CN113455690A - Method for preparing non-tobacco-agilawood type cigarette material by wet papermaking technology - Google Patents
Method for preparing non-tobacco-agilawood type cigarette material by wet papermaking technology Download PDFInfo
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- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
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Abstract
The invention discloses a method for preparing a non-tobacco-agilawood type cigarette material by using a wet papermaking technology, which comprises the following steps: a. selecting agilawood and natural plant fiber as raw materials according to the mass parts of 70-95 parts and 5-30 parts respectively; b. extracting by utilizing an agilawood raw material, and carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; c. pulping and manufacturing the obtained solid-phase substance X and natural plant fibers to obtain a non-tobacco-heavy fragrance type tobacco material sheet base, and concentrating the filtrate Y to obtain a concentrated solution Z; d. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain the non-tobacco-agilawood-type tobacco material. Solves the problem that the non-tobacco-heavy fragrance type cigarette material is prepared by a wet papermaking process without using a formula of a non-tobacco raw material as a main leaf group, such as a processed product of the stem of Chinese eaglewood (shovelling and hooking), natural plant fiber and the like in the prior art.
Description
Technical Field
The invention relates to the technical field of tobacco sheet production by a paper making method (wet method), in particular to a method for preparing a non-tobacco-agilawood type tobacco material by using a wet method paper making technology.
Background
The production process technology of the tobacco sheet (also called reconstituted tobacco) is developed for more than half a century and mainly goes through three stages of a rolling method, a thick pulp method and a paper-making method, and the paper-making method (wet method) production process technology is dominant in the market of China due to strong plasticity and good filling property. Paper-making (wet) tobacco sheet production the main raw material sources are tobacco by-products such as: tobacco fragments, tobacco dust, tobacco stems, cigarette ash, and the like. At present, the tobacco sheets become an indispensable part in Chinese style cigarette leaf group formulas, and the tobacco sheets applied to the cigarette leaf group formulas have the functions of reducing harm and tar, stabilizing product quality, highlighting cigarette style characteristics and the like.
The cigarette paper of the cigarette and the inner cigar sleeve of the machine-made cigar are used as the essential cigarette auxiliary material for designing the cigarette and the machine-made cigar and can be used for wrapping and forming cigarette tobacco shreds (cigar cores of the machine-made cigars). The cigarette paper and the inner cigar sleeve of the machine-made cigar sold in the market of China at present are basically designed, produced and processed by taking different types and proportions of wood pulp, hemp pulp, straw pulp and the like as raw materials.
Internationally, WTO is added in self countries, particularly after the tobacco control framework convention takes effect formally, Chinese tobacco faces more serious challenges, and the domestic tobacco industry faces new normality under new economic environment after continuous high growth. Therefore, the innovation of cigarette design and development is increased by various cigarette industry enterprises in China, new cigarettes are developed in recent years, and no matter the cigarette package design is changed, the appearance of the cigarettes with different flavors and tastes is changed, so that more opportunities are provided for tobacco consumers to select the cigarettes and the mechanism cigars. However, with the increasing demands of tobacco consumers on the safety, functionality and individuality of cigarettes and mechanism cigars, the innovation of tobacco materials is a problem to be solved urgently in high-quality development of the industry. The traditional tobacco sheet takes tobacco byproducts as raw materials, is applied to a cigarette leaf group formula, mainly represents the original tobacco fragrance, and has limited effect of highlighting other fragrance notes; the cigarette paper and the machine-made cigar inner cover which are designed and produced by only taking wood pulp, hemp pulp, straw pulp and the like as raw materials generally have the problems of wood miscellaneous gas or other miscellaneous gas and the like, and have negative influence on sensory quality.
Aquilaria sinensis is the main resource of Chinese eaglewood, and is mainly distributed in Guangdong and Hainan. Is a traditional and rare medicinal material in China, Japan, India and middle east China, and has various pharmacological actions of spasmolysis, asthma relieving, sedation, analgesia, blood pressure reduction, antibiosis and the like. The ancient expression "heavy sandalwood dragon musk" means agilawood, which is listed as the top-class fragrance since ancient times and is always used as high-grade perfume.
In recent years, innovative research on tobacco materials by industrial workers is uninterrupted, and the tobacco sheets prepared from ginkgo leaves, fennel, gynostemma pentaphylla, ginseng, scutellaria baicalensis, platycodon grandiflorum, liquorice, reed rhizome and tobacco byproducts by Zhengchengqian and the like fully retain insoluble effective medicinal components and are coordinated with tobacco fragrance and good in safety; the magnolia flower is added into the tobacco sheet coating liquid in a powder form, such as Zhang wenlong, and the like, so that the effects of covering miscellaneous gases and reducing smoke stimulation are achieved to a certain extent; plum mothers and the like use tea leaves and tea stems as raw materials to manufacture tea leaf sheets for cigarettes, and the influence of the tea leaf sheets on the sensory quality of the cigarettes is researched; chenyinghua invention (patent number: 201210165130.0) combines the powder of agilawood leaf and tobacco component into agilawood tobacco sheet to enrich the tobacco fragrance; the invention relates to a plum noble life invention (patent number: 201310137653. X), which is characterized in that agilawood slices are prepared by adding adhesive and alcoholizing biological agent into agilawood leaf powder and utilizing a thick pulp method; xueshigao et al (patent number: 201310207429.3) discloses a method for preparing agilawood tobacco sheets for cigarette leaf groups by extracting agilawood powder with alcohol, pulping, and mixing with tobacco pulp; the invention of Haiying et al (patent number: 201610252062.0) discloses a method for processing interlayer agilawood reconstituted tobacco by adjusting paper making and forming processes of alcohol extraction, pulping and tobacco pulp of agilawood powder; the invention of Zhougui Yuan et al (patent number: 201610252063.5) discloses a method for preparing reconstituted agilawood tobacco leaves by mixing agilawood powder in a coating liquid and coating with the help of ultrasound assistance. However, the contents of the non-tobacco-aromatic tobacco material prepared by taking non-tobacco raw materials as main leaf group formulas based on the processed product of the stem part of the agilawood (shovelling and shredding), natural plant fibers and the like through a wet papermaking process are not reported.
Disclosure of Invention
The invention aims to provide a method for preparing a non-tobacco-agilawood-type cigarette material by using a wet papermaking technology, which solves the problem that the non-tobacco-agilawood-type cigarette material is prepared by using a wet papermaking technology without using an agilawood stem processing product (shoveling and shredding), natural plant fibers and the like which all use non-tobacco raw materials as a main leaf group formula in the prior art.
In order to solve the technical problems, the invention adopts the following technical scheme:
a method for preparing a non-tobacco-agilawood type cigarette material by using a wet papermaking technology comprises the following steps: a. selecting agilawood and natural plant fiber as raw materials according to the mass parts of 70-95 parts and 5-30 parts respectively; b, extracting by utilizing an agilawood raw material, and performing solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; c. pulping and manufacturing the obtained solid-phase substance X and natural plant fibers to obtain a non-tobacco-heavy fragrance type tobacco material sheet base, and concentrating the filtrate Y to obtain a concentrated solution Z; d. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain the non-tobacco-agilawood-type tobacco material.
After the non-tobacco-agilawood type tobacco material is obtained, different treatment processes are adopted according to different final application targets of the tobacco material, for example, the application targets are cigarette paper of cigarettes and inner eggplant sleeves of machine-made cigars, and the tobacco material can be further subjected to calendaring, slitting and rewinding treatment in a production process link according to the actual requirements of the application targets; the calendering refers to calendering the tobacco material by a calender under a certain rolling condition so as to change the physical properties of the tobacco material, such as smoothness, air permeability and the like, and it needs to be stated that not all the tobacco materials need to be calendered, which depends on the product design requirements; the cutting-rewinding refers to that in the production process link, a cutting-rewinding machine is utilized to cut and rewind a mother roll of the cigarette material according to the design requirement so as to obtain the cigarette paper of the cigarette and the required width of the inner cigar sleeve of the machine-made cigar;
compared with the prior art, the process flow disclosed in the application does not need to add other production process equipment, the method is simple and efficient, the implementation is easy, the additional production and manufacturing cost is not increased basically, and the non-tobacco-heavy fragrance type sheet and the auxiliary materials are prepared according to the adjustment of the raw material formula, the process parameters, the coating liquid formula and the like. The non-tobacco-agilawood type sheet can be applied to a cigarette tobacco leaf composition formula to partially or completely replace the traditional tobacco sheet; the auxiliary material of 'non-tobacco-agilawood' type can be applied to cigarettes and machine-made cigars to replace cigarette paper of the traditional cigarettes and inner cigar sleeves of the machine-made cigars. Compared with the traditional tobacco sheet using tobacco as raw material, and the cigarette paper and the machine-made cigar inner eggplant sleeve which only use plant fiber as raw material, the invention selects the tobacco material prepared by non-tobacco raw materials such as agilawood and natural plant fiber, etc., thereby enlarging the application range of the agilawood and improving the economic value of the agilawood; the cigarette additive is applied to cigarette products, and has the function of improving the sensory quality of cigarettes: for example, the aroma of the cigarette product such as agilawood, costustoot and honey is increased, the aroma of the tobacco is enriched, bad miscellaneous gas is covered, the sensory stimulation is reduced, and the like, thereby providing a material basis for the diversified and personalized development of Chinese style cigarettes and comprehensively improving the competitiveness of the Chinese tobacco market.
As a further preferred aspect of the present invention, the agilawood raw material in step a is any one or a combination of shoveling and shredding stems of aquilaria sinensis belonging to the family of reshorridae; and a, selecting agilawood raw materials, preprocessing agilawood, wherein the preprocessing of agilawood comprises the steps of identifying the agilawood raw materials by naked eyes manually, removing foreign matters, pathological changes and mildewed parts, and drying the agilawood raw materials by using an oven at 40 ℃ until the water content is 9-12%.
The shoveling and crushing refers to the crushed material of the Chinese eaglewood bark which is shoveled off by the roughly processed Chinese eaglewood pieces, and the oil and fat content is less; the thread hooking is the crushed material hooked by the fine-processing eaglewood blocks, is closer to the agilawood core material than shoveled and crushed, and contains a small amount of grease.
As a further preferred aspect of the present invention, the natural plant fiber in step a is any one of softwood pulp, hardwood pulp, hemp pulp, straw pulp and cotton pulp or a combination thereof.
As a further preferred aspect of the present invention, the extraction step in step b is: mixing lignum Aquilariae Resinatum raw material and water at a weight ratio of 1:5-20, extracting at 50-90 deg.C for 1-5 hr, and performing solid-liquid separation to obtain solid phase X and filtrate Y.
As a further preferred aspect of the present invention, the pulping in the pulping and papermaking process in the step c can be realized by any one of the following manners: mixing the solid-phase substance X and natural plant fibers according to the absolute dry part ratio of 70-95: 5-30, and pulping together; secondly, independently pulping the solid-phase substance X, adding the independently pulped natural plant fibers according to the proportion, and fully mixing; the paper making process is to make paper with dynamic or static paper former.
As a further optimization of the invention, when the application target of the manufactured tobacco material is to replace the traditional tobacco sheet, the beating degree of the pulp is 30-65 SR during the pulping; when the application target of the manufactured cigarette material is to replace cigarette paper of the traditional cigarette and an inner eggplant sleeve of a machine-made cigar, the pulp beating degree is 60-95 SR degrees during pulping.
As a further preference of the invention, when the application of the prepared smoking material is aimed at replacing the conventional tobacco sheet, the absolute dry basis weight of the sheet of the "non-tobacco-agilawood type" sheet in step c is 35g/m2～80g/m2When the application target of the prepared tobacco material is to replace the cigarette paper of the traditional cigarette and the inner eggplant sleeve of the machine-made cigar, the absolute dry basis weight of the base of the auxiliary material of the non-tobacco-agilawood type in the step c is 20g/m2～45g/m2。
In a further preferred embodiment of the present invention, the filtrate Y is concentrated in step c under reduced pressure using a rotary evaporator.
In a further preferred embodiment of the present invention, the coating liquid mixed with the concentrated solution Z in the step d is obtained by adding any one or a combination of propylene glycol, glycerol and an agilawood extract having an agilawood characteristic to the concentrated solution Z, which have a moisturizing effect, and sufficiently mixing the mixture.
And fully mixing to obtain a coating liquid, wherein the solid content percentage of each material in the coating liquid is as follows:
| kind of material | Percent of solid content |
| Concentrate Z | 5%—40% |
| Propylene glycol | 0.01%—5% |
| Glycerol | 0.01%—5% |
| Agilawood extract | 0.0001%—5% |
As a further preference of the present invention, the drying temperature in the step d is 100-120 ℃.
Compared with the prior art, the invention can at least achieve one of the following beneficial effects:
1. the adjustment of the raw material formula, the coating liquid formula and the process parameters meets the physical performance requirements of machining the non-tobacco-heavy fragrance type sheet and the auxiliary materials when producing cigarettes or machine-made cigars, and simultaneously obtains better sensory experience when smoking.
2. The application range of the agilawood is expanded, and the economic value of the agilawood is improved.
3. Provides a material basis for the diversified and personalized development of Chinese cigarettes and comprehensively improves the competitiveness of the Chinese tobacco market.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the present invention is further described in detail with reference to the following embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the invention and are not intended to limit the invention.
Specific example 1:
a method for preparing a non-tobacco-agilawood type cigarette material by using a wet papermaking technology comprises the following steps: a. selecting agilawood and natural plant fiber as raw materials according to the mass parts of 70-95 parts and 5-30 parts respectively; b, extracting by utilizing an agilawood raw material, and performing solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; c. pulping and manufacturing the obtained solid-phase substance X and natural plant fibers to obtain a non-tobacco-heavy fragrance type tobacco material sheet base, and concentrating the filtrate Y to obtain a concentrated solution Z; d. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain the non-tobacco-agilawood-type tobacco material.
Specific example 2:
this example further illustrates, on the basis of specific example 1, a method for preparing a "non-tobacco-agilawood" smoking material by using a wet papermaking technique, including the steps of: a. selecting agilawood and wood pulp as raw materials according to 85 parts and 15 parts by weight, and pretreating agilawood when the agilawood raw materials are selected, wherein the pretreatment of the agilawood comprises the steps of identifying the agilawood raw materials by naked eyes manually, removing foreign matters, pathological changes and mildewed parts, and drying the agilawood raw materials by using an oven at 40 ℃ until the water content is 9%; b. extracting with agilawood raw material, mixing the agilawood raw material and water according to a weight ratio of 1:5 during extraction, extracting for 1h at 50 ℃, and then carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; c. is prepared from the obtained solid substance X and natural plant fiberMaking pulp to obtain 'non-tobacco-heavy fragrance type' tobacco material sheet base, wherein the pulp beating degree is 30 DEG SR during pulping, and the absolute dry basis weight of the sheet base formed by making the pulp is 35g/m2Simultaneously, concentrating the filtrate Y to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain a non-tobacco-agilawood-type tobacco material, wherein the coating liquid mixed with the concentrated solution Z contains the following materials in percentage by solid content: mixing concentrate Z5%, propylene glycol 0.01%, glycerol 0.01%, and lignum Aquilariae Resinatum extract 0.0001% to obtain coating solution; the drying temperature in step e is 100 ℃.
Specific example 3:
this example further illustrates, on the basis of specific example 1, a method for preparing a "non-tobacco-agilawood" smoking material by using a wet papermaking technique, including the steps of: a. selecting agilawood and wood pulp as raw materials according to 85 parts and 15 parts by mass respectively, and pretreating agilawood when the agilawood raw materials are selected, wherein the pretreatment of the agilawood comprises the steps of removing foreign matters, pathological changes and mildewed parts of the agilawood raw materials after the agilawood raw materials are identified by human eyes, and drying the agilawood raw materials by using an oven at 40 ℃ until the water content is 12%; b. extracting by utilizing an agilawood raw material, mixing the agilawood raw material and water according to a weight ratio of 1:20 during extraction, extracting for 5 hours at 90 ℃, and then carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; c. pulping the obtained solid substance X and natural plant fiber to obtain 'non-tobacco-heavy fragrance type' tobacco material sheet base, wherein the pulping degree of the pulp is 65 DEG SR during pulping, and the absolute dry basis weight of the sheet base molded by paper making is 80g/m2Simultaneously, concentrating the filtrate Y to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain a non-tobacco-agilawood-type tobacco material, wherein the solid content percentage of each material in the coating liquid mixed with the concentrated solution Z is as follows: mixing the concentrated solution Z40%, propylene glycol 5%, glycerol 5%, and lignum Aquilariae Resinatum extract 5% to obtain coating solution; the drying temperature in step e was 120 ℃.
Specific example 4:
this example is the basis for specific example 1The preparation method of the non-tobacco-agilawood type cigarette material by using the wet papermaking technology is further explained, and comprises the following steps: a. selecting agilawood and wood pulp as raw materials according to 85 parts and 15 parts by mass respectively, and pretreating agilawood when the agilawood raw materials are selected, wherein the pretreatment of the agilawood comprises the steps of removing foreign matters, pathological changes and mildewed parts of the agilawood raw materials after the agilawood raw materials are identified by human eyes, and drying the agilawood raw materials by using an oven at 40 ℃ until the moisture content is 10%; b. extracting with agilawood raw material, mixing the agilawood raw material and water according to a weight ratio of 1:15 during extraction, extracting for 2.5h at 65 ℃, and then carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; c. pulping the obtained solid substance X and natural plant fiber to obtain 'non-tobacco-heavy fragrance type' tobacco material sheet base, wherein the pulping degree of the pulp is 50 DEG SR during pulping, and the absolute dry weight of the sheet base molded by paper making is 45g/m2Simultaneously, concentrating the filtrate Y to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain a non-tobacco-agilawood-type tobacco material, wherein the solid content percentage of each material in the coating liquid mixed with the concentrated solution Z is as follows: 25% of concentrated solution Z, 2.5% of propylene glycol, 2.5% of glycerol and 2.5% of agilawood extract are mixed to prepare a coating liquid; the drying temperature in step e was 115 ℃.
The non-tobacco-agilawood type slices obtained in examples 2 to 4 were cut into shreds by a shredder, and the shreds were rolled into the same blank tobacco tube, and sensory quality was judged by professional smokers, and the comprehensive sensory quality ranking was: example 4 is superior to example 3 and to example 2.
On the basis of example 4, the influence of the raw material ratio on the sensory quality of the non-tobacco-agilawood type sheet is studied, and comparative examples 1 to 3 are different from example 4 only in the raw material ratio, which is detailed in table 1:
TABLE 1 Effect of raw material formulation on the sensory quality of non-tobacco-eaglewood type sheets
| Kind of raw material | Comparative example 1 | Comparative example 2 | Example 4 | Comparative example 3 |
| Agilawood | 70% | 80% | 85% | 95% |
| Natural plant fiber | 30% | 20% | 15% | 5% |
| Sensory quality evaluation | Slightly apparent agilawood style characteristics Now is lignum Aquilariae Resinatum, baked incense and sweet Fragrant, woody and obvious smell, nasal cavity A burning sensation and dry throat Stings, mouth stings and coating sensation | The style and the characteristics of the agilawood are more obvious, is prepared from eaglewood, baked fragrant and honey Sweet and fragrant, woody and smelly, nasal Obvious stimulation to the cavity and throat and mouth The cavity has a coating feel | The style and the characteristics of the agilawood are more obvious, is prepared from eaglewood, baked incense, Sweet fragrance and nasal irritation Obviously, the mouth cavity has a cool back Fluid-producing feeling, slight coating | The style and characteristics of Chinese eaglewood are more obvious Now containing agilawood, roasted incense, costustoot, The fragrance of the honey is that the honey is sweet,fine and soft texture And, the nasal cavity shows slight burr and mouth Has clean cavity and cooling effect jin-gan-Gao (jin-gan-Gao-san) |
As shown in the table above, sensory quality determination was performed by ranking method, and the overall quality ranking was: comparative example 3 > example 4 > comparative example 2 > comparative example 1.
According to sensory quality judgment, through the adjustment of the raw material proportion, along with the improvement of the proportion of the agilawood raw material in the integral formula of the non-tobacco-heavy fragrance type sheet, the style and the characteristics of the agilawood are enhanced, the aroma richness and the smoke texture are improved, the stimulation to the mouth, the nose and the throat is reduced, and the comfort is obviously improved.
Specific example 5:
this example further illustrates, on the basis of specific example 1, a method for preparing a "non-tobacco-agilawood" smoking material by using a wet papermaking technique, including the steps of: a. selecting 40 parts, 10 parts and 10 parts of agilawood by weight, hooking filaments of agilawood, shoveling and crushing agilawood, broad-leaf wood pulp and softwood pulp as raw materials, and pretreating agilawood when selecting the agilawood raw materials, wherein the pretreatment of agilawood comprises the steps of removing foreign matters, pathological changes and mildewed parts of the agilawood raw materials after the agilawood raw materials are identified by naked eyes manually, and drying the agilawood raw materials by using an oven at 40 ℃ until the moisture is 10%; b. extracting by utilizing an agilawood raw material, mixing the agilawood raw material and water according to a weight ratio of 1:13 during extraction, extracting for 2 hours at 55 ℃, and then carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; c. pulping the obtained solid substance X and natural plant fiber to obtain 'non-tobacco-heavy fragrance type' tobacco material sheet base, wherein the pulping degree of the pulp is 55 DEG SR during pulping, and the absolute dry weight of the sheet base molded by paper making is 50g/m 2Simultaneously, concentrating the filtrate Y to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain the non-tobacco-agilawood-type tobacco material, wherein the drying temperature is 120 ℃, and the solid content percentages of all materials in the coating liquid mixed with the concentrated solution Z are respectively configured according to the table 2.
Comparative examples 4 to 7 in table 2 differ only in the composition of the coating liquid, and the "non-tobacco-agilawood-type" sheets obtained in comparative examples 4 to 7 were cut into pieces by a shredder and wrapped in the same blank tobacco tube, and subjected to sensory quality judgment by a professional inspector to study the influence of the composition of the coating liquid on the sensory quality of the "non-tobacco-agilawood-type" sheets.
TABLE 2 Effect of coating liquid composition on the sensory quality of "non-tobacco-eaglewood-type" sheets
| Coating liquid component | Comparative example 4 | Comparative example 5 | Comparative example 6 | Comparative example 7 |
| Concentrate Z | — | 20% | — | 20% |
| Propylene glycol | — | — | 1.5% | 1.5% |
| Glycerol | — | — | 1.5% | 1.5% |
| Agilawood extract | — | — | 1.5% | 1.5% |
| Sensory quality assessment Price of | Style characteristics of lignum Aquilariae Resinatum Weak, the wood gas is obvious, stimulation of nasal cavity and throat Obvious burning sensation The strong, stinging mouth, residue is remained | The style and the characteristics of the agilawood are better It is shown that the Chinese eaglewood is contained, The roasted fragrance and the honey sweet fragrance are obtained, woody air display, nasal hair Stabbing, slight burning and burning mouth Residual in the cavity, cool and promote the secretion of saliva | Agilawood style characteristic tip It is shown that the Chinese eaglewood is contained, Roasted incense with woody smell Clear, dry throat of nasal cavity Thorns, oral coatings and residues Leave behind | Style characteristics of lignum Aquilariae Resinatum More pronounced, it is manifested as sinking Incense, roasted incense, aucklandia root, Sweet and fragrant honey Abundant, slightly obvious nasal cavity Burr and cooling of the mouth Promoting the secretion of saliva |
As shown in the table above, sensory quality determination was performed by ranking method, and the overall quality ranking was: comparative example 7 > comparative example 5 > comparative example 6 > comparative example 4.
The sensory quality judgment shows that the adjustment of the components of the coating liquid has influence on the sensory quality of the non-tobacco-heavy fragrance type sheet, and compared with the comparative example 4, the increase of the concentrated solution Z or the increase of the humectant and the agilawood extract in a certain range has different contributions to the improvement of the sensory quality.
Specific example 6:
this embodiment is described in detail1, the preparation method of the non-tobacco-agilawood type tobacco material by using the wet papermaking technology is further explained, and comprises the following steps: a. selecting agilawood and wood pulp as raw materials according to 70 parts and 30 parts by mass, and pretreating agilawood when the agilawood raw materials are selected, wherein the pretreatment of the agilawood comprises the steps of removing foreign matters, pathological changes and mildewed parts of the agilawood raw materials after the agilawood raw materials are identified by human eyes, and drying the agilawood raw materials by using an oven at 40 ℃ until the moisture content is 10%; b. extracting with agilawood raw material, mixing the agilawood raw material and water according to a weight ratio of 1:5 during extraction, extracting for 1h at 50 ℃, and then carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; c. pulping the obtained solid substance X and natural plant fiber to obtain 'non-tobacco-heavy fragrance type' tobacco material sheet base, wherein the pulping degree of the pulp is 60 DEG SR during pulping, and the absolute dry basis weight of the sheet base molded by paper making is 20g/m 2Simultaneously, concentrating the filtrate Y to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain a non-tobacco-agilawood-type tobacco material, wherein the coating liquid mixed with the concentrated solution Z contains the following materials in percentage by solid content: mixing concentrate Z5%, propylene glycol 0.01%, glycerol 0.01%, and lignum Aquilariae Resinatum extract 0.0001% to obtain coating solution; the drying temperature in step e is 100 ℃.
Specific example 7:
this example further illustrates, on the basis of specific example 1, a method for preparing a "non-tobacco-agilawood" smoking material by using a wet papermaking technique, including the steps of: a. selecting agilawood and wood pulp as raw materials according to 70 parts and 30 parts by mass, and pretreating agilawood when the agilawood raw materials are selected, wherein the pretreatment of the agilawood comprises the steps of removing foreign matters, pathological changes and mildewed parts of the agilawood raw materials after the agilawood raw materials are identified by human eyes, and drying the agilawood raw materials by using an oven at 40 ℃ until the moisture content is 10%; b. extracting by utilizing an agilawood raw material, mixing the agilawood raw material and water according to a weight ratio of 1:20 during extraction, extracting for 5 hours at 90 ℃, and then carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; c. pulping and papermaking by using the obtained solid-phase substance X and natural plant fiber To the tobacco material base of 'non-tobacco-heavy fragrance type', the beating degree of the pulp is 95 DEG SR in the pulping process, and the absolute dry weight of the base molded by paper making is 45g/m2Simultaneously, concentrating the filtrate Y to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain a non-tobacco-agilawood-type tobacco material, wherein the coating liquid mixed with the concentrated solution Z contains the following materials in percentage by solid content: mixing the concentrated solution Z40%, propylene glycol 5%, glycerol 5%, and lignum Aquilariae Resinatum extract 5% to obtain coating solution; the drying temperature in step e was 120 ℃.
Specific example 8:
this example further illustrates, on the basis of specific example 1, a method for preparing a "non-tobacco-agilawood" smoking material by using a wet papermaking technique, including the steps of: a. selecting agilawood and wood pulp as raw materials according to 70 parts and 30 parts by mass, and pretreating agilawood when the agilawood raw materials are selected, wherein the pretreatment of the agilawood comprises the steps of removing foreign matters, pathological changes and mildewed parts of the agilawood raw materials after the agilawood raw materials are identified by human eyes, and drying the agilawood raw materials by using an oven at 40 ℃ until the moisture content is 10%; b. extracting by utilizing an agilawood raw material, mixing the agilawood raw material and water according to a weight ratio of 1:13 during extraction, extracting for 3 hours at the temperature of 60 ℃, and then carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; c. pulping the obtained solid substance X and natural plant fiber to obtain 'non-tobacco-heavy fragrance type' tobacco material sheet base, wherein the pulping degree of the pulp is 80 DEG SR during pulping, and the absolute dry weight of the sheet base molded by paper making is 35g/m 2Simultaneously, concentrating the filtrate Y to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain a non-tobacco-agilawood-type tobacco material, wherein the coating liquid mixed with the concentrated solution Z contains the following materials in percentage by solid content: 23% of concentrated solution Z, 2% of propylene glycol, 2.5% of glycerol and 2.5% of agilawood extract are mixed to prepare a coating liquid; the drying temperature in step e was 116 ℃.
The auxiliary materials of the non-tobacco-agilawood type obtained in the examples 6 to 8 are used for replacing cigarette paper of cigarettes or inner cigar sleeves of machine-made cigars to be rolled and formed into samples, and after the samples are prepared, professional smoke panel evaluators judge the sensory quality, wherein the comprehensive sensory quality sequence is as follows: example 8 is superior to example 7 and example 6, the comprehensive sensory quality of example 6 is the worst, and example 7 shows that the auxiliary materials are easy to absorb water and generate surface sticky phenomenon during sample preparation due to the fact that the humectant and the agilawood extract are used in a high proportion.
On the basis of example 8, the auxiliary materials of the comparative examples 8-10, namely the non-tobacco and agilawood type, are prepared, and are rolled and molded to prepare samples for replacing cigarette paper of cigarettes or inner cigar sleeves of machine-made cigars, so that the influence of different raw material ratios on the sensory quality and the rolling molding of the sample preparation samples of the auxiliary materials of the non-tobacco and agilawood type is researched, and sensory quality judgment is carried out by professional smokers after the samples are prepared, and the details are shown in table 3.
TABLE 3 influence of different raw material ratios on sensory quality and roll forming of "non-tobacco-eaglewood type" auxiliary material sample preparation samples
| Kind of raw material | Example 8 | Comparative example 8 | Comparative example 9 | Comparative example 10 |
| Agilawood | 70% | 80% | 85% | 95% |
| Natural plant fiber | 30% | 20% | 15% | 5% |
| Sensory quality evaluation | The style characteristics of the agilawood are slightly obvious, it is expressed as dry grass fragrant and heavy Fragrant, roasted fragrant and sweet-scented with honey, slight wood-like qi manifesting slightly in the nasal cavity Has obvious scorching and moist mouthfeel Sweet with slight stings | The style and the characteristics of the agilawood are better Obviously showing the fragrance of the dried grass, Agilawood, costustoot, roasted incense, Sweet and fragrant, slight nasal cavity Has burr and good taste Moist, sweet and slight stings | The style and the characteristics of the agilawood are more obvious, is expressed by dried grass incense, agilawood, Roasted incense, aucklandia root and sweet incense Rich charm and charm, fine texture Gentle, slight irritation of nasal cavity Clear cavity, cool back and promote the production of body fluid | Physical properties of paper are better Poor in the property of being difficult to be formed into paper, sensory quality evaluation was not conducted Price of |
| Roll forming | The paper has good tensile property and capacity Easy rolling system | The tensile property of the paper is good, easy to roll | The tensile property of the paper is better, easy to roll | No good paper was obtained Open, unfinished roll |
As shown in the table above, the main influence of the raw material ratio on the non-tobacco-heavy flavor type auxiliary materials comprises the sensory quality and the rolling forming process. Excluding comparative example 10 which could not be rolled, and performing sensory quality determination by a ranking method, wherein the comprehensive quality ranking is as follows: comparative example 9 > comparative example 8 > example 8.
The sensory quality judgment shows that the raw material proportion is adjusted, the sensory quality of cigarette paper based on the non-tobacco-agilawood auxiliary material for replacing cigarettes or a sample formed by rolling an inner eggplant sleeve of a machine-made cigar is influenced, the main expression is that along with the improvement of the proportion of the agilawood raw material in the integral formula of the non-tobacco-agilawood auxiliary material, the agilawood style characteristic of the sample is enhanced, and the richness of the aroma, the smoke texture and the comfort of the mouth, the nose and the throat are improved.
Specific example 9:
this example further illustrates, on the basis of specific example 1, a method for preparing a "non-tobacco-agilawood" smoking material by using a wet papermaking technique, including the steps of: a. selecting 45 parts, 35 parts, 7 parts and 6 parts of hooked thread, shoveled and crushed eaglewood, broad-leaved wood pulp, softwood pulp and hemp pulp as raw materials according to the mass parts, and pretreating the eaglewood when selecting the raw materials of the eaglewood, wherein the pretreatment of the eaglewood comprises the steps of removing foreign matters, pathological changes and mildewing parts of the raw materials of the eaglewood after the raw materials of the eaglewood are identified by naked eyes manually, and drying the raw materials of the eaglewood in an oven at 40 ℃ until the water content is 10%; b. extracting with agilawood raw material, mixing the agilawood raw material and water according to a weight ratio of 1:15 during extraction, extracting for 3.5h at 65 ℃, and then carrying out solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; c. pulping and manufacturing the obtained solid-phase substance X and natural plant fibers to obtain a non-tobacco-heavy fragrance type tobacco material sheet base, wherein the pulping degree of pulp is 85 DEG SR during pulping, the sheet base is manufactured and molded according to the absolute dry ration shown in the table 4, and meanwhile, the filtrate Y is concentrated to obtain a concentrated solution Z; e. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain a non-tobacco-agilawood-type tobacco material, wherein the coating liquid mixed with the concentrated solution Z contains the following materials in percentage by solid content: mixing the concentrated solution Z20%, propylene glycol 3%, glycerol 3%, and lignum Aquilariae Resinatum extract 3% to obtain coating solution; the drying temperature in step e was 117 ℃.
Comparative examples 11 to 14 in table 4 are different only in the quantitative absolute dry basis of the sheet, the auxiliary materials of the "non-tobacco-agilawood type" obtained in comparative examples 11 to 14 are used for replacing cigarette paper of cigarettes or inner cigar sleeve rolling and forming samples of machine-made cigars, the quantitative absolute dry basis of different sheet bases is studied, the influence on the sensory quality and the rolling and forming of the samples of the auxiliary materials of the "non-tobacco-agilawood type" is studied, and sensory quality judgment is carried out by professional smokers after sample preparation.
TABLE 4 influence of different base absolute dry quantities on sensory quality and roll forming of "non-tobacco-eaglewood type" auxiliary material sample preparation
| Base of film | Comparative example 11 | Comparative example 12 | Comparative example 13 | Comparative example 14 |
| Absolute dry basis weight (g/m)2） | 20 | 30 | 40 | 45 |
| Sensory quality evaluation | Physical property of paper Poor and difficult performance Is made by paper making Type I, do not proceed Sensory quality assessment Price of | Style characteristics of lignum Aquilariae Resinatum More obviously, it is dry Baking grass scent, eaglewood Sweet and fragrant smell, aucklandia root and honey Fragrant and slightly pronounced nasal cavity Burr and cooling of the mouth Promoting the secretion of saliva or body fluid, with a slight coating | The style and the characteristics of the agilawood are better Apparently, it is represented as hay Incense, agilawood, roasted incense, The costustoot and the honey are sweet and fragrant, slightly coarse texture and mouth feeling Cavity fluid production accompanied with coating Feeling of | The style and the characteristics of the agilawood are better Apparently, it is represented as hay Incense, agilawood, roasted incense, The costustoot and the honey are sweet and fragrant, coarse texture and oral cavity Generation of body fluid with residues, Coating layer |
| Roll forming | Are not better obtained Paper of (2) Finish rolling | Tensile properties of paper Better and easy to roll | Tensile properties of paper Is easy to be rolled | Tensile properties of paper Good, but quantitative, same as Easy sample application amount 'cracking' and sample preparation The probability of failure is higher |
As shown in the table above, the main influence of the absolutely dry basis weight of the sheet on the non-tobacco-heavy flavor type auxiliary material comprises the sensory quality and the rolling forming process. The roll forming of the sample is influenced by the excessively low and high absolute dry quantity of the sheet base; excluding comparative example 11 which could not be rolled, and performing sensory quality determination by a ranking method, wherein the comprehensive quality ranking is as follows: comparative example 12 > comparative example 13 > comparative example 14;
according to sensory quality judgment, the absolute dry quantity of the tablet base is adjusted, and the sensory quality of cigarette paper of a cigarette or an inner cigar sleeve rolling forming sample of a machine-made cigar which is based on a non-tobacco-agilawood auxiliary material for replacing cigarettes is influenced, and the sensory quality is mainly expressed in the aspects of smoke texture and sensory comfort.
Although the invention has been described herein with reference to a number of illustrative embodiments thereof, it should be understood that numerous other modifications and embodiments can be devised by those skilled in the art that will fall within the spirit and scope of the principles of this disclosure. More specifically, various variations and modifications are possible in the component parts and/or arrangements of the subject combination arrangement within the scope of the disclosure and claims of this application. In addition to variations and modifications in the component parts and/or arrangements, other uses will also be apparent to those skilled in the art.
Claims (10)
1. A method for preparing a non-tobacco-agilawood type cigarette material by using a wet papermaking technology is characterized by comprising the following steps: the method comprises the following steps: a. selecting agilawood and natural plant fiber as raw materials according to the mass parts of 70-95 parts and 5-30 parts respectively; b, extracting by utilizing an agilawood raw material, and performing solid-liquid separation to obtain a solid-phase substance X and a filtrate Y; c. pulping and manufacturing the obtained solid-phase substance X and natural plant fibers to obtain a non-tobacco-heavy fragrance type tobacco material sheet base, and concentrating the filtrate Y to obtain a concentrated solution Z; d. and finally, coating the coating liquid mixed with the concentrated solution Z on a non-tobacco-agilawood-type tobacco material sheet base, and drying to obtain the non-tobacco-agilawood-type tobacco material.
2. The method for preparing a non-tobacco-agilawood-type tobacco material by using a wet papermaking technology according to claim 1, wherein the method comprises the following steps: the agilawood raw material in the step a is any one or a combination of shoveling and hooking stems of aquilaria sinensis of the Thymelaeaceae family; and a, selecting agilawood raw materials, preprocessing agilawood, wherein the preprocessing of agilawood comprises the steps of identifying the agilawood raw materials by naked eyes manually, removing foreign matters, pathological changes and mildewed parts, and drying the agilawood raw materials by using an oven at 40 ℃ until the water content is 9-12%.
3. The method for preparing a non-tobacco-agilawood-type tobacco material by using a wet papermaking technology according to claim 1, wherein the method comprises the following steps: the natural plant fiber in the step a is any one or combination of softwood pulp, hardwood pulp, hemp pulp, straw pulp and cotton pulp.
4. The method for preparing a non-tobacco-agilawood-type tobacco material by using a wet papermaking technology according to claim 1, wherein the method comprises the following steps: the extraction step in the step b is as follows: mixing lignum Aquilariae Resinatum raw material and water at a weight ratio of 1:5-20, extracting at 50-90 deg.C for 1-5 hr, and performing solid-liquid separation to obtain solid phase X and filtrate Y.
5. The method for preparing a non-tobacco-agilawood-type tobacco material by using a wet papermaking technology according to claim 1, wherein the method comprises the following steps: the pulping in the pulping and papermaking process in the step c can be realized by any one of the following modes: mixing the solid-phase substance X and natural plant fibers according to the absolute dry part ratio of 70-95: 5-30, and pulping together; secondly, independently pulping the solid-phase substance X, adding the independently pulped natural plant fibers according to the proportion, and fully mixing; the paper making process is to make paper with dynamic or static paper former.
6. The method for preparing a non-tobacco-agilawood-type tobacco material by using a wet papermaking technology as claimed in claim 5, wherein the method comprises the following steps: when the application target of the manufactured tobacco material is to replace the traditional tobacco sheet, the beating degree of the pulp is 30-65 SR degrees during pulping; when the application target of the manufactured cigarette material is to replace cigarette paper of the traditional cigarette and an inner cigar sleeve of a machine-made cigar, the beating degree of the pulp is 60-95 SR degrees during pulping.
7. The method for preparing a non-tobacco-agilawood-type tobacco material by using a wet papermaking technology according to claim 1, wherein the method comprises the following steps: when the application target of the prepared tobacco material is to replace the traditional tobacco sheet, the absolute dry basis weight of the sheet of the non-tobacco-agilawood sheet in the step c is 35g/m2～80g/m2When the application target of the prepared tobacco material is to replace the cigarette paper of the traditional cigarette and the inner eggplant sleeve of the machine-made cigar, the absolute dry basis weight of the base sheet of the auxiliary material of the non-tobacco-agilawood type in the step c is 20g/m2～45g/m2。
8. The method for preparing a non-tobacco-agilawood-type tobacco material by using a wet papermaking technology according to claim 1, wherein the method comprises the following steps: and c, concentrating the filtrate Y in the step c by adopting a rotary evaporator for reduced pressure concentration.
9. The method for preparing a non-tobacco-agilawood-type tobacco material by using a wet papermaking technology according to claim 1, wherein the method comprises the following steps: the coating liquid mixed with the concentrated solution Z in the step d is obtained by adding any one or combination of propylene glycol, glycerol and agilawood extract with an agilawood characteristic with a moisturizing effect into the concentrated solution Z and fully mixing.
10. The method for preparing a non-tobacco-agilawood-type tobacco material by using a wet papermaking technology according to claim 1, wherein the method comprises the following steps: the drying temperature in the step d is 100-120 ℃.
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| CN114960271A (en) * | 2022-05-31 | 2022-08-30 | 云南中烟工业有限责任公司 | Preparation and application of cigar curing sheet with prominent berry, soil and pepper flavors |
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| CN114960271A (en) * | 2022-05-31 | 2022-08-30 | 云南中烟工业有限责任公司 | Preparation and application of cigar curing sheet with prominent berry, soil and pepper flavors |
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