CN103783651A - Application of supercritically-extracted aquilaria sinensis in tobacco reproduction technology with paper making method - Google Patents

Application of supercritically-extracted aquilaria sinensis in tobacco reproduction technology with paper making method Download PDF

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CN103783651A
CN103783651A CN201410031103.4A CN201410031103A CN103783651A CN 103783651 A CN103783651 A CN 103783651A CN 201410031103 A CN201410031103 A CN 201410031103A CN 103783651 A CN103783651 A CN 103783651A
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aquilaria sinensis
tobacco
suspension culture
papermaking
extracted
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CN103783651B (en
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薛冬
金岚峰
张合川
袁益来
陈晶波
徐如彦
蔡文高
朱亚峰
眭凯
刘玉坤
窦昆鹏
袁广翔
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JIANGSU XINYUAN TOBACCO SHEET CO Ltd
China Tobacco Jiangsu Industrial Co Ltd
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JIANGSU XINYUAN TOBACCO SHEET CO Ltd
China Tobacco Jiangsu Industrial Co Ltd
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Abstract

The invention discloses the application of supercritically-extracted aquilaria sinensis in the tobacco remanufacturing technology with the paper making method. The specific preparation technology comprises the first step of extraction, wherein tobacco raw materials are mixed and added with water to be extracted; the second step of separation, wherein after extraction is finished, extracted liquid and solid raw material residues are obtained through solid-liquid separation; the third step of aquilaria sinensis supercritical extraction, wherein dried and meshed aquilaria sinensis is extracted through the supercritical carbon dioxide fluid to obtain extracts and residues, the obtained extracts are dispersed by absolute ethyl alcohol and then blended into the extracted liquid obtained in the second step, the mixture is concentrated to manufacture coating liquid, the obtained residues are blended into the solid raw material residues obtained in the second step, mixing and pulping are conducted, and tobacco piece bases are manufactured through the paper manufacturing technology with pulp; the fourth step of coating, wherein the tobacco piece bases are coated with the coating liquid, and remanufactured tobacco products are manufactured through drying and cutting. The preparation technology is simple, the cost is low, limited aquilaria sinensis resources are effectively utilized, and the sensory quality of aquilaria sinensis cigarettes is improved.

Description

A kind of supercritical extract suspension culture of Aquilaria sinensis is in the application of producing in papermaking-method reconstituted tobaccos technique
Technical field
The present invention relates to a kind of technique of papermaking-method reconstituted tobaccos, be specifically related to a kind of supercritical extract suspension culture of Aquilaria sinensis in the application of producing in papermaking-method reconstituted tobaccos technique, belong to reconstituted tobacco technical field.
Background technology
Papermaking-method reconstituted tobaccos technology is take offal, tobacco leaf fragment, offal etc. as raw material, use paper technology processing to make the product with tobacco suction taste, papermaking-method reconstituted tobaccos, owing to having resistance to good processability, falling the features such as burnt effect is remarkable, product quality plasticity is strong, has obtained using widely at tobacco business.Suspension culture of Aquilaria sinensis is the famous and precious Chinese medicinal herbs of tradition, the needed by human biological element amount containing is extremely abundant, it is the important foundation that keeps human normal vital movement, and the elimination of multiple disadvantage factor in body is benefited, mainly can be used for catharsis and toxin expelling, help sleep, hypoglycemic, lipopenicillinase, beneficial gas benefit essence, the ventilation of invigorating blood circulation, adjusting endocrine, anti-disease, anti-aging always, build up health etc.It is elegant in smell, long that suspension culture of Aquilaria sinensis burning produces, and having sets aside all worries allays excitement, promoting the circulation of qi is had one's ideas straightened out, magical effect of restoring consciouness benefit body.Existing suspension culture of Aquilaria sinensis is inhaled the cigarette product listing of taste in the market, market reaction is good, but in prior art, just in pipe tobacco process, sprays the herbal mediciments such as some suspension culture of Aquilaria sinensis, addition limits because of technology for making tobacco threds, and it is poor that prepared suspension culture of Aquilaria sinensis is inhaled the organoleptic quality of cigarette product of taste.
Summary of the invention
The problem existing for above-mentioned prior art, the invention provides a kind of supercritical extract suspension culture of Aquilaria sinensis in the application of producing in papermaking-method reconstituted tobaccos technique, this preparation method's technique is simple, cost is low, can make the papermaking-method reconstituted tobaccos finished product that there is suspension culture of Aquilaria sinensis fragrance and inhale taste, can make the harmony more of suspension culture of Aquilaria sinensis cigarette product flue gas, comfortable exquisiteness simultaneously.
To achieve these goals, a kind of supercritical extract suspension culture of Aquilaria sinensis of the present invention, in the application of producing in papermaking-method reconstituted tobaccos technique, comprises the following steps:
(1) extraction: extraction adds water after raw tobacco material is mixed;
(2) separate: after having extracted, through Separation of Solid and Liquid, be extracted liquid and solid-state raw material residue;
(3) supercritical extract suspension culture of Aquilaria sinensis: the suspension culture of Aquilaria sinensis after drying and crushing is extracted after supercritical carbon dioxide extraction 1-3h to thing and residue, supercritical extract temperature is 30-50 ℃, extracting pressure is 15-25MPa, gained extract is mixed in the extract being fitted in step (2) after disperseing with absolute ethyl alcohol, through the concentrated coating fluid of making, residue obtained mixing in the solid-state raw material residue being fitted in step (2), mixes making beating, makes tobacco sheet base by papermaking process;
(4) coating: coating fluid is applied on tobacco sheet base, drying, cuts and make reconstituted tobacco finished product.
Further, described postcritical extraction temperature is 40-45 ℃, and extracting pressure is 15-20MPa.
Further, the weight that the extract of described suspension culture of Aquilaria sinensis and residue thereof are added into accounts for the 20-80% of papermaking-method reconstituted tobaccos finished weight.
Further, the beating degree of described making beating is 30-50 ° of SR.
Further, the quantitative of described reconstituted tobacco finished product is 100-120g, and spreading rate is 30-60%.
The invention has the beneficial effects as follows: this supercritical extract suspension culture of Aquilaria sinensis adopts supercritical carbon dioxide extraction suspension culture of Aquilaria sinensis in the application of producing in papermaking-method reconstituted tobaccos technique, and the extract of suspension culture of Aquilaria sinensis and residue are added in the coating fluid and slurry of papermaking-method reconstituted tobaccos, effectively utilize limited suspension culture of Aquilaria sinensis resource, and can reduce production costs, make the papermaking-method reconstituted tobaccos finished product that there is suspension culture of Aquilaria sinensis fragrance and inhale taste, the suspension culture of Aquilaria sinensis cigarette product excitant simultaneously making is little, flue gas exquisiteness, pleasant impression is comfortable.
The specific embodiment
Below in conjunction with specific embodiment, the invention will be further described.
Embodiment 1
First by the extraction that adds water after raw tobacco material (comprising 30-60% offal, 10-40% fragment, 10-40% offal, 10-20% wood pulp and 10-20% calcium carbonate etc.) mixing, after having extracted, through Separation of Solid and Liquid, be extracted liquid and solid-state raw material residue, then the suspension culture of Aquilaria sinensis after drying and crushing being adopted to supercritical carbon dioxide fluid is 30 ℃ in extraction temperature, extracting pressure is to extract 3h under the condition of 15MPa, be extracted thing and residue, gained extract disperses with absolute ethyl alcohol and mixes in the extract that is fitted on gained after expression separation, through the concentrated coating fluid of making, residue obtained mixing in the solid-state raw material residue that is fitted on gained after expression separation, mix making beating, the beating degree of making beating is 30 ° of SR, make tobacco sheet base by papermaking process, the extract of the suspension culture of Aquilaria sinensis being wherein added into and residue weight account for 20% of papermaking-method reconstituted tobaccos finished weight, finally coating fluid is applied on tobacco sheet base, spreading rate is 30%, by dry, cut and make the quantitatively reconstituted tobacco finished product for 100g.
The papermaking-method reconstituted tobaccos sample 1 that the same papermaking-method reconstituted tobaccos composition of raw materials that does not add suspension culture of Aquilaria sinensis extract and residue is made contrasts with the interpolation extract of suspension culture of Aquilaria sinensis and the papermaking-method reconstituted tobaccos sample 2 of residue, please have the sensory evaluating smoking expert of qualification to smoke panel test, smoking result is as shown in table 1.Specific practice: by sample chopping, roll into cigarette, put into constant temperature (22 ℃ ± 1) constant humidity (relative humidity is 60% ± 2%) more than case inner equilibrium 48h.
Table 1 table of comparisons of smokeing panel test
Figure BDA0000460330650000031
Embodiment 2
First by the extraction that adds water after raw tobacco material (comprising 30-60% offal, 10-40% fragment, 10-40% offal, 10-20% wood pulp and 10-20% calcium carbonate etc.) mixing, after having extracted, through Separation of Solid and Liquid, be extracted liquid and solid-state raw material residue, then adopt supercritical carbon dioxide fluid to extract the suspension culture of Aquilaria sinensis after drying and crushing, it is preferably 40 ℃ in extraction temperature, extracting pressure is to extract 2h under the condition of 20MPa, be extracted thing and residue, gained extract disperses with absolute ethyl alcohol and mixes in the extract that is fitted on gained after expression separation, through the concentrated coating fluid of making, residue obtained mixing in the solid-state raw material residue that is fitted on gained after expression separation, mix making beating, the beating degree of making beating is 40 ° of SR, make tobacco sheet base by papermaking process, the extract of the suspension culture of Aquilaria sinensis being wherein added into and residue weight account for 50% of papermaking-method reconstituted tobaccos finished weight, finally coating fluid is applied on tobacco sheet base, spreading rate is 45%, by dry, cut and make the quantitatively reconstituted tobacco finished product for 110g.
The papermaking-method reconstituted tobaccos sample 1 that the same papermaking-method reconstituted tobaccos composition of raw materials that does not add suspension culture of Aquilaria sinensis extract and residue is made contrasts with the interpolation extract of suspension culture of Aquilaria sinensis and the papermaking-method reconstituted tobaccos sample 2 of residue, please have the sensory evaluating smoking expert of qualification to smoke panel test, smoking result is as shown in table 2.Specific practice: by sample chopping, roll into cigarette, put into constant temperature (22 ℃ ± 1) constant humidity (relative humidity is 60% ± 2%) more than case inner equilibrium 48h.
Table 2 table of comparisons of smokeing panel test
Figure BDA0000460330650000032
Embodiment 3
First by the extraction that adds water after raw tobacco material (comprising 30-60% offal, 10-40% fragment, 10-40% offal, 10-20% wood pulp and 10-20% calcium carbonate etc.) mixing, after having extracted, through Separation of Solid and Liquid, be extracted liquid and solid-state raw material residue, then adopt supercritical carbon dioxide fluid to extract the suspension culture of Aquilaria sinensis after drying and crushing, it is preferably 45 ℃ in extraction temperature, extracting pressure is to extract 2h under the condition of 15MPa, be extracted thing and residue, gained extract disperses with absolute ethyl alcohol and mixes in the extract that is fitted on gained after expression separation, through the concentrated coating fluid of making, residue obtained mixing in the solid-state raw material residue that is fitted on gained after expression separation, mix making beating, the beating degree of making beating is 40 ° of SR, make tobacco sheet base by papermaking process, the extract of the suspension culture of Aquilaria sinensis being wherein added into and residue weight account for 50% of papermaking-method reconstituted tobaccos finished weight, finally coating fluid is applied on tobacco sheet base, spreading rate is 45%, by dry, cut and make the quantitatively reconstituted tobacco finished product for 110g.
The papermaking-method reconstituted tobaccos sample 1 that the same papermaking-method reconstituted tobaccos composition of raw materials that does not add suspension culture of Aquilaria sinensis extract and residue is made contrasts with the interpolation extract of suspension culture of Aquilaria sinensis and the papermaking-method reconstituted tobaccos sample 2 of residue, please have the sensory evaluating smoking expert of qualification to smoke panel test, smoking result is as shown in table 3.Specific practice: by sample chopping, roll into cigarette, put into constant temperature (22 ℃ ± 1) constant humidity (relative humidity is 60% ± 2%) more than case inner equilibrium 48h.
Table 3 table of comparisons of smokeing panel test
Embodiment 4
First by the extraction that adds water after raw tobacco material (comprising 30-60% offal, 10-40% fragment, 10-40% offal, 10-20% wood pulp and 10-20% calcium carbonate etc.) mixing, after having extracted, through Separation of Solid and Liquid, be extracted liquid and solid-state raw material residue, then the suspension culture of Aquilaria sinensis after drying and crushing being adopted to supercritical carbon dioxide fluid is 50 ℃ in extraction temperature, extracting pressure is to extract 1h under the condition of 25MPa, be extracted thing and residue, gained extract disperses with absolute ethyl alcohol and mixes in the extract that is fitted on gained after expression separation, through the concentrated coating fluid of making, residue obtained mixing in the solid-state raw material residue that is fitted on gained after expression separation, mix making beating, the beating degree of making beating is 50 ° of SR, make tobacco sheet base by papermaking process, the extract of the suspension culture of Aquilaria sinensis being wherein added into and residue weight account for 80% of papermaking-method reconstituted tobaccos finished weight, finally coating fluid is applied on tobacco sheet base, spreading rate is 60%, by dry, cut and make the quantitatively reconstituted tobacco finished product for 120g.
The papermaking-method reconstituted tobaccos sample 1 that the same papermaking-method reconstituted tobaccos composition of raw materials that does not add suspension culture of Aquilaria sinensis extract and residue is made contrasts with the interpolation extract of suspension culture of Aquilaria sinensis and the papermaking-method reconstituted tobaccos sample 2 of residue, please have the sensory evaluating smoking expert of qualification to smoke panel test, smoking result is as shown in table 4.Specific practice: by sample chopping, roll into cigarette, put into constant temperature (22 ℃ ± 1) constant humidity (relative humidity is 60% ± 2%) more than case inner equilibrium 48h.
Table 4 table of comparisons of smokeing panel test
Figure BDA0000460330650000051
In sum, this supercritical extract suspension culture of Aquilaria sinensis can make the papermaking-method reconstituted tobaccos finished product that has suspension culture of Aquilaria sinensis fragrance and inhale taste for the production of the technique of papermaking-method reconstituted tobaccos, and excitant is little, flue gas exquisiteness, and pleasant impression is comfortable.

Claims (5)

1. supercritical extract suspension culture of Aquilaria sinensis, in an application of producing in papermaking-method reconstituted tobaccos technique, is characterized in that, comprises the following steps: (1) extraction: extraction adds water after raw tobacco material is mixed;
(2) separate: after having extracted, through Separation of Solid and Liquid, be extracted liquid and solid-state raw material residue;
(3) supercritical extract suspension culture of Aquilaria sinensis: the suspension culture of Aquilaria sinensis after drying and crushing is extracted after supercritical carbon dioxide extraction 1-3h to thing and residue, supercritical extract temperature is 30-50 ℃, extracting pressure is 15-25MPa, gained extract is mixed in the extract being fitted in step (2) after disperseing with absolute ethyl alcohol, through the concentrated coating fluid of making, residue obtained mixing in the solid-state raw material residue being fitted in step (2), mixes making beating, makes tobacco sheet base by papermaking process;
(4) coating: coating fluid is applied on tobacco sheet base, drying, cuts and make reconstituted tobacco finished product.
2. a kind of supercritical extract suspension culture of Aquilaria sinensis according to claim 1, in the application of producing in papermaking-method reconstituted tobaccos technique, is characterized in that, described postcritical extraction temperature is 40-45 ℃, and extracting pressure is 15-20MPa.
3. a kind of supercritical extract suspension culture of Aquilaria sinensis according to claim 1, in the application of producing in papermaking-method reconstituted tobaccos technique, is characterized in that, the weight that the extract of described suspension culture of Aquilaria sinensis and residue thereof are added into accounts for the 20-80% of papermaking-method reconstituted tobaccos finished weight.
4. a kind of supercritical extract suspension culture of Aquilaria sinensis according to claim 1, in the application of producing in papermaking-method reconstituted tobaccos technique, is characterized in that, the beating degree of described making beating is 30-50 ° of SR.
5. a kind of supercritical extract suspension culture of Aquilaria sinensis according to claim 1, in the application of producing in papermaking-method reconstituted tobaccos technique, is characterized in that, the quantitative of described reconstituted tobacco finished product is 100-120g, and spreading rate is 30-60%.
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CN104172470A (en) * 2014-06-23 2014-12-03 惠州市欧野科技有限公司 Plant filler cigarette holder
CN104824838A (en) * 2015-03-31 2015-08-12 川渝中烟工业有限责任公司 Method for applying tobacco flavor extracted from tobacco branches to snus
CN106659231A (en) * 2014-06-24 2017-05-10 菲利普莫里斯生产公司 Reconstituted tobacco sheets and related methods
CN113455690A (en) * 2020-03-31 2021-10-01 中烟施伟策(云南)再造烟叶有限公司 Method for preparing non-tobacco-agilawood type cigarette material by wet papermaking technology
CN113455691A (en) * 2020-03-31 2021-10-01 中烟施伟策(云南)再造烟叶有限公司 Agilawood-containing auxiliary material for cigarettes and tobacco product
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CN114747790A (en) * 2021-01-08 2022-07-15 中烟施伟策(云南)再造烟叶有限公司 Wet-process powder forming preparation method containing agilawood tobacco auxiliary material and tobacco product
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Publication number Priority date Publication date Assignee Title
CN104172470A (en) * 2014-06-23 2014-12-03 惠州市欧野科技有限公司 Plant filler cigarette holder
CN106659231A (en) * 2014-06-24 2017-05-10 菲利普莫里斯生产公司 Reconstituted tobacco sheets and related methods
US10791756B2 (en) 2014-06-24 2020-10-06 Philip Morris Products S.A. Reconstituted tobacco sheets and related methods
CN104824838A (en) * 2015-03-31 2015-08-12 川渝中烟工业有限责任公司 Method for applying tobacco flavor extracted from tobacco branches to snus
US11766067B2 (en) 2017-05-15 2023-09-26 Nicoventures Trading Limited Ground tobacco composition
CN113455690A (en) * 2020-03-31 2021-10-01 中烟施伟策(云南)再造烟叶有限公司 Method for preparing non-tobacco-agilawood type cigarette material by wet papermaking technology
CN113455691A (en) * 2020-03-31 2021-10-01 中烟施伟策(云南)再造烟叶有限公司 Agilawood-containing auxiliary material for cigarettes and tobacco product
CN114732146A (en) * 2021-01-08 2022-07-12 中烟施伟策(云南)再造烟叶有限公司 Method for preparing non-tobacco-agilawood type cigarette material by wet papermaking powder forming technology
CN114747790A (en) * 2021-01-08 2022-07-15 中烟施伟策(云南)再造烟叶有限公司 Wet-process powder forming preparation method containing agilawood tobacco auxiliary material and tobacco product

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