CN105559132B - A kind of preparation method of functional form reconstituted tobacco and application - Google Patents
A kind of preparation method of functional form reconstituted tobacco and application Download PDFInfo
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- CN105559132B CN105559132B CN201610031290.5A CN201610031290A CN105559132B CN 105559132 B CN105559132 B CN 105559132B CN 201610031290 A CN201610031290 A CN 201610031290A CN 105559132 B CN105559132 B CN 105559132B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
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Abstract
The invention discloses a kind of preparation method of functional form reconstituted tobacco and application, comprise the following steps:1) tobacco leaf dead meal is obtained into offal extract solution and residue by immersion extraction, separation of solid and liquid;2) stalk extract solution will be obtained after the soaking extraction of offal, separation and obstructs slag;3) residue and stalk slag silk are mixed, adds wood pulp cellulose, slurry is made;4) non-cigarette material is crushed, screened, the non-cigarette material after screening is added in slurry and mixed, slurry is manufactured paper with pulp into chip base;Or adding the non-cigarette material after screening in slurry during slurry is manufactured paper with pulp;5) stalk concentrate, offal concentrate, spices are allocated into obtain coating fluid;6) by coating solution to substrate, reconstituted tobacoo is made through drying, section.The present invention is added in slurries after non-cigarette material is crushed, and is then manufactured paper with pulp, and non-cigarette material high-temperature process, applicable raw materials species extensively, the characteristic perfume of non-cigarette material will not be kept to greatest extent, the quality of reconstituted tobacoo is improved.
Description
Technical field
The invention belongs to technical field of tobacco, and in particular to a kind of preparation method of functional form reconstituted tobacco and application.
Background technology
Reconstituted tobacco, also known as reconstituted tobacoo, homogeneous tobacco leaf or recombination tobacco leaf, local Filling power is high, have good burning performance, tar
The low characteristic of burst size, it is the effective of Tar to be substituted with reconstituted tobacco or partly substitute traditional pipe tobacco to prepare cigarette
One of means.
The process for preparing reconstituted tobacco using paper process generally includes, to tobacco material immersion, extraction, extract to be concentrated
Afterwards as coating fluid, slag charge after immersion carries out the defibrination step such as manufacture paper with pulp and is prepared into paper substrate, and coating solution is dried in paper substrate
After obtain reconstituted tobacco.During the higher extraction of temperature and concentration etc., there be a part to inhaling taste and fragrance in tobacco material
The material of contribution can volatilize, decomposes, convert.So as to which the reconstituted tobacco for causing paper process to prepare has fragrance shortcoming and pungent
The defects such as sense aggravation, influence its sense organ suction quality.
The tangerine grass of Application No. 2014105533996 is prepared in the method for functional form reconstituted tobacco, is added in reconstituted tobacco
Non-tobacco material tangerine grass, tangerine grass instead of the wood pulp cellulose in reconstituted tobacco paper substrate, and still, the invention has the following disadvantages:1、
To non-cigarette material have higher selectivity, some be difficult mashing and the volatile foaming of enrichment process non-cigarette material at this
It can not be applied in method;2nd, non-cigarette material extract solution is in concentration process, under long-time high temperature (60-80 DEG C), fragrance matter
It can change, change its original style and features;3rd, non-cigarette material is after existing method is handled, the physics of plant in itself
Structure is varied widely, and is unfavorable for the holding of style and features.
The patent of invention of Application No. 2014108393456, orange peel is made after the powder of suitable particulate, coated
Cheng Zhong, paper substrate is added to by orange peel powder, improves the properties of reconstituted tobacco, by the more scientific height of the active ingredient of orange peel
Effect ground is applied in the preparation of reconstituted tobacco.But there is following drawback in the invention:1st, orange peel powder is during coating
It is added in paper substrate, is only applicable to the addition of a small amount of orange peel powder, because, if the amount of orange peel powder is more, by applying
Cloth is attached on paper substrate, after coating fluid is dried, and orange peel powder is then easily split away off from paper substrate, scaling-off serious;2nd, tangerine
Sub- skin powder is attached on paper substrate by coating, is then occurred it cannot be guaranteed that be well mixed with coating fluid due to orange peel powder
The phenomenon that orange peel powder is unevenly coated on paper substrate, influences the quality stability of product;3rd, the invention is only applicable to again
Addition orange peel powder in tobacco leaf is made, other non-cigarette materials can not be applied to, so, the method scope of application of the invention is tight
It is limited again.
In a word, the powder of non-cigarette material is added in reconstituted tobacco, original style and features of non-cigarette material can be kept, but
It is that the product produced has easily scaling-off defect, if non-cigarette material be fixed using adhesive, the use of adhesive
Certain influence is produced to the taste of inhaling of thin slice;Meanwhile, the applicable non-cigarette material of Same Way is single, with larger limitation.
The content of the invention
There is provided a kind of preparation side of functional form reconstituted tobacco in order to solve technical problem present in prior art by the present invention
Method and application.
To achieve these goals, the technical solution adopted by the present invention is as follows:
A kind of preparation method of functional form reconstituted tobacco, comprises the following steps:
1) tobacco leaf dead meal is obtained into offal extract solution and residue by immersion extraction, separation of solid and liquid;
2) stalk extract solution will be obtained after the soaking extraction of offal, separation and obstructs slag;
3) stalk slag is obtained into stalk slag silk through fiber uncoiling machine solution fibre;
4) residue and stalk slag silk are mixed, adds wood pulp cellulose, slurry is made;
5) non-cigarette material is crushed, screened, the non-cigarette material after screening is added in slurry and mixed, slurry is manufactured paper with pulp into
Chip base;Or adding the non-cigarette material after screening in slurry during slurry is manufactured paper with pulp;
6) stalk extract solution is concentrated to give stalk concentrate, offal extract solution is concentrated to give offal concentrate;
7) stalk concentrate, offal concentrate, spices are allocated into obtain coating fluid;
8) by coating solution to substrate, reconstituted tobacoo is made through drying, section.
It is added in slurry and mixes after non-cigarette material is crushed, slurry is then manufactured paper with pulp into chip base, can be by non-cigarette material
Powder is evenly distributed in chip base, is increased the active force between non-cigarette material powder and other materials, is effectively reduced scaling-off
Rate.Non- cigarette material needs not move through the immersion extraction process of early stage, can preferably keep original physiological structure and style special
Levy, go for various non-cigarette materials.Simultaneously as powder is dispensed directly onto in chip base, those can be retained and be not easy
The material being extracted, makes style more natural.
It is preferred that, step 1) in, the mass ratio of tobacco leaf dead meal and soak is 1:6-1:12.
It is preferred that, the soak is water, and the temperature of immersion extraction is 60-90 DEG C, and the time of immersion extraction is 20-
50min。
It is preferred that, step 2) in, the soak of offal immersion extraction is water, and the time of immersion extraction is 20-50min, leaching
The temperature of bubble extraction is 60-90 DEG C.
It is preferred that, step 4) in, it is 5%-15% that the wood pulp cellulose of addition, which accounts for the overall mass fraction of mixture,.Wood pulp is fine
Dimension plays increase chip base wet strength, the tensile index of improvement chip base, tear index, air permeability, absorbability.
It is preferred that, step 5) in, non-cigarette material is size-reduced, the granularity after screening is 80-100 mesh.
When the granularity of non-cigarette material powder is 80-100 mesh, non-cigarette material powder can be well mixed with slurries, and
After chip base is manufactured paper with pulp into, it is tightly combined between other materials of non-cigarette material powder and paper substrate, effectively reduces rate of slag falling, and
Non- cigarette material is uniformly distributed in chip base, effectively increase the quality stability of product.
It is preferred that, step 5) in, non-cigarette material powder is 10%-60% in the mass percent of obtained reconstituted tobacoo.
It is preferred that, step 6) and step 7) in concentrate concentration be 35%-45%.
It is preferred that, step 7) in, the absolute dry mass ratio of stalk concentrate and offal concentrate is 2:8-6:4.
It is preferred that, the non-cigarette material is the non-cigarette material and plant flowers, the non-cigarette material of leaf class of wooden class.
It is further preferred that the non-cigarette material of wooden class is agalloch eaglewood or radix glycyrrhizae, plant flowers, leaf class material are mugwort leaf
Or chrysanthemum.
It is preferred that, step 8) in, the spreading rate of coating fluid is 30%-45%.
Reconstituted tobacco prepared by the preparation method of above-mentioned functions type reconstituted tobacco.
Application of the preparation method of above-mentioned functions type reconstituted tobacco in reconstituted tobacco is prepared.
Beneficial effects of the present invention are:
1st, the present invention is added in slurry after can non-cigarette material be crushed, and then slurry is manufactured paper with pulp, this method is not
High-temperature process can be carried out to non-cigarette material, applicable raw materials species extensively, the characteristic perfume of non-cigarette material can be kept to greatest extent,
Improve the quality of reconstituted tobacoo;
2nd, contrast non-cigarette material and tobacco material extract, concentrate jointly, the process of slurrying, solve non-tobacco raw-material
Component is the problem of the feature perfume that concentration process volatile zone comes changes, while solving a part of non-cigarette material extract solution can not concentrate
So as to cause the problem of it can not be applied to reconstituted tobacoo product;
3rd, non-cigarette material powder is added in slurries, and controls the granularity of non-cigarette material powder in 80-100 mesh so that
Non- cigarette material is well mixed in the slurry, is added the active force between non-cigarette material powder and slurry, is efficiently solved scaling-off
Rate is high, the problem of non-cigarette material powder spreads uneven.
Brief description of the drawings
Fig. 1 is the process chart of the present invention.
Embodiment
The invention will be further described with reference to the accompanying drawings and examples.
Embodiment 1
As shown in figure 1, a kind of preparation method of functional form reconstituted tobacco, comprises the following steps:
1) it is 1 by solid-to-liquid ratio by tobacco leaf dead meal:8 amount adds clear water, and the temperature of immersion extraction is 85 DEG C, immersion extraction
Time be 30min, to obtaining mixing offal extract solution and residue after compound separation of solid and liquid;
2) it is 1 by solid-to-liquid ratio by offal:8 amount adds clear water, and the temperature of immersion extraction is 85 DEG C, soaks the time of extraction
For 30min, to obtaining stem extracting solution and stalk slag after compound separation of solid and liquid;
3) stalk slag is obtained into stalk slag silk through fiber uncoiling machine solution fibre;
4) by step 1) in residue and step 3) in the silk mixing of stalk slag after, the wood pulp for adding mass fraction 10% is fine
Dimension, carries out defibrination, the beating degree of slurry is 28 ° of SR, and concentration is 3% by mixture;
5) mugwort leaf is crushed, screened, powder size is 80 mesh, by the mugwort leaf powder after screening according to slurry over dry matter
Amount 40% is added to step 4) in mix in obtained slurry, slurry is manufactured paper with pulp into chip base;Or by the mugwort leaf powder after screening
Added during slurry is manufactured paper with pulp in slurry;
6) by step 1) in obtained offal extract solution pass through filtration, purification, the offal extract solution after purification is dense through evaporating
Contracting, concentrate concentration after concentration is 40%, by step 2) in stalk liquid carry out filtration, purification, the stalk liquid after purification is dense through evaporating
Contracting, the concentrate concentration after concentration is 40%;By offal concentrate and stalk concentrate according to absolute dry mass ratio be 6:4 are mixed
Close, add spices and be deployed into coating fluid;
7) by coating solution to step 5) in obtained chip base, reconstituted tobacoo is made through drying, section.
Smoke panel test experiment
By the reconstituted tobacco chopping of preparation, added according to 20% ratio in cigarette composition and be put into climatic chamber inner equilibrium
48h, is made cigarette, as sample sets, and will be not added with the cigarette of reconstituted tobacco as a control group, by sample sets and control group with
Machine is numbered, and the group of smokeing panel test being made up of the member of smoking for possessing qualification of smokeing panel test carries out sensory evaluating smoking.
Effect assessment
Smoking result shows:Compared with control group, the cigarette of the reconstituted tobacco prepared with the inventive method is added
With obvious mugwort leaf odor characteristic, comfortable taste, with cigarette perfume natural fusion.
Mugwort leaf can not together be extracted with tobacco leaf dead meal, concentrated.Reason is that mixed extract bubbles in concentration process
Boiling is severe, and foam is pumped with vacuum, and mixed extract can not be concentrated.
Rate of slag falling is tested
By the reconstituted tobacco of preparation, climatic chamber inner equilibrium 48h is put into, as sample sets, 20g samples is weighed, is shaking
Vibrations 10min is carried out in sieve, powder is separated with sheet, the quality of remaining sheet is weighed, calculates rate of slag falling.
Rate of slag falling=(MJust-MIt is surplus)/MJust
MJustFor the quality of initial sample, MIt is surplusFor the quality of remaining large stretch of sample.
The rate of slag falling of sample sets is 1 ‰.
Embodiment 2
As shown in figure 1, a kind of preparation method of functional form reconstituted tobacco, comprises the following steps:
1) it is 1 by solid-to-liquid ratio by tobacco leaf dead meal:6 amount adds clear water, and the temperature of immersion extraction is 65 DEG C, immersion extraction
Time be 50min, to obtaining mixing offal extract solution and residue after compound separation of solid and liquid;
2) it is 1 by solid-to-liquid ratio by offal:8 amount adds clear water, and the temperature of immersion extraction is 90 DEG C, soaks the time of extraction
For 20min, to obtaining stem extracting solution and stalk slag after compound separation of solid and liquid;
3) stalk slag is obtained into stalk slag silk through fiber uncoiling machine solution fibre;
4) by step 1) in residue and step 3) in the silk mixing of stalk slag after, the wood pulp for adding mass fraction 15% is fine
Dimension, carries out defibrination, the beating degree of slurry is 28 ° of SR, and concentration is 3% by mixture;
5) agalloch eaglewood is crushed, screened, powder size is 80 mesh, by the agalloch eaglewood powder after screening according to slurry over dry matter
Amount 60% is added to step 4) in mix in obtained slurry, slurry is manufactured paper with pulp into chip base;Or by the agalloch eaglewood powder after screening
Added during slurry is manufactured paper with pulp in slurry;
6) by step 1) in obtained offal extract solution pass through filtration, purification, the offal extract solution after purification is dense through evaporating
Contracting, concentrate concentration after concentration is 45%, by step 2) in stalk liquid carry out filtration, purification, the stalk liquid after purification is dense through evaporating
Contracting, the concentrate concentration after concentration is 35%;By offal concentrate and stalk concentrate according to absolute dry mass ratio be 2:8 are mixed
Close, add spices and be deployed into coating fluid;
7) by coating solution to step 5) in obtained chip base, reconstituted tobacoo is made through drying, section.
Smoke panel test experiment
By the reconstituted tobacco chopping of preparation, added according to 10% ratio in cigarette composition and be put into climatic chamber inner equilibrium
48h, is made cigarette, as sample sets, and will be not added with the cigarette of reconstituted tobacco as a control group, by sample sets and control group with
Machine is numbered, and the group of smokeing panel test being made up of the member of smoking for possessing qualification of smokeing panel test carries out sensory evaluating smoking.
Agalloch eaglewood can not together be extracted with tobacco leaf dead meal, concentrated.It in the flavor matter of agalloch eaglewood is mainly oil that reason, which is,
Dissolubility, Extraction medium is water, it is impossible to effectively the aroma component in agalloch eaglewood is effectively extracted.
Effect assessment
Smoking result shows:Compared with control group, the cigarette of the reconstituted tobacco prepared with the inventive method is added
With obvious agalloch eaglewood odor characteristic, comfortable taste, with cigarette perfume natural fusion.
Rate of slag falling experiment is carried out with identical method, the rate of slag falling of sample sets is 1.2 ‰.
Embodiment 3
As shown in figure 1, a kind of preparation method of functional form reconstituted tobacco, comprises the following steps:
1) it is 1 by solid-to-liquid ratio by tobacco leaf dead meal:12 amount adds clear water, and the temperature of immersion extraction is 75 DEG C, immersion extraction
The time taken is 50min, to obtaining mixing offal extract solution and residue after compound separation of solid and liquid;
2) it is 1 by solid-to-liquid ratio by offal:10 amount adds clear water, and the temperature of immersion extraction is 60 DEG C, immersion extraction when
Between be 50min, to obtained after compound separation of solid and liquid stem extracting solution and stalk slag;
3) stalk slag is obtained into stalk slag silk through fiber uncoiling machine solution fibre;
4) by step 1) in residue and step 3) in the silk mixing of stalk slag after, the wood pulp for adding mass fraction 5% is fine
Dimension, carries out defibrination, the beating degree of slurry is 28 ° of SR, and concentration is 3% by mixture;
5) chrysanthemum and radix glycyrrhizae are crushed respectively, screened, powder size is 80 mesh, by the chrysanthemum powder and licorice powder after screening
End is 7 according to mass ratio:3 are mixed, and mixed-powder then is added into step 4 according to slurry absolute dry mass 30%) in
To slurry in mix, slurry is manufactured paper with pulp into chip base;Or adding mixed-powder in slurry during slurry is manufactured paper with pulp;
6) by step 1) in obtained offal extract solution pass through filtration, purification, the offal extract solution after purification is dense through evaporating
Contracting, concentrate concentration after concentration is 45%, by step 2) in stalk liquid carry out filtration, purification, the stalk liquid after purification is dense through evaporating
Contracting, the concentrate concentration after concentration is 35%;By offal concentrate and stalk concentrate according to absolute dry mass ratio be 1:1 is mixed
Close, add spices and be deployed into coating fluid;
7) by coating solution to step 5) in obtained chip base, reconstituted tobacoo is made through drying, section.
Smoke panel test experiment
By the reconstituted tobacco chopping of preparation, climatic chamber inner equilibrium 24h is put into, cigarette is made, as sample sets, and with
Cigarette made from the reconstituted tobacco that chrysanthemum powder, radix glycyrrhizae powder are together prepared with tobacco leaf dead meal by immersion extraction is made
For control group, by sample sets and control group random number, the group of smokeing panel test being made up of the member of smoking for possessing qualification of smokeing panel test is felt
Official smokes panel test.Effect assessment
Smoking result shows:Compared with control group, the cigarette of the reconstituted tobacco prepared with the inventive method is added
With obvious Scent of Chrysanthemum feature, comfortable taste, with cigarette perfume natural fusion, control sample Scent of Chrysanthemum feature is not obvious, chrysanthemum
Fragrance is slightly different compared with sample sets.
Rate of slag falling experiment is carried out with identical method, the rate of slag falling of sample sets is 0.9 ‰.
It can be seen that, method of the invention goes for a variety of non-cigarette materials, has a wide range of applications, and do not interfere with non-cigarette
The local flavor of material, when efficiently solving non-cigarette material powder addition in the prior art, the high disadvantage of caused reconstituted tobacco rate of slag falling
End.
Although above-mentioned the embodiment of the present invention is described with reference to accompanying drawing, not to invention protection domain
Limitation, one of ordinary skill in the art should be understood that on the basis of technical scheme those skilled in the art are not required to
Pay various modifications or deform still within the scope of the present invention that creative work can make.
Claims (8)
1. a kind of preparation method of functional form reconstituted tobacco, it is characterised in that:Comprise the following steps:
1)Tobacco leaf dead meal is obtained into offal extract solution and residue by immersion extraction, separation of solid and liquid;
2)Stalk extract solution will be obtained after the soaking extraction of offal, separation and obstruct slag;
3)Stalk slag is obtained into stalk slag silk through fiber uncoiling machine solution fibre;
4)By residue and stalk slag silk mixing, wood pulp cellulose is added, slurry is made, the wood pulp cellulose of addition accounts for mixture entirety
Mass fraction is 5%-15%;
5)Non- cigarette material is crushed, screened, the non-cigarette material after screening is added in slurry and mixed, slurry is manufactured paper with pulp in flakes
Base;Or adding the non-cigarette material after screening in slurry during slurry is manufactured paper with pulp, non-cigarette material is size-reduced, the granularity after screening
For 80-100 mesh, the mass percent of non-cigarette material powder in the slurry is 10%-60%, and the non-cigarette material is non-for wooden class
Cigarette material and plant flowers, the non-cigarette material of leaf class;
6)Stalk extract solution is concentrated to give stalk concentrate, offal extract solution is concentrated to give offal concentrate;
7)Stalk concentrate, offal concentrate, spices are allocated into obtain coating fluid;
8)By on coating solution to chip base, reconstituted tobacoo is made through drying, section.
2. preparation method according to claim 1, it is characterised in that:Step 1)In, the matter of tobacco leaf dead meal and soak
Amount is than being 1:6-1:12;
Soak is water, and the temperature of immersion extraction is 60-90 DEG C, and the time of immersion extraction is 20-50min.
3. preparation method according to claim 1, it is characterised in that:Step 2)In, the soak of offal immersion extraction is
Water, the time of immersion extraction is 20-50min, and the temperature of immersion extraction is 60-90 DEG C.
4. preparation method according to claim 1, it is characterised in that:Step 6)With step 7)Middle stalk concentrate and offal are dense
The concentration of contracting liquid is 35%-45%, and the absolute dry mass ratio of stalk concentrate and offal concentrate is 2:8-6:4.
5. preparation method according to claim 1, it is characterised in that:The non-cigarette material of wooden class is agalloch eaglewood or sweet
Grass, plant flowers, leaf class material are mugwort leaf or chrysanthemum.
6. preparation method according to claim 1, it is characterised in that:Step 8)In, the spreading rate of coating fluid is 30%-
45%。
7. reconstituted tobacco prepared by the preparation method of any functional form reconstituted tobaccos of claim 1-6.
8. application of the preparation method of any functional form reconstituted tobaccos of claim 1-6 in reconstituted tobacco is prepared.
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CN113455691A (en) * | 2020-03-31 | 2021-10-01 | 中烟施伟策(云南)再造烟叶有限公司 | Agilawood-containing auxiliary material for cigarettes and tobacco product |
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CN102524932B (en) * | 2010-12-21 | 2013-11-13 | 湖北中烟工业有限责任公司 | Method for applying natural solid flavors and fragrances to papermaking-reconstructed tobacco sheets |
CN102599635B (en) * | 2012-03-10 | 2014-09-10 | 广东中烟工业有限责任公司 | Preparation method of tobacco sheet from cabo and tobacco waste |
CN103519340B (en) * | 2013-10-14 | 2015-05-13 | 安徽中烟工业有限责任公司 | Method for manufacturing cigarette paper making process slices with burley tobacco stems as raw materials |
CN103734897A (en) * | 2013-12-13 | 2014-04-23 | 浙江中烟工业有限责任公司 | Reproduced tobacco leaves adopting discarded tobacco leaf raw material formula and preparing method thereof |
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