CN110506849A - Bamboo shoot process residue juice comprehensive processing and utilization method - Google Patents
Bamboo shoot process residue juice comprehensive processing and utilization method Download PDFInfo
- Publication number
- CN110506849A CN110506849A CN201910705380.1A CN201910705380A CN110506849A CN 110506849 A CN110506849 A CN 110506849A CN 201910705380 A CN201910705380 A CN 201910705380A CN 110506849 A CN110506849 A CN 110506849A
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- China
- Prior art keywords
- bamboo shoot
- process residue
- shoot process
- juice
- bamboo
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Classifications
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- C12P19/04—Polysaccharides, i.e. compounds containing more than five saccharide radicals attached to each other by glycosidic bonds
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- C—CHEMISTRY; METALLURGY
- C12—BIOCHEMISTRY; BEER; SPIRITS; WINE; VINEGAR; MICROBIOLOGY; ENZYMOLOGY; MUTATION OR GENETIC ENGINEERING
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- D21H11/00—Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
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- D07—ROPES; CABLES OTHER THAN ELECTRIC
- D07B—ROPES OR CABLES IN GENERAL
- D07B2205/00—Rope or cable materials
- D07B2205/10—Natural organic materials
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Abstract
A kind of bamboo shoot process residue juice comprehensive processing and utilization method, comprising: bamboo shoot process residue is squeezed, to isolate bamboo shoot process residue juice and solid matter；Alternatively, carrying out boiling to bamboo shoots, cooking liquor is obtained, using cooking liquor as bamboo shoot process residue juice；With bamboo shoot process residue sap extraction bamboo shoot process residue crude protein；Extraction process includes: that bamboo shoot process residue juice is obtained the first filtrate and bamboo shoot process residue particulate through plate-frame filtering；First filtrate is subjected to micro-filtration, obtains the second filtrate and bamboo shoot process residue particulate；Second filtrate is concentrated by ultrafiltration membrance filter, obtains third concentrate and third filter liquor；Third concentrate is centrifuged or is filtered, is separated by solid-liquid separation with realizing, to obtain the 4th liquid and bamboo shoot process residue crude protein.The bamboo shoot process residue juice comprehensive processing and utilization method makes full use of bamboo shoot process residue juice.
Description
Technical field
The present invention relates to bamboo shoot process field more particularly to a kind of bamboo shoot process residue juice comprehensive processing and utilization sides
Method.
Background technique
Bamboo shoot process will cut off the bamboo shoot head (bamboo shoot head refers to the old part in bamboo shoot root) of bamboo shoots lower end aging, and remove outside
Bamboo shoot shell (bamboo shoot shell is also referred to as bamboo shoot clothing).Bamboo shoot head and bamboo shoot shell can be collectively referred to as: bamboo shoot process residue.
The bamboo shoot process residue of thousands of tons contains cellulose very rich, protein and polysaccharide etc., but does not have
It is utilized effectively.Specifically, a bamboo shoots, it is remaining by the bamboo shoot process as leftover bits and pieces that there are about 70% parts sometimes
Object, and be dropped.Such raw material availability is too low, causes production cost excessively high, causes the significant wastage of bamboo shoots resource.Together
When, these bamboo shoot process residues become waste material, it is necessary to transport countryside stacking to and many freight charges is needed also seriously to pollute environment.
Summary of the invention
Problems solved by the invention is to provide a kind of bamboo shoot process residue comprehensive processing and utilization method and bamboo shoot process is surplus
Excess juice comprehensive processing and utilization method preferably utilizes bamboo shoot process residue preferably to utilize bamboo shoot process residue
Juice.
To solve the above problems, the present invention provides bamboo shoot process residue comprehensive processing and utilization method, comprising: to bamboo shoots plus
Work residue is squeezed, to isolate bamboo shoot process residue juice and solid matter；To the bamboo shoot process residue juice
Liquid carries out first and utilizes；The solid matter is isolated into bamboo shoot process residue particulate and bamboo shoot process residue fiber；It is right
The bamboo shoot process residue particulate carries out second and utilizes；Third utilization is carried out to the bamboo shoot process residue fiber.
Optionally, the mode squeezed to the bamboo shoot process residue is concora crush mode, fashion of extrusion or rolls
Mode.
Optionally, squeeze the pressure range used to the bamboo shoot process residue as 15MPa~150MPa.
Optionally, the solid matter is isolated into the bamboo shoot process residue particulate and the bamboo shoot process residue
Fiber includes: to carry out rubbing silk to the solid matter；It is described rub silk after, be dried；After the drying, screening point is carried out
From to isolate the bamboo shoot process residue particulate and the bamboo shoot process residue fiber.
Optionally, the solid matter is isolated into the bamboo shoot process residue particulate and the bamboo shoot process residue
Fiber includes: to carry out rubbing silk to the solid matter；It is described rub silk after, water is added in the solid matter, formation can flow
The mixture of dynamic state；Screening separation is carried out to the mixture, to isolate the bamboo shoot process residue particulate and described
Bamboo shoot process residue fiber.
Optionally, to the bamboo shoot process residue juice it is described first using include it is following it is several utilize at least its
One of: as mushroom culture solution；For extracting vegetable protein；For extracting polysaccharide；It is looked for for extracting bamboo shoot process residue
Element；For extracting tabasheer ketone.
Optionally, it includes: remaining to the bamboo shoot process for utilizing to described the first of the bamboo shoot process residue juice
Object juice ferments, by the bamboo shoot process residue juice after the fermentation be used to prepare plant culture nutrient solution or
Liquid fertilizer.
Optionally, to the bamboo shoot process residue particulate it is described second using include it is following it is several utilize at least its
One of: as feed；As organic fertilizer fermentation raw material；As mushroom planted medium ingredient.
Optionally, utilizing to described the second of the bamboo shoot process residue particulate includes: to be used as production functional sugar, crystallite
The raw material of cellulose or dietary fiber；Inducer as production cellulase；Inducer as production hemicellulase.
Optionally, utilizing to the third of the bamboo shoot process residue fiber includes by the bamboo shoot process residue
Fiber is used to make at least one of following product: making in make mattress, rope, does the wash apparatus, wood plastic composite, resists
Bacterium insole, headrest, pillow, textile material, paper, special fibre.
To solve the above problems, the present invention also provides a kind of bamboo shoot process residue comprehensive processing and utilization methods, comprising:
Bamboo shoots are subjected to boiling, obtain cooking liquor；From the bamboo shoots after boiling, bamboo shoot process residue is isolated；To the bamboo
Bamboo shoot industrial wood waste is squeezed, to isolate bamboo shoot process residue juice and solid matter；It is remaining to the bamboo shoot process
Object juice carries out first and utilizes；The solid matter is isolated into bamboo shoot process residue particulate and bamboo shoot process residue fiber
Dimension；Second is carried out to the bamboo shoot process residue particulate to utilize；Third utilization is carried out to the bamboo shoot process residue fiber；
By the cooking liquor, it is also used as the bamboo shoot process residue juice, described first is carried out and utilizes.
To solve the above problems, the present invention also provides a kind of bamboo shoot process residue juice comprehensive processing and utilization method,
It include: to be squeezed to bamboo shoot process residue, to isolate bamboo shoot process residue juice and solid matter；Alternatively, to bamboo
Bamboo shoot carry out boiling, cooking liquor are obtained, using the cooking liquor as bamboo shoot process residue juice；With the bamboo shoot process residue
Sap extraction bamboo shoot process residue crude protein；The bamboo shoot process residue described in the bamboo shoot process residue sap extraction is thick
Albumen includes: that the bamboo shoot process residue juice is obtained the first filtrate and bamboo shoot process residue particulate through plate-frame filtering；
First filtrate is subjected to micro-filtration, obtains the second filtrate and bamboo shoot process residue particulate；Second filtrate is passed through super
Membrane filtration concentration, obtains third concentrate and third filter liquor；The third concentrate is centrifuged or is filtered, to realize
It is separated by solid-liquid separation, to obtain the 4th liquid and bamboo shoot process residue crude protein.
Optionally, the third filter liquor is used for the component as mushroom culture medium.
Optionally, before the third concentrate is centrifuged or is filtered, the third concentrate is heated to 70-
100 DEG C, 0-30min is kept the temperature, is cooled to 40 DEG C hereinafter, precipitating；In the precipitating and then carry out the centrifugation or filtering.
Optionally, the method also includes the 4th liquid is obtained the 5th filtrate and bamboo shoot process residue through micro-filtration
Crude protein；5th clear liquid is concentrated by ultrafiltration membrance filter, obtains the 6th concentrate and the 6th filter liquor；It is dense the described 6th
It is 66-80% that ethyl alcohol to volume fraction of ethanol is added in contracting liquid；It is separated by solid-liquid separation by being centrifuged or filtering, collects sediment；
The sediment ethanol washing obtains bamboo shoot process residue polysaccharide.
Optionally, the third filter liquor and the 6th filter liquor are concentrated by nanofiltration membrane, obtain the 7th concentrate
And the 7th filter liquor；7th filter liquor is dried, bamboo shoot process residue pigment is obtained.
It optionally, is spray drying to the drying that the 7th concentrate carries out.
Optionally, the 7th filter liquor is concentrated through reverse osmosis membrane filtration, and passes through polar macroporous resin adsorption, Zhi Houtong
It crosses ethanol elution and obtains the eluent containing flavones, evaporate the eluent and obtain tabasheer ketone.
Optionally, in the evaporation process, the ethyl alcohol in the eluent is recycled.
To solve the above problems, the present invention also provides another bamboo shoot process residue juice comprehensive processing and utilization sides
Method, comprising: bamboo shoot process residue is squeezed, to isolate bamboo shoot process residue juice and solid matter；Alternatively, right
Bamboo shoots carry out boiling, cooking liquor are obtained, using the cooking liquor as bamboo shoot process residue juice；The bamboo shoot process is remaining
Object juice is as mushroom culture solution to produce bacteria cellulose；Using the bamboo shoot process residue juice as the mushroom culture
Liquid includes: that sugar or molasses are added to mass percentage concentration in the bamboo shoot process residue juice to produce the bacteria cellulose
2-5%, it is 1.26-2.52mmol/L that potassium ion to molar concentration, which is added, and it is 0.63- that phosphate anion to molar concentration, which is added,
1.26mmol/L is added sulfate ion to mass percentage concentration 0.073-0.292%, it is dense to quality percentage that ammonium ion is added
0.027-0.108% is spent, mixing liquid is formed；The mixing is adjusted with alkali, basic anhydride, basic carbonate or bicarbonate
The pH value of liquid becomes the mushroom culture solution to 3-6；Mushroom is accessed to the mushroom culture liquid；It is sent out in 25-40 DEG C of standing
Ferment 2-5 days, obtain the bacteria cellulose.
Optionally, the mushroom is acetic acid Pseudomonas, gluconobacter suboxydans category, gluconic acid Acetobacter, the glycoxidative bar of grape
Bacterium, rhizobium, Sarcina, pseudomonas, achromobacter, Alcaligenes, Aerobacter, azotobacter, soil
One or more of Bacillus, onion pseudomonas sp, campylobacter jejuni, gluconate pyracetobacillus.
In the one aspect of technical solution of the present invention, comprehensive process is carried out to bamboo shoot process residue and is utilized, by
The ingredient of bamboo shoot process residue is isolated bamboo shoot process residue juice, bamboo shoot process residue particulate and bamboo shoot process by step
Then residue fiber carries out valuable comprehensive utilization respectively, realize the reasonable utilization to bamboo shoot process residue, make bamboo
Bamboo shoot industrial wood waste becomes raw material from waste material, reduces bamboo shoot process residue and discharges pollution on the environment, also, processes life
The case where basically reaching no any trash discharge during producing, has taken into account economic interests and environmental protection.
Further, in the other side of technical solution of the present invention, comprehensive process is carried out to bamboo shoot process residue juice
With utilization.Bamboo shoot process residue itself is relatively inexpensive, and therefore, bamboo shoot process residue juice is also cheap, and the method, energy
Bamboo shoot process residue juice (bamboo shoot shell juice) is enough set to turn waste into wealth.Corresponding juice can be fully utilized in correlation method and technique
, it can be realized zero-emission, therefore, still taken into account economic interests and environmental protection.
Detailed description of the invention
Fig. 1 is bamboo shoot process residue comprehensive processing and utilization method flow schematic diagram in embodiment；
Fig. 2 is bamboo shoot process residue juice comprehensive processing and utilization method flow schematic diagram in embodiment.
Specific embodiment
It is not comprehensive to the utilization of bamboo shoot process residue in existing now technology, add for this purpose, the present invention provides corresponding synthesis
Work utilizes method.
Fig. 1 shows a kind of specific bamboo shoot process residue comprehensive processing and utilization method, and raw material therein is selected as bamboo shoot
Shell, therefore, what Fig. 1 was shown is also bamboo shoot shell comprehensive processing and utilization method.
Fig. 1 shows that bamboo shoot shell comprehensive processing and utilization method includes: to squeeze to bamboo shoot shell, to isolate bamboo shoot shell juice and consolidate
Body substance；Then, first is carried out to bamboo shoot shell juice to utilize；Later, solid matter is isolated into bamboo shoot shell particulate and bamboo shoot shell fiber；This
Afterwards, second is carried out to bamboo shoot shell particulate to utilize, third utilization is carried out to bamboo shoot shell fiber.
Bamboo shoot process residue abundance, as previously described, there are about 70% parts by conduct sometimes for a bamboo shoots
The bamboo shoot process residue of leftover bits and pieces and be dropped.Therefore, it in all kinds of bamboo shoots source places or bamboo shoot process place, can collect
To a large amount of bamboo shoot process residue.Also, all kinds of bamboo (phyllostachys bambusoides, sinocalamus latiflorus, green bamboo, black bamboo, bitter bamboo, Jiangnan bamboo, broken bamboos, mountain
Ridge bamboo and mangosteen), it may be suitable for comprehensive processing and utilization method of the invention.
Before squeezing bamboo shoot process residue, (clean) first can be cleaned to bamboo shoot process residue, with removal
The impurity being mingled in collected bamboo shoot process residue, such as weeds, sandstone and soil.Cleaning can carry out once, can also
It is multiple to carry out.Cleaning is bamboo shoot process residue juice, bamboo shoot process residue particulate and the bamboo of subsequent production in order to prevent
Bamboo shoot industrial wood waste fiber has unwanted impurity.Such as to advantageously reduce bamboo shoot process residue juice, bamboo shoot process surplus
Micro organism quantity in excess particulate and bamboo shoot process residue fiber, delays corruption, or prevents bamboo shoot process residue thin
Grain is with inorganic impurity without pure.
In some embodiments, the mode squeezed to the bamboo shoot process residue can be concora crush mode, extruding
Mode rolls mode.Corresponding to above-mentioned various squeezing modes, the squeezer accordingly used can be belt-type horizontal squeezer,
It is also possible to piston type squeezer, can also be expeller.In some instances, sugar-cane press can be directly used
Accordingly squeezed.
But in general, the squeezing to bamboo shoot process residue, preferably uses concora crush mode to carry out, belt-type horizontal pressure is used accordingly
Crusher, this helps to protect the bigger bamboo shoots industrial wood waste fiber of more multiple-length.Certainly, the mode rolled is also ideal
, this mode is equally smaller to the destruction of bamboo shoot process residue fiber.
Meanwhile in some embodiments, two ways can be incorporated, i.e., is carried out in such a way that pressure and stone roller combine
Squeezing, this is communicated with the subsequent gradually boosting squeezing mentioned, and such operation, further effect contributes to bamboo shoots and adds
The dehydration of work residue is squeezed the juice, and more bamboo shoot process residue juice are obtained, also in some embodiments, it is subsequent obtain it is more dry
Dry bamboo shoot process residue particulate and bamboo shoot process residue fiber provides condition.
Wherein, the bamboo shoot process residue is squeezed, can be carried out under normal temperature and pressure (referring to air pressure).At this time may be used
To find, in method of the invention, corresponding bamboo shoot process residue does not need other any special places in addition to necessary cleaning
Reason.Due to being to carry out squeezing processing under conditions of room temperature, even more heat without heating or in advance and etc., therefore,
Energy consumption is more saved, technique is simplified.
In order not to destroy bamboo shoot process residue fiber, in some embodiments, the bamboo shoot process residue is pressed
The pressure range used is squeezed to control in 15MPa~150MPa.The pressure of squeezing need to enable to the rupture of bamboo shoot process residue to release
Juice is released, simultaneously as the present invention is subsequent will to be made full use of bamboo shoot process residue fiber (in some scenarios, bamboo shoots add
Work residue fiber keeps long length to be advantageous as far as possible).Therefore, the pressure particularly used squeezing is controlled and is adjusted
It is whole.Research by inventor to finally obtained bamboo shoot process residue fiber, and combine each factor in the present invention
With condition (pressure range etc. as being realized can squeezer), pressure is arranged in corresponding OK range the present invention.
In some embodiments, in squeezing, although the pressure of use is controlled in above-mentioned respective range, in order to more
It realizes well and squeezes out to bamboo shoot process residue juice, can be squeezed in such a way that pressure is stepped up, and using multiple
The mode taken, corresponding bamboo shoot process residue juice to be squeezed out as best one can.
Squeezing mode above-mentioned is the loading angle analysis from bamboo shoot process residue when being squeezed process.Such as
Whether fruit is from additional liquid (such as water) angle analysis is added, and in some embodiments, corresponding squeezing preferentially can be using dry
Squeezing method carries out, that is, does not need that other liquid are additionally added, so that it may be squeezed accordingly.
The solid matter is isolated into the bamboo shoot process residue particulate and the bamboo shoot process residue fiber package
It includes: the solid matter being carried out to rub silk；Screening separation is carried out, later to isolate the bamboo shoot process residue particulate and institute
State bamboo shoot process residue fiber.Therefore, rubbing silk and screening is the step for further separating the ingredient of the solid matter
Suddenly.
Specific a kind of process for rubbing silk and screening, as shown in Figure 1, solid matter is isolated bamboo shoot shell particulate and bamboo shoot shell fibre
The step of dimension includes: to carry out rubbing silk to the solid matter；Screening separation is carried out, later to isolate the bamboo shoot shell particulate and institute
State bamboo shoot shell fiber.
As previously mentioned, bamboo shoot head is the bamboo shoot process lower end aging part to be cut off.Since bamboo shoot head radical length is smaller, institute
After rubbing silk or crush, the fibre length that bamboo shoot head obtains is usually smaller than the fibre length that bamboo shoot shell obtains.
Correspondingly, the process for rubbing silk is usually by the way that by solid matter to be processed, (bamboo shoot process is remaining in some embodiments
Solid dried object after object squeeze juice) be delivered to wire kneading machine rub broken room, rubbed broken indoor high rotation hammer leaf and rubbing plate phase
Interaction, solid matter is rubbed broken, achievees the purpose that separation of material.
It should be noted that the process for rubbing silk has hammer leaf to two effects of the strike of corresponding material and rubbing.In order to guarantee
Longer fiber is finally obtained, it is more preferable using the effect for rubbing silk.But in some embodiments, using general grinding mode,
Respective fiber and particle can also be allowed to separate, grinding mode is only used, be likely to result in the fracture of more multifilament.
After rubbing silk, corresponding solid matter is separated into bamboo shoot process residue particulate and bamboo shoot process residue fiber
Dimension.But separation at this time, the not separation of real meaning, they are still to mix, only from original organic one
Body structure becomes silk (fiber) grain (particulate grain) mixing at this time.This mixture mixed, subsequent needs pass through
Screening can separate.
In some embodiments, said mixture can be sieved with corresponding screening plant, such as the sieve of certain mesh number
Subnetting screening.Since the technique of front ensure that bamboo shoot process residue fiber maintenance is stayed more intact, bamboo shoot process is surplus
Excess fiber has been able to maintain certain length, and this facilitates corresponding screening process and is easier to carry out.
In one embodiment, can it is described rub silk after, be first dried, after the drying, then carry out screening point
From.It should be noted that drying herein is a special drying: although the squeezing of front, as far as possible by bamboo shoot process
Residue juice is squeezed out, thus separated with solid matter, but solid matter inevitably also has a certain amount of moisture, because
This, carries out this drying, precisely in order to being further reduced the moisture in respective mixtures.
In one embodiment, corresponding screening separation can specifically use vibrosieve, can be using corresponding vibration
Screening plant carries out, and the powder sieved is corresponding bamboo shoot process residue particulate, and the part not leaked out above,
It is then bamboo shoot process residue fiber.Bamboo shoot process residue particulate and bamboo shoot process residue fiber can be collected respectively,
It is utilized with carrying out subsequent corresponding second using with third.
It should be noted that in another embodiment, it is thin that the solid matter is isolated the bamboo shoot process residue
Grain and the bamboo shoot process residue fiber include: to carry out rubbing silk to the solid matter；It is described rub silk after, in the solid
Water is added in substance, forms the mixture of flowable state；Screening separation is carried out to the mixture, to isolate the bamboo shoots
Industrial wood waste particulate and the bamboo shoot process residue fiber.This mode needs in the follow-up process, then is separated from the water
Bamboo shoot process residue particulate out, and dried accordingly.It, can also be using other particulates and fibre in other embodiments
The separation method of dimension.
In some embodiments, it may include following several for utilizing to described the first of the bamboo shoot process residue juice
Using at least one: as mushroom culture solution, for extracting vegetable protein, for extracting polysaccharide, for extracting bamboo shoots
Industrial wood waste pigment and for extracting tabasheer ketone.The comprehensive processing and utilization side of the subsequent bamboo shoot process residue juice of this specification
Method, to mushroom culture solution, the first benefit extracted vegetable protein, extract polysaccharide, extraction bamboo shoot process residue pigment and tabasheer ketone
With being illustrated using corresponding some specific examples.
As previously mentioned, bamboo shoot shell is the part outside bamboo shoots.It, may be through before bamboo shoot shell and bamboo shoot meat separation during bamboo shoot process
Boiling is crossed, this bamboo shoot shell by preparatory boiling, subsequent to squeeze in resulting juice juice, protein content can reduce.
It, can (bamboo shoots refer at least part of with bamboo shoot shell and bamboo shoot head herein by boiling bamboo shoots in some embodiments
Bamboo shoots) resulting cooking liquor also carries out subsequent corresponding first and utilizes as bamboo shoot process residue juice.Specifically, can be with
Bamboo shoots are subjected to boiling, obtain cooking liquor；From the bamboo shoots after boiling, bamboo shoot process residue is isolated；To the bamboo
Bamboo shoot industrial wood waste is squeezed, to isolate bamboo shoot process residue juice and solid matter；It is remaining to the bamboo shoot process
Object juice carries out first and utilizes；The solid matter is isolated into bamboo shoot process residue particulate and bamboo shoot process residue fiber
Dimension；Second is carried out to the bamboo shoot process residue particulate to utilize；Third utilization is carried out to the bamboo shoot process residue fiber；
Also, by the cooking liquor, it is also used as the bamboo shoot process residue juice, described first is carried out and utilizes.
In some embodiments, utilizing also to described the first of the bamboo shoot process residue juice may include: to institute
It states bamboo shoot process residue juice to ferment, the bamboo shoot process residue juice after the fermentation is used to prepare plant
The nutrient solution of culture.In specific example, can use bioactivity yeast generates bamboo shoot process residue juice containing ethyl alcohol
Fermented liquid；The corresponding fermented liquid (bamboo shoot process residue juice) for including at least bioactivity yeast is re-introduced into curing
Container, and ferment the corresponding time.Later, the liquid after fermentation, so that it may as nutrient solution, be cultivated for plant.
In some embodiments, described first using also may include: to send out the bamboo shoot process residue juice
The bamboo shoot process residue juice after the fermentation is used for as liquid fertilizer of plant, such as orchid fertilizer etc. by ferment.
In some embodiments, it may include following several for utilizing to described the second of the bamboo shoot process residue particulate
Using at least one: as feed, as organic fertilizer fermentation raw material, and as mushroom planted medium ingredient.
In some embodiments, utilizing to described the second of the bamboo shoot process residue particulate also may include: to be used as
Produce the raw material of functional sugar, microcrystalline cellulose or dietary fiber；Alternatively, being used as the inducer of production cellulase zytase.
Bamboo shoot process residue particulate includes the ingredients such as cellulose and hemicellulose, and cellulose and hemicellulose are micro-organisms fibres
The inducer of plain enzyme and zytase is tieed up, while being also the carbon source of micro-organisms cellulase and zytase., can be used to
Produce the inducer of cellulase and hemicellulase.
In some embodiments, utilizing to the third of the bamboo shoot process residue fiber includes adding the bamboo shoots
Work residue fiber Wesy is at least one for making following product: making in make mattress, rope, does the wash apparatus (such as kitchen
Cleaning ball), wood plastic composite, antibacterial insoles, headrest, pillow, textile material (garment material), paper i.e. by bamboo shoot process residue
Fibres be used for papermaking, such as making speciality paper), special fibre.
Bamboo shoot process residue fiber has good gas permeability, instant water absorption, stronger wearability and good dye
The characteristics such as color have natural antibacterial, antibacterial, anti-mite, deodorization and anti-ultraviolet function.Therefore, bamboo shoot process residue is utilized
Fiber, which makes mattress, has good market.Meanwhile bamboo shoot process residue fiber can make bed together with other materials
Pad, for example, the coconut palm palm fibre of a part, the common mattress for making respective performances can be added in bamboo shoot process residue fiber.
When bamboo shoot process residue fiber is as textile material, bamboo shoot process residue fiber usually requires advanced traveling one
The processing of step., can be blended with the progress of cotton, hair, fiber crops, thin,tough silk and chemical fibre after processing, for woven or knitting.And bamboo shoot process
Residue fiber yarn can be used for summer sleeping mat, sheet, curtain, scarf etc., such as frivolous using that can produce with the blended method of polyvinyl
Garment material.
Further, bamboo shoot process residue fiber can produce the woven fabric and knitting fabric of various specifications.It is woven
Fabric can be used for making curtain, jacket, easy dress, Western-style clothes suit, shirt, sheet and towel, bath towel etc..Being knitted fabric is suitable for
Make underwear, undershirt, T-shirt, socks etc..
Bamboo shoot process residue fiber Wesy is in papermaking, such as production speciality paper, including is used for bamboo shoot process residue fiber
Paper handkerchief manufacture also includes the manufacture for the paper such as painting and calligraphy (similar to rice paper), and use bamboo shoot process residue fiber for
The bamboo shoot process residue fiber unbleached paper towel of the health environment-friendly of raw material has good service performance, and to environment friend
It is good.
Bamboo shoot process residue comprehensive processing and utilization method provided by the invention carries out comprehensive add to bamboo shoot process residue
Work and utilization, it is thin gradually to isolate bamboo shoot process residue juice, bamboo shoot process residue for the ingredient of bamboo shoot process residue
Grain and bamboo shoot process residue fiber, then carry out valuable comprehensive utilization respectively, realize to bamboo shoot process residue
Reasonable utilization makes bamboo shoot process residue become raw material from waste material, reduces bamboo shoot process residue and discharges the dirt caused by environment
Dye, also, the case where basically reaching no any trash discharge in the process is processed, it has taken into account economic interests and environment is protected
Shield.
The present invention also provides a kind of bamboo shoot process residue juice comprehensive processing and utilization method.
The described method includes: being squeezed to the bamboo shoot process residue such as bamboo shoot shell or bamboo shoot head, to isolate bamboo shoot process
Residue juice and solid matter；Then, with the bamboo shoot process residue sap extraction bamboo shoot process residue crude protein (one
Kind vegetable protein).
In further embodiments, the method is also possible to include: to carry out boiling to bamboo shoots, cooking liquor is obtained, by institute
Cooking liquor is stated as bamboo shoot process residue juice；Then, remaining with the bamboo shoot process residue sap extraction bamboo shoot process
Object crude protein.The reason of carrying out boiling to bamboo shoots can refer to foregoing teachings.
It should be noted that solid matter is the solid slag part after corresponding squeezing, it usually still remains with one
Determine moisture, only moisture content is usually very low.
Wherein, may include: with the bamboo shoot process residue sap extraction bamboo shoot process residue crude protein will be described
Bamboo shoot process residue juice obtains the first filtrate and bamboo shoot process residue particulate through 20-200 mesh plate-frame filtering；It will be described
First filtrate carries out micro-filtration, obtains the second filtrate and bamboo shoot process residue particulate；Second filtrate is passed through into ultrafiltration membrane mistake
Filter concentration (realizes concentration by filtering), obtains third concentrate and third filter liquor；The third concentrate is centrifuged
Or filtering, it is separated by solid-liquid separation with realizing, to obtain the 4th liquid and bamboo shoot process residue crude protein.
In some embodiments, the third filter liquor can be used for the component as mushroom culture medium.
It in some embodiments, can be dense by the third before the third concentrate is centrifuged or is filtered
Contracting liquid is heated to 70-100 DEG C, keeps the temperature 0-30min, is cooled to 40 DEG C hereinafter, precipitating；Described in the precipitating and then progress
Centrifugation or filtering.
In some embodiments, corresponding comprehensive processing and utilization method further includes that the 4th liquid is obtained the through micro-filtration
Five filtrates and bamboo shoot process residue crude protein；5th clear liquid by ultrafiltration membrance filter be concentrated, obtain the 6th concentrate and
6th filter liquor；It is the 66-80% (body of ethyl alcohol upon mixing that ethyl alcohol to volume fraction of ethanol is added in the 6th concentrate
Volume fraction in system is 66-80%, can be directly added into high concentration ethanol, such as straight alcohol, then adjust to corresponding concentration)；
It is separated by solid-liquid separation by being centrifuged or filtering, collects sediment；The sediment is the ethyl alcohol of 66%-80% with volume fraction
(this ethyl alcohol can be with high concentration ethanol through overregulating to obtain) is washed, and bamboo shoot process residue polysaccharide is obtained.Certainly, may be used
First directly to add corresponding high concentration ethanol (such as straight alcohol) in sediment, then adds corresponding water adjustment and add so that being equivalent to
Enter the ethyl alcohol that volume fraction is 66%-80%, is washed；But be directly added into volume fraction be 66%-80% ethyl alcohol into
Row washing effect is more preferably.
In some embodiments, the third filter liquor and the 6th filter liquor can be concentrated by nanofiltration membrane, is obtained
Obtain the 7th concentrate and the 7th filter liquor；7th filter liquor is dried, bamboo shoot process residue pigment is obtained.
It in some embodiments, can be spray drying to the drying that the 7th concentrate carries out.
In some embodiments, the 7th filter liquor can be concentrated through reverse osmosis membrane filtration, and by polar macroporous
Resin adsorption obtains the eluent containing flavones by ethanol elution later, evaporates the eluent and obtain tabasheer ketone.This technique
Under, the ethyl alcohol in the eluent can be recycled in evaporation process.
As shown in Fig. 2, this specification is specifically further described by taking bamboo shoot shell juice comprehensive processing and utilization method as an example, institute
The method of stating includes:
Bamboo shoot shell is squeezed, to isolate bamboo shoot shell juice and solid matter；Corresponding expressing process can refer to aforementioned
Fig. 1 corresponding contents；
With the bamboo shoot shell sap extraction bamboo shoot shell crude protein (this is a kind of specific and first utilizes)；
It include multiple steps with the bamboo shoot shell sap extraction bamboo shoot shell crude protein, specific as follows:
By the bamboo shoot shell juice through 80 mesh plate-frame filterings, the first filtrate and bamboo shoot shell particulate are obtained (to the second of bamboo shoot shell particulate
Using previous embodiment corresponding contents can be referred to)；
First filtrate is subjected to micro-filtration, (utilizing to the second of bamboo shoot shell particulate can for the second filtrate of acquisition and bamboo shoot shell particulate
To refer to previous embodiment corresponding contents)；
Second filtrate is concentrated by ultrafiltration membrance filter, obtains third concentrate and third filter liquor；In some realities
It applies in example, the molecular cut off of used ultrafiltration membrane is 3kd-30kd；In some embodiments, it can be concentrated with ultrafiltration membrane
After 2-5 times, add water in concentrate, then be concentrated, the step for be in order to clean, further to remove impurity；
The third concentrate is centrifuged or is filtered, is separated by solid-liquid separation with realizing, to obtain the 4th liquid and bamboo shoot shell
Crude protein.It after bamboo shoot shell crude protein is separated, can be dried, in order to more preferably save.
Wherein, bamboo shoot shell crude protein refers to that (bamboo shoot shell crude protein is in solid matter to protein content in 30% to 80% composition
Non-fiber part).And can be made in bamboo shoot shell crude protein using the method for the present invention, the content of albumen may be up to 70-
80%.Bamboo shoot shell crude protein is not reach very pure degree not by being further purified, and directly utilization at this time can be with
It is the raw material as feed.However, bamboo shoot shell crude protein can also according to subsequent actual product needs, be further processed (including
Purification), being made as food, perhaps health care product (vegetable protein health care product) can also be directly as animal feed or as animal
The adding ingredient etc. of feed.
As shown in Fig. 2, the third filter liquor can be used for the component as mushroom culture medium.
It should be noted that the process that third concentrate is centrifuged or is filtered can be to make third that liquid precipitate, In be concentrated
1-10 times of clear water mixing is added in precipitating, refilters or is centrifuged, and repeat corresponding operating 1-3 times, the solid collected, institute
Stating solid is bamboo shoot process residue crude protein.
As shown in Fig. 2, the third concentrate can be added before the third concentrate is centrifuged or is filtered
Heat keeps the temperature 0-30min to 70-100 DEG C, is cooled to 40 DEG C hereinafter, precipitating；It is described precipitating and then carry out it is described centrifugation or
Filtering.Heating including is preferably precipitated after making some albuminous degenerations for preferably protein precipitation.And the cooling after heating,
It is to precipitate corresponding solid completely as far as possible, it is easier to separate.
As shown in Fig. 2, the comprehensive processing and utilization method can also include that the 4th liquid is obtained the 5th through micro-filtration
Filtrate and bamboo shoot shell crude protein.As it can be seen that this step can further obtain corresponding bamboo shoot shell crude protein.
5th clear liquid is concentrated by ultrafiltration membrance filter, obtains the 6th concentrate and the 6th filter liquor.Surpass in this step
The molecular cut off of filter membrane is similarly 3kd-30kd, also, equally can after being concentrated 2-5 times using ultrafiltration membrane, add water to
In concentrate, then it is concentrated again.
It is 66-80% that ethyl alcohol to volume fraction of ethanol is added in the 6th concentrate.
It is separated by solid-liquid separation by being centrifuged or filtering, collects sediment.
The sediment obtains bamboo shoot shell polysaccharide (this with the ethanol washing (washing times can be for 2-5 times) of 66%-80%
It is another specific and the first utilization).Bamboo shoot shell polysaccharide can be used for the ingredient of corresponding health care product, or directly as health care product,
It has anti-oxidant, anti-aging, antitumor and raising immunity (immunological regulation) and other effects, is a kind of biological function macromolecular.
As shown in Fig. 2, the third filter liquor and the 6th filter liquor can also be concentrated by nanofiltration membrane, the is obtained
Seven concentrates and the 7th filter liquor；7th filter liquor is dried, obtain bamboo shoot shell pigment (this be it is another specifically and the
One utilizes).
Bamboo shoot shell pigment is natural pigment, can be used as the purposes such as food additives.
Correspondingly, nanofiltration membrane have filtering and concentrating effect (i.e. by a part moisture filter, be retained in film it is corresponding at
For concentrate), in some embodiments, it can use it and realize that concentration is 2-10 times of concentration.
It should be noted that third filter liquor and the 6th filter liquor can be and mix and then pass through nanofiltration membrane
Filtering and concentrating, for obtaining bamboo shoot shell pigment；Third filter liquor and the 6th filter liquor can also respectively carry out corresponding nanofiltration
Film filtering and concentrating (filtering and concentrating) can refer to shown in Fig. 2 respectively for bamboo shoot shell pigment is obtained.
As shown in Fig. 2, the 6th filter liquor adds in addition to third filter liquor and the 6th filter liquor can be used for obtaining bamboo shoot shell pigment
Enter ethyl alcohol to be centrifuged or filtered again, and corresponding filtrate, it can equally mix to the 6th filter liquor, it is dense by nanofiltration membrane
Contracting is used further to obtain bamboo shoot shell pigment.
In addition, the 6th filter liquor is also washed after above-mentioned centrifugation or filtering, specifically can be ethanol washing, washed
The liquid for washing out can equally be mixed to the 6th filter liquor, be used further to obtain bamboo shoot shell pigment by nanofiltration membrane concentration.
As shown in Fig. 2, being spray drying to the drying that the 7th concentrate carries out.Spray drying is to bamboo shoot shell obtained
The form and quality of pigment are advantageous.
7th filter liquor is concentrated through reverse osmosis membrane (RO film), and by polar macroporous resin adsorption, passes through second later
Alcohol elution obtains the eluent containing flavones, evaporate the eluent obtain tabasheer ketone (this be it is another specifically and the first benefit
With).
Tabasheer ketone can also serve as food additives, or ingredient or independent health care product as health care product.Tabasheer ketone
With functions such as anti-oxidant and anti-corrosions.
In some embodiments, reverse osmosis membrane filtration concentration is also possible to be concentrated to 2-5 times of concentration.
In some embodiments, the ethyl alcohol in the eluent can be recycled in the evaporation process.
In other embodiments, corresponding bamboo shoot process residue juice comprehensive processing and utilization method, is also possible to
The following steps are included: squeezed to bamboo shoot process residue, with isolate bamboo shoot process residue juice and solid matter (or
Person carries out boiling to bamboo shoots, cooking liquor is obtained, using the cooking liquor as bamboo shoot process residue juice)；The bamboo shoots are added
Work residue juice is as mushroom culture solution to produce bacteria cellulose；Using the bamboo shoot process residue juice as the bacterium
Class culture solution includes: that sugar or molasses are added to concentration in the bamboo shoot process residue juice to produce the bacteria cellulose
(mass percentage concentration) 2-5% is added potassium ion to molar concentration 1.26-2.52mmol/L, phosphate anion (phosphate radical is added
Ion is to be referred to as, it includes phosphate anion, phosphoric acid hydrogen radical ion and dihydrogen phosphate ions) to molar concentration 0.63-
Sulfate ion is added to mass percentage concentration 0.073-0.292% (mass percentage concentration) in 1.26mmol/L, be added ammonium root from
Son forms mixing liquid to mass percentage concentration 0.027-0.108% (mass percentage concentration)；With alkali, basic anhydride, alkalinity
Carbonate or bicarbonate adjust the pH value of the mixing liquid to 3-6, become the mushroom culture solution；To the mushroom culture
Liquid accesses mushroom；25-40 DEG C standing for fermentation 2-5 days, obtain the bacteria cellulose.
Specifically, the mushroom can be acetic acid bacteria category, gluconobacter suboxydans category, gluconic acid Acetobacter, grape glycosyloxy
Change bacillus, rhizobium, Sarcina, pseudomonas, achromobacter, Alcaligenes, Aerobacter, azotobacter,
One or more of Agrobacterium, onion pseudomonas sp, campylobacter jejuni, gluconate pyracetobacillus.
Specifically in bamboo shoot shell juice comprehensive processing and utilization method, for be illustrated, one of which includes: to bamboo shoot using method
Shell is squeezed, and (alternatively, the bamboo shoots with bamboo shoot shell are carried out boiling, obtains boiling to isolate bamboo shoot shell juice and solid matter
Liquid, using the cooking liquor as bamboo shoot process residue juice；Again or will only be bamboo shoot meat bamboo shoots carry out boiling, obtain boiling
Liquid, using the cooking liquor as bamboo shoot process residue juice)；Using the bamboo shoot shell juice as mushroom culture solution to produce bacterium
Cellulose；It includes: that sugar is added in the bamboo shoot shell juice that the bamboo shoot shell juice, which is produced bacteria cellulose as mushroom culture solution,
Or molasses are added potassium ion to concentration 0.0585g/L (1.5mmol/L), phosphate anion are added to concentration to concentration 3%
0.080g/L (1.0mmol/L) is added sulfate ion to concentration 0.290%, ammonium ion is added to concentration 0.100%, shape
At mixing liquid；The pH value of the mixing liquid is adjusted to 5 with alkali, basic anhydride, basic carbonate or bicarbonate；To institute
After stating mixing liquid progress high-temperature sterilization, mushroom is accessed；It is left to ferment 3 days at 30 DEG C, it can obtain corresponding bacterial fibers
Element.
It should be noted that in the aforementioned method that the bamboo shoot shell juice is produced bacteria cellulose as mushroom culture solution
In the process, high-temperature sterilization can not also be carried out to the mixing liquid, because, in some cases without high-temperature sterilization, favorably
The microorganism assisted fermentation present in the certain environment of utilization.
In further embodiments, the concentration of sugar or molasses is added in the bamboo shoot shell juice is preferably 4-5%, and bamboo shoot shell juice contains
Sugar amount is lower, and more sugar or molasses is preferably added.In the prior art, culture bacteria cellulose may using coconut water or
Fruit syrup etc., in contrast, higher cost, and in the application is relatively inexpensive using bamboo shoot shell juice, it is only necessary to pass through for these methods
Appropriate same cheap sugar or molasses is added, the good culture to bacteria cellulose may be implemented, therefore, has preferably economical
Benefit and market prospects, are more worthy to be popularized.
In some embodiments, the molar concentration of potassium ion and phosphate anion can be correspondingly, as potassium ion mole be dense
Degree is twice of phosphoric acid hydrogen radical ion molar concentration, at this point it is possible to by the way that K is added2HPO4To realize.
In further embodiments, sulfate ion is added to concentration 0.210%, ammonium ion is added to concentration
0.050%, form mixing liquid.Likewise, at this point it is possible to realizing the addition of both ions by the way that ammonium sulfate is added.
The pH value of the mixing liquid is adjusted to 5 with alkali, basic anhydride, basic carbonate or bicarbonate, specifically,
PH value is adjusted using sodium hydroxide；After carrying out high-temperature sterilization to the mixing liquid, mushroom is accessed；3 are left to ferment at 30 DEG C
It, it can obtain corresponding bacteria cellulose.
In some embodiments, it is also possible to alkali, basic anhydride, basic carbonate or bicarbonate, to adjust pH value.
It should be noted that in each step of bamboo shoot process residue juice comprehensive processing and utilization method, either its
In the liquid that generates of which procedure of processing, may be used to nutrient media components, with fermented-producing bacteria cellulose, or for making
Standby plant culture solution, or for as liquid fertilizer etc..Wherein, some liquid are used directly for nutrient media components, some
Liquid is then to be used for nutrient media components after isolating corresponding other ingredients.
As shown in the above, bamboo shoot process residue itself is relatively inexpensive, and therefore, bamboo shoot process residue juice is also honest and clean
Valence, and the comprehensive processing and utilization method, can make bamboo shoot process residue juice (bamboo shoot shell juice) turn waste into wealth.Although some
In embodiment, bamboo shoot process residue all kinds of embodiment steps of juice comprehensive processing and utilization method and operation are different, still, various
Specific method is still that corresponding juice can be fully utilized, and can be realized zero-emission, therefore, still taken into account economic interests and
Environmental protection.
Although present disclosure is as above, present invention is not limited to this.Anyone skilled in the art are not departing from this
It in the spirit and scope of invention, can make various changes or modifications, therefore protection scope of the present invention should be with claim institute
Subject to the range of restriction.
Claims (10)
1. a kind of bamboo shoot process residue juice comprehensive processing and utilization method characterized by comprising
Bamboo shoot process residue is squeezed, to isolate bamboo shoot process residue juice and solid matter；Alternatively, to bamboo shoots
Boiling is carried out, cooking liquor is obtained, using the cooking liquor as bamboo shoot process residue juice；
With the bamboo shoot process residue sap extraction bamboo shoot process residue crude protein；
The bamboo shoot process residue crude protein described in the bamboo shoot process residue sap extraction includes:
By the bamboo shoot process residue juice through plate-frame filtering, the first filtrate and bamboo shoot process residue particulate are obtained；
First filtrate is subjected to micro-filtration, obtains the second filtrate and bamboo shoot process residue particulate；
Second filtrate is concentrated by ultrafiltration membrance filter, obtains third concentrate and third filter liquor；
The third concentrate is centrifuged or is filtered, is separated by solid-liquid separation with realizing, to obtain the 4th liquid and bamboo shoot process
Residue crude protein.
2. bamboo shoot process residue juice comprehensive processing and utilization method as described in claim 1, which is characterized in that by described
Three filter liquors are for the component as mushroom culture medium.
3. bamboo shoot process residue juice comprehensive processing and utilization method as claimed in claim 2, which is characterized in that will be described
Before third concentrate is centrifuged or is filtered, the third concentrate is heated to 70-100 DEG C, keeps the temperature 0-30min, it is cooling
To 40 DEG C hereinafter, precipitating；In the precipitating and then carry out the centrifugation or filtering.
4. bamboo shoot process residue juice comprehensive processing and utilization method as claimed in claim 3, which is characterized in that further include by
4th liquid obtains the 5th filtrate and bamboo shoot process residue crude protein through micro-filtration；
5th clear liquid is concentrated by ultrafiltration membrance filter, obtains the 6th concentrate and the 6th filter liquor；
It is 66-80% that ethyl alcohol to volume fraction of ethanol is added in the 6th concentrate；
It is separated by solid-liquid separation by being centrifuged or filtering, collects sediment；
The sediment ethanol washing obtains bamboo shoot process residue polysaccharide.
5. bamboo shoot process residue juice comprehensive processing and utilization method as claimed in claim 4, which is characterized in that by described
Three filter liquors and the 6th filter liquor are concentrated by nanofiltration membrane, obtain the 7th concentrate and the 7th filter liquor；By the described 7th
Filter liquor is dried, and obtains bamboo shoot process residue pigment.
6. bamboo shoot process residue juice comprehensive processing and utilization method as claimed in claim 5, which is characterized in that described
The drying that seven concentrates carry out is spray drying.
7. bamboo shoot process residue juice comprehensive processing and utilization method as claimed in claim 5, which is characterized in that the described 7th
Filter liquor is concentrated through reverse osmosis membrane filtration, and by polar macroporous resin adsorption, contains flavones by ethanol elution acquisition later
Eluent, evaporate the eluent and obtain tabasheer ketone.
8. bamboo shoot process residue juice comprehensive processing and utilization method as claimed in claim 7, which is characterized in that in the steaming
During hair, the ethyl alcohol in the eluent is recycled.
9. a kind of bamboo shoot process residue juice comprehensive processing and utilization method characterized by comprising
Bamboo shoot process residue is squeezed, to isolate bamboo shoot process residue juice and solid matter；Alternatively, to bamboo shoots
Boiling is carried out, cooking liquor is obtained, using the cooking liquor as bamboo shoot process residue juice；
Using the bamboo shoot process residue juice as mushroom culture solution to produce bacteria cellulose；
Include: to produce the bacteria cellulose using the bamboo shoot process residue juice as the mushroom culture solution
Sugar or molasses is added to mass percentage concentration 2-5% in the bamboo shoot process residue juice, be added potassium ion to mole
Concentration 1.26-2.52mmol/L is added phosphate anion to molar concentration 0.63-1.26mmol/L, sulfate ion is added extremely
Mass percentage concentration 0.073-0.292% is added ammonium ion to mass percentage concentration 0.027-0.108%, forms mixed liquor
Body；
The pH value for adjusting the mixing liquid with alkali, basic anhydride, basic carbonate or bicarbonate becomes described to 3-6
Mushroom culture solution；
Mushroom is accessed to the mushroom culture solution；
25-40 DEG C standing for fermentation 2-5 days, obtain the bacteria cellulose.
10. bamboo shoot process residue juice comprehensive processing and utilization method as claimed in claim 9, which is characterized in that the bacterium
Class is acetic acid Pseudomonas, gluconobacter suboxydans category, gluconic acid Acetobacter, glucose oxidation and bacillus, rhizobium, sarcine
Category, pseudomonas, achromobacter, Alcaligenes, Aerobacter, azotobacter, Agrobacterium, Pseudomonas cepacia
One or more of category, campylobacter jejuni, gluconate pyracetobacillus.
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