CN110946324A - Production method of ginsenoside gel filter stick - Google Patents
Production method of ginsenoside gel filter stick Download PDFInfo
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- CN110946324A CN110946324A CN201911363407.XA CN201911363407A CN110946324A CN 110946324 A CN110946324 A CN 110946324A CN 201911363407 A CN201911363407 A CN 201911363407A CN 110946324 A CN110946324 A CN 110946324A
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- ginsenoside
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/022—Applying additives to filter materials with liquid additives, e.g. application of plasticisers
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Abstract
The invention relates to a production method of a ginsenoside gel filter stick, which comprises the steps of preparing ginsenoside gel, adding the ginsenoside gel, cooling, drying, packaging and the like. The filter stick produced by the method has stable quality, the addition amount of the saponin gel is uniform, the mouthfeel characteristics of the ginsenoside are obvious, the irritation of the oral cavity and the throat is low, no obvious miscellaneous gas is generated, and the aftertaste is clean and comfortable.
Description
[ technical field ] A method for producing a semiconductor device
The invention belongs to the technical field of tobacco processing. More specifically, the invention relates to a production method of a ginsenoside gel filter stick.
[ background of the invention ]
Along with the continuous improvement of living standard, people's health consciousness is also stronger and stronger. Smokers desire to reduce the harm caused by smoking as much as possible while achieving psychological and physiological satisfaction through smoking. However, in recent years, with the gradual progress of traditional cigarette tar reduction and harm reduction, the development of a cigarette which can not only meet the harm reduction requirements of smokers, but also keep high cigarette aroma and low harm of the cigarette becomes an important research topic in the tobacco industry in the present year. The important aroma components with special aroma and special functions in the plants are selected to be added into the cigarettes, so that the method is an effective way for compensating the aroma of the cigarettes for the loss of aroma substances caused by tar reduction and harm reduction, and has an important promoting effect on enriching the aroma of the cigarettes and endowing the cigarettes with special functions.
Ginsenoside (Ginsenoside) is a sterol compound, and triterpene saponin mainly exists in human medicinal materials, and has effects of resisting tumor, resisting arrhythmia, and enhancing immunity. In addition, the human saponin has unique fragrance and can coordinate the fragrance of cigarettes. Therefore, the ginsenoside is selected to be added into the cigarette, and has important effects on compensating the cigarette fragrance and enriching the cigarette fragrance.
The perfuming of the cigarette can improve the physical and chemical properties of the cigarette, round the smoke, modify the fragrance of the cigarette, improve the smoking taste, and establish the style of the product, which influences the acceptability of the smokers to a certain extent. At present, the main flavoring mode is to add essence directly to tobacco shreds or add flavor to the end of a filter tip. However, the flavoring mode has the problems of short essence retention time, short cigarette shelf life, uneven essence release and the like, but the addition of the gel aroma-carrying substance in the filter stick can not only compensate the aroma loss, but also solve the defects of the existing flavoring mode.
Aiming at the technical defects existing at present, the inventor invents a method for adding a ginsenoside gel filter stick through a large amount of experimental research and analysis.
[ summary of the invention ]
[ problem to be solved ]
The invention aims to provide a method for producing a ginsenoside gel filter stick.
[ solution ]
The invention is realized by the following technical scheme.
The invention relates to a production method of a ginsenoside gel filter stick.
The production method comprises the following steps:
A. preparation of ginsenoside gel
Dissolving 2-10 parts by weight of ginsenoside in 2-20 parts by weight of solvent to obtain a ginsenoside solution, adding 5-40 parts by weight of solidification modifier, 0.01-0.1 part by weight of emulsifier and 50-90 parts by weight of temperature phase change material into the solution, stirring and mixing uniformly, heating for dissolving, and then cooling for shaping to obtain ginsenoside gel;
B. adding ginsenoside gel
B, filling the ginsenoside gel obtained in the step A into a hot melting tank, adjusting a spray head of the hot melting tank to be aligned to the central axis of the filter stick, adjusting the temperature of the hot melting tank to 40-90 ℃ to melt the ginsenoside gel, and spraying the ginsenoside gel liquid into the filter stick by a pump;
C. cooling and drying
C, putting the filter stick added with the ginsenoside gel obtained in the step B on a drying rack in order, cooling and drying for 8-12 hours, and forming a ginsenoside gel strip at the central axis position of the filter stick;
D. package with a metal layer
And C, sealing and packaging the cooled and dried ginsenoside gel filter stick obtained in the step C.
According to a preferred embodiment of the present invention, in step a, the weight ratio of the ginsenoside, the solvent, the solidification modifier, the emulsifier and the temperature phase change material is 4-8: 6-15: 15-30: 0.03 to 0.08: 62 to 78.
According to another preferred embodiment of the present invention, in step a, the solvent is one or more solvents selected from the group consisting of propylene glycol, MCT, glycerol, and glycerol diacetate.
According to another preferred embodiment of the present invention, in step A, the coagulation modifier is one or more coagulation modifiers selected from lauric acid, myristic acid, palmitic acid, stearic acid, arachidic acid, or behenic acid.
According to another preferred embodiment of the present invention, in step a, the emulsifier is one or more emulsifiers selected from the group consisting of polyoxyethylene sorbitan monooleate, polyacrylamide or glyceryl monostearate.
According to another preferred embodiment of the present invention, in step a, the temperature phase change material is one or more temperature phase change materials selected from polyethylene glycol 1000, polyethylene glycol 1500, polyethylene glycol 2000 or polypropylene glycol.
According to another preferred embodiment of the present invention, in the step a, the uniformly mixed mixture is heated and dissolved at a temperature of 40 to 90 ℃ for 30 to 90 min.
According to another preferred embodiment of the present invention, in the step B, the pump flow of the hot melt tank is controlled to be 50 to 1000 ml/min.
According to another preferred embodiment of the present invention, in the step C, the cooling and drying are performed at a temperature of 25 to 35 ℃ and a relative humidity of 40 to 70% to obtain the ginsenoside gel strip having a water content of 2.280% by weight or less.
According to another preferred embodiment of the present invention, in the step C, the diameter of the ginsenoside gel strip is 0.1-0.4 mm.
The present invention will be described in more detail below.
The invention relates to a production method of a ginsenoside gel filter stick.
The production method comprises the following steps:
A. preparation of ginsenoside gel
Dissolving 2-10 parts by weight of ginsenoside in 2-20 parts by weight of solvent to obtain a ginsenoside solution, adding 5-40 parts by weight of solidification modifier, 0.01-0.1 part by weight of emulsifier and 50-90 parts by weight of temperature phase change material into the solution, stirring and mixing uniformly, heating for dissolving, and then cooling for shaping to obtain ginsenoside gel;
in the invention, the main functions of the ginsenoside in the ginsenoside gel filter stick are to reduce the smoke temperature, improve the autoimmune function and enhance the disease resistance.
The ginsenosides used in the present invention are currently marketed products, for example, sold under the name of east ginsenosides by Jingyu county, Congda, ecological development Limited.
According to the invention, the solvent has the basic functions of mixing and dissolving the ginsenoside, the solidification modifier, the emulsifier and the temperature phase change material in the preparation of the ginsenoside gel, and also has the function of a smoke agent.
The solvent is one or more solvents selected from propylene glycol, MCT (medium chain triglyceride), glycerol or glycerol diacetate. The solvents used in the present invention are all products currently marketed, such as propylene glycol sold under the trade name of tao propylene glycol by zhenzhou sandutu chemical, MCT sold under the trade name of e jidao MCT by shannan wenchang coco runou food ltd, glycerol sold under the trade name of zhongxin glycerol, glycerol diacetate sold under the trade name of yao hui glycerol diacetate by kunming yao comedo trade ltd.
In the invention, when the dosage of the ginsenoside is 2-10 parts by weight, if the dosage of the solvent is less than 2 parts by weight, the ginsenoside can not be completely dissolved; if the amount of the solvent is more than 20 parts by weight, the coagulation time of the ginsenoside gel is too long or the coagulation cannot be performed; therefore, the amount of the solvent is preferably 2 to 20 parts by weight, more preferably 6 to 15 parts by weight.
According to the invention, the basic function of the coagulation modifier in preparing the ginsenoside gel is to improve the coagulation performance of the ginsenoside gel.
The coagulation modifier is one or more coagulation modifiers selected from lauric acid, myristic acid, palmitic acid, stearic acid, arachidic acid or behenic acid. The coagulation modifiers used in the present invention are commercially available products, such as lauric acid sold under the trade name of coconut lauric acid by Fuqing chemical Co., Ltd, myristic acid sold under the trade name of maleic myristic acid by Shanghai Yachen chemical Co., Ltd, palmitic acid sold under the trade name of Emery palmitic acid by Shanghai Yachen chemical Co., Ltd, stearic acid sold under the trade name of Chunjin stearic acid 1801 by Guangzhou Cilin chemical Co., Ltd, arachidic acid sold under the trade name of Tianli arachidic acid by Sainta Tianli Biotech Co., Ltd, and behenic acid sold under the trade name of Kramal behenic acid by Shanghai spectral vibration Biotech Co., Ltd.
In the invention, when the dosage of the ginsenoside is 2-10 parts by weight, if the dosage of the solidification modifier is less than 5 parts by weight, the gel is not solidified or the solidification time is too long; if the amount of the solidification modifier is more than 40 parts by weight, the gel solidification process is too fast, and equipment is easily blocked when the solidification modifier is added; therefore, the amount of the solidification modifier used is suitably 5 to 40 parts by weight, preferably 15 to 30 parts by weight.
According to the invention, the emulsifier has the basic functions of changing the surface tension of the gel, improving the dispersion degree of the ginsenoside in the gel and preventing the ginsenoside gel from layering.
The emulsifier is one or more selected from polyoxyethylene sorbitan monooleate, polyacrylamide or glyceryl monostearate. The emulsifiers used in the present invention are all products currently marketed, for example polyoxyethylene sorbitan monooleate (Tween 80) sold under the trade name dx polyoxyethylene sorbitan monooleate by Shanghai Yuanmu Biotech Co., Ltd, sorbitan monooleate sold under the trade name California S-80 sorbitan monooleate by Haian petrochemical Mills of Jiangsu province, polyacrylamide sold under the trade name France Edison Polyacrylamide (PAM) by Chengdu Sunshan chemical Co., Ltd, glyceryl monostearate sold under the trade name California glyceryl monostearate by pure Jia trade Co., Ltd, Guangzhou.
In the invention, when the dosage of the ginsenoside is 2-10 parts by weight, if the dosage of the emulsifier is less than 0.01 part by weight, the emulsification effect is poor, the layering phenomenon is easy to occur, and the quality of the produced ginsenoside gel filter stick is uneven; if the amount of the emulsifier is more than 0.1 part by weight, the emulsifying effect is not obviously increased, so that the resource waste is caused, and the production cost is increased; accordingly, the emulsifier is suitably used in an amount of 0.01 to 0.1 part by weight, preferably 0.03 to 0.08 part by weight.
According to the invention, the temperature phase change material has the basic function of forming solid gel at normal temperature to protect ginsenoside, providing phase change when being heated, absorbing heat and releasing ginsenoside.
The temperature phase change material is one or more temperature phase change materials selected from polyethylene glycol 1000, polyethylene glycol 1500, polyethylene glycol 2000 or polypropylene glycol. The temperature phase change material used in the present invention is a product currently commercially available, such as polyethylene glycol 1000 sold under the trade name of Adita polyethylene glycol 1000 by Tanta union chemical Co., Ltd, polyethylene glycol 1500 sold under the trade name of Sangda polyethylene glycol 1500 by Sangda chemical (Nantong) Co., Ltd, polyethylene glycol 2000 sold under the trade name of Dow polyethylene glycol 2000 by West land chemical Co., Ltd, Guangzhou, and polyallylene alcohol sold under the trade name of neutralized santai polyallylene alcohol by Tianjin and Shengtai chemical Co., Ltd.
In the invention, when the dosage of the ginsenoside is 2-10 parts by weight, if the dosage of the phase-change material is lower than 50 parts by weight, the obtained ginsenoside gel cannot be solidified at normal temperature and cannot play a role in protecting the ginsenoside; if the amount of the phase change material is more than 90 parts by weight, the relative content of ginsenoside is reduced, and the characteristic of ginsenoside is not obvious when heat is absorbed and released; therefore, the amount of the temperature phase change material is preferably 50 to 90 parts by weight, more preferably 62 to 78 parts by weight.
Preferably, the weight ratio of the ginsenoside, the solvent, the solidification modifier, the emulsifier to the temperature phase change material is 4-8: 6-15: 15-30: 0.03 to 0.08: 62 to 78.
In the step, the mixture of the ginsenoside, the solvent, the solidification modifier, the emulsifier and the temperature phase change material which are uniformly mixed is heated and dissolved for 30-90 min at the temperature of 40-90 ℃.
In the invention, when the heating and dissolving time is 30-90 min, if the heating temperature is lower than 40 ℃, the ginsenoside gel is in a semi-molten or solid state, and the adding equipment is easy to block; if the heating temperature is higher than 90 ℃, the characteristics of the ginsenoside can be changed; therefore, the heating temperature is between 40 and 90 ℃;
when the heating temperature is 40-90 ℃, if the heating time is less than 30min, the melting is incomplete and is in a semi-molten state; if the heating time is longer than 90min, the properties of the ginsenoside are changed; therefore, the heating time is preferably 30-90 min;
in the present invention, the cooling shaping is understood to be a process of allowing the hot mixture of step a to slowly cool and solidify under natural conditions.
B. Adding ginsenoside gel
B, filling the ginsenoside gel obtained in the step A into a hot melting tank, adjusting a spray head of the hot melting tank to be aligned to the central axis of the filter stick, adjusting the temperature of the hot melting tank to 40-90 ℃ to melt the ginsenoside gel, and spraying the ginsenoside gel liquid into the filter stick by a pump;
the hot melt tank is a device generally used in the art, and is, for example, a product sold under the trade name of Jian JKN-JZG-00 hot melt tank by Wenzhou Jiankun machines, Inc.
According to the invention, the pump flow of the hot melting tank is controlled to be 50-1000 ml/min. If the pump flow of the hot melting tank is less than 50ml/min, the production efficiency is too low, and the cost is increased; if the pump flow of the hot melting tank is more than 1000ml/min, the flow rate is too high, and the quality of the produced ginsenoside filter stick is unstable; therefore, the pump flow of the hot melting tank is properly controlled to be 50-1000 ml/min;
C. cooling and drying
C, putting the filter stick added with the ginsenoside gel obtained in the step B on a drying rack in order, cooling and drying for 8-12 hours, and forming a ginsenoside gel strip at the central axis position of the filter stick;
the drying rack used by the invention is a movable multi-layer grid design, and the specification of the mesh sheet is 97cm multiplied by 63cm multiplied by 50 layers; the standard grid is 5 multiplied by 5cm meshes; the diameter of the net wire is 5mm multiplied by 3 mm; the layer height is 50mm conventionally, and four cun universal wheels are installed to the base, and the net piece adopts the plastic spraying technology, and it is the equipment that generally uses in this technical field, for example is by Shenzhen city Longhua new district big unrestrained motherwort silk screen printing five metals factory with trade name motherwort drying rack selling product.
According to the invention, the cooling and drying are carried out under the conditions of the temperature of 25-35 ℃ and the relative humidity of 40-70% to obtain the ginsenoside gel strip with the water content of below 2.280% by weight.
The water content was determined according to the GB/T6283 standard method.
In the present invention, the diameter of the ginsenoside gel strip is measured according to a standard method combining an image light microscope (YM-DVM) with a sampling assay, and is 0.1 to 0.4 mm.
D. Package with a metal layer
And C, sealing and packaging the cooled and dried ginsenoside gel filter stick obtained in the step C.
The apparatus used for sealed packaging in accordance with the present invention is, for example, a packaging apparatus sold by Tokyo lathe processing plant in Pingyang county under the trade name BZJ paper straw packer.
According to the cigarette smoking model specified by national standard YC/T29-1996, simulated smoking is carried out, a smoking evaluation group consisting of 10 experts is organized, a filter stick of the ginsenoside gel produced by the method replaces a filter stick of 1956 brands of Hongtai mountain as a test sample, the 1956 brands of Hongtai mountain are not changed as a comparison sample, and smoking evaluation is carried out simultaneously according to the method described in the application specification.
[ advantageous effects ]
The invention has the beneficial effects that: the method for producing the ginsenoside gel filter stick has the advantages of complete flow, simplicity in operation, labor saving and the like; the used substances such as solidification modifier, solvent, emulsifier, temperature phase-change material and the like are all easily available raw materials. The filter stick produced by the method has stable quality, the addition amount of the saponin gel is uniform, the mouthfeel characteristics of the ginsenoside are obvious, the irritation of the oral cavity and the throat is low, no obvious miscellaneous gas is generated, and the aftertaste is clean and comfortable.
[ description of the drawings ]
[ detailed description ] embodiments
The invention will be better understood from the following examples.
Example 1: production of ginsenoside gel filter stick
The implementation steps of this example are as follows:
A. preparation of ginsenoside gel
Dissolving 6 weight parts of ginsenoside sold under the trade name of Aodon ginsenoside by Jingyu county Congda forestry ecological development Limited company in 20 weight parts of propylene glycol solvent sold under the trade name of Dow propylene glycol by Zhengzhou Chengda chemical company to obtain ginsenoside solution, then, 5 parts by weight of a lauric acid coagulant sold under the trade name of coconut lauric acid by Fuqing chemical Co., Ltd, Guangzhou, 0.01 part by weight of a polyoxyethylene sorbitan monooleate emulsifier sold under the trade name of dx polyoxyethylene sorbitan monooleate by Yuanmo Biotech Co., Ltd, Shanghai, and 50 parts by weight of a polyethylene glycol 1000 temperature phase change material sold under the trade name of Adita polyethylene glycol 1000 by Adita chemical Co., Ltd, Wuxi, were added to the solution, and mixed uniformly with stirring, heating at 90 deg.C for 30min for dissolving, and cooling for shaping to obtain ginsenoside gel;
B. adding ginsenoside gel
Putting the ginsenoside gel obtained in the step A into a hot melting tank sold by Wenzhou Jiankun machinery limited company under the trade name Jian JKN-JZG-00 hot melting tank, adjusting a spray head of the hot melting tank to be aligned with the central axis of the filter stick, adjusting the temperature of the hot melting tank to 40 ℃ to melt the ginsenoside gel, and controlling the pump flow of the hot melting tank to be 600ml/min to spray ginsenoside gel liquid into the filter stick by a pump;
C. cooling and drying
D, putting the filter stick added with the ginsenoside gel obtained in the step B on a drying rack sold by Shenzhen Longhua New district Dalangkuncui silkscreen hardware factory with a trade name Kuncui drying rack, and cooling and drying for 10.5 hours at the temperature of 25-35 ℃ and the relative humidity of 40-70% to form a ginsenoside gel strip at the central axis position of the filter stick, wherein the water content is below 2.280% by weight by adopting the method described in the specification; its diameter is 0.1 mm;
D. package with a metal layer
The cooled dried ginsenoside gel filter rods obtained in step C were seal wrapped using a wrapping device sold by Takara lathe processing in Pingyang county under the trade name BZJ paper straw packer.
The ginsenoside gel filter stick produced in the embodiment replaces a filter stick of 1956 brand cigarettes in Hongtai mountain as a test sample, and cigarette of 1956 brand cigarettes in Hongtai mountain is not changed as a comparison sample, and evaluation is carried out simultaneously according to the method described in the application specification.
Example 2: production of ginsenoside gel filter stick
The implementation steps of this example are as follows:
A. preparation of ginsenoside gel
Dissolving 8 weight parts of ginsenoside sold under the trade name Aodong ginsenoside by Congda forestry ecological development Co., Ltd, Jingyu county in 9 weight parts of MCT solvent sold under the trade name E Mechindao MCT by Hainan Wenchang coconut-friendly food Co., Ltd to obtain a ginsenoside solution, adding 26 weight parts of myristic acid solidification modifier sold under the trade name Malaysia myristic acid by Shanghai Yacheng chemical engineering Co., Ltd, 0.08 weight part of sorbitan monooleate emulsifier sold under the trade name Haishuhua S-80 sorbitan monooleate by Hainan petrochemical plant of Jiangsu province and 66 weight parts of polyethylene glycol 1500 temperature phase change material sold under the trade name Sangda polyethylene glycol 1500 by Sangda chemical (Nantong) Co., Ltd, stirring and mixing uniformly, heating and dissolving for 54min at 70 deg.C, cooling and shaping, obtaining ginsenoside gel;
B. adding ginsenoside gel
Putting the ginsenoside gel obtained in the step A into a hot melting tank sold by Wenzhou Jiankun machinery limited company under the trade name Jian JKN-JZG-00 hot melting tank, adjusting a spray head of the hot melting tank to be aligned with the central axis of the filter stick, adjusting the temperature of the hot melting tank to 50 ℃ to melt the ginsenoside gel, and controlling the pump flow of the hot melting tank to be 50ml/min to spray ginsenoside gel liquid into the filter stick by a pump;
C. cooling and drying
D, putting the filter stick added with the ginsenoside gel obtained in the step B on a drying rack sold by Shenzhen Longhua New district Dalangkuncui silkscreen hardware factory with a trade name Kuncui drying rack, and cooling and drying for 8.0 hours at the temperature of 25-35 ℃ and the relative humidity of 40-70% to form a ginsenoside gel strip at the central axis position of the filter stick, wherein the water content is below 2.280% by weight by adopting the method described in the specification; its diameter is 0.3 mm;
D. package with a metal layer
The cooled dried ginsenoside gel filter rods obtained in step C were seal wrapped using a wrapping device sold by Takara lathe processing in Pingyang county under the trade name BZJ paper straw packer.
The ginsenoside gel filter stick produced in the embodiment replaces a filter stick of 1956 brand cigarettes in Hongtai mountain as a test sample, and cigarette of 1956 brand cigarettes in Hongtai mountain is not changed as a comparison sample, and evaluation is carried out simultaneously according to the method described in the application specification.
Example 3: production of ginsenoside gel filter stick
The implementation steps of this example are as follows:
A. preparation of ginsenoside gel
Dissolving 2 weight parts of ginsenoside sold under the trade name Aodon ginsenoside by Conrada forestry ecological development Co., Jingyu county in 5 weight parts of glycerol diacetate solvent sold under the trade name Yao comedo diacetate glycerol ester by Kunming Yao HuamaoMao Co., Ltd to obtain a ginsenoside solution, adding 33 weight parts of behenic acid coagulation modifier sold under the trade name Clara behenic acid by Shanghai spectral vibration Biotech Co., Ltd, 0.10 weight parts of polyacrylamide emulsifier sold under the trade name France Edison Polyacrylamide (PAM) by Chengdu Xiang chemical engineering Co., Ltd and 82 weight parts of polyallylate temperature change material sold under the trade name Zhongtai polyallylate by Tianjin neutralization chemical engineering Co., Ltd, stirring and mixing uniformly, heating and dissolving at 50 deg.C for 78min, cooling and shaping, obtaining ginsenoside gel;
B. adding ginsenoside gel
Putting the ginsenoside gel obtained in the step A into a hot melting tank sold by Wenzhou Jiankun machinery limited company under the trade name Jian JKN-JZG-00 hot melting tank, adjusting a spray head of the hot melting tank to be aligned with the central axis of the filter stick, adjusting the temperature of the hot melting tank to 80 ℃ to melt the ginsenoside gel, and controlling the pump flow of the hot melting tank to be 800ml/min to spray ginsenoside gel liquid into the filter stick by a pump;
C. cooling and drying
D, putting the filter stick added with the ginsenoside gel obtained in the step B on a drying rack sold by Shenzhen Longhua New district Dalangkuncui silkscreen hardware factory with a trade name Kuncui drying rack, and cooling and drying for 9.2 hours under the conditions of the temperature of 25-35 ℃ and the relative humidity of 40-70% to form a ginsenoside gel strip at the central axis position of the filter stick, wherein the water content is below 2.280% by weight by adopting the method described in the specification; its diameter is 0.2 mm;
D. package with a metal layer
The cooled dried ginsenoside gel filter rods obtained in step C were seal wrapped using a wrapping device sold by Takara lathe processing in Pingyang county under the trade name BZJ paper straw packer.
The ginsenoside gel filter stick produced in the embodiment replaces a filter stick of 1956 brand cigarettes in Hongtai mountain as a test sample, and cigarette of 1956 brand cigarettes in Hongtai mountain is not changed as a comparison sample, and evaluation is carried out simultaneously according to the method described in the application specification.
Example 4: production of ginsenoside gel filter stick
The implementation steps of this example are as follows:
A. preparation of ginsenoside gel
4 parts by weight of ginsenoside sold under the trade name Aodon ginsenoside by Jingyu county Congda forestry ecological development Limited was dissolved in 2 parts by weight of a mixture solvent composed of propylene glycol sold under the trade name of Dow propylene glycol by Zhengzhou Chengda chemical company and MCT sold under the trade name of E Mezkusan agricultural MCT by Hainan Wenchang Youyu food Limited in a weight ratio of 1:1 to obtain a ginsenoside solution, and then 19 parts by weight of a mixture coagulation modifier composed of palmitic acid sold under the trade name of Emery palmitic acid by Shanghai Yacheng chemical company and stearic acid sold under the trade name of spring gold stearic acid 1801 by Guanghai Qinling chemical corporation in a weight ratio of 1:2, 0.06 parts by weight of polyoxyethylene sorbitan monooleate sold under the trade name of dx polyoxyethylene sorbitan monooleate by Shanghai Muslim biological science Limited and Kangsu Kaisha Petroleum S-80 sold under the trade name of Hainan Petroleum S-80 by Jiangsu province chemical plant Mixing a mixture emulsifier consisting of sorbitan monooleate sold as water sorbitol monooleate in a weight ratio of 1:1 with 90 parts by weight of a mixture temperature phase-change material consisting of polyethylene glycol 1000 sold under the trade name of Adita polyethylene glycol 1000 by Toita union chemical Co., Ltd, and polyethylene glycol 1500 sold under the trade name of Sangda polyethylene glycol 1500 by Sangda chemical (Nantong) Co., Ltd in a weight ratio of 1:2, stirring and mixing uniformly, heating and dissolving at 80 ℃ for 42min, and cooling and shaping to obtain ginsenoside gel;
B. adding ginsenoside gel
Putting the ginsenoside gel obtained in the step A into a hot melting tank sold by Wenzhou Jiankun machinery limited company under the trade name Jian JKN-JZG-00 hot melting tank, adjusting a spray head of the hot melting tank to be aligned with the central axis of the filter stick, adjusting the temperature of the hot melting tank to 90 ℃ to melt the ginsenoside gel, and controlling the pump flow of the hot melting tank to be 1000ml/min to spray ginsenoside gel liquid into the filter stick by a pump;
C. cooling and drying
D, putting the filter stick added with the ginsenoside gel obtained in the step B on a drying rack sold by Shenzhen Longhua New district Dalangkuncui silkscreen hardware factory with a trade name Kuncui drying rack, and cooling and drying for 10.0 hours at the temperature of 25-35 ℃ and the relative humidity of 40-70% to form a ginsenoside gel strip at the central axis position of the filter stick, wherein the water content is below 2.280% by weight by adopting the method described in the specification; its diameter is 0.3 mm;
D. package with a metal layer
The cooled dried ginsenoside gel filter rods obtained in step C were seal wrapped using a wrapping device sold by Takara lathe processing in Pingyang county under the trade name BZJ paper straw packer.
The ginsenoside gel filter stick produced in the embodiment replaces a filter stick of 1956 brand cigarettes in Hongtai mountain as a test sample, and cigarette of 1956 brand cigarettes in Hongtai mountain is not changed as a comparison sample, and evaluation is carried out simultaneously according to the method described in the application specification.
Example 5: production of ginsenoside gel filter stick
The implementation steps of this example are as follows:
A. preparation of ginsenoside gel
10 parts by weight of ginsenoside sold under the trade name Aodon ginsenoside by Kangda forestry ecological development Co., Ltd, Jingyu county, was dissolved in 17 parts by weight of a mixture solvent composed of Nainan Wenchang coconut-friendly food Co., Ltd under the trade name eJi Ji-Hua-Yong food Co., Ltd, and glyceryl diacetate sold under the trade name Yao-Hua-Di-glyceryl diacetate by Kunming Yao-Hua Co., Ltd, in a weight ratio of 1:3 to obtain a ginsenoside solution, and then 40 parts by weight of myristic acid sold under the trade name maleic myristic acid by Shanghai Yao engineering Co., Ltd, arachic acid sold under the trade name Tianli arachic acid by Sainta Tianli Biotech Co., Ltd, and 0.04 parts by weight of a mixture solidification modifier composed of arachic acid sold under the trade name Clara behenic acid by Shanghai Biotech Co., Ltd, and 0.04 parts by weight of polyoxyethylene sorbitan monooleate sold under the trade name dX by Shanghai Yu Yongmu Biotech Co., Ltd, in a weight ratio of 2:1 A mixture emulsifier composed of commercially available polyoxyethylene sorbitan monooleate and polyacrylamide sold under the trade name of France Edison Polyacrylamide (PAM) by Kyoho chemical industry Co., Ltd in a weight ratio of 2:1, and 74 parts by weight of a mixture temperature phase change material composed of polyethylene glycol 1000 sold under the trade name of Adita polyethylene glycol 1000 by Staunto chemical industry Co., Ltd and polyethylene glycol 2000 sold under the trade name of American Dow polyethylene glycol 2000 by Western L chemical industry Co., Ltd, Guangzhou in a weight ratio of 2:1, stirring and mixing uniformly, heating and dissolving for 66min at a temperature of 60 ℃, and then cooling and shaping to obtain ginsenoside gel;
B. adding ginsenoside gel
Putting the ginsenoside gel obtained in the step A into a hot melting tank sold by Wenzhou Jiankun machinery limited company under the trade name Jian JKN-JZG-00 hot melting tank, adjusting a spray head of the hot melting tank to be aligned with the central axis of the filter stick, adjusting the temperature of the hot melting tank to 70 ℃ to melt the ginsenoside gel, and controlling the pump flow of the hot melting tank to be 100ml/min to spray ginsenoside gel liquid into the filter stick by a pump;
C. cooling and drying
D, putting the filter stick added with the ginsenoside gel obtained in the step B on a drying rack sold by Shenzhen Longhua New district Dalangkuncui silkscreen hardware factory with a trade name Kuncui drying rack, and cooling and drying for 11.2 hours under the conditions of the temperature of 25-35 ℃ and the relative humidity of 40-70% to form a ginsenoside gel strip at the central axis position of the filter stick, wherein the water content is below 2.280% by weight by adopting the method described in the specification; its diameter is 0.2 mm;
D. package with a metal layer
The cooled dried ginsenoside gel filter rods obtained in step C were seal wrapped using a wrapping device sold by Takara lathe processing in Pingyang county under the trade name BZJ paper straw packer.
The ginsenoside gel filter stick produced in the embodiment replaces a filter stick of 1956 brand cigarettes in Hongtai mountain as a test sample, and cigarette of 1956 brand cigarettes in Hongtai mountain is not changed as a comparison sample, and evaluation is carried out simultaneously according to the method described in the application specification.
Example 6: production of ginsenoside gel filter stick
The implementation steps of this example are as follows:
A. preparation of ginsenoside gel
5 parts by weight of ginsenoside sold under the trade name Aodon ginsenoside by Kangda forestry ecological development Co., Ltd, Jingyu county, was dissolved in 13 parts by weight of glycerin sold under the trade name Zhonghui glycerin, prepared by Jinan Zhonghui chemical Co., Ltd, and glyceryl diacetate sold under the trade name Yao Huai glyceryl diacetate, prepared by Kunming Yao Huai commercial Co., Ltd, to obtain a ginsenoside solution, 12 parts by weight of lauric acid sold under the trade name Coco lauric acid, myristic acid sold under the trade name Malayaki myristic acid, prepared by Shanghai Yao chemical Co., Ltd, and behenic acid sold under the trade name Clara behenic acid, prepared by Shanghai spectral biology Co., Ltd, were added to the solution to obtain a mixture coagulation modifier, prepared by weight of myristic acid, prepared by Franciscow chemical Co., Ltd, prepared by France French press, prepared by France Polyacrylamide (PAM), prepared by 0.02 parts by weight of Polyacrylamide (PAM) sold under the trade name Youngia Polyacrylamide (PAM), prepared by Youngi chemical Co., Ltd The method comprises the following steps of mixing acrylamide and glyceryl monostearate sold under the trade name of California glyceryl monostearate by pure Jia trade company Limited in Guangzhou according to a weight ratio of 1:3 to obtain a mixture emulsifier, mixing 58 parts by weight of a mixture temperature phase change material composed of polyethylene glycol 1500 sold under the trade name of Sangda chemical engineering (Nantong) Limited and polyallyl alcohol sold under the trade name of neutralizing Shengtai polyallyl alcohol by Tianjin neutralizing Shengtai chemical company Limited according to a weight ratio of 1:1, stirring and mixing uniformly, heating and dissolving for 90min at a temperature of 40 ℃, and then cooling and shaping to obtain ginsenoside gel;
B. adding ginsenoside gel
Putting the ginsenoside gel obtained in the step A into a hot melting tank sold by Wenzhou Jiankun machinery limited company under the trade name Jian JKN-JZG-00 hot melting tank, adjusting a spray head of the hot melting tank to be aligned with the central axis of the filter stick, adjusting the temperature of the hot melting tank to 60 ℃ to melt the ginsenoside gel, and controlling the pump flow of the hot melting tank to be 300ml/min to spray ginsenoside gel liquid into the filter stick by a pump;
C. cooling and drying
D, putting the filter stick added with the ginsenoside gel obtained in the step B on a drying rack sold by Shenzhen Longhua New district Dalangkuncui silkscreen hardware factory with a trade name Kuncui drying rack, and cooling and drying for 12.0 hours at the temperature of 25-35 ℃ and the relative humidity of 40-70% to form a ginsenoside gel strip at the central axis position of the filter stick, wherein the water content is below 2.280% by weight by adopting the method described in the specification; its diameter is 0.4 mm;
D. package with a metal layer
The cooled dried ginsenoside gel filter rods obtained in step C were seal wrapped using a wrapping device sold by Takara lathe processing in Pingyang county under the trade name BZJ paper straw packer.
The ginsenoside gel filter stick produced in the embodiment replaces a filter stick of 1956 brand cigarettes in Hongtai mountain as a test sample, and cigarette of 1956 brand cigarettes in Hongtai mountain is not changed as a comparison sample, and evaluation is carried out simultaneously according to the method described in the application specification.
Claims (10)
1. A production method of a ginsenoside gel filter stick is characterized by comprising the following steps:
A. preparation of ginsenoside gel
Dissolving 2-10 parts by weight of ginsenoside in 2-20 parts by weight of solvent to obtain a ginsenoside solution, adding 5-40 parts by weight of solidification modifier, 0.01-0.1 part by weight of emulsifier and 50-90 parts by weight of temperature phase change material into the solution, stirring and mixing uniformly, heating for dissolving, and then cooling for shaping to obtain ginsenoside gel;
B. adding ginsenoside gel
B, filling the ginsenoside gel obtained in the step A into a hot melting tank, adjusting a spray head of the hot melting tank to be aligned to the central axis of the filter stick, adjusting the temperature of the hot melting tank to 40-90 ℃ to melt the ginsenoside gel, and spraying the ginsenoside gel liquid into the filter stick by a pump;
C. cooling and drying
C, putting the filter stick added with the ginsenoside gel obtained in the step B on a drying rack in order, cooling and drying for 8-12 hours, and forming a ginsenoside gel strip at the central axis position of the filter stick;
D. package with a metal layer
And C, sealing and packaging the cooled and dried ginsenoside gel filter stick obtained in the step C.
2. The production method according to claim 1, wherein in the step A, the weight ratio of the ginsenoside, the solvent, the solidification modifier, the emulsifier and the temperature phase change material is 4-8: 6-15: 15-30: 0.03 to 0.08: 62 to 78.
3. The process according to claim 1 or 2, wherein in step A, the solvent is one or more solvents selected from the group consisting of propylene glycol, MCT, glycerol and glycerol diacetate.
4. The production process according to claim 1 or 2, wherein in the step A, the coagulation modifier is one or more coagulation modifiers selected from lauric acid, myristic acid, palmitic acid, stearic acid, arachidic acid, or behenic acid.
5. The production method according to claim 1 or the above, characterized in that in step a, the emulsifier is one or more emulsifiers selected from the group consisting of polyoxyethylene sorbitan monooleate, polyacrylamide and glyceryl monostearate.
6. The method according to claim 1 or 2, wherein in step a, the temperature phase change material is one or more temperature phase change materials selected from polyethylene glycol 1000, polyethylene glycol 1500, polyethylene glycol 2000 or polypropylene glycol.
7. The production method according to claim 1, wherein in the step A, the uniformly mixed mixture is heated and dissolved at a temperature of 40 to 90 ℃ for 30 to 90 min.
8. The production method according to claim 1, wherein in the step B, the pump flow rate of the hot melt tank is controlled to 50 to 1000 ml/min.
9. The production method according to claim 1, wherein in the step C, the cooling and drying are performed at a temperature of 25 to 35 ℃ and a relative humidity of 40 to 70% to obtain the ginsenoside gel strip having a water content of 2.280% or less by weight.
10. The method according to claim 1, wherein in step C, the diameter of the ginsenoside gel strip is 0.1-0.4 mm.
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