CN103919267B - A kind of preparation method of novel tobacco goods - Google Patents
A kind of preparation method of novel tobacco goods Download PDFInfo
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- CN103919267B CN103919267B CN201410120206.8A CN201410120206A CN103919267B CN 103919267 B CN103919267 B CN 103919267B CN 201410120206 A CN201410120206 A CN 201410120206A CN 103919267 B CN103919267 B CN 103919267B
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Abstract
The invention discloses a kind of preparation method of novel tobacco goods.The present invention is coated with a kind of new coating fluid on the reconstituted tobacco paper substrate of punching, obtain and specifically raw tobacco material is rolled into cigarette bundle, control described cigarette Shu Jinhang suction fuel, pumping velocity is kept to be at the uniform velocity and cigarette Shu Jinliang minimizing is glowed, collect gas gas-phase objects and the granule phase substance of main flume respectively, by by collect after the gas gas-phase objects condensation that obtains with granule phase substance composition mixture, using mixture as coating solution on reconstituted tobacco paper substrate, directly roll after drying and obtain described novel tobacco goods.The present invention is based on traditional tobacco planting industry growth requirement, set about from change traditional cigarette production technology, by conventional cigarette " burning during use ", advance to and carry out in the preparation process of cigarette, burning and sucking in cigarette consumption process can be effectively reduced based on the present invention, " second-hand-cigarette " that remarkable minimizing side-stream smoke brings, also provides technical foundation for meeting the demand of people to cigarette charm to a greater degree simultaneously.
Description
Technical field
The present invention relates to the preparing technical field of tobacco product, more specifically, relate to a kind of preparation method of novel tobacco goods.
Background technology
Cigarette is modal one in tobacco product.Although cigarette exists certain harmfulness to health, be still subject to liking of many people.
Its manufacturing process of existing cigarette roughly will through the technological process of production of tobacco first baking, beating and double roasting, tobacco fermentation, cigarette composition, cigarette primary processing, cigarette bundle system volume, cigarette package seven sports.The trial test method of cigarette burns and sucks.In the process that cigarette burns and sucks, complicated chemical change and physical change can be produced, generate thousands of kinds of original non-existent flavor matters in tobacco material, form the distinctive charm of cigarette.Cigarette can produce main flume and side-stream smoke in the process burnt and sucked because the burning of cigarette is very complicated physics, a chemical change process, cigarette burn and suck the material composition generated in process not exclusively behave understand and control.
Cigarette can produce main flume and side-stream smoke in the process burnt and sucked, the flue gas of the filter end sucking-off from cigarette during suction is called main flume (MainstreamSmoke, be called for short MS), suction gap discharges from fire end and the flue gas that spreads direct entered environment through cigarette paper is called side-stream smoke (SidestreamSmoke is called for short SS).Containing the material harmful to person health in main flume, as the material such as polycyclic aromatic hydrocarbon, free radical, there are some researches show, in side-stream smoke, contained harmful substances is far above main flume, therefore smoking is except harm smoker health, the passive suction side-stream smoke of people around, health also suffers damage.
In order to ensure the health of people, occur the substitute products of some cigarettes, as electronic cigarette; The principle of electronic cigarette is stored in cigarette bullet nicotine and a small amount of aroma component, then gasified out by modes such as heating.Although electronic cigarette can imitate the taste of cigarette to a certain extent, even can be changed by formula adjustment and more taste, but the charm due to cigarette is by the result of thousands of kinds of flavor matter comprehensive functions, the artificial formula of electronic cigarette cannot the charm of real simulation cigarette, therefore electronic cigarette and the actual of smoking experience difference still comparatively greatly, and this series products fails to obtain good effect.In prior art, people will obtain the distinctive charm of cigarette, just cannot invariably need by burning and sucking, and this just invariably cannot bring larger negative effect to health of people.
Meanwhile, the outward appearance of the products such as existing electronic cigarette differs comparatively large with cigarette, be also difficult to the favor obtaining consumer.Prepare a kind of not burning cigarette with cigarette outward appearance, there is practical significance.
Summary of the invention
The object of the invention is to overcome the deficiencies in the prior art, a kind of preparation method of novel tobacco goods is provided.The method has broken technical thought prepared by traditional cigarette, the process that burns and sucks of cigarette is completed in advance in the preparation process of tobacco product, the coating fluid simultaneously the present invention obtained combines the reconstituted tobacco paper substrate of punching, obtain good effect, and product prepared by the method has the outward appearance of cigarette, is more easily esthetically acceptable to the consumers.
Object of the present invention is achieved by following technical solution:
A kind of preparation method of novel tobacco goods is provided, comprises the steps:
S1. reconstituted tobacco paper substrate is prepared: described reconstituted tobacco paper substrate adopts paper process to prepare, and the offal slag after impregnation process and/or residue obtain reconstituted tobacco paper substrate through defibrination, handsheet, pressing and drying;
S2. the reconstituted tobacco paper substrate prepared at S1 punches;
S3. coating fluid is prepared;
S4. on the reconstituted tobacco paper substrate of the coating liquid prepared by S3 after S2 punching, dry, roll into described tobacco product;
Wherein, described in S3, the preparation of coating fluid comprises the following steps:
S31. raw tobacco material is rolled into cigarette bundle;
S32. control described cigarette Shu Jinhang suction fuel, keep pumping velocity be at the uniform velocity and cigarette Shu Jinliang minimizing is glowed, collect gas gas-phase objects and the granule phase substance of main flume respectively; With granule phase substance composition mixture and described coating fluid after gas gas-phase objects condensation.
Sum up through the large quantity research of the present invention, the flue gas extract coating obtained by mode of the present invention is made when novel tobacco goods are smoked panel test when not lighting and people can be made to have sensory experience very close when burning and sucking with traditional cigarette.If aspirated according to the mode of normal simulation human body suction, the sensory experience that the flue gas extract coating of gained is made when the charm of novel tobacco goods and traditional cigarette burn and suck differs greatly.
Meanwhile, the reconstituted tobacco paper substrate being coated with coating fluid is directly rolled into tobacco product by the present invention, and this tobacco product and cigar have similar outward appearance, are more easily esthetically acceptable to the consumers.Simultaneously, reconstituted tobacco paper substrate punches, be conducive to the absorption of reconstituted tobacco paper substrate to coating fluid on the one hand, punch on reconstituted tobacco paper substrate on the other hand, suitable passage is formed in tobacco product, to be more convenient for the fragrance volatilizing of tobacco product, to realize smelling and hear cigarette flavor or obtain abundant stimulus to the sense organ by suction action.
Wherein, in S2, the aperture of punching is preferably 0.4 ~ 0.8mm, pitch of holes 1 ~ 3mm, hole array pitch 1.5 ~ 2mm.
As one more preferably scheme, in S2, the aperture of punching is 0.6mm, pitch of holes 2mm, hole array pitch 1.8mm.
Only there is suction by control and suck velocity interpolation cigarette bundle when burning in the present invention and minimizing of trying one's best is glowed, and those skilled in the art can regulate the pumping velocity of needs to realize according to the composition of cigarette bundle.
The present invention by control and suck velocity interpolation cigarette bundle only occur when burning suction and as far as possible minimizing glow, ensure the volatile ingredient volatilization that cigarette is intrafascicular and form flue gas and avoid coking and naked light burning simultaneously.Those skilled in the art can regulate the pumping velocity of needs to realize in conjunction with this area routine techniques according to the component characteristic of cigarette bundle.If the composition of cigarette bundle is with reference to existing conventional cigarette cigarette, cigarette aspirates smoothly to adopt conventional swabbing pressure to ensure.Preferably, when described cigarette bundle characteristic is close with existing Cigarette, and cigarette beam specification is long 80 ~ 100mm, and circular cross section diameter is 7 ~ 10mm, or when the square cross section length of side is 7 ~ 10mm, the swabbing pressure of employing is 35mL/puffs(2s) ~ 60mL/puffs(2s).
Wherein, in S31, described cigarette bundle tobacco leaf is directly rolled into pencil to obtain, or by tobacco leaf chopping Final finishing bunchy.The parcel of cigarette bundle appearance does not do considered critical.Preferably, the specification of described cigarette bundle is preferably long 80 ~ 100mm, and cross section can be any shape, circular or square, and the diameter of circular cross section is 7 ~ 10mm, if square, the length of side is 7 ~ 10mm.Described tobacco leaf is that conventional cigarette prepares to carry out the tobacco leaf of chopping technique when producing, and conveniently technology is through the tobacco leaf of the treatment step such as first roasting, beating and double roasting, tobacco fermentation, cigarette composition of tobacco leaf.Treatment process before tobacco leaf chopping is with reference to prior art.
Preferably, the specification of described cigarette bundle is long 80 ~ 100mm, and circular cross section diameter is 7 ~ 10mm, or when the square cross section length of side is 7 ~ 10mm, the swabbing pressure of employing is 35mL/puffs(2s) ~ 60mL/puffs(2s).
In S31, described tobacco leaf makes cigarette bundle, can be to roll separately single tobacco leaf, also can according to the needs of charm, adopts diverse tobacco leaf to carry out arranging in pairs or groups and jointly roll.
Aspirating described cigarette Shu Jinhang in S32, can be adopt smoking apparatus to aspirate separately a cigarette bundle; Also can be more than two cigarette Shu Jinhang are aspirated simultaneously.When smoking apparatus is simultaneously to more than two cigarette bundle suctions, these cigarette bundles can be the cigarette bundles be all made up of same tobacco leaf, also can be according to charm needs, the cigarette bundle be made up separately of different types of tobacco leaf.
In S32, the gas gas-phase objects in main flume and the collection mode of granule phase substance, can with reference to prior art.Granule phase substance can pass through glass fiber filter material (such as cambridge filter) and collect, and gas gas-phase objects can be obtained by the mode of condensation.The temperature of condensation is preferably about-60 DEG C.
In S4, the coating weight of coating fluid is generally 5 ~ 15 paper substrate quality %.
In S4, can according to the needs of novel tobacco goods charm, the coating weight of adjustment coating fluid.
In S4, can according to the needs of novel tobacco goods excitant power, the pH value of adjustment coating fluid.
In order to discharging of making that the smell of novel tobacco goods of the present invention can be better, consumer, when using tobacco product of the present invention, can coordinate heater to heat tobacco product.
Described heater provides suitable temperature to tobacco product, and the mode of heating can be electrical heating, or other on-fuel mode of heating.
Compared with prior art, the present invention has following beneficial effect:
The present invention fundamentally carries out the innovation of technical thought, change the preparation method of the preparation cigarette of traditional cigarette industry, by conventional cigarette " burning during use ", advance to and carry out in the preparation process of cigarette, in preparation process, use at the uniform velocity suction to instead of existing smoker one and take out a suction stopped, as long as and the generation of side-stream smoke produced in the stage of resting of suction, thus the side-stream smoke produced when decreasing original artificial suction, improve the utilization rate of tobacco leaf; Simultaneously, based on present invention process, time smoker uses tobacco product of the present invention, tobacco product itself is not containing side-stream smoke, and do not need again burning, therefore the generation of side-stream smoke is not had, avoid the existence of second-hand-cigarette, also provide technical foundation for meeting the demand of people to cigarette charm to a greater degree simultaneously, on the reconstituted tobacco paper substrate of the coating liquid that new technology is prepared by the present invention after science punching, obtain beyond thought effect, for preparation smells cigarette and incombustible cigarette provides strong technical foundation.
The present invention's method used does not depart from tobacco itself, and the tobacco planting industry traditional on China does not produce any impact and impact; By the control of preparation technology, effectively can also control the content of harmful substance in cigarette, reduce product to the negative effect of health of people.
The outward appearance of tobacco product of the present invention and conventional cigarette products closer to, be more easily esthetically acceptable to the consumers.
Accompanying drawing explanation
Fig. 1 is punching paper substrate structural representation, and 1 represents the hole on paper substrate, and 2 represent pitch of holes, and 3 represent hole array pitch.
Fig. 2 coating fluid preparation technology of the present invention schematic flow sheet.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is further explained, but embodiments of the present invention is not limited in any way.Unless stated otherwise, involved in embodiment reagent, method are the conventional reagent in this area and method.
The redried that tobacco leaf picking used in embodiment is conventional, arranges bunchy through chopping.In embodiment, smoking apparatus used adopts Britain Cerulean company SM450 linear pattern smoking machine.
Embodiment 1
A kind of preparation method of novel tobacco goods is provided, comprises the steps:
S1. reconstituted tobacco paper substrate is prepared: described reconstituted tobacco paper substrate adopts paper process to prepare, and the offal slag after impregnation process and/or residue obtain reconstituted tobacco paper substrate through defibrination, handsheet, pressing and drying;
S2. the reconstituted tobacco paper substrate prepared at S1. punches; The aperture of punching is 0.4mm, pitch of holes 1mm, hole array pitch 1.5mm.
S3. coating fluid is prepared;
S4., on the reconstituted tobacco paper substrate of the coating liquid prepared by S3 after S2 punching, coating weight is 5 ~ 15%, and dry, size rolls as required makes described tobacco product.
Preparation technology's schematic flow sheet of described coating fluid is shown in shown in accompanying drawing 2, comprises the following steps:
Tangerine three (A) redried leaf tobacco in S31.2012 Xiangxi, rolls into cylindrical shape cigarette bundle (long 84mm, diameter 7.8mm);
S32. adopt smoking machine to described cigarette Shu Jinhang suction fuel, control and suck speed is at the uniform velocity (35mL/puffs(2s)) and cigarette Shu Jinliang minimizing is glowed, collected the granule phase substance of main flume by cambridge filter, at-60 DEG C, the gas gas-phase objects of main flume is reclaimed in condensation; The granule phase substance collected with the washing of ethanol, propane diols, glycerine or their mixed solution and dissolving and gas gas-phase objects, solution usage is appropriate.
The vapor condensation thing prepare the present embodiment and the mixture of granule phase substance carry out composition detection, and main component is as follows: gas phase composition is mainly: the acid of hydro carbons, aldehydes, ketone, heterocyclic compound, low molecular weight volatile and ester class etc.Ideal composition is mainly: alkaloids (based on nicotine), neutral aldoketones (based on solanone, Megastigmatrienone (5 isomers)), higher fatty acids and ester class (oleic acid, linoleic acid, leukotrienes and ester thereof) thereof etc.Be shown in Table 1:
Table 1
Contrast 1: prepare coating fluid with tobacco leaf of the same race through same treatment, carrier adopts the reconstituted tobacco do not punched.
Contrast 2: be prepared into conventional cigarette through throwing, cigarette bundle system volume, cigarette package with tobacco leaf of the same race.
To smoke panel test contrast: professional does not light tobacco product prepared by embodiment 1, aspirates; Contrast 1 preparation tobacco product contrast 2 conventional cigarette light after aspirate.Jealous, fragrance, the rhythm of comparative product
Taste the results are shown in Table shown in 2:
Table 2
| embodiment 1 tobacco product | contrast 1 tobacco product | contrast 2 conventional cigarette |
| moderate concentration, the soft silk floss of flue gas, exquisiteness, loose, elegant, aroma quality is better, and to a kind of fresh impression of people, oral cavity pleasant impression is clean, and perfume quantity is sufficient. | moderate concentration, the soft silk floss of flue gas, exquisiteness, loose, elegant, aroma quality is better, and to a kind of fresh impression of people, oral cavity pleasant impression is clean, but perfume quantity is less, and perfume quantity is slightly deficient. | moderate concentration, flue gas is full, and aroma quality is better, and perfume quantity is sufficient.Tobacco flavor is pure, and oral cavity remains less, and comfort level is better. |
Experiment finds, adopt the tobacco product that the inventive method prepares, the pleasurable fragrance that traditional cigarette flue gas brings people can be obtained by suction, the pure and fresh thin silk floss of fragrance, before carrier does not punch, the less initial analysis of perfume quantity all volatile materials can not be evaporated from paper substrate at the pressure of simple suction, makes perfume quantity less because being short of some fragrance matter.And on carrier after punching, perfume quantity and aroma quality have obvious lifting.
Embodiment 2
A kind of preparation method of novel tobacco goods is provided, comprises the steps:
S1. reconstituted tobacco paper substrate is prepared: described reconstituted tobacco paper substrate adopts paper process to prepare, and the offal slag after impregnation process and/or residue obtain reconstituted tobacco paper substrate through defibrination, handsheet, pressing and drying;
S2. the reconstituted tobacco paper substrate prepared at S1. punches; The aperture of punching is 0.6mm, pitch of holes 1.5mm, hole array pitch 2mm.
S3. coating fluid is prepared:
S4., on the reconstituted tobacco paper substrate of the coating liquid prepared by step S3. after S2. punching, coating weight is 5 ~ 15%, and dry, size rolls as required makes described tobacco product.
The preparation of coating fluid is carried out as follows:
Tangerine three (C1) redried leaf tobacco in S31.2012 Guizhou, rolls into cylindrical shape cigarette bundle (long 80mm, diameter 7.7mm) after chopping;
S32. adopt smoking machine to described cigarette Shu Jinhang suction fuel, control and suck speed is at the uniform velocity (45mL/puffs(2s)) and cigarette Shu Jinliang minimizing is glowed, collected the granule phase substance of main flume by cambridge filter, at-60 DEG C, the gas gas-phase objects of main flume is reclaimed in condensation; The granule phase substance collected with the washing of ethanol, propane diols, glycerine or their mixed solution and dissolving and gas gas-phase objects.
Contrast 1: prepare coating fluid with tobacco leaf of the same race through same treatment, carrier adopts the reconstituted tobacco do not punched.
Contrast 2: be prepared into conventional cigarette with tobacco leaf of the same race.
To smoke panel test contrast: professional does not light tobacco product prepared by embodiment 2, aspirates, the conventional cigarette of contrast is aspirated after lighting.Jealous, fragrance, the charm of comparative product the results are shown in Table shown in 2:
Table 2
| embodiment 2 tobacco product | contrast 1 tobacco product | contrast 2 conventional cigarette |
| moderate concentration, the soft silk floss of flue gas, exquisiteness, loose, aroma quality is better, and perfume quantity is sufficient, and the sensation of this perfume (or spice) of tobacco is better, and residual less, comfort level is better. | moderate concentration, the soft silk floss of flue gas, exquisiteness, loose, aroma quality is better, but perfume quantity is less, and the sensation of this perfume (or spice) of tobacco is better, and residual less, comfort level is fair. | moderate concentration, flue gas is full, and aroma quality is better, and perfume quantity is sufficient.Tobacco flavor is pure, and oral cavity remains less, and comfort level is better. |
Experiment finds, adopt the tobacco product that the inventive method prepares, the pleasurable fragrance that traditional cigarette flue gas brings people can be obtained by suction, the pure and fresh thin silk floss of fragrance, before carrier does not punch, the less initial analysis of perfume quantity all volatile materials can not be evaporated from paper substrate at the pressure of simple suction, makes perfume quantity less because being short of some fragrance matter.And on carrier after punching, perfume quantity and aroma quality have obvious lifting.
Embodiment 3
A kind of preparation method of novel tobacco goods is provided, comprises the steps to prepare:
S1. reconstituted tobacco paper substrate is prepared: described reconstituted tobacco paper substrate adopts paper process to prepare, and the offal slag after impregnation process and/or residue obtain reconstituted tobacco paper substrate through defibrination, handsheet, pressing and drying;
S2. the reconstituted tobacco paper substrate prepared at S1. punches; The aperture of punching is 0.8mm, pitch of holes 3mm, hole array pitch 2mm.
S3. coating fluid is prepared;
S4., on the reconstituted tobacco paper substrate of the coating liquid prepared by step S3. after S2. punching, coating weight is 5 ~ 15%, and dry, size rolls as required makes described tobacco product.
The preparation of coating fluid is carried out as follows:
Tangerine three (A) redried leaf tobacco in S31.2012 Yunnan, rolls into cigarette bundle (long 90mm, diameter 8.2mm);
S32. adopt smoking machine to described cigarette Shu Jinhang suction fuel, control and suck speed is at the uniform velocity (40mL/puffs(2s)) and cigarette Shu Jinliang minimizing is glowed, collected the granule phase substance of main flume by cambridge filter, at-80 DEG C, the gas gas-phase objects of main flume is reclaimed in condensation; The granule phase substance collected with the washing of ethanol, propane diols, glycerine or their mixed solution and dissolving and gas gas-phase objects.
Contrast 1: prepare coating fluid with tobacco leaf of the same race through same treatment, carrier adopts the reconstituted tobacco do not punched.
Contrast 2: be prepared into conventional cigarette through throwing, cigarette bundle system volume, cigarette package with tobacco leaf of the same race.
To smoke panel test contrast: professional does not light tobacco product prepared by embodiment 3, aspirates, the conventional cigarette of contrast is aspirated after lighting.Jealous, fragrance, the charm of comparative product the results are shown in Table shown in 3:
Table 3
| embodiment 3 tobacco product | contrast 1 tobacco product | contrast 2 conventional cigarette |
| moderate concentration, the soft silk floss of flue gas, exquisiteness, loose, aroma quality is better, and perfume quantity is sufficient, and the sensation of this perfume (or spice) of tobacco is better, and residual less, oral cavity is cleaner. | moderate concentration, the soft silk floss of flue gas, exquisiteness, loose, aroma quality is better, and perfume quantity is less, and the sensation of this perfume (or spice) of tobacco is better, and residual less, oral cavity is cleaner. | moderate concentration, flue gas is fine and soft, elegant, and aroma quality is better, and perfume quantity is sufficient.Tobacco flavor is pure, and oral cavity remains less, and comfort level is better. |
Experiment finds, adopt the tobacco product that the inventive method prepares, the pleasurable fragrance that traditional cigarette flue gas brings people can be obtained by suction, the pure and fresh thin silk floss of fragrance, before carrier does not punch, perfume quantity is less, and initial analysis all volatile materials can not be evaporated from paper substrate at the pressure of simple suction, makes perfume quantity less because being short of some fragrance matter.And on carrier after punching, perfume quantity and aroma quality have obvious lifting.
Claims (7)
1. a preparation method for novel tobacco goods, is characterized in that, comprises the steps:
S1. reconstituted tobacco paper substrate is prepared: described reconstituted tobacco paper substrate adopts paper process to prepare, and the offal slag after impregnation process and/or residue obtain reconstituted tobacco paper substrate through defibrination, handsheet, pressing and drying;
S2. the reconstituted tobacco paper substrate prepared at S1 punches;
S3. coating fluid is prepared;
S4. on the reconstituted tobacco paper substrate of the coating liquid prepared by S3 after S2 punching, dry, roll into described tobacco product;
Wherein, described in S3, the preparation of coating fluid comprises the following steps:
S31. raw tobacco material is rolled into cigarette bundle;
S32. control described cigarette Shu Jinhang suction fuel, keep pumping velocity be at the uniform velocity and cigarette Shu Jinliang minimizing is glowed, collect gas gas-phase objects and the granule phase substance of main flume respectively; With granule phase substance composition mixture and described coating fluid after gas gas-phase objects condensation,
In S32, the pressure that described cigarette Shu Jinhang aspirates is determined according to the aerosol spraying of 35mL ~ 60mL in 2 second duration,
Gas gas-phase objects described in S32 is collected by the mode of condensation, and the temperature of condensation is less than-60 DEG C.
2. the preparation method of novel tobacco goods according to claim 1, it is characterized in that, in S2, the aperture of punching is 0.4 ~ 0.8mm, pitch of holes 1 ~ 3mm, hole array pitch 1.5 ~ 2mm.
3. the preparation method of novel tobacco goods according to claim 1, it is characterized in that, in S2, the aperture of punching is 0.6mm, pitch of holes 2mm, hole array pitch 1.8mm.
4. the preparation method of novel tobacco goods according to claim 1, is characterized in that, in S31, described raw tobacco material is the tobacco leaf that conventional cigarette prepares to carry out chopping technique when producing.
5. the preparation method of novel tobacco goods according to claim 1, is characterized in that, in S31, described raw tobacco material is tobacco leaf or the formula tobacco leaf group of single variety.
6. the preparation method of novel tobacco goods according to claim 1, it is characterized in that, in S32, granule phase substance is collected by glass fiber filter material.
7. the preparation method of novel tobacco goods according to claim 1, is characterized in that, in S2, described punching is punched to paper substrate for adopting laser, electrostatic or mechanical punching device.
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| CN104687233B (en) * | 2014-12-30 | 2017-10-10 | 广东中烟工业有限责任公司 | The preparation method and orange flavor reconstituted tobacco of a kind of orange flavor reconstituted tobacco |
| DE102018112221A1 (en) * | 2018-05-22 | 2019-11-28 | Hauni Maschinenbau Gmbh | A method of producing tobacco material for use in HNB tobacco articles and HNB tobacco articles |
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| WO2007123046A1 (en) * | 2006-04-20 | 2007-11-01 | Japan Tobacco Inc. | Menthol delivery system for charcoal filter cigarette |
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| US5413122A (en) * | 1992-02-18 | 1995-05-09 | R. J. Reynolds Tobacco Company | Method of providing flavorful and aromatic compounds |
| CN102266116A (en) * | 2011-06-08 | 2011-12-07 | 广东中烟工业有限责任公司 | Reconstituted tobacco leaf and preparation method and application thereof |
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