105146741B CN 201510531220 A CN201510531220 A CN 201510531220A CN 105146741 B CN105146741 B CN 105146741B
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Abstract
The invention belongs to tobacco aromaticss technical field, a kind of natural herbal enzymolysis liquid and preparation method thereof and the application in cigarette are disclosed.Natural herbal enzymolysis liquid of the present invention is made by the following method：It will be crushed after barrenwort, rheum officinale, saline cistanche, psoralea corylifolia, fleece-flower root drying, sieving；The natural herbal particle obtained after sieve, plus enzymolysis liquid are weighed, enzymolysis catalysis, filtering, concentration produces natural herbal enzymolysis liquid.Application of the natural herbal enzymolysis liquid in cigarette：Natural herbal enzymolysis liquid in cigarette shreds, thin slice or offal weight 0.1 20 ‰ ratio, in the solution for being dissolved in certain density ethanol or certain density ethanol and propane diols, and be equably sprayed on cigarette shreds, thin slice or offal, and cigarette is rolled into, improve the comfortableness of cigarette product.
Description
Technical field
The invention belongs to tobacco aromaticss technical field, and in particular to a kind of natural herbal enzymolysis liquid and preparation method thereof and
Application in cigarette.
Background technology
Tobacco flavoring determines the peculiar style of tobacco, sets off and enriches cigarette perfume, and addition essence spice for cigarette is to tobacco
It is very big that product, which inhale contribution, and it is an important component of cigarette brand, therefore tobacco adds cigarette particular perfume, is changed
The composition of fragrance matter, is to influence a key factor of cigarette brand and quality, therefore can not ignore.China possesses rich
This rich grass resource, natural herbal extract is added at present, and oneself turns into the developing direction that Chinese-style cigarette is developed.
The extraction overwhelming majority of natural herbal use traditional extraction process, i.e. decocting method, infusion process, percolation, plus
Heat reflow method etc..Conventional method equipment investment is few, and operation is simple.Method generally existing extraction efficiency is low, impurity is more for these,
Solvent load is big, time-consuming, power consumption is big, thermal sensitivity, volatile effective component are easily caused in extraction process decomposes or loss etc.
Problem.
Natural herbal prescription in the present invention is made up of barrenwort, rheum officinale, saline cistanche, psoralea corylifolia, the fleece-flower root, due to this
Careless prescription has nourishing lung and kidney, effect of clear throat, so the comfortableness of cigarette product can be improved by adding in cigarette product.River
Cigarette once carried out extracting application using alcohol-water extraction method to the herbal prescription in west, and 101263930A " protect by a kind of Chinese medicine
The manufacturing process of strong type cigarette ".Time-consuming for alcohol-water extraction method, power consumption big, efficiency is low.Therefore, prior art has much room for improvement.
The content of the invention
For above-mentioned problem, there is provided a kind of natural herbal enzymolysis liquid for cigarette.The hydrolyzate is in not shadow
In the case of ringing cigarette main aroma feature, the comfortableness of cigarette product can be more improved.
Another object of the present invention is the preparation method for providing above-mentioned natural herbal enzymolysis liquid.
It is also an object of the present invention to provide the application of above-mentioned natural herbal enzymolysis liquid.
The present invention to achieve the above object, takes following technical scheme to be achieved：
A kind of preparation method of natural herbal enzymolysis liquid, comprises the following steps：
(1) each component in natural herbal prescription is mixed, crushed, choose the particle of 60-80 mesh, add appropriate distillation
Water, adjustment pH is 4.0~5.0, and water temperature is 50 DEG C, soaks 1h；
(2) complex enzyme is added to be digested；
(3) enzymolysis product is filtered, enzymolysis liquid is obtained；
(4) enzymolysis liquid being filtrated to get is concentrated under reduced pressure in 40~50 DEG C, produces natural herbal enzymolysis liquid；
The natural herbal prescription includes the following components of parts by weight：1~5 part of barrenwort, 1~5 part of rheum officinale, saline cistanche
1~2 part, 1~3 part of psoralea corylifolia, 1~2 part of the fleece-flower root.
Preferably, the natural herbal prescription includes the following components of parts by weight：5 parts of barrenwort, 5 parts of rheum officinale, meat desert
1 part of Rong, 3 parts of psoralea corylifolia, 1 part of the fleece-flower root.
Preferably, the mass ratio of natural herbal prescription particle and distilled water is 1 in step (1):8.
Preferably, complex enzyme is that mass ratio is 3 in step (2):5 cellulase and pectase.
Preferably, complex enzyme addition accounts for the 2% of natural herbal prescription granular mass in step (2).
Preferably, hydrolysis temperature is 30~50 DEG C in step (2), and enzymolysis time is 3h.
Preferably, it is concentrated under reduced pressure into step (4) identical with natural herbal prescription granular mass.
Because the material composition in the natural herbal prescription is mainly cellulose, hemicellulose, pectic substance, lignin etc.,
Therefore cellulase, pectase are the main enzymes that bioanalysis prepares natural herbal enzymolysis liquid.Due in Chinese medicine preparation process,
Pass through " processing " stage, protein matter therein is removed substantially, so protease is no longer added in this research, simplify system
Standby technique, while cost-effective.
The invention also discloses a kind of natural herbal enzymolysis liquid being prepared from by the above method.
Application of the natural herbal enzymolysis liquid of the present invention in cigarette, it is specific as follows：Natural herbal enzymolysis liquid is dissolved in body
In ethanol and the mixed liquor of propane diols that the ethanol or volume fraction that fraction is 95% are 95%, cigarette cigarette is uniformly sprayed at
On silk, thin slice or offal, cigarette is rolled into.
Preferably, the addition of the natural herbal enzymolysis liquid be cigarette shreds, thin slice or offal weight 0.1~
20‰。
Compared with prior art, beneficial effects of the present invention are as follows：
(1) natural herbal enzymolysis liquid of the invention is prepared from by biological enzyme, compared with prior art, with ring
Guarantor, energy-conservation, efficient advantage.
(2) present invention realizes that bioanalysis prepares natural herbal enzymolysis liquid by cellulase, pectase, simplifies preparation work
Skill, while cost-effective.
(3) natural herbal enzymolysis liquid of the invention is applied in cigarette, is not influenceing the situation of cigarette main aroma feature
Under, it can more improve the comfortableness of cigarette product.
Embodiment
Below in conjunction with specific embodiment, the present invention is further illustrated.
A kind of preparation method of natural herbal enzymolysis liquid, comprises the following steps：
(1) will be by 1~5 part of barrenwort, 1~5 part of rheum officinale, 1~2 part of saline cistanche, 1~3 part of psoralea corylifolia, 1~2 part of fleece-flower root
Each component mixing in the natural herbal prescription of composition, crushes, chooses the particle of 60-80 mesh, add appropriate distilled water, adjust pH
For 4.0~5.0, water temperature is 50 DEG C, soaks 1h；
(2) complex enzyme is added to be digested；
(3) enzymolysis product is filtered, enzymolysis liquid is obtained；
(4) enzymolysis liquid being filtrated to get is concentrated under reduced pressure in 40~50 DEG C, produces natural herbal enzymolysis liquid；
The mass ratio of natural herbal prescription particle and distilled water is preferably 1 in step (1):8.
Complex enzyme is that mass ratio is 3 in step (2):5 cellulase and pectase.
Complex enzyme addition accounts for the 2% of natural herbal prescription granular mass in step (2).
Hydrolysis temperature is 30~50 DEG C in step (2), and enzymolysis time is 3h.
It is concentrated under reduced pressure into step (4) identical with natural herbal prescription granular mass.
Because the material composition in the natural herbal prescription is mainly cellulose, hemicellulose, pectic substance, lignin etc.,
Therefore cellulase, pectase are the main enzymes that bioanalysis prepares natural herbal enzymolysis liquid.Due in Chinese medicine preparation process,
Pass through " processing " stage, protein matter therein is removed substantially, so protease is no longer added in this research, simplify system
Standby technique, while cost-effective.
Above-mentioned natural herbal enzymolysis liquid can be applied in cigarette, specific as follows：Natural herbal enzymolysis liquid is dissolved in volume
In ethanol and the mixed liquor of propane diols that the ethanol or volume fraction that fraction is 95% are 95%, be uniformly sprayed at cigarette shreds,
On thin slice or offal, cigarette is rolled into.The addition of natural herbal enzymolysis liquid is the 0.1 of cigarette shreds, thin slice or offal weight
~20 ‰.
Elaborate for two example two below：
Embodiment 1
The natural herbal prescription that will be made up of 5kg barrenwort, 5kg rheum officinales, 1kg saline cistanches, 3kg psoralea corylifolias, the 1kg fleece-flowers root
Mixing, is crushed, and chooses the particle of 60-80 mesh.Distilled water is added, wherein, the mass ratio of natural herbal prescription particle and distilled water
For 1:8.Adjustment pH is 4.0-5.0, and water temperature is 50 DEG C, soaks 1h.According to cellulase:Pectase=3:5 ratio (quality
Than) complex enzyme is prepared, and added by 2% addition (on the basis of quality of herbal prescription particle), enzyme is carried out at 40 DEG C
Solve 3h；After the completion of enzymolysis, the natural herbal enzymolysis liquid of acquisition is subjected to decompression suction filtration, filtrate is concentrated under reduced pressure into 40~50 DEG C
Herbal prescription granular mass is identical, produces natural herbal enzymolysis liquid.
Extract dilution is uniformly sprayed onto into hard gold sage with 0.2 ‰ adding proportions with miniaturised nebuliser to match somebody with somebody in quadrate lope group,
Sealed and deposited with band after sprinkling, after 4 hours, sample cigarette is rolled with cigarette device is made, deposit in climatic chamber 48 small
When.It is added to application effect in cigarette and is shown in Table 1.
Embodiment 2
The natural herbal prescription that will be made up of 5kg barrenwort, 5kg rheum officinales, 1kg saline cistanches, 3kg psoralea corylifolias, the 1kg fleece-flowers root
Mixing, is crushed, and chooses the particle of 60-80 mesh.Distilled water is added, wherein, the mass ratio of natural herbal prescription particle and distilled water
For 1:8.Adjustment pH is 4.0-5.0, and water temperature is 50 DEG C, soaks 1h.According to cellulase:Pectase=3:5 ratio (quality
Than) complex enzyme is prepared, and added by 2% addition (on the basis of quality of herbal prescription particle), enzyme is carried out at 50 DEG C
Solve 3h；After the completion of enzymolysis, the natural herbal enzymolysis liquid of acquisition is subjected to decompression suction filtration, filtrate is concentrated under reduced pressure into 40~50 DEG C
Herbal prescription granular mass is identical, produces natural herbal enzymolysis liquid.
Extract dilution is uniformly sprayed onto into hard gold sage with 0.2 ‰ adding proportions with miniaturised nebuliser to match somebody with somebody in quadrate lope group,
Sealed and deposited with band after sprinkling, after 4 hours, sample cigarette is rolled with cigarette device is made, deposit in climatic chamber 48 small
When.It is added to application effect in cigarette and is shown in Table 1.
The natural herbal enzymolysis liquid application effect table of table 1
The natural herbal enzymolysis liquid of the present invention is applied in cigarette, in the case where not influenceing cigarette main aroma feature,
It can more improve the comfortableness of cigarette product.
The technical scheme provided above the embodiment of the present invention is described in detail, specific case used herein
Principle and embodiment to the embodiment of the present invention are set forth, and the explanation of above example is only applicable to help and understands this
The principle of inventive embodiments；Simultaneously for those of ordinary skill in the art, according to the embodiment of the present invention, in specific embodiment party
It will change in formula and application, in summary, this specification content should not be construed as limiting the invention.
Claims (8)
1. a kind of preparation method of natural herbal enzymolysis liquid, it is characterised in that comprise the following steps：
(1) each component in natural herbal prescription is mixed, crushed, choose the particle of 60-80 mesh, add appropriate distilled water, institute
The mass ratio for stating natural herbal prescription particle and distilled water is 1:8；It is 4.0~5.0 to adjust pH, and water temperature is 50 DEG C, soaks 1h；
(2) complex enzyme is added to be digested；
(3) enzymolysis product is filtered, enzymolysis liquid is obtained；
(4) enzymolysis liquid being filtrated to get is concentrated under reduced pressure in 40~50 DEG C, produces natural herbal enzymolysis liquid；
The natural herbal prescription includes the following components of parts by weight：1~5 part of barrenwort, 1~5 part of rheum officinale, saline cistanche 1~2
Part, 1~3 part of psoralea corylifolia, 1~2 part of the fleece-flower root；
Complex enzyme is that mass ratio is 3 in step (2):5 cellulase and pectase.
2. the preparation method of natural herbal enzymolysis liquid according to claim 1, it is characterised in that the natural herbal prescription
Following components including parts by weight：5 parts of barrenwort, 5 parts of rheum officinale, 1 part of saline cistanche, 3 parts of psoralea corylifolia, 1 part of the fleece-flower root.
3. the preparation method of natural herbal enzymolysis liquid according to claim 1, it is characterised in that complex enzyme in step (2)
Addition accounts for the 2% of natural herbal prescription granular mass.
4. the preparation method of natural herbal enzymolysis liquid according to claim 1, it is characterised in that enzymolysis temperature in step (2)
Spend for 30~50 DEG C, enzymolysis time is 3h.
5. the preparation method of natural herbal enzymolysis liquid according to claim 1, it is characterised in that decompression is dense in step (4)
It is reduced to identical with natural herbal prescription granular mass.
6. a kind of natural herbal enzymolysis liquid being prepared from by any one of Claims 1 to 5 methods described.
7. a kind of application of natural herbal enzymolysis liquid as claimed in claim 6 in cigarette, it is characterised in that the natural herbal
Enzymolysis liquid is dissolved in the mixed liquor of the ethanol that the ethanol that volume fraction is 95% or volume fraction are 95% and propane diols, uniformly
It is sprayed on cigarette shreds, thin slice or offal, rolls into cigarette.
8. application of the natural herbal enzymolysis liquid according to claim 7 in cigarette, it is characterised in that the natural herbal
The addition of enzymolysis liquid is 0.1~the 20 ‰ of cigarette shreds, thin slice or offal weight.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106190560A (en) * | 2016-08-04 | 2016-12-07 | 江西中烟工业有限责任公司 | A kind of flavouring essence for tobacco and preparation method thereof |
| CN107981400A (en) * | 2017-12-08 | 2018-05-04 | 江西中烟工业有限责任公司 | A kind of production method of Chinese medicine cigarette and its Chinese medicine additive |
| CN108077997A (en) * | 2017-12-12 | 2018-05-29 | 江西中烟工业有限责任公司 | A kind of preparation method and applications of cigarette filter combination |
| CN109007955B (en) * | 2018-06-21 | 2021-12-31 | 重庆中烟工业有限责任公司 | Tobacco stem extract, preparation method thereof and tobacco product |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1106239A (en) * | 1994-10-11 | 1995-08-09 | 南昌卷烟厂 | Chinese medicinal health cigarette and its prodn. method |
| CN104694254A (en) * | 2015-01-09 | 2015-06-10 | 成都宏亿实业集团有限公司 | Red ginseng extract, and preparation method and application thereof |
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| CN101263930A (en) * | 2008-01-16 | 2008-09-17 | 江西中烟工业公司 | Manufacturing technology of Chinese medicine health-care cigarette |
| CN103710150B (en) * | 2014-01-13 | 2014-12-31 | 红塔烟草(集团)有限责任公司 | Tobacco flavor and preparation method thereof |
| CN104194932B (en) * | 2014-08-13 | 2016-08-24 | 河南中烟工业有限责任公司 | A kind of Chinese chestnut essence, its preparation method and the application in cigarette |
| CN104824837B (en) * | 2015-03-31 | 2016-10-19 | 川渝中烟工业有限责任公司 | The method that tobacco aromatics using is applied to buccal cigarette is extracted from fireworks |
| CN104818120A (en) * | 2015-04-29 | 2015-08-05 | 湖北中烟工业有限责任公司 | Cigarette black plum extract and preparation method thereof |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1106239A (en) * | 1994-10-11 | 1995-08-09 | 南昌卷烟厂 | Chinese medicinal health cigarette and its prodn. method |
| CN104694254A (en) * | 2015-01-09 | 2015-06-10 | 成都宏亿实业集团有限公司 | Red ginseng extract, and preparation method and application thereof |
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