CN107625194A - A kind of preparation method of reconstituted tobacco - Google Patents
A kind of preparation method of reconstituted tobacco Download PDFInfo
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- CN107625194A CN107625194A CN201710765320.XA CN201710765320A CN107625194A CN 107625194 A CN107625194 A CN 107625194A CN 201710765320 A CN201710765320 A CN 201710765320A CN 107625194 A CN107625194 A CN 107625194A
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- reconstituted tobacco
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Abstract
The present invention relates to tobacco leaf preparing technical field, and in particular to a kind of preparation method of reconstituted tobacco.The present invention is first by soda boiling by the lignin dissolution in offal and offal, lignin deposit is come out with organic acid again, filter off and remove, the defects of xylon gas relatively appear when being burnt so as to reduce in traditional reconstituted tobacco, mixed again by the filter residue of bagasse and removal lignin, in the presence of cellulase and microorganism, the cell membrane fiber content in reconstituted tobacco slurry is further reduced, mitigates the generation of the penetrating odor of tobacco leaf caused by being burnt due to this kind of fibrous matter；The present invention utilizes microbiological treatment offal, tobacco leaf and bagasse, improve the fragrance of reconstituted tobacco, in addition, the glucose that is rich in bagasse and Maillard reaction occurs under thermodynamic activity through amino acid caused by microbial degradation from bean curd, Chinese yam, produce unique tobacco flavor, the fragrance of reconstituted tobacco of the present invention is further increased, is had broad application prospects.
Description
Technical field
The present invention relates to tobacco leaf preparing technical field, and in particular to a kind of preparation method of reconstituted tobacco.
Background technology
According to statistics, during cigarette and redrying, the leftover bits and pieces such as nearly 25% tobacco leaf, offal is there are about and gone out of use, it is impossible to directly
For production of cigarettes, the waste of resource is caused.As a regulating measure of tobacco resource regeneration, with offal, offal,
Tobacco cut etc. is raw material, and sheet or thread reconstituted tobacco technology is made using specific processing technology, develops in recent decades
Very fast, its processing technology also experienced roll-in method, thick slurry method, 3 stages of paper process.
At present, papermaking-method reconstituted tobaccos are mainly produced using two-step process.In actual production, due to various factors
Influence, quite a few in reconstituted tobacco raw material is to fragrance and the contributive material of smoke in extraction, concentration and pulping and paper-making etc.
Process is lost in and is destroyed；Moreover, papermaking-method reconstituted tobaccos have one it is intrinsic the defects of, due to offal, offal intensity itself very
It is low, in order to adapt to needs of manufacturing paper with pulp, the non-tobacco fibers such as wood pulp are added generally during manufacturing paper with pulp, but easily produce in burning
The negative effect of wooden miscellaneous gas.Contain the cell membrane classes such as substantial amounts of cellulose, hemicellulose, lignin i.e. in its chemical composition
Material, these materials show the features such as flue gas is coarse pungent, xylon gas are heavy, excitant is big when burning and sucking.Therefore, domestic mesh
The preceding papermaking-method reconstituted tobaccos by two-step process production, be all short of in various degree there is tobacco aroma on aesthetic quality,
Smoke deficiency, xylon gas compared with appear, excitant is larger the shortcomings of.
Therefore, invention one kind give off a strong fragrance, xylon gas it is soft, the preparation method of nonirritant reconstituted tobacco is to reproducing cigarette
Leaf preparing technical field has positive meaning.
The content of the invention
Present invention mainly solves technical problem, for traditional reconstituted tobacco at present on aesthetic quality it is all different degrees of
There is tobacco aroma shortcoming, xylon gas compared with appear, excitant is larger the shortcomings that, there is provided a kind of preparation side of reconstituted tobacco
Method.
In order to solve the above-mentioned technical problem, the technical solution adopted in the present invention is：
A kind of preparation method of reconstituted tobacco, it is characterised in that specifically preparation process is：
（1）Will offal and offal and sodium hydroxide solution mix after obtain mixed liquor, by mixed liquor heating boil processing 1~
2h, boil after processing terminates and be separated by filtration, respectively obtain filtrate and filter residue, filter residue is standby；
（2）Above-mentioned filtrate is adjusted into pH to 5.5~6.0 with citric acid solution, filters, is separated except heavy after staticly settling 2~3h
Form sediment, obtain pretreatment filtrates, then pretreatment filtrates are concentrated under reduced pressure, obtain concentrating filtrate, it is standby；
（3）Mixing slag is obtained after standby filter residue and bagasse are mixed, after gained mixing slag and bean curd and Chinese yam are mixed
As fermentation substrate and it is fitted into fermentation tank, then cellulase and bacillus subtilis bacteria suspension is added into fermentation tank, sealing
Fermentation；
（4）After above-mentioned fermentation ends, tunning is taken out, is separated by filtration to obtain ferment filtrate and fermentation filter residue, ferment filter residue
It is standby, it is transferred in round-bottomed flask by ferment filtrate high-temperature sterilization, then by the ferment filtrate after sterilizing, is added with temperature adjustment heating mantle
Heat, and start agitator, stirring reaction, obtain reaction solution；
（5）Above-mentioned reaction solution and standby concentration filtrate are mixed to get concentration maceration extract, then above-mentioned fermentation filter residue is beaten
Machine carries out mashing processing, and it is 31.0 ° of SR to control beating degree, obtains reproducing cigarette slurry, and reconstruction cigarette slurry is passed through into paper machine pulp feeding system point
Not Jin Ru double cylinder extrusion coating paper machines upper wet end and lower wet end, shaping of manufacturing paper with pulp obtain wet substrate；
（6）The tobacco powder of the uniform mesh of spreading 100 in above-mentioned off line wet substrate, then by upper and lower net wet substrate compound suppressing, answered
Wet substrate is closed, finally compound wet substrate is immersed in above-mentioned concentration maceration extract after soaking 1~2h and taken out, dried and crush, you can
Obtain a kind of reconstituted tobacco.
Step（1）Described in offal and the mass ratio of offal and sodium hydroxide solution be 1:2:10, sodium hydroxide is molten
The mass fraction of liquid is 10%.
Step（2）Described in the mode being concentrated under reduced pressure be：Pretreatment filtrates are put into concentration tank, reduce pressure inside the tank
To 1000~1200Pa, be concentrated under reduced pressure 20~30min, obtains concentrating filtrate.
Step（3）Described in filter residue and bagasse mass ratio be 5:1, mixing slag and bean curd and the mass ratio of Chinese yam
For 10:1:1, the addition of cellulase is the 1% of fermentation substrate quality, and the concentration of bacillus subtilis bacteria suspension is 107cfu/
ML, the addition of bacillus subtilis bacteria suspension are the 10% of fermentation substrate quality, and the temperature of sealing and fermenting is 30~40 DEG C, close
The time of seal ferment is 3~5 days.
Step（4）Described in stirring reaction temperature be 90~100 DEG C, the time of stirring reaction is 3~5h.
Step（5）Described in reaction solution and concentration filtrate mass ratio be 1:5, manufacture paper with pulp and control upper and lower net base when being molded
Piece is quantitatively 30g/m2。
Step（6）Described in the spreading amounts of tobacco powder of 100 mesh be 5g/m2。
The beneficial effects of the invention are as follows：
（1）The present invention first mixes offal and offal with alkali lye, and heating is boiled, will be wooden in offal and offal by soda boiling
Element dissolving, then come out lignin deposit with organic acid, filter off and remove, xylon gas when being burnt so as to reduce in traditional reconstituted tobacco
The defects of relatively appearing, then mixed by the filter residue of bagasse and removal lignin, in the presence of cellulase and microorganism, enter
One step reduces the cell membrane fiber content in reconstituted tobacco slurry, mitigates the thorn of tobacco leaf caused by being burnt due to this kind of fibrous matter
Swash the generation of property smell；
（2）The present invention utilizes microbiological treatment offal, tobacco leaf and bagasse, can be by the sugar wherein contained, protein, fruit
The mass degradations such as glue, organic acid, so as to avoid this kind of substance combustion from producing peculiar smell, the fragrance of reconstituted tobacco is improved, in addition, sweet
The glucose that is rich in bagasse and U.S. drawing occurs under thermodynamic activity through amino acid caused by microbial degradation from bean curd, Chinese yam
Moral is reacted, and produces the tobacco flavor of uniqueness, further increases the fragrance of reconstituted tobacco of the present invention, before having wide application
Scape.
Embodiment
It is that 10% sodium hydroxide solution is 1 in mass ratio by offal and offal and mass fraction:2:Mixed after 10 mixing
Liquid is closed, 1~2h of processing is boiled into mixed liquor heating, boils after processing terminates and is separated by filtration, respectively obtain filtrate and filter residue, filter residue
It is standby；By filtrate with concentration be 1mol/L citric acid solutions regulation pH to 5.5~6.0, filtered after staticly settling 2~3h, separate
Precipitation is removed, obtains pretreatment filtrates, then pretreatment filtrates are put into concentration tank, reduction pressure inside the tank to 1000~
1200Pa, be concentrated under reduced pressure 20~30min, obtains concentrating filtrate；It is 5 in mass ratio by filter residue and bagasse:Mixed after 1 mixing
Slag is closed, is 10 in mass ratio by gained mixing slag and bean curd and Chinese yam:1:Fermentation substrate is used as after 1 mixing and loads fermentation tank
In, then the concentration 10 of the cellulase of addition fermentation substrate quality 1% and fermentation substrate quality 10% into fermentation tank7Cfu/mL's
Bacillus subtilis bacteria suspension, it is sealed by fermentation 3~5 days at 30~40 DEG C after being stirred；After fermentation ends, fermentation is taken out
Product, it is separated by filtration to obtain ferment filtrate and fermentation filter residue, fermentation filter residue is standby, and ferment filtrate is put into high-temperature sterilization box,
15~20min of high-temperature sterilization at 120 DEG C, then the ferment filtrate after sterilizing is transferred to and burnt with the round bottom of agitator and thermometer
In bottle, heated with temperature adjustment heating mantle, and start agitator, 3~5h of stirring reaction, obtains reaction solution at 90~100 DEG C；
It is 1 in mass ratio by reaction solution and standby concentration filtrate:5 are mixed to get concentration maceration extract, then above-mentioned fermentation filter residue is used and beaten
Pulp grinder carries out mashing processing, and it is 31.0 ° of SR to control beating degree, obtains reproducing cigarette slurry, and reconstruction cigarette slurry is passed through into paper machine pulp feeding system
The upper wet end of double cylinder extrusion coating paper machines and lower wet end are respectively enterd, is quantitatively 30g/m by upper and lower net substrate2, manufacture paper with pulp and be molded
To wet substrate；By addition it is 5g/m in off line wet substrate2The tobacco powder of the uniform mesh of spreading 100, then by upper and lower net wet substrate with
0.5~0.8MPa pressure bonding compacting, obtains compound wet substrate, finally immerses compound wet substrate in above-mentioned concentration maceration extract
Taken out after 1~2h of immersion, dry and crush, you can obtain a kind of reconstituted tobacco.
Example 1
It is that 10% sodium hydroxide solution is 1 in mass ratio by offal and offal and mass fraction:2:Mixed after 10 mixing
Liquid, processing 1h is boiled into mixed liquor heating, boils after processing terminates and is separated by filtration, respectively obtain filtrate and filter residue, filter residue is standby；
By filtrate with concentration be 1mol/L citric acid solutions regulation pH to 5.5, filtered after staticly settling 2h, separate except precipitation, obtain
Pretreatment filtrates, then pretreatment filtrates are put into concentration tank, pressure inside the tank is reduced to 1000Pa, and be concentrated under reduced pressure 20min, obtains
Concentrate filtrate；It is 5 in mass ratio by filter residue and bagasse:Mixing slag is obtained after 1 mixing, by gained mixing slag and bean curd and mountain
Medicine is 10 in mass ratio:1:Fermentation substrate is used as after 1 mixing and is fitted into fermentation tank, then fermentation substrate matter is added into fermentation tank
The cellulase of amount 1% and the concentration 10 of fermentation substrate quality 10%7Cfu/mL bacillus subtilis bacteria suspension, after being stirred
It is sealed by fermentation 3 days at 30 DEG C；After fermentation ends, tunning is taken out, is separated by filtration to obtain ferment filtrate and fermentation filter residue,
The filter residue that ferments is standby, ferment filtrate is put into high-temperature sterilization box, the high-temperature sterilization 15min at 120 DEG C, then by the hair after sterilizing
Ferment filtrate is transferred in the round-bottomed flask with agitator and thermometer, is heated with temperature adjustment heating mantle, and starts agitator,
Stirring reaction 3h, obtains reaction solution at 90 DEG C；It is 1 in mass ratio by reaction solution and standby concentration filtrate:5 are mixed to get concentration
Maceration extract, then above-mentioned fermentation filter residue is subjected to mashing processing with beater, it is 31.0 ° of SR to control beating degree, obtains reproducing cigarette slurry,
Cigarette slurry will be reproduced the upper wet end of double cylinder extrusion coating paper machines and lower wet end are respectively enterd by paper machine pulp feeding system, by upper and lower net base
Piece is quantitatively 30g/m2, shaping of manufacturing paper with pulp obtains wet substrate；By addition it is 5g/m in off line wet substrate2The uniform mesh of spreading 100
Tobacco powder, then upper and lower net wet substrate is suppressed with 0.5MPa pressure bonding, compound wet substrate is obtained, finally by compound wet basis
Piece is immersed in above-mentioned concentration maceration extract to be taken out after immersion 1h, is dried and is crushed, you can obtains a kind of reconstituted tobacco.
Example 2
It is that 10% sodium hydroxide solution is 1 in mass ratio by offal and offal and mass fraction:2:Mixed after 10 mixing
Liquid, processing 1h is boiled into mixed liquor heating, boils after processing terminates and is separated by filtration, respectively obtain filtrate and filter residue, filter residue is standby；
By filtrate with concentration be 1mol/L citric acid solutions regulation pH to 5.8, filtered after staticly settling 2h, separate except precipitation, obtain
Pretreatment filtrates, then pretreatment filtrates are put into concentration tank, pressure inside the tank is reduced to 1100Pa, and be concentrated under reduced pressure 25min, obtains
Concentrate filtrate；It is 5 in mass ratio by filter residue and bagasse:Mixing slag is obtained after 1 mixing, by gained mixing slag and bean curd and mountain
Medicine is 10 in mass ratio:1:Fermentation substrate is used as after 1 mixing and is fitted into fermentation tank, then fermentation substrate matter is added into fermentation tank
The cellulase of amount 1% and the concentration 10 of fermentation substrate quality 10%7Cfu/mL bacillus subtilis bacteria suspension, after being stirred
It is sealed by fermentation 4 days at 35 DEG C；After fermentation ends, tunning is taken out, is separated by filtration to obtain ferment filtrate and fermentation filter residue,
The filter residue that ferments is standby, ferment filtrate is put into high-temperature sterilization box, the high-temperature sterilization 18min at 120 DEG C, then by the hair after sterilizing
Ferment filtrate is transferred in the round-bottomed flask with agitator and thermometer, is heated with temperature adjustment heating mantle, and starts agitator,
Stirring reaction 4h, obtains reaction solution at 95 DEG C；It is 1 in mass ratio by reaction solution and standby concentration filtrate:5 are mixed to get concentration
Maceration extract, then above-mentioned fermentation filter residue is subjected to mashing processing with beater, it is 31.0 ° of SR to control beating degree, obtains reproducing cigarette slurry,
Cigarette slurry will be reproduced the upper wet end of double cylinder extrusion coating paper machines and lower wet end are respectively enterd by paper machine pulp feeding system, by upper and lower net base
Piece is quantitatively 30g/m2, shaping of manufacturing paper with pulp obtains wet substrate；By addition it is 5g/m in off line wet substrate2The uniform mesh of spreading 100
Tobacco powder, then upper and lower net wet substrate is suppressed with 0.7MPa pressure bonding, compound wet substrate is obtained, finally by compound wet basis
Piece is immersed in above-mentioned concentration maceration extract to be taken out after immersion 1h, is dried and is crushed, you can obtains a kind of reconstituted tobacco.
Example 3
It is that 10% sodium hydroxide solution is 1 in mass ratio by offal and offal and mass fraction:2:Mixed after 10 mixing
Liquid, processing 2h is boiled into mixed liquor heating, boils after processing terminates and is separated by filtration, respectively obtain filtrate and filter residue, filter residue is standby；
By filtrate with concentration be 1mol/L citric acid solutions regulation pH to 6.0, filtered after staticly settling 3h, separate except precipitation, obtain
Pretreatment filtrates, then pretreatment filtrates are put into concentration tank, pressure inside the tank is reduced to 1200Pa, and be concentrated under reduced pressure 30min, obtains
Concentrate filtrate；It is 5 in mass ratio by filter residue and bagasse:Mixing slag is obtained after 1 mixing, by gained mixing slag and bean curd and mountain
Medicine is 10 in mass ratio:1:Fermentation substrate is used as after 1 mixing and is fitted into fermentation tank, then fermentation substrate matter is added into fermentation tank
The cellulase of amount 1% and the concentration 10 of fermentation substrate quality 10%7Cfu/mL bacillus subtilis bacteria suspension, after being stirred
It is sealed by fermentation 5 days at 40 DEG C；After fermentation ends, tunning is taken out, is separated by filtration to obtain ferment filtrate and fermentation filter residue,
The filter residue that ferments is standby, ferment filtrate is put into high-temperature sterilization box, the high-temperature sterilization 20min at 120 DEG C, then by the hair after sterilizing
Ferment filtrate is transferred in the round-bottomed flask with agitator and thermometer, is heated with temperature adjustment heating mantle, and starts agitator,
Stirring reaction 5h, obtains reaction solution at 100 DEG C；It is 1 in mass ratio by reaction solution and standby concentration filtrate:5 be mixed to get it is dense
Contracting maceration extract, then above-mentioned fermentation filter residue is subjected to mashing processing with beater, it is 31.0 ° of SR to control beating degree, obtains reproducing cigarette
Slurry, cigarette slurry will be reproduced the upper wet end of double cylinder extrusion coating paper machines and lower wet end are respectively enterd by paper machine pulp feeding system, by upper and lower net
Substrate is quantitatively 30g/m2, shaping of manufacturing paper with pulp obtains wet substrate；By addition it is 5g/m in off line wet substrate2Uniform spreading 100
Purpose tobacco powder, then upper and lower net wet substrate is suppressed with 0.1MPa pressure bonding, compound wet substrate is obtained, finally will be compound wet
Substrate is immersed in above-mentioned concentration maceration extract to be taken out after immersion 2h, is dried and is crushed, you can obtains a kind of reconstituted tobacco.
Reference examples
Reference examples are used as using the reconstituted tobacco of company of Guangdong Province production
Cigarette is made in reconstituted tobacco in reconstituted tobacco produced by the present invention and reference examples, carrying out sense organ by 7 people groups comments
Valency, as a result as described in Table 1：
Table 1
| Assessment item | Example 1 | Example 2 | Example 3 | Reference examples |
| Perfume quantity | It is more sufficient | It is more sufficient | Foot | Have |
| Exquisiteness | It is still fine and smooth | It is finer and smoother | It is fine and smooth | It is rougher |
| Sweet sense | It is medium | It is stronger | It is stronger | It is poor |
| Concentration | It is medium | It is medium | It is medium | It is denseer |
| Wooden miscellaneous gas | Nothing | Nothing | Nothing | Have |
| Excitant | Nothing | It is micro- to have | Nothing | It is larger |
| Pleasant impression | Shang Shi | Shang Shi | Shang Shi | Shang Shi |
Note：Perfume quantity：Foot, it is relatively sufficient, still sufficient, have, be less, be few；Exquisiteness：It is fine and smooth, still fine and smooth, finer and smoother, rougher, coarse；
Sweet sense：By force, it is stronger, medium, poor, poor；Concentration：It is dense, denseer, medium, thin, light；Miscellaneous gas：Without, it is relatively light, have, it is slightly heavy, compared with
Again, again；Excitant：Without, micro- have, have, slightly having, be bigger, be larger, be big；Pleasant impression：Comfortably, relatively comfortable, Shang Shi, suitable, stagnant tongue is owed.
Reconstituted tobacco produced by the present invention is sweet it can be seen from Analyses Methods for Sensory Evaluation Results in above table feels stronger, fragrance
Rich to increase with perfume quantity, xylon gas are slight, and excitant is low, have broad application prospects.
Claims (6)
1. a kind of preparation method of reconstituted tobacco, it is characterised in that specifically preparation process is：
（1）Will offal and offal and sodium hydroxide solution mix after obtain mixed liquor, by mixed liquor heating boil processing 1~
2h, boil after processing terminates and be separated by filtration, respectively obtain filtrate and filter residue, filter residue is standby；
（2）Above-mentioned filtrate is adjusted into pH to 5.5~6.0 with citric acid solution, filters, is separated except heavy after staticly settling 2~3h
Form sediment, obtain pretreatment filtrates, then pretreatment filtrates are concentrated under reduced pressure, obtain concentrating filtrate, it is standby；
（3）Mixing slag is obtained after standby filter residue and bagasse are mixed, after gained mixing slag and bean curd and Chinese yam are mixed
As fermentation substrate and it is fitted into fermentation tank, then cellulase and bacillus subtilis bacteria suspension is added into fermentation tank, sealing
Fermentation；
（4）After above-mentioned fermentation ends, tunning is taken out, is separated by filtration to obtain ferment filtrate and fermentation filter residue, ferment filter residue
It is standby, it is transferred in round-bottomed flask by ferment filtrate high-temperature sterilization, then by the ferment filtrate after sterilizing, is added with temperature adjustment heating mantle
Heat, and start agitator, stirring reaction, obtain reaction solution；
（5）Above-mentioned reaction solution and standby concentration filtrate are mixed to get concentration maceration extract, then above-mentioned fermentation filter residue is beaten
Machine carries out mashing processing, and it is 31.0 ° of SR to control beating degree, obtains reproducing cigarette slurry, and reconstruction cigarette slurry is passed through into paper machine pulp feeding system point
Not Jin Ru double cylinder extrusion coating paper machines upper wet end and lower wet end, shaping of manufacturing paper with pulp obtain wet substrate；
（6）The tobacco powder of the uniform mesh of spreading 100 in above-mentioned off line wet substrate, then by upper and lower net wet substrate compound suppressing, answered
Wet substrate is closed, finally compound wet substrate is immersed in above-mentioned concentration maceration extract after soaking 1~2h and taken out, dried and crush, you can
Obtain a kind of reconstituted tobacco.
2. according to a kind of preparation method of reconstituted tobacco described in claim 1, it is characterised in that：Step（1）Described in
The mass ratio of offal and offal and sodium hydroxide solution is 1:2:10, the mass fraction of sodium hydroxide solution is 10%.
3. according to a kind of preparation method of reconstituted tobacco described in claim 1, it is characterised in that：Step（2）Described in
The mode being concentrated under reduced pressure is：Pretreatment filtrates are put into concentration tank, pressure inside the tank is reduced to 1000~1200Pa, is concentrated under reduced pressure
20~30min, obtain concentrating filtrate.
4. according to a kind of preparation method of reconstituted tobacco described in claim 1, it is characterised in that：Step（3）Described in
The mass ratio of filter residue and bagasse is 5:1, mixing slag and bean curd and the mass ratio of Chinese yam are 10:1:1, the addition of cellulase
Measure as the 1% of fermentation substrate quality, the concentration of bacillus subtilis bacteria suspension is 107Cfu/mL, bacillus subtilis bacteria suspension
Addition is the 10% of fermentation substrate quality, and the temperature of sealing and fermenting is 30~40 DEG C, and the time of sealing and fermenting is 3~5 days.
5. according to a kind of preparation method of reconstituted tobacco described in claim 1, it is characterised in that：Step（4）Described in
The temperature of stirring reaction is 90~100 DEG C, and the time of stirring reaction is 3~5h.
6. according to a kind of preparation method of reconstituted tobacco described in claim 1, it is characterised in that：Step（5）Described in
Reaction solution and the mass ratio of concentration filtrate are 1:5, manufacture paper with pulp and control upper and lower net substrate quantitatively equal when being molded
According to a kind of preparation method of reconstituted tobacco described in claim 1, it is characterised in that：Step（6）Described in 100
The spreading amount of purpose tobacco powder is 5g/m2。
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| CN108477662A (en) * | 2018-04-11 | 2018-09-04 | 湖北中烟工业有限责任公司 | A kind of manufacturing process of burley tobaccos characteristic reconstituted tobacco |
| CN108851194A (en) * | 2018-07-17 | 2018-11-23 | 陈汉林 | A kind of honeysuckle health care cigarette and preparation method thereof |
| CN108968132A (en) * | 2018-10-09 | 2018-12-11 | 湖北中烟工业有限责任公司 | A kind of preparation method of reconstituted tobacco coating fluid |
| CN110876486A (en) * | 2019-11-21 | 2020-03-13 | 于曦华 | Rosemary cigarette and processing method thereof |
| CN112471573A (en) * | 2020-12-31 | 2021-03-12 | 广西壮族自治区亚热带作物研究所（广西亚热带农产品加工研究所） | Method for improving tobacco leaf quality |
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| CN108968132A (en) * | 2018-10-09 | 2018-12-11 | 湖北中烟工业有限责任公司 | A kind of preparation method of reconstituted tobacco coating fluid |
| CN108968132B (en) * | 2018-10-09 | 2021-08-03 | 湖北中烟工业有限责任公司 | Preparation method of reconstituted tobacco coating liquid |
| CN110876486A (en) * | 2019-11-21 | 2020-03-13 | 于曦华 | Rosemary cigarette and processing method thereof |
| CN112471573A (en) * | 2020-12-31 | 2021-03-12 | 广西壮族自治区亚热带作物研究所（广西亚热带农产品加工研究所） | Method for improving tobacco leaf quality |
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Application publication date: 20180126 |