CN105105334A - Spice slow-release filter tip additive with polymer covering film as well as preparation method and application thereof - Google Patents

Spice slow-release filter tip additive with polymer covering film as well as preparation method and application thereof Download PDF

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Publication number
CN105105334A
CN105105334A CN201510421524.2A CN201510421524A CN105105334A CN 105105334 A CN105105334 A CN 105105334A CN 201510421524 A CN201510421524 A CN 201510421524A CN 105105334 A CN105105334 A CN 105105334A
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China
Prior art keywords
filter tip
coated
molecular film
cigarette
spice
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CN201510421524.2A
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Chinese (zh)
Inventor
何沛
刘春波
申钦鹏
刘志华
王昆淼
张凤梅
司晓喜
朱瑞芝
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China Tobacco Yunnan Industrial Co Ltd
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China Tobacco Yunnan Industrial Co Ltd
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Priority to CN201510421524.2A priority Critical patent/CN105105334A/en
Publication of CN105105334A publication Critical patent/CN105105334A/en
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Abstract

The invention relates to a spice slow-release filter tip additive with a polymer covering film as well as a preparation method and an application thereof, which belong to the technical field of cigarettes. The spice slow-release filter tip additive with the polymer covering film is of a three-layer sandwich structure, an inner core is made from porous materials, the covering film is made from polymers, and spices are fixed in a middle layer of the additive. The filter tip additive is added to a cigarette holder in an adding manner of ordinary filter tip particles, so as to prepare a cigarette. When the cigarette is smoked, the position of the particles in a filter tip is kneaded by hand, so that the spices in a sandwich layer are released, the aroma and flavor of smoke are increased, and the quality of the cigarette is increased. After the filter tip additive which is prepared by using the method is added to the cigarette, the non-burning section of the cigarette can be effectively perfumed, so that the aroma in an early manufacturing stage is prevented from being quickly volatilized, and the aroma and flavor of the cigarette can be kept for a long time.

Description

Spice slow-releasing additives of filter tip of a kind of coated by high-molecular film and preparation method thereof and application
Technical field
The invention belongs to technical field of cigarettes, spice slow-releasing additives of filter tip being specifically related to a kind of coated by high-molecular film and preparation method thereof and application.
Background technology
Since first cigarette filter making filtering material with cotton from nineteen thirty comes out, filter tip just becomes a pith in Cigarette design.But until the 1950's, along with the exploitation of acetate fiber, cigarette with filter tip just starts the accreditation obtaining consumer.Along with the progress of tobacco science and technology and the continuous change of consumer demand, cigarette filter plays more and more key player in cigarette.The effect of cigarette filter has been transitioned into carrying brand culture from the effect of simple filtration flue gas, and the effect of transmitting product individuality comes up.Especially, in high-grade cigarette, it had both embodied image and the individual character of product, had enriched again high quality, improved the price grade of product.
In the last few years, there is darker change in cigarette filter, from common single cellulose acetate filter, to polynary filter tip, and the filter tip future development that multiple material is made.These novel filter tips obtain the favor of cigarette manufacturer and consumer just gradually.The functional filter tip of flavouring humectation type also increases gradually, but the flavored type filter tip used at present exists same problem mostly, and namely fragrance component release is very fast.Although short-term is deposited generally can not affect suction kind, long-term storage, especially long-term storage under hot environment, spices loses in mouth rod will become comparatively obvious.Therefore how overcoming the deficiencies in the prior art is problems that current technical field of cigarettes needs solution badly.
Summary of the invention
The object of the invention is to solve the deficiencies in the prior art, spice slow-releasing additives of filter tip that a kind of coated by high-molecular film is provided and preparation method thereof, adopting three-layer sandwich frame mode, spices being fixed on the middle level of additive.After the additives of filter tip using the inventive method to prepare adds cigarette, effectively can carry out perfuming in cigarette non-burning section, stop the fragrance at manufacture initial stage to volatilize fast, make cigarette keep flavor and taste for a long time.
The technical solution used in the present invention is as follows:
A preparation method for the spice slow-releasing additives of filter tip of coated by high-molecular film, in comprising the steps: porous material particle to drop into and adsorbing in spices or spice solution, after having adsorbed, is dried to porous material particle and does not hang with drop; Again porous material particle is immersed in Polymer Solution and take out drying after 30-60 minute, to forming one deck polymeric membrane at porous material particle surface, namely obtain taking porous material as core, middle level is spices, and macromolecule is the three-layer sandwich type spice slow-releasing additives of filter tip of film;
In described Polymer Solution, solute and spices do not dissolve each other, and solvent is innoxious solvent.The granular size of porous material particle is not limit, obviously can feel particle during hand extruding filter tip.
Further, preferably, described porous material is active carbon, montmorillonite, molecular sieve, sponge or porous resin.
Further, preferably, described spices is hydrophilic fragrance or hydrophobicity spices.
Further, preferably, described spices is water.
Further, preferably, described macromolecule has certain loose structure, and can water-soluble or ethanol; In described Polymer Solution, high molecular mass concentration is 3%-10%, and the solvent of Polymer Solution is water or ethanol.
Further, preferably, described Polymer Solution is the ethanolic solution of the aqueous solution of sodium alginate, the aqueous solution of polyvinylpyrrolidone, the aqueous solution of silica gel or ethyl cellulose.
Further, preferably, the preparation method of the spice slow-releasing additives of filter tip of described coated by high-molecular film, comprises the steps:
Be that 2.8-3.3mm sponge particles drops in pure water by diameter, after having adsorbed, be dried to sponge particles and do not hang with water droplet; Sponge particles being immersed mass concentration is in the ethanolic solution of the ethyl cellulose of 5% again, takes out dry after 4s, forms one deck polymeric membrane, namely obtain the spice slow-releasing additives of filter tip of coated by high-molecular film on sponge particles surface.
Further, preferably, the preparation method of the spice slow-releasing additives of filter tip of described coated by high-molecular film, comprises the steps:
Be that 1.8-2.2mm activated carbon granule drops in Rosa Damascana by diameter, after having adsorbed, be dried to Rosa Damascana and do not hang with oil droplet; Activated carbon granule being immersed mass concentration is in the sodium alginate aqueous solution of 10% again, takes out dry after 4s, forms one deck polymeric membrane, namely obtain the spice slow-releasing additives of filter tip of coated by high-molecular film on activated carbon granule surface.
The application of spice slow-releasing additives of filter tip in cigarette of the coated by high-molecular film that above-mentioned preparation method obtains.
The application of spice slow-releasing additives of filter tip in cigarette of the coated by high-molecular film that above-mentioned preparation method obtains, it is characterized in that, the spice slow-releasing additives of filter tip of coated by high-molecular film is joined in mouth rod in the mode that common filter tip particle adds, can be often prop up mouth rod one, also can be often prop up mouth rod many, then make cigarette.
Common porous material is made graininess by the present invention, drop in spices or spice solution and carry out spices absorption, utilize porous material by sorbing material surface in the molecule short time of spices, when being dried to rapidly after porous material particle do not hang with drop after absorption completes, immerse in Polymer Solution rapidly again, make its surface form one deck coated by high-molecular film.This polymeric membrane is porous polymeric membranes, can stop the quick volatilization of perfume molecules, but is unlikely to hinder oozing out of follow-up perfume molecules.When cigarette smoking, can rub this additive granules with the hands by pinching with hand, the spices of partial adsorbates then because of squeezing action, and can ooze out from the hole of polymeric membrane; In addition, polymeric membrane also can be punctured by porous material particle or crush, and releases spices, thus reaches the effect of flue gas flavouring.
compared with prior art, its beneficial effect is in the present invention:
The spice slow-releasing additives of filter tip that the preparation method of the spice slow-releasing additives of filter tip of coated by high-molecular film of the present invention obtains adopts three-layer sandwich structure, porous material also increases the volume of additive while absorption spices, save the consumption of spices, compared with conventional method, saved the consumption of 45-62%, and sample treatment is simple, controllability is good, product is stablized, and security is high.
The spice slow-releasing additives of filter tip of coated by high-molecular film of the present invention has good slow release effect, and adds in cigarette, substantially prolongs the release time of fragrance component and can not affect the resting period of suction; Compared with conventional method, the sustained release time of fragrance component adds 0.8-1.3 doubly, and the resting period that can not affect suction is 2-3 times of traditional product.
Compared with wrapping up spices method with traditional dripping pill, additive spices release of the present invention more relaxes, and can not significantly change cigarette sense organ style because of the using method of the surface breakdown of traditional dripping pill.Traditional mouth rod dripping pill uses and all adopts flash disruption top layer, makes all release of spices moment; And the method that additive of the present invention adopts spices to permeate via polymeric membrane hole, spices is discharged and more relaxes, do not affect cigarette sense organ style.
Accompanying drawing explanation
The structural representation of the spice slow-releasing filter tip particulate additive of Fig. 1 coated by high-molecular film of the present invention.
Wherein, 1-porous material, the spices of 2-load, 3-polymeric membrane.
Detailed description of the invention
Below in conjunction with embodiment, the present invention is described in further detail.
It will be understood to those of skill in the art that the following example only for illustration of the present invention, and should not be considered as limiting scope of the present invention.Unreceipted concrete technology or condition person in embodiment, according to the technology described by the document in this area or condition or carry out according to product description.Agents useful for same or the unreceipted production firm person of instrument, being can by buying the conventional products obtained.
The present invention after having adsorbed, is dried to porous material particle and does not hang with drop in being dropped into by porous material particle and adsorbing in spices or spices or spice solution; Again porous material particle being immersed in Polymer Solution and take out drying after 30-60 minute, to forming one deck polymeric membrane at porous material particle surface, namely obtaining filter tip particulate additive as shown in Figure 1.Filter tip particulate additive is three-layer sandwich type spice slow-releasing additives of filter tip, and with porous material 1 for core, middle level is the spices 2 of load, and surface is polymeric membrane 3; The mode that this additives of filter tip adds with common filter tip particle is joined in mouth rod, and prepares cigarette.When aspirating this cigarette, pinch the position of this particle on filter tip with hand rubbing, the spices in sandwich of layers is discharged, increase the flavor and taste of flue gas, improve cigarette quality.
Embodiment 1
Be in the sponge particles input pure water of 2.8-3.3mm by diameter, after having adsorbed, dry a little, particle is not dripped.Particle being dropped into mass concentration is in the ethanolic solution of the ethyl cellulose of 5% again, can take out drying after 4s, and namely obtaining sponge is core, and middle level is water, and ethyl cellulose is the three-layer sandwich type additives of filter tip of film.The mode that this additives of filter tip adds with common filter tip particle is joined in mouth rod, and prepares cigarette.When aspirating this cigarette, pinch the position of this particle on filter tip with hand rubbing, the water in sandwich of layers is discharged, reach the requirement increasing flue gas moisture content.
Embodiment 2
Be in the porous resin particle input peppermint oil of about 3mm by diameter, after having adsorbed, dry a little, make particle surface not hang oil droplet.Be in the sodium alginate aqueous solution of 10% particle being dropped into mass concentration, can remove drying after 4s, namely obtaining porous resin particle is core, and middle level is peppermint oil, and sodium alginate is the three-layer sandwich type additives of filter tip of film.The mode that this additives of filter tip adds with common filter tip particle is joined in mouth rod, and prepares cigarette.When aspirating this cigarette, pinch the position of this particle on filter tip with hand rubbing, the peppermint oil in sandwich of layers is discharged, reaches and improve flue gas flavor and taste, increase the effect of oral cavity and the refrigerant sense of nasal cavity.
Embodiment 3
Be in the activated carbon granule input Rosa Damascana of 1.8-2.2mm by diameter, after having adsorbed, dry a little, make particle surface not hang oil droplet.Be in the sodium alginate aqueous solution of 10% particle being dropped into mass concentration, can remove drying after 3s, namely obtaining activated carbon granule is core, and middle level is Rosa Damascana, and sodium alginate is the three-layer sandwich type additives of filter tip of film.The mode that this additives of filter tip adds with common filter tip particle is joined in mouth rod, and prepares cigarette.When aspirating this cigarette, pinch the position of this particle on filter tip with hand rubbing, the Rosa Damascana in sandwich of layers is discharged, reaches and improve flue gas flavor and taste, promote the effect of cigarette quality.
Embodiment 4
Be that in the hexane solution of porous resin particle input ambroxide of about 2mm, wherein the mass percentage concentration of ambroxide is 18%, after having adsorbed, dry a little, makes particle surface not hang oil droplet by diameter.Be in the aqueous povidone solution of 3% particle being dropped into mass concentration, can remove drying after 5s, namely obtaining porous resin particle is core, and middle level is ambroxide, and polyvinylpyrrolidone is the three-layer sandwich type additives of filter tip of film.The mode that this additives of filter tip adds with common filter tip particle is joined in mouth rod, and prepares cigarette.When aspirating this cigarette, pinch the position of this particle on filter tip with hand rubbing, the ambroxide in sandwich of layers is discharged, reaches and improve flue gas flavor and taste, promote the effect of cigarette quality.
Embodiment 5
Be in the porous resin particle input vanilla essential oil of about 2mm by diameter, after having adsorbed, dry a little, make particle surface not hang oil droplet.Be in the aqueous solution of silica gel of 10% particle being dropped into mass concentration, can remove drying after 3-5s, namely obtaining porous resin particle is core, and middle level is vanilla absolute oil, and silica gel is the three-layer sandwich type additives of filter tip of film.The mode that this additives of filter tip adds with common filter tip particle is joined in mouth rod, and prepares cigarette.When aspirating this cigarette, pinch the position of this particle on filter tip with hand rubbing, the vanilla absolute oil in sandwich of layers is discharged, reaches and improve flue gas flavor and taste, promote the effect of cigarette quality.
Embodiment 6
Be in the montmorillonite particle input geraniol of about 1mm by diameter, after having adsorbed, dry a little, make particle surface not hang oil droplet.Be in the ethyl cellulose ethanolic solution of 7% particle being dropped into mass concentration, can remove drying after 3-5s, namely obtaining montmorillonite particle is core, and middle level is geraniol, and ethyl cellulose is the three-layer sandwich type additives of filter tip of film.The mode that this additives of filter tip adds with common filter tip particle is joined in mouth rod, and prepares cigarette.When aspirating this cigarette, pinch the position of this particle on filter tip with hand rubbing, the geraniol in sandwich of layers is discharged, reaches and improve flue gas flavor and taste, promote the effect of cigarette quality.
Embodiment 7
Be in the gama-alumina sieve particle input anise alcohol of about 1mm by diameter, after having adsorbed, dry a little, make particle surface not hang oil droplet.Be in the ethyl cellulose ethanolic solution of 4% particle being dropped into mass concentration, can remove drying after 3-5s, namely obtaining gama-alumina sieve particle is core, and middle level is anise alcohol, and ethyl cellulose is the three-layer sandwich type additives of filter tip of film.The mode that this additives of filter tip adds with common filter tip particle is joined in mouth rod, and prepares cigarette.When aspirating this cigarette, pinch the position of this particle on filter tip with hand rubbing, the anise alcohol in sandwich of layers is discharged, reaches and improve flue gas flavor and taste, promote the effect of cigarette quality.
More than show and describe general principle of the present invention, principal character and advantage of the present invention.The technical staff of the industry should understand; the present invention is not restricted to the described embodiments; what describe in above-described embodiment and description just illustrates principle of the present invention; without departing from the spirit and scope of the present invention; the present invention also has various changes and modifications, and these changes and improvements all fall in the claimed scope of the invention.Application claims protection domain is defined by appending claims and equivalent thereof.

Claims (10)

1. the preparation method of the spice slow-releasing additives of filter tip of a coated by high-molecular film, it is characterized in that, in comprising the steps: porous material particle to drop into and adsorbing in spices or spice solution, after having adsorbed, be dried to porous material particle and do not hang with drop; Again porous material particle is immersed in Polymer Solution and take out drying after 30-60 minute, to forming one deck polymeric membrane at porous material particle surface, namely obtain taking porous material as core, middle level is spices, and macromolecule is the three-layer sandwich type spice slow-releasing additives of filter tip of film;
Macromolecule in described Polymer Solution and spices do not dissolve each other, and solvent is innoxious solvent.
2. the preparation method of the spice slow-releasing additives of filter tip of coated by high-molecular film according to claim 1, is characterized in that, described porous material is active carbon, montmorillonite, molecular sieve, sponge or porous resin.
3. the preparation method of the spice slow-releasing additives of filter tip of coated by high-molecular film according to claim 1, is characterized in that, described spices is hydrophilic fragrance or hydrophobicity spices.
4. the preparation method of the spice slow-releasing additives of filter tip of coated by high-molecular film according to claim 1, is characterized in that, described spices is water.
5. the preparation method of the spice slow-releasing additives of filter tip of coated by high-molecular film according to claim 1, is characterized in that, described macromolecule has loose structure, and can water-soluble or ethanol, and in Polymer Solution, high molecular mass concentration is 3%-10%; The solvent of Polymer Solution is water or ethanol.
6. the preparation method of the spice slow-releasing additives of filter tip of coated by high-molecular film according to claim 1, it is characterized in that, described Polymer Solution is the ethanolic solution of the aqueous solution of sodium alginate, the aqueous solution of polyvinylpyrrolidone, the aqueous solution of silica gel or ethyl cellulose.
7. the preparation method of the spice slow-releasing additives of filter tip of coated by high-molecular film according to claim 1, is characterized in that, comprise the steps:
Be that 2.8-3.3mm sponge particles drops in pure water by diameter, after having adsorbed, be dried to sponge particles and do not hang with water droplet; Sponge particles being immersed mass concentration is in the ethanolic solution of the ethyl cellulose of 5% again, takes out dry after 4s, forms one deck polymeric membrane, namely obtain the spice slow-releasing additives of filter tip of coated by high-molecular film on sponge particles surface.
8. the preparation method of the spice slow-releasing additives of filter tip of coated by high-molecular film according to claim 1, is characterized in that, comprise the steps:
Be that 1.8-2.2mm activated carbon granule drops in Rosa Damascana by diameter, after having adsorbed, be dried to Rosa Damascana and do not hang with oil droplet; Activated carbon granule being immersed mass concentration is in the sodium alginate aqueous solution of 10% again, takes out dry after 4s, forms one deck polymeric membrane, namely obtain the spice slow-releasing additives of filter tip of coated by high-molecular film on activated carbon granule surface.
9. the application of spice slow-releasing additives of filter tip in cigarette of the coated by high-molecular film that the preparation method of the spice slow-releasing additives of filter tip of the coated by high-molecular film described in claim 1-8 obtains.
10. the application of spice slow-releasing additives of filter tip in cigarette of coated by high-molecular film that obtain of the preparation method of the spice slow-releasing additives of filter tip of coated by high-molecular film according to claim 9, it is characterized in that, the spice slow-releasing additives of filter tip of coated by high-molecular film is joined in mouth rod in the mode that common filter tip particle adds, can be often prop up mouth rod one, also can be often prop up mouth rod many, then make cigarette.
CN201510421524.2A 2015-07-17 2015-07-17 Spice slow-release filter tip additive with polymer covering film as well as preparation method and application thereof Pending CN105105334A (en)

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CN106418687A (en) * 2016-11-11 2017-02-22 湖北中烟工业有限责任公司 Preparation of novel cigarette sweet material and application method thereof
CN107028218A (en) * 2017-05-25 2017-08-11 云南中烟工业有限责任公司 A kind of method for preparing geranyl acetone slow-release material
CN107156905A (en) * 2017-06-16 2017-09-15 云南中烟工业有限责任公司 A kind of manufacture method of cigarette filter tip particle
CN108618198A (en) * 2018-04-04 2018-10-09 华南农业大学 A kind of control release type flavouring essence for tobacco film and its preparation method and application
CN109645561A (en) * 2019-02-18 2019-04-19 重庆中烟工业有限责任公司 Cigarette capsule and preparation method thereof and cigarette filter
CN109700071A (en) * 2019-03-01 2019-05-03 南通醋酸纤维有限公司 A kind of structure, preparation method and application that can quickly reduce cigarette smoke temperature
CN109875114A (en) * 2019-04-17 2019-06-14 云南中烟工业有限责任公司 A kind of cigarette functional microsphere and the preparation method and application thereof with nucleocapsid interlayer structure
CN109965346A (en) * 2019-04-18 2019-07-05 江西中烟工业有限责任公司 A kind of cigarette filter tip preparation method of bulky grain solid-state perfume (or spice) pearl
CN110720662A (en) * 2019-10-29 2020-01-24 重庆中烟工业有限责任公司 Special-shaped composite filter tip rod
CN110801049A (en) * 2019-11-07 2020-02-18 云南中烟工业有限责任公司 Cigarette filter tip aroma sustained-release particles and preparation method thereof
CN111150094A (en) * 2018-11-08 2020-05-15 湖南中烟工业有限责任公司 Superfine fiber functional filter stick tow with fragrance carrying and smoke phenol content selectively reducing functions and preparation and application thereof

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CN106418687B (en) * 2016-11-11 2019-09-10 湖北中烟工业有限责任公司 A kind of preparation of new cigarette sweet material and its application method
CN106418687A (en) * 2016-11-11 2017-02-22 湖北中烟工业有限责任公司 Preparation of novel cigarette sweet material and application method thereof
CN107028218A (en) * 2017-05-25 2017-08-11 云南中烟工业有限责任公司 A kind of method for preparing geranyl acetone slow-release material
CN107028218B (en) * 2017-05-25 2019-10-11 云南中烟工业有限责任公司 A method of preparing geranyl acetone slow-release material
CN107156905A (en) * 2017-06-16 2017-09-15 云南中烟工业有限责任公司 A kind of manufacture method of cigarette filter tip particle
CN108618198B (en) * 2018-04-04 2020-08-07 华南农业大学 Controlled-release tobacco essence film and preparation method and application thereof
CN108618198A (en) * 2018-04-04 2018-10-09 华南农业大学 A kind of control release type flavouring essence for tobacco film and its preparation method and application
CN111150094A (en) * 2018-11-08 2020-05-15 湖南中烟工业有限责任公司 Superfine fiber functional filter stick tow with fragrance carrying and smoke phenol content selectively reducing functions and preparation and application thereof
CN109645561A (en) * 2019-02-18 2019-04-19 重庆中烟工业有限责任公司 Cigarette capsule and preparation method thereof and cigarette filter
CN109700071A (en) * 2019-03-01 2019-05-03 南通醋酸纤维有限公司 A kind of structure, preparation method and application that can quickly reduce cigarette smoke temperature
CN109875114A (en) * 2019-04-17 2019-06-14 云南中烟工业有限责任公司 A kind of cigarette functional microsphere and the preparation method and application thereof with nucleocapsid interlayer structure
CN109875114B (en) * 2019-04-17 2021-09-14 云南中烟工业有限责任公司 Functional microsphere with core-shell sandwich structure for cigarettes and preparation method and application thereof
CN109965346A (en) * 2019-04-18 2019-07-05 江西中烟工业有限责任公司 A kind of cigarette filter tip preparation method of bulky grain solid-state perfume (or spice) pearl
CN109965346B (en) * 2019-04-18 2021-06-08 江西中烟工业有限责任公司 Preparation method of large-particle solid aromatic beads for cigarette filter tip rod
CN110720662A (en) * 2019-10-29 2020-01-24 重庆中烟工业有限责任公司 Special-shaped composite filter tip rod
CN110801049A (en) * 2019-11-07 2020-02-18 云南中烟工业有限责任公司 Cigarette filter tip aroma sustained-release particles and preparation method thereof

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