CN110584196A - Preparation method of blasting bead with essential oil components - Google Patents
Preparation method of blasting bead with essential oil components Download PDFInfo
- Publication number
- CN110584196A CN110584196A CN201910998610.8A CN201910998610A CN110584196A CN 110584196 A CN110584196 A CN 110584196A CN 201910998610 A CN201910998610 A CN 201910998610A CN 110584196 A CN110584196 A CN 110584196A
- Authority
- CN
- China
- Prior art keywords
- essential oil
- blasting
- beads
- bead
- preparing
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/061—Use of materials for tobacco smoke filters containing additives entrapped within capsules, sponge-like material or the like, for further release upon smoking
Abstract
The invention discloses a preparation method of a popping pearl with essential oil components, which comprises the following steps of S1, preparing essential oil essence emulsion: weighing a certain amount of purified water, adding reducing sugar and amino acid to prepare a sugar ammonia solution, adjusting the pH value of the sugar ammonia solution, adding calcium carbide and neodecanoic acid glyceride into the sugar ammonia solution, uniformly mixing, mixing the uniformly mixed solution and essential oil according to the mass ratio, stirring for emulsifying in a high-speed shearing homogenizer, and preparing the essential oil essence emulsion. The invention can realize automatic production by using the circulating flow forming liquid, ensures the multilayer composition of the coating skin structure by bead blasting crosslinking treatment, ensures that the emulsifying degree of the essence can be higher by mixing calcium carbide and the neodecanoate glyceride, can quickly diffuse in a cigarette filter tip by core liquid demulsification, has pleasant and natural fragrance of the essential oil fragrance after being pinched, can be harmonized with the fragrance of cigarettes, can effectively improve the quality of low-grade tobacco, reduces wood miscellaneous gas, increases the fragrance of the cigarettes, and has better application effect in the cigarettes.
Description
Technical Field
The invention relates to the technical field of preparation of bead blasting for cigarettes, in particular to a preparation method of bead blasting with essential oil components.
Background
The popping beads, also called as pills, brittle capsules and beads, have the feeling of popping when being squeezed, and are mainly used in cigarettes at present, namely popping bead cigarettes. The bead blasting smoke means: the cigarette with the filter tip provided with the liquid small rubber beads (the bead blasting for the cigarette) can make the cigarette more fragrant in the sucking process, strengthen the fragrance or the characteristic and make a smoker feel more comfortable. However, most of the existing bead-blasting cigarettes wrap the bead-blasting in the cigarette filter stick, so that consumers cannot see the bead-blasting in the cigarette filter stick and can only touch the bead-blasting by fingers to release essence in the bead-blasting cigarette.
Besides traditional perfuming of cigarette tobacco shreds and various auxiliary materials, various new technologies are continuously applied, such as perfuming cotton threads, embedding and the like, and bead blasting for cigarettes can be said to be the most widely applied embedding technology. However, no matter how to improve the cigarette fragrance, the method can not leave the cigarette flavor, and the existing flavor adding method has partial defects.
Disclosure of Invention
Based on the technical problems in the background art, the invention provides a preparation method of an exploded bead with essential oil components.
The invention provides a preparation method of a popping bead with essential oil components, which comprises the following steps:
s1: preparing an essential oil essence emulsion: weighing a certain amount of purified water, adding reducing sugar and amino acid to prepare a sugar ammonia solution, adjusting the pH value of the sugar ammonia solution, adding calcium carbide and neodecanoic acid glyceride into the sugar ammonia solution, uniformly mixing, mixing the uniformly mixed solution and essential oil according to a mass ratio, and stirring for emulsification in a high-speed shearing homogenizer to prepare an essential oil essence emulsion;
s2: preparing an explosive bead forming liquid: preparing sodium alginate aqueous solution, adding polysaccharide or low acyl gellan gum or glycerol, adding surfactant, adding curing agent and emulsifier, adding acetic acid, and mixing to obtain bead blasting forming solution;
s3: bead blasting and forming: circularly flowing the bead blasting forming liquid in the S2 under the action of a magnetic stirrer, dripping the essential oil and essence emulsion into the flowing bead blasting forming liquid by using three-phase flow dripping pill equipment, dripping the emulsion into the forming liquid to form a ball shape, growing until the coating skin meets the thickness requirement, removing the forming liquid or floccule on the surface of the bead by using slow running water, and fishing out;
s4: and (3) bead blasting surface crosslinking: preparing a cross-linking solution by glutaraldehyde and triglyceride, putting the washed exploded beads into the cross-linking solution to stabilize the surface of the coating, standing, washing and fishing out;
s5: and (3) bead blasting, drying and shaping: after cross-linking treatment, the blasting beads with the coating in a wet state are placed in a drying room to rapidly treat surface moisture and internal part moisture, then the blasting beads are put into a rotary drum to be dried, and the dried blasting beads are placed in a temperature and humidity balance environment to stand until the water content meets the requirement of finished blasting beads;
s6: bead blasting screening and detection: the blasting rate, the essential oil content rate, the volume and other indexes of the blasting beads are spot checked and detected through screening equipment, and the blasting beads are guaranteed not to be broken or unmatched when thrown on a production line.
Preferably, the sugar ammonia solution in S1 is prepared from any one of glucose, xylose and galactose and any one of methionine, proline, glycine, valine and proline, the calcium carbide in S1 is used as a curing agent, the neodecanoate glyceride is used as an emulsifier, and the neodecanoate glyceride is used with a viscosity increaser CMC as an auxiliary agent.
Preferably, the curing agent may be CaCO3Or CaCl2Or Ca (NO)3)2Any one, and the emulsifier can be replaced by any one of tween and span.
Preferably, the surfactant in S2 is any one of span 20, monoglyceride and sucrose ester.
Preferably, the three-phase flow dropping pill equipment comprises three-phase flow dripper equipment for outputting concentric liquid columns formed by core materials and wall materials of the blasting beads, wherein a forming structure is connected below drippers of the three-phase flow dripper equipment in a closed manner, the three-phase drippers integrate ports of water, emulsion and forming liquid, the forming structure is used for containing circulating liquid, the dripped concentric liquid columns form blasting bead dropping pills under the action of the circulating liquid, and a filtering and collecting structure is connected below the forming structure and used for screening the formed blasting beads from the circulating liquid.
Preferably, the temperature of the drying room is controlled at 150-250 ℃, the drying temperature in the rotary drum is 20-25 ℃ and the constant temperature, and the drying time is 2-2.5 h.
The beneficial effects of the invention are as follows:
1. the forming liquid which circularly flows is used in the forming process of the popping beads, so that the automatic industrial production of the popping bead forming can be realized, the formed popping beads are subjected to cross-linking treatment, the multilayer compounding of a coating skin structure is ensured, the popping beads are more stable in the drying process, the emulsifying degree of the essence can be higher by mixing the calcium carbide and the neodecanoic acid glyceride, and the bitter taste of the essence can not exist;
2. in the bead blasting forming process, the essence emulsion is dried in the coating skin and then becomes a viscous state, the essence emulsion can be quickly adsorbed at a cigarette holder, the coating skin has certain brittleness, and meanwhile, the core liquid can be demulsified, so that the bead blasting can be quickly diffused in a cigarette holder rod, after the bead blasting forming process is carried out, the essence aroma is more pleasant and natural and rich, the essential oil aroma can be harmonized with the tobacco aroma, the quality of low-grade tobacco can be effectively improved, the wood miscellaneous gas is reduced, the tobacco aroma is increased, and the bead blasting forming process has a better application effect in cigarettes.
Drawings
FIG. 1 is a preparation flow chart of the preparation method of the popsicle with essential oil components provided by the invention.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
Referring to fig. 1, a method for preparing a popping bead with essential oil components comprises the following steps:
s1: preparing an essential oil essence emulsion: weighing a certain amount of purified water, adding reducing sugar and amino acid to prepare a sugar ammonia solution, adjusting the pH value of the sugar ammonia solution, adding calcium carbide and neodecanoic acid glyceride into the sugar ammonia solution, uniformly mixing, mixing the uniformly mixed solution and essential oil according to a mass ratio, and stirring for emulsification in a high-speed shearing homogenizer to prepare an essential oil essence emulsion;
s2: preparing an explosive bead forming liquid: preparing sodium alginate aqueous solution, adding polysaccharide or low acyl gellan gum or glycerol, adding surfactant, adding curing agent and emulsifier, adding acetic acid, and mixing to obtain bead blasting forming solution;
s3: bead blasting and forming: circularly flowing the bead blasting forming liquid in the S2 under the action of a magnetic stirrer, dripping the essential oil and essence emulsion into the flowing bead blasting forming liquid by using three-phase flow dripping pill equipment, dripping the emulsion into the forming liquid to form a ball shape, growing until the coating skin meets the thickness requirement, removing the forming liquid or floccule on the surface of the bead by using slow running water, and fishing out;
s4: and (3) bead blasting surface crosslinking: preparing a cross-linking solution by glutaraldehyde and triglyceride, putting the washed exploded beads into the cross-linking solution to stabilize the surface of the coating, standing, washing and fishing out;
s5: and (3) bead blasting, drying and shaping: after cross-linking treatment, the blasting beads with the coating in a wet state are placed in a drying room to rapidly treat surface moisture and internal part moisture, then the blasting beads are put into a rotary drum to be dried, and the dried blasting beads are placed in a temperature and humidity balance environment to stand until the water content meets the requirement of finished blasting beads;
s6: bead blasting screening and detection: the blasting rate, the essential oil content rate, the volume and other indexes of the blasting beads are spot checked and detected through screening equipment, and the blasting beads are guaranteed not to be broken or unmatched when thrown on a production line.
In the invention, the sugar ammonia solution in S1 can be prepared from any one of glucose, xylose and galactose and any one of methionine, proline, glycine, valine and proline, calcium carbide in S1 is used as a curing agent, neodecanoate glyceride is used as an emulsifier, CMC is used as a tackifier when the neodecanoate glyceride is used, and CaCO is used as the curing agent3Or CaCl2Or Ca (NO)3)2Any one of the above three-phase flow dropping pill equipment with emulsifier Tween or span replacing surfactant in S2 with span 20, monoglyceride and sucrose ester comprises concentric liquid column composed of core material and wall material for outputting exploded beads, wherein the lower part of the dropping head of the three-phase flow dropping pill equipment is hermetically connected with a forming structure, the three-phase dropping head integrates ports of water, emulsion and forming liquid, the forming structure is used for containing circulating liquid, the dropped concentric liquid column forms exploded bead drop pills under the action of the circulating liquid, and the lower part of the forming structure is connected with a filtering and collecting structure for screening out formed and formed pellets from the circulating liquidThe temperature of the bead blasting drying room is controlled at 150-250 ℃, the drying temperature in the rotary drum is 20-25 ℃ and the constant temperature, and the drying time is 2-2.5 h.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and the technical solutions and the inventive concepts thereof according to the present invention should be equivalent or changed within the scope of the present invention.
Claims (6)
1. The preparation method of the popping beads with the essential oil components is characterized by comprising the following steps:
s1: preparing an essential oil essence emulsion: weighing a certain amount of purified water, adding reducing sugar and amino acid to prepare a sugar ammonia solution, adjusting the pH value of the sugar ammonia solution, adding calcium carbide and neodecanoic acid glyceride into the sugar ammonia solution, uniformly mixing, mixing the uniformly mixed solution and essential oil according to a mass ratio, and stirring for emulsification in a high-speed shearing homogenizer to prepare an essential oil essence emulsion;
s2: preparing an explosive bead forming liquid: preparing sodium alginate aqueous solution, adding polysaccharide or low acyl gellan gum or glycerol, adding surfactant, adding curing agent and emulsifier, adding acetic acid, and mixing to obtain bead blasting forming solution;
s3: bead blasting and forming: circularly flowing the bead blasting forming liquid in the S2 under the action of a magnetic stirrer, dripping the essential oil and essence emulsion into the flowing bead blasting forming liquid by using three-phase flow dripping pill equipment, dripping the emulsion into the forming liquid to form a ball shape, growing until the coating skin meets the thickness requirement, removing the forming liquid or floccule on the surface of the bead by using slow running water, and fishing out;
s4: and (3) bead blasting surface crosslinking: preparing a cross-linking solution by glutaraldehyde and triglyceride, putting the washed exploded beads into the cross-linking solution to stabilize the surface of the coating, standing, washing and fishing out;
s5: and (3) bead blasting, drying and shaping: after cross-linking treatment, the blasting beads with the coating in a wet state are placed in a drying room to rapidly treat surface moisture and internal part moisture, then the blasting beads are put into a rotary drum to be dried, and the dried blasting beads are placed in a temperature and humidity balance environment to stand until the water content meets the requirement of finished blasting beads;
s6: bead blasting screening and detection: the blasting rate, the essential oil content rate, the volume and other indexes of the blasting beads are spot checked and detected through screening equipment, and the blasting beads are guaranteed not to be broken or unmatched when thrown on a production line.
2. The method for preparing popsicles with essential oil components of claim 1, wherein the sugar ammonia solution in S1 is prepared from any one of glucose, xylose and galactose and any one of methionine, proline, glycine, valine and proline, the calcium carbide in S1 is a curing agent, the neodecanoate glyceride is an emulsifier, and the neodecanoate glyceride is supplemented with CMC (carboxy methyl cellulose) as a tackifier.
3. A method for preparing a popple with essential oil component as claimed in claim 2, wherein the solidifying agent is CaCO3Or CaCl2Or Ca (NO)3)2Any one, and the emulsifier can be replaced by any one of tween and span.
4. The method for preparing popping pearls with essential oil components, which is characterized in that the surfactant in the S2 is any one of span 20, monoglyceride and sucrose ester.
5. The method for preparing popping beads with essential oil components, according to claim 1, wherein the three-phase flow dropping pill device comprises a three-phase flow dropper device for outputting concentric liquid columns formed by core materials and wall materials of popping beads, wherein a forming structure is connected below the dropper of the three-phase flow dropper device in a closed manner, the three-phase dropper device integrates ports of water, emulsion and forming liquid, the forming structure is used for containing circulating liquid, the dropped concentric liquid columns form popping bead dropping pills under the action of the circulating liquid, and a filtering and collecting structure is connected below the forming structure and used for screening out the formed popping beads from the circulating liquid.
6. The method for preparing exploded beads with essential oil components as claimed in claim 1, wherein the temperature of the drying chamber is controlled at 150 ℃ to 250 ℃, the drying temperature in the rotary drum is 20-25 ℃ and the constant temperature, and the drying time is 2-2.5 h.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910998610.8A CN110584196A (en) | 2019-10-21 | 2019-10-21 | Preparation method of blasting bead with essential oil components |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201910998610.8A CN110584196A (en) | 2019-10-21 | 2019-10-21 | Preparation method of blasting bead with essential oil components |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110584196A true CN110584196A (en) | 2019-12-20 |
Family
ID=68851267
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201910998610.8A Pending CN110584196A (en) | 2019-10-21 | 2019-10-21 | Preparation method of blasting bead with essential oil components |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN110584196A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112168891A (en) * | 2020-09-30 | 2021-01-05 | 石家庄以岭药业股份有限公司 | Preparation method and application of essential oil blasting bead containing traditional Chinese medicine composition |
Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102824887A (en) * | 2012-09-14 | 2012-12-19 | 云南烟草科学研究院 | Preparation method of controlled-release soft capsules for cigarettes |
| CN103045360A (en) * | 2012-12-06 | 2013-04-17 | 深圳波顿香料有限公司 | Cigarette filter stick essence capsule, method for preparing same and cigarette |
| US20140147396A1 (en) * | 2012-11-27 | 2014-05-29 | Sol-Gel Technologies Ltd. | Compositions for the treatment of rosacea |
| CN105419349A (en) * | 2015-12-14 | 2016-03-23 | 贵州中烟工业有限责任公司 | Cigarette capsule wall material with humidity resistance and application thereof |
| CN105536656A (en) * | 2015-12-14 | 2016-05-04 | 贵州中烟工业有限责任公司 | Brittle capsules for tobacco products and production method and application thereof |
| CN106387990A (en) * | 2016-11-22 | 2017-02-15 | 中国烟草总公司郑州烟草研究院 | High-nicotine tobacco extract and application thereof |
| CN108851216A (en) * | 2018-08-28 | 2018-11-23 | 中国烟草总公司郑州烟草研究院 | A kind of wax packet emulsion type cigarette capsule and preparation method thereof |
| CN109536280A (en) * | 2018-11-27 | 2019-03-29 | 湖北中烟工业有限责任公司 | The quick-fried pearl preparation method of cigarette of internal essence further progress Maillard reaction after molding |
| CN109628230A (en) * | 2019-02-20 | 2019-04-16 | 上海烟草集团有限责任公司 | A kind of preparation method and application of natural tobacco aromaticss |
| CN109907367A (en) * | 2019-03-01 | 2019-06-21 | 江西中烟工业有限责任公司 | A kind of quick-fried pearl of cigarette gel and preparation method thereof |
| CN110122921A (en) * | 2019-04-25 | 2019-08-16 | 贵州兰馨时尚茶品有限公司 | A kind of preparation method of the quick-fried pearl of black tea |
| CN110283661A (en) * | 2019-07-03 | 2019-09-27 | 云南氪莱铂科技有限公司 | A kind of quick-fried pearl of cigarette gel and preparation method thereof |
-
2019
- 2019-10-21 CN CN201910998610.8A patent/CN110584196A/en active Pending
Patent Citations (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102824887A (en) * | 2012-09-14 | 2012-12-19 | 云南烟草科学研究院 | Preparation method of controlled-release soft capsules for cigarettes |
| US20140147396A1 (en) * | 2012-11-27 | 2014-05-29 | Sol-Gel Technologies Ltd. | Compositions for the treatment of rosacea |
| CN103045360A (en) * | 2012-12-06 | 2013-04-17 | 深圳波顿香料有限公司 | Cigarette filter stick essence capsule, method for preparing same and cigarette |
| CN105419349A (en) * | 2015-12-14 | 2016-03-23 | 贵州中烟工业有限责任公司 | Cigarette capsule wall material with humidity resistance and application thereof |
| CN105536656A (en) * | 2015-12-14 | 2016-05-04 | 贵州中烟工业有限责任公司 | Brittle capsules for tobacco products and production method and application thereof |
| CN106387990A (en) * | 2016-11-22 | 2017-02-15 | 中国烟草总公司郑州烟草研究院 | High-nicotine tobacco extract and application thereof |
| CN108851216A (en) * | 2018-08-28 | 2018-11-23 | 中国烟草总公司郑州烟草研究院 | A kind of wax packet emulsion type cigarette capsule and preparation method thereof |
| CN109536280A (en) * | 2018-11-27 | 2019-03-29 | 湖北中烟工业有限责任公司 | The quick-fried pearl preparation method of cigarette of internal essence further progress Maillard reaction after molding |
| CN109628230A (en) * | 2019-02-20 | 2019-04-16 | 上海烟草集团有限责任公司 | A kind of preparation method and application of natural tobacco aromaticss |
| CN109907367A (en) * | 2019-03-01 | 2019-06-21 | 江西中烟工业有限责任公司 | A kind of quick-fried pearl of cigarette gel and preparation method thereof |
| CN110122921A (en) * | 2019-04-25 | 2019-08-16 | 贵州兰馨时尚茶品有限公司 | A kind of preparation method of the quick-fried pearl of black tea |
| CN110283661A (en) * | 2019-07-03 | 2019-09-27 | 云南氪莱铂科技有限公司 | A kind of quick-fried pearl of cigarette gel and preparation method thereof |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112168891A (en) * | 2020-09-30 | 2021-01-05 | 石家庄以岭药业股份有限公司 | Preparation method and application of essential oil blasting bead containing traditional Chinese medicine composition |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105813486B (en) | Smoking product with liquid release component | |
| JP2022519878A (en) | Filling material blended with aerosol-forming materials | |
| CN107802032A (en) | A kind of discontinuous temperature causes production method and the application of the fragrant filter stick of phase change gel load | |
| JP2022519754A (en) | Reconstructed cacao husk fiber material | |
| HUE029271T2 (en) | Smoking article with liquid delivery material | |
| CN114269168B (en) | Reconstituted cocoa material for aerosol generation | |
| CN109480329A (en) | A kind of emulsion process prepares the cigarette method of quick-fried pearl | |
| CN105813485B (en) | Smoking article with liquid delivery material | |
| CN107156903B (en) | Cigarette filter tip particle material with double-layer structure and manufacturing method thereof | |
| CN112656024A (en) | Preparation method of cooling and aroma-enhancing particles for HNB (household Natural gas) cigarettes and cooling and aroma-enhancing particles for HNB cigarettes | |
| CN105105334A (en) | Spice slow-release filter tip additive with polymer covering film as well as preparation method and application thereof | |
| AU2014375322A1 (en) | Smoking article with liquid release component | |
| CN104687233B (en) | The preparation method and orange flavor reconstituted tobacco of a kind of orange flavor reconstituted tobacco | |
| CN109007971A (en) | A kind of slow-release fragrance gel combination and preparation method thereof | |
| CN109875113B (en) | Graphene-based cigarette core line and preparation method and application thereof | |
| CN106723341A (en) | Fragrance slow-release material composition and sustained release spices colloid and application thereof | |
| CN104172471A (en) | Brittle capsule with ginseng characteristic aroma as well as preparation method and application thereof | |
| CN202774109U (en) | Filter stick containing aroma slow release capsule for cigarette | |
| CN113100477A (en) | Puffed bead for fragrant cigarettes and preparation method thereof | |
| CN110584196A (en) | Preparation method of blasting bead with essential oil components | |
| CN108936800A (en) | Tobacco hollow bead and preparation method thereof and cigarette filter rod | |
| CN104910863A (en) | Filter rod center line rubber and preparation process thereof | |
| CN111184247B (en) | Polyvinyl alcohol-based fragrance slow-release material, composite sheet, preparation method of composite sheet and application of composite sheet in heating non-combustible tobacco products | |
| CN111184256A (en) | Sugar candy orange essence bead for cigarettes and preparation method thereof | |
| CN109645555A (en) | A kind of preparation method and application for the fruity perfume (or spice) line in Novel heating not burning tobacco |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20191220 |
|
| RJ01 | Rejection of invention patent application after publication |