CN111802687B - Atomizing agent containing conjugated linoleic acid and saponin and cigarette without burning during heating - Google Patents
Atomizing agent containing conjugated linoleic acid and saponin and cigarette without burning during heating Download PDFInfo
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- CN111802687B CN111802687B CN202010731911.7A CN202010731911A CN111802687B CN 111802687 B CN111802687 B CN 111802687B CN 202010731911 A CN202010731911 A CN 202010731911A CN 111802687 B CN111802687 B CN 111802687B
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- saponin
- linoleic acid
- atomizing agent
- conjugated linoleic
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- 239000003795 chemical substances by application Substances 0.000 title claims abstract description 43
- 229940108924 conjugated linoleic acid Drugs 0.000 title claims abstract description 37
- JBYXPOFIGCOSSB-GOJKSUSPSA-N 9-cis,11-trans-octadecadienoic acid Chemical compound CCCCCC\C=C\C=C/CCCCCCCC(O)=O JBYXPOFIGCOSSB-GOJKSUSPSA-N 0.000 title claims abstract description 36
- OYHQOLUKZRVURQ-IXWMQOLASA-N linoleic acid Natural products CCCCC\C=C/C\C=C\CCCCCCCC(O)=O OYHQOLUKZRVURQ-IXWMQOLASA-N 0.000 title claims abstract description 36
- 229930182490 saponin Natural products 0.000 title claims abstract description 31
- 150000007949 saponins Chemical class 0.000 title claims abstract description 31
- 239000001397 quillaja saponaria molina bark Substances 0.000 title claims abstract description 28
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 16
- 235000017709 saponins Nutrition 0.000 title abstract description 26
- 238000010438 heat treatment Methods 0.000 title abstract description 15
- 238000010521 absorption reaction Methods 0.000 claims abstract description 18
- 239000002904 solvent Substances 0.000 claims abstract description 12
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 51
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 45
- 241000208125 Nicotiana Species 0.000 claims description 29
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 29
- 229930187719 Soyasaponin Natural products 0.000 claims description 12
- KYWSCMDFVARMPN-LCSVLAELSA-N Saikosaponin D Chemical compound O([C@@H]1[C@@H](O)[C@H](O[C@@H]2[C@@]([C@H]3[C@]([C@@H]4[C@@]([C@@]5(C[C@@H](O)[C@]67CO[C@]5([C@@H]6CC(C)(C)CC7)C=C4)C)(C)CC3)(C)CC2)(C)CO)O[C@@H]([C@@H]1O)C)[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O KYWSCMDFVARMPN-LCSVLAELSA-N 0.000 claims description 4
- 229930192014 saikosaponin Natural products 0.000 claims description 4
- 238000010348 incorporation Methods 0.000 claims description 3
- 239000002994 raw material Substances 0.000 claims description 3
- 229930182494 ginsenoside Natural products 0.000 claims description 2
- 229940089161 ginsenoside Drugs 0.000 claims description 2
- 229930187479 gypenoside Natural products 0.000 claims description 2
- ZRBFCAALKKNCJG-UHFFFAOYSA-N gypenoside-XVII Natural products C1CC(C2(CCC3C(C)(C)C(OC4C(C(O)C(O)C(CO)O4)O)CCC3(C)C2CC2O)C)(C)C2C1C(C)(CCC=C(C)C)OC(C(C(O)C1O)O)OC1COC1OC(CO)C(O)C(O)C1O ZRBFCAALKKNCJG-UHFFFAOYSA-N 0.000 claims description 2
- 239000000463 material Substances 0.000 claims description 2
- 229930189407 platycodin Natural products 0.000 claims description 2
- 230000001953 sensory effect Effects 0.000 abstract description 3
- 235000019505 tobacco product Nutrition 0.000 abstract description 3
- 230000000391 smoking effect Effects 0.000 abstract description 2
- 238000000889 atomisation Methods 0.000 abstract 1
- 238000003756 stirring Methods 0.000 description 30
- 239000000779 smoke Substances 0.000 description 10
- 230000000052 comparative effect Effects 0.000 description 8
- 238000005303 weighing Methods 0.000 description 8
- 238000002156 mixing Methods 0.000 description 6
- 239000000203 mixture Substances 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 238000011282 treatment Methods 0.000 description 5
- 238000000034 method Methods 0.000 description 4
- 239000000443 aerosol Substances 0.000 description 3
- 238000004880 explosion Methods 0.000 description 3
- 238000005507 spraying Methods 0.000 description 3
- TWCMVXMQHSVIOJ-UHFFFAOYSA-N Aglycone of yadanzioside D Natural products COC(=O)C12OCC34C(CC5C(=CC(O)C(O)C5(C)C3C(O)C1O)C)OC(=O)C(OC(=O)C)C24 TWCMVXMQHSVIOJ-UHFFFAOYSA-N 0.000 description 2
- PLMKQQMDOMTZGG-UHFFFAOYSA-N Astrantiagenin E-methylester Natural products CC12CCC(O)C(C)(CO)C1CCC1(C)C2CC=C2C3CC(C)(C)CCC3(C(=O)OC)CCC21C PLMKQQMDOMTZGG-UHFFFAOYSA-N 0.000 description 2
- 244000068988 Glycine max Species 0.000 description 2
- 235000010469 Glycine max Nutrition 0.000 description 2
- HPEUJPJOZXNMSJ-UHFFFAOYSA-N Methyl stearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC HPEUJPJOZXNMSJ-UHFFFAOYSA-N 0.000 description 2
- DTOSIQBPPRVQHS-PDBXOOCHSA-N alpha-linolenic acid Chemical compound CC\C=C/C\C=C/C\C=C/CCCCCCCC(O)=O DTOSIQBPPRVQHS-PDBXOOCHSA-N 0.000 description 2
- 235000020661 alpha-linolenic acid Nutrition 0.000 description 2
- 238000002485 combustion reaction Methods 0.000 description 2
- POULHZVOKOAJMA-UHFFFAOYSA-N dodecanoic acid Chemical compound CCCCCCCCCCCC(O)=O POULHZVOKOAJMA-UHFFFAOYSA-N 0.000 description 2
- 238000001035 drying Methods 0.000 description 2
- KEMQGTRYUADPNZ-UHFFFAOYSA-N heptadecanoic acid Chemical compound CCCCCCCCCCCCCCCCC(O)=O KEMQGTRYUADPNZ-UHFFFAOYSA-N 0.000 description 2
- IPCSVZSSVZVIGE-UHFFFAOYSA-N hexadecanoic acid Chemical compound CCCCCCCCCCCCCCCC(O)=O IPCSVZSSVZVIGE-UHFFFAOYSA-N 0.000 description 2
- PFOARMALXZGCHY-UHFFFAOYSA-N homoegonol Natural products C1=C(OC)C(OC)=CC=C1C1=CC2=CC(CCCO)=CC(OC)=C2O1 PFOARMALXZGCHY-UHFFFAOYSA-N 0.000 description 2
- 229960004488 linolenic acid Drugs 0.000 description 2
- KQQKGWQCNNTQJW-UHFFFAOYSA-N linolenic acid Natural products CC=CCCC=CCC=CCCCCCCCC(O)=O KQQKGWQCNNTQJW-UHFFFAOYSA-N 0.000 description 2
- -1 saturated fatty acid ester Chemical class 0.000 description 2
- 150000004671 saturated fatty acids Chemical class 0.000 description 2
- WRIDQFICGBMAFQ-UHFFFAOYSA-N (E)-8-Octadecenoic acid Natural products CCCCCCCCCC=CCCCCCCC(O)=O WRIDQFICGBMAFQ-UHFFFAOYSA-N 0.000 description 1
- OVOUKWFJRHALDD-UHFFFAOYSA-N 2-[2-(2-acetyloxyethoxy)ethoxy]ethyl acetate Chemical compound CC(=O)OCCOCCOCCOC(C)=O OVOUKWFJRHALDD-UHFFFAOYSA-N 0.000 description 1
- LQJBNNIYVWPHFW-UHFFFAOYSA-N 20:1omega9c fatty acid Natural products CCCCCCCCCCC=CCCCCCCCC(O)=O LQJBNNIYVWPHFW-UHFFFAOYSA-N 0.000 description 1
- QSBYPNXLFMSGKH-UHFFFAOYSA-N 9-Heptadecensaeure Natural products CCCCCCCC=CCCCCCCCC(O)=O QSBYPNXLFMSGKH-UHFFFAOYSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 description 1
- FBPFZTCFMRRESA-JGWLITMVSA-N D-glucitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-JGWLITMVSA-N 0.000 description 1
- 239000005639 Lauric acid Substances 0.000 description 1
- 239000005642 Oleic acid Substances 0.000 description 1
- ZQPPMHVWECSIRJ-UHFFFAOYSA-N Oleic acid Natural products CCCCCCCCC=CCCCCCCCC(O)=O ZQPPMHVWECSIRJ-UHFFFAOYSA-N 0.000 description 1
- 235000021314 Palmitic acid Nutrition 0.000 description 1
- 229920001214 Polysorbate 60 Polymers 0.000 description 1
- 235000021355 Stearic acid Nutrition 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- IZMOTZDBVPMOFE-UHFFFAOYSA-N dimethyl dodecanedioate Chemical compound COC(=O)CCCCCCCCCCC(=O)OC IZMOTZDBVPMOFE-UHFFFAOYSA-N 0.000 description 1
- 239000006185 dispersion Substances 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical compound CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 1
- CAMHHLOGFDZBBG-UHFFFAOYSA-N epoxidized methyl oleate Natural products CCCCCCCCC1OC1CCCCCCCC(=O)OC CAMHHLOGFDZBBG-UHFFFAOYSA-N 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 235000008216 herbs Nutrition 0.000 description 1
- 238000005470 impregnation Methods 0.000 description 1
- QXJSBBXBKPUZAA-UHFFFAOYSA-N isooleic acid Natural products CCCCCCCC=CCCCCCCCCC(O)=O QXJSBBXBKPUZAA-UHFFFAOYSA-N 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- WQEPLUUGTLDZJY-UHFFFAOYSA-N n-Pentadecanoic acid Natural products CCCCCCCCCCCCCCC(O)=O WQEPLUUGTLDZJY-UHFFFAOYSA-N 0.000 description 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical group CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 description 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 229920000136 polysorbate Polymers 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 230000001007 puffing effect Effects 0.000 description 1
- 230000003381 solubilizing effect Effects 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 239000008117 stearic acid Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004094 surface-active agent Substances 0.000 description 1
- 230000002195 synergetic effect Effects 0.000 description 1
- 235000021122 unsaturated fatty acids Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D1/00—Cigars; Cigarettes
- A24D1/20—Cigarettes specially adapted for simulated smoking devices
Abstract
The invention discloses an atomizing agent containing conjugated linoleic acid and saponin and a cigarette which is not combusted by heating. The atomization agent comprises 2-10 parts by volume of saponin, 15-30 parts by volume of conjugated linoleic acid and 30-100 parts by volume of solvent. The atomizing agent obviously increases the fluidity of the atomizing agent by adding the conjugated linoleic acid and the saponin under the condition of ensuring sufficient heated smoking, so that the atomizing agent is more easily soaked in tobacco products and the absorption capacity of the atomizing agent is increased. In addition, saponins also contribute to the sensory quality of the puff.
Description
Technical Field
The invention relates to the field of tobacco, in particular to an atomizing agent containing conjugated linoleic acid and saponin and a heating non-combustion cigarette.
Background
The low-temperature non-burning cigarette is used as a novel tobacco product, and the development of the cigarette is rapid in recent years. The tobacco is heated by adopting a heating and non-burning mode, but the tobacco can generate visible smoke as the traditional cigarette, and the harmful substances in the smoke are greatly reduced due to the non-burning characteristic. The smoke aerosol is used as a key factor for determining the comprehensive quality of the smoke aerosol and has important influence on the sensory quality of the smoke. Because the low-temperature cigarette has lower heating temperature, the taste is not as full as the traditional cigarette, and the smoke is not as obvious as the traditional cigarette, the tobacco treatment mode is continuously improved, and simultaneously, higher requirements are provided for the atomizing agent.
CN109602074A discloses a tobacco atomizing agent and a method for improving the absorption of the traditional tobacco atomizing agent. The atomizing agent for the cigarette is prepared from sorbitol, glycerol, triethylene glycol diacetate, methyl stearate and dimethyl dodecanedioate according to the mass ratio of 1: 10-20: 10-20: 5-10: 2-6: 0.6-1.0 by weight. After being uniformly mixed, the tobacco leaves in the formula are subjected to steam explosion treatment under the conditions of 30-50 ℃, steam explosion time less than 0.01 second, steam pressure of 0.4-0.8 MPa and pressure retention time of 10-60 seconds, the prepared atomizing agent is quickly scattered into the tobacco leaves after the treatment is finished, then the tobacco leaves are conveyed to a leaf storage cabinet, moisture is balanced, and the tobacco leaves are taken out after being fully absorbed for preparing the cut tobacco.
In the above prior art, although the viscosity is lowered by adding the saturated fatty acid ester to increase the absorption amount of the atomizing agent, the absorption amount is still not preferable as a whole.
Disclosure of Invention
The invention aims to provide a spraying agent containing lauryl alcohol and unsaturated fatty acid ester and a heating non-combustion cigarette, which can improve the absorption amount of the spraying agent on tobacco shreds.
The inventor has found that the conjugated linoleic acid has a lower boiling point than the saturated fatty acid value, and can generate obvious smoke at the heating temperature of heating non-combustible cigarettes, so that the heated smoke yield of the atomizing agent is increased. The saponin consists of aglycone and sugar chains, wherein the aglycone has lipophilicity of different degrees, and the sugar chains have stronger hydrophilicity, so that the saponin can reduce the molecular compatibility difference between the conjugated linoleic acid and a solvent, thereby improving the dispersion uniformity of the conjugated linoleic acid in the dissolution of the solvent and improving the absorption capacity of the atomizing agent on tobacco shreds. Based on this, the invention of the present application has been completed.
According to a first aspect of the present invention, there is provided a conjugated linoleic acid, saponin aerosol, comprising 2 to 10 parts by volume of saponin, preferably 2 to 8 parts by volume, such as 2 parts, 2.5 parts, 3 parts, 4 parts, 5 parts, 6 parts, 8 parts, 9 parts, 9.5 parts or 10 parts; 15 to 30 parts of conjugated linoleic acid, preferably, 15 to 20 parts, for example, 15 parts, 15.5 parts, 16 parts, 18 parts, 20 parts, 22 parts, 23 parts, 26 parts, 28 parts, 29 parts or 30 parts; and 30 to 100 parts of a solvent, preferably 40 to 80 parts, and specifically may be 30 parts, 31 parts, 32 parts, 35 parts, 40 parts, 45 parts, 50 parts, 60 parts, 65 parts, 70 parts, 80 parts, 90 parts, 95 parts, 98 parts, 100 parts, or the like.
In an alternative embodiment, the saponin is selected from one or at least two of soyasaponin, saikosaponin, platycodin, ginsenoside, gypenoside and spina date seed saponin. The saponins of the specific types have better effect of promoting the conjugated linoleic acid to be uniformly dispersed in the solvent.
The saponin source can be extracted from Chinese herbs by means known in the art, and is also commercially available.
In an alternative embodiment, the conjugated linoleic acid is one or at least two selected from the group consisting of oleic acid, linolenic acid, lauric acid, palmitic acid, heptadecanoic acid, and linolenic acid. The conjugated linoleic acids of the specific types can be well promoted by the saponin to be uniformly dispersed in the solvent.
It is common knowledge that such solvents are also referred to as smoke formers in some applications, and act to cause smoke when smoked. The solvent may be conventional glycerol. In order to further improve the dispersibility of the solvent to the saponin and the conjugated linoleic acid, propylene glycol can be added to play a role in solubilizing.
The volume ratio of the glycerol to the propylene glycol is 1: 0.4 to 0.8, for example, 1: 0.4, 1: 0.45, 1: 0.5, 1: 0.55, 1: 0.6, 1: 0.7, 1: 0.75, 1: 0.80, etc. The specific volume ratio can obtain better uniform dispersity for conjugated linoleic acid and saponin.
According to a second aspect of the present invention, there is provided a heat-not-burn cigarette, wherein the cut tobacco is obtained by incorporating the above-mentioned atomizing agent into cut tobacco raw material.
It is known to those skilled in the art that the mode of operation of "incorporation" herein may be impregnation, spraying, etc. After the doping step, drying may be performed at a desired temperature.
In order to enhance the incorporation effect, the tobacco shred raw material may be subjected to conventional treatments, such as puffing treatment, or steam explosion.
It should be noted that the amount of the above-mentioned atomizing agent can be selected according to actual needs. For example, it may be 50wt% or less (based on 100wt% of the mass of the cut tobacco material). If the amount of the additive exceeds this range, there may be a phenomenon that the atomized agent is not absorbed into the tobacco too much, that is, the atomized agent is difficult to permeate into the tobacco.
The invention has the beneficial effects that: the atomizing agent obviously increases the fluidity of the atomizing agent by adding the conjugated linoleic acid and the saponin under the condition of ensuring sufficient heated smoking, so that the atomizing agent is more easily soaked in tobacco products and the absorption capacity of the atomizing agent is increased. In addition, saponins also contribute to the sensory quality of the puff.
Detailed Description
In order to make the objects, technical solutions and advantages of the embodiments of the present application clearer, the technical solutions of the embodiments of the present application will be clearly and completely described below, and it is obvious that the described embodiments are some embodiments of the present application, but not all embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present application.
Example 1
S1, weighing 30 parts of glycerol, 50 parts of propylene glycol, 16 parts of conjugated linoleic acid and 4 parts of soyasaponin according to the volume parts;
s2, blending propylene glycol and glycerol, stirring on a magnetic stirrer, adding the soyasaponin powder during stirring, and continuously stirring for dissolving for 1 h. The stirring temperature is controlled to be about 50 ℃.
S3, adding conjugated linoleic acid into S2, and magnetically stirring for more than 1 h under the water bath heating condition of 25 ℃ to fully and uniformly mix.
Example 2
S1, weighing 60 parts of glycerol, 40 parts of propylene glycol, 30 parts of conjugated linoleic acid and 6 parts of saikosaponin according to the volume parts;
s2, blending propylene glycol and glycerol, stirring on a magnetic stirrer, adding the soyasaponin powder during stirring, and continuously stirring for dissolving for 1 h. The stirring temperature is controlled to be about 50 ℃.
S3, adding conjugated linoleic acid into S2, and magnetically stirring for more than 1 h under the water bath heating condition of 25 ℃ to fully and uniformly mix.
Example 3
S1, weighing 17 parts of glycerol, 13 parts of propylene glycol, 15 parts of conjugated linoleic acid and 2 parts of saikosaponin according to the volume parts;
s2, blending propylene glycol and glycerol, stirring on a magnetic stirrer, adding the soyasaponin powder during stirring, and continuously stirring for dissolving for 1 h. The stirring temperature is controlled to be about 50 ℃.
S3, adding conjugated linoleic acid into S2, and magnetically stirring for more than 1 h under the water bath heating condition of 25 ℃ to fully and uniformly mix.
Example 4
S1, weighing 60 parts of glycerol, 40 parts of propylene glycol, 20 parts of conjugated linoleic acid and 8 parts of soyasaponin according to the volume parts;
s2, blending propylene glycol and glycerol, stirring on a magnetic stirrer, adding the soyasaponin powder during stirring, and continuously stirring for dissolving for 1 h. The stirring temperature is controlled to be about 50 ℃.
S3, adding conjugated linoleic acid into S2, and magnetically stirring for more than 1 h under the water bath heating condition of 25 ℃ to fully and uniformly mix.
Example 5
S1, weighing 50 parts of glycerol, 20 parts of propylene glycol, 15 parts of conjugated linoleic acid and 6 parts of soyasaponin according to the volume parts;
s2, blending propylene glycol and glycerol, stirring on a magnetic stirrer, adding the soyasaponin powder during stirring, and continuously stirring for dissolving for 1 h. The stirring temperature is controlled to be about 50 ℃.
S3, adding conjugated linoleic acid into S2, and magnetically stirring for more than 1 h under the water bath heating condition of 25 ℃ to fully and uniformly mix.
Example 6
S1, weighing 100 parts of glycerol, 20 parts of conjugated linoleic acid and 8 parts of soyasaponin according to the volume parts;
s2, blending propylene glycol and glycerol, stirring on a magnetic stirrer, adding the soyasaponin powder during stirring, and continuously stirring for dissolving for 1 h. The stirring temperature is controlled to be about 50 ℃.
S3, adding conjugated linoleic acid into S2, and magnetically stirring for more than 1 h under the water bath heating condition of 25 ℃ to fully and uniformly mix.
Comparative example 1
The procedure of example 4 was repeated except that no soybean saponin was added.
Comparative example 2
The procedure is as in example 4 except that conjugated linoleic acid is not added.
Comparative example 3
The soybean saponin was replaced with tween 60, and the procedure was otherwise the same as in example 4.
Comparative example 4
The conjugated linoleic acid was replaced with stearic acid, otherwise as in example 4.
Evaluation of
Weighing a certain mass of cut tobacco M0, placing the cut tobacco M0 into a container, slowly adding the atomizing agents of the examples and the comparative examples into the container, wherein when the adding mass of the atomizing agent is recorded as M, the theoretical adding ratio W = (M/M0). times.100%; and (3) after the atomizing agent is fully absorbed by the cut tobacco, placing the cut tobacco into a constant temperature and humidity box (LHS-150 HC-I), balancing for 3 hours at the temperature of 25 ℃ and the humidity of 20%, fully drying to remove the atomizing agent remained on the surface of the cut tobacco, and weighing the mass m1 of the cut tobacco after absorbing the atomizing agent. The measured addition ratio and the effective absorption ratio (the effective absorption ratio directly reflects the absorption amount of the atomizing agent) are calculated according to the following formulas:
the addition ratio = (m 1-m 0)/m 0 × 100% was found.
Effective absorption ratio = (measured addition ratio/theoretical addition ratio) × 100%.
As can be seen from the above table, the effective absorption ratio of the application example 3 is significantly larger than that of the comparative examples 1 and 2, which illustrates the synergistic promotion effect of the saponin and the conjugated linoleic acid on the effective absorption ratio of the atomizing agent;
the effective absorption ratio of the saponin of the application is obviously higher than that of the saponin of the comparative example 3, which shows that the saponin of the application has a certain promotion effect on the effective absorption ratio of the atomizing agent compared with the common surfactant Tween;
the effective absorption ratio of the conjugated linoleic acid is obviously higher than that of the saturated fatty acid with the same carbon number in the comparative example 4, which shows the obvious promotion effect of the conjugated linoleic acid on the effective absorption ratio of the atomizing agent.
Furthermore, those skilled in the art will appreciate that while some embodiments herein include some features included in other embodiments, rather than other features, combinations of features of different embodiments are meant to be within the scope of the application and form different embodiments. For example, in the claims, any of the claimed embodiments may be used in any combination.
Those of ordinary skill in the art will understand that: the above embodiments are only used for illustrating the technical solutions of the present application, and not for limiting the same, although the present application is described in detail with reference to the foregoing embodiments, those skilled in the art should understand that: it is possible to modify the solutions described in the previous embodiments or to substitute some or all of the technical features thereof without departing from the scope of the claims.
Claims (7)
1. An atomizing agent containing conjugated linoleic acid and saponin is characterized by comprising 2-10 parts by volume of saponin, 15-30 parts by volume of conjugated linoleic acid and 30-100 parts by volume of a solvent; the absorption ratio of the atomizing agent on the tobacco shreds is 90.3% -94.5%.
2. The atomizing agent according to claim 1, wherein the atomizing agent comprises 2 to 8 parts by volume of saponin, 15 to 20 parts by volume of conjugated linoleic acid, and 40 to 80 parts by volume of a solvent.
3. A nebulant according to claim 1 wherein the saponin is selected from one or at least two of soyasaponin, saikosaponin, platycodin, ginsenoside, gypenoside and spina date seed saponin.
4. The nebulant according to claim 1, wherein said solvent comprises glycerol and propylene glycol.
5. The atomizing agent according to claim 4, wherein the volume ratio of the glycerol to the propylene glycol is 1: 0.4 to 0.8.
6. A heat-nonflammable cigarette, characterized in that cut tobacco is obtained by incorporating the atomizing agent according to claim 1 into cut tobacco raw material.
7. A heated non-combustible cigarette according to claim 6 wherein the incorporation of the atomising agent is no more than 50% by weight of the mass of the cut tobacco material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010731911.7A CN111802687B (en) | 2020-07-27 | 2020-07-27 | Atomizing agent containing conjugated linoleic acid and saponin and cigarette without burning during heating |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202010731911.7A CN111802687B (en) | 2020-07-27 | 2020-07-27 | Atomizing agent containing conjugated linoleic acid and saponin and cigarette without burning during heating |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN111802687A CN111802687A (en) | 2020-10-23 |
| CN111802687B true CN111802687B (en) | 2022-04-29 |
Family
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| CN111802687A (en) | 2020-10-23 |
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