CN114680363A - Processing method of flavor type reconstituted tobacco - Google Patents

Processing method of flavor type reconstituted tobacco Download PDF

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Publication number
CN114680363A
CN114680363A CN202210539474.8A CN202210539474A CN114680363A CN 114680363 A CN114680363 A CN 114680363A CN 202210539474 A CN202210539474 A CN 202210539474A CN 114680363 A CN114680363 A CN 114680363A
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tobacco
essence
flavor
reconstituted tobacco
drying
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Chinese (zh)
Inventor
王昊
聂广军
杨俊鹏
张敦铁
陈丽舟
刘兴乐
庄虎
刘华臣
罗诚浩
朱峰
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China Tobacco Hubei Industrial LLC
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China Tobacco Hubei Industrial LLC
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Priority to CN202210539474.8A priority Critical patent/CN114680363A/en
Publication of CN114680363A publication Critical patent/CN114680363A/en
Priority to PCT/CN2022/133164 priority patent/WO2023221441A1/en
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/14Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00Preparing tobacco in the factory
    • A24B3/12Steaming, curing, or flavouring tobacco

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Abstract

The invention provides a processing method of flavor type reconstituted tobacco, which comprises the following steps: grinding part of tobacco raw materials after expansion treatment to obtain tobacco powder; drying and homogenizing the tobacco powder and the liquid essence under reduced pressure at low temperature to obtain powder essence; crushing the residual tobacco raw materials, mixing the crushed residual tobacco raw materials with a solid auxiliary agent and a liquid auxiliary agent, homogenizing, forming, and performing multi-stage drying to obtain a tobacco material; and spraying the powdered essence onto the surface of the tobacco material from a low-temperature drying area to a post-treatment stage, and performing post-treatment to obtain the flavor reconstituted tobacco. In the production of reconstituted tobacco, on one hand, the original flavor and the original fragrance of tobacco are maintained in the drying process, the baking fragrance is better maintained, and the influence of different spices on the forming of the reconstituted tobacco is reduced; on the other hand, the method is suitable for showing the characteristics of different flavor products.

Description

Processing method of flavor type reconstituted tobacco
Technical Field
The invention relates to the technical field of heating cigarettes, in particular to a processing method of flavor type reconstituted tobacco.
Background
The heated cigarette is a novel cigarette, is used in a heating mode instead of a combustion mode, and is generally heated at the temperature of about 350 ℃. When the heated cigarette is smoked, the tobacco substrate is heated, the atomizing agents such as glycerin and propylene glycol volatilize to form aerosol, and meanwhile, different volatile substances are heated to participate in forming aerosol, so that the fragrance is enriched, and different consumption experiences are met.
At present, the mainstream cigarette with electric heating mainly has the flavors of tobacco, mint, fruits and the like, wherein the flavor cigarette with mint, fruits and the like is added with a volatile essence additive with a high proportion of low boiling point, and is usually added into a tobacco substrate (reconstituted tobacco) or a filter stick. In the production process of flavor type reconstituted tobacco, blended essence is uniformly mixed with liquid additives such as water, glycerol and the like and additives, then the mixture is stirred with tobacco powder and solid additives, and the mixture is formed by rolling or tape casting and the like, and then dried, adjusted in moisture content, shredded or rolled to prepare reconstituted tobacco products which are used for rolling heated cigarettes. In the drying process, the temperature is generally about 100 ℃, and in the process of adjusting the moisture through a heat exchange mode, volatile aroma components, particularly low-boiling-point substances are volatilized more, so that the waste of essence and the consumption of process energy are caused, and the product quality of the dried flavor reconstituted tobacco is also influenced.
Therefore, in order to reduce the loss of volatile flavor substances in the drying process, essence needs to be treated, the production process of the reconstituted tobacco is improved, the loss of essence additives in the process is reduced, and the quality of the flavored reconstituted tobacco is improved.
In chinese patent publication No. CN 112056607 a, an on-line perfuming device and method for a perfume with high and low boiling point components is disclosed, which adopts a mode of separately perfuming the high boiling point component and the low boiling point component in the production process of cast reconstituted tobacco, wherein the high boiling point component is directly sprayed on the upper surface of the reconstituted tobacco slurry in a liquid form; the low-boiling-point components are sprayed on a steel belt behind the head box in a liquid state, and as the drying process is carried out, the low-boiling-point component condensed water on the lower surface of the reconstituted tobacco pulp is heated and evaporated and enters the inside of the reconstituted tobacco pulp, and the high-boiling-point component condensed water on the upper surface of the reconstituted tobacco pulp is not evaporated and still remains on the upper surface of the reconstituted tobacco pulp; thereby completing the on-line perfuming of the spice with high and low boiling point components to the reconstituted tobacco pulp. Although the above way of perfuming by several times avoids the volatilization loss of the low boiling point components in the drying process, as the whole essence is finished, the essence needs to be processed by second fractionation or prepared in groups during preparation, and the integrity of the essence can be potentially affected. Meanwhile, the two components of essence are not uniformly distributed in the reconstituted tobacco in the technical process, and the heat release efficiency is influenced when the reconstituted tobacco is heated and sucked.
Disclosure of Invention
The invention aims to provide a processing method of flavor type reconstituted tobacco, which has the advantages of low loss of volatile flavor substances with low boiling points, good product stability and relatively stable release of the flavor substances after heating.
In view of this, the application provides a processing method of flavor type reconstituted tobacco, comprising the following steps:
grinding part of tobacco raw materials after expansion treatment to obtain tobacco powder; drying and homogenizing the tobacco powder and the liquid essence under reduced pressure at low temperature to obtain powder essence;
crushing the residual tobacco raw materials, mixing the crushed residual tobacco raw materials with a solid auxiliary agent and a liquid auxiliary agent, homogenizing, forming, and performing multi-stage drying to obtain a tobacco material;
and spraying the powder essence on the surface of the tobacco material from a low-temperature drying area to a post-treatment stage, and performing post-treatment to obtain the flavor type reconstituted tobacco.
Preferably, the mass ratio of the part of tobacco raw materials to the rest of tobacco raw materials is (10-25%): (75% to 90%).
Preferably, the liquid essence comprises a microcapsule auxiliary agent, and the microcapsule auxiliary agent is selected from one or more of modified starch, guar gum and sodium alginate.
Preferably, the mass ratio of the tobacco powder to the liquid essence to the microcapsule auxiliary agent is (75-95): (5-25): (1-2).
Preferably, in the step of obtaining the powder essence, the low temperature is less than 20 ℃.
Preferably, the solid auxiliary agent is selected from one or two of hydroxymethyl cellulose and sodium alginate, and the liquid auxiliary agent comprises an atomizing agent, cellulose and water.
Preferably, the solid auxiliary agent accounts for 0.5-3.0 wt% of the mixed material, the atomizing agent accounts for 10-25 wt% of the mixed material, and the cellulose accounts for 0.5-3.0 wt% of the mixed material.
Preferably, in the step of obtaining the tobacco material, the temperature of the multistage drying is less than 110 ℃, and the moisture content of the homogenized material is 25-65%.
Preferably, the temperature in the low-temperature drying area is not higher than the maximum thermal weight loss temperature of the powder essence.
Preferably, the post-treatment comprises shredding and coiling which are carried out in sequence.
The application provides a processing method of flavor reconstituted tobacco, which changes the application mode of reconstituted tobacco liquid essence into powder application, and adjusts the application area from the low-temperature area before the drying process to the post-treatment stage in the drying process; in the production process of the reconstituted tobacco, the loss of low-boiling-point volatile flavor substances is reduced, the energy consumption in the drying process is reduced, and the production cost of the reconstituted tobacco is reduced; in the production of reconstituted tobacco, on one hand, the original flavor and the original fragrance of tobacco are maintained in the drying process, the baking fragrance is better maintained, and the influence of different spices on the forming of the reconstituted tobacco is reduced; on the other hand, the method is suitable for showing the characteristics of different flavor products; finally, the product characteristics of the reconstituted tobacco prepared by the method are stable, after heating, the release of the fragrance substances is relatively stable, and the integrity of different essence components is reserved.
Drawings
FIG. 1 is a schematic view of a processing flow of flavor type reconstituted tobacco according to the present invention;
FIG. 2 is a heat loss profile of a mint-type reconstituted tobacco sample cigarette processed according to example 1 of the present invention as compared to a mint-type sample cigarette from a control process.
Detailed Description
For a further understanding of the invention, reference will now be made to the preferred embodiments of the invention by way of example, and it is to be understood that the description is intended to further illustrate features and advantages of the invention, and not to limit the scope of the claims.
In order to avoid excessive loss of the low-boiling-point essence in the process of the reconstituted tobacco, the integrity of the essence components is maintained, and the smoking experience is improved. The processing flow schematic diagram of the flavor type reconstituted tobacco is shown in figure 1, and the embodiment of the invention discloses a processing method of the flavor type reconstituted tobacco, which comprises the following steps:
grinding part of tobacco raw materials after expansion treatment to obtain tobacco powder; drying and homogenizing the tobacco powder and the liquid essence under reduced pressure at low temperature to obtain powder essence;
crushing the residual tobacco raw materials, mixing the crushed residual tobacco raw materials with a solid auxiliary agent and a liquid auxiliary agent, homogenizing, forming, and performing multi-stage drying to obtain a tobacco material;
and spraying the powdered essence onto the surface of the tobacco material from a low-temperature drying area to a post-treatment stage, and performing post-treatment to obtain the flavor reconstituted tobacco.
In the production process of flavor type reconstituted tobacco, the tobacco raw material is divided into two parts, wherein one part of the tobacco raw material is processed by the traditional tobacco expansion process to obtain expanded tobacco shreds, the expanded tobacco shreds are crushed to be less than 150 meshes and used as an adsorption substance of liquid essence, and the adsorption substance and the liquid essence are dried and homogenized under reduced pressure at low temperature to obtain powder essence. In the present application, the tobacco material may specifically include tobacco leaves, fragments, stems and other conventional tobacco materials. The content rate of the expanded tobacco shreds is 8-10%. The liquid essence comprises a microcapsule auxiliary agent, and the microcapsule auxiliary agent is selected from one or more of modified starch, guar gum and sodium alginate. The mass ratio of the powder essence to the liquid essence to the microcapsule auxiliary agent is (75-95): (5-25): (1-2). The low temperature condition is less than 20 ℃. The drying under reduced pressure and homogenization are procedures well known to those skilled in the art, and there is no particular limitation in this application.
On the basis, the other part of tobacco raw materials are crushed, mixed with the solid auxiliary agent and the liquid auxiliary agent, homogenized and formed, and subjected to multistage drying to obtain the tobacco material. In this process, the tobacco material is comminuted to less than 150 mesh. The solid auxiliary agent is selected from one or two of carboxymethyl cellulose and sodium alginate; the liquid adjuvant comprises a nebulant, cellulose and water, wherein the nebulant is a mixture of glycerol and propylene glycol. In the mixture obtained by mixing the three materials, the content of the solid auxiliary agent is 0.5-3.0 wt%, the content of the atomizing agent in the liquid auxiliary agent is 10-25 wt%, and the content of the cellulose is 0.5-3.0 wt%. The water content of the homogenized material is 25-65%. Also, the homogeneous forming and the multistage drying are technical means well known to those skilled in the art, and are not specifically described herein; in the present application, the temperature of the multi-stage drying is less than 110 ℃, more specifically, the temperature of the multi-stage drying is less than 95 ℃.
In the present application, the mass ratio of the partial tobacco raw material to the residual tobacco raw material is (10% -25%) according to the requirement of the product: (75% to 90%).
The maximum thermal weight loss temperature of the powdered essence is T1, the powdered essence is uniformly sprayed along the running direction of the tobacco material from a low-temperature drying area to a post-treatment stage, multiple or front-back spraying can be carried out if necessary, and subsequent shredding or coiling is carried out after spraying, so that the production of the flavor type reconstituted tobacco is completed. The temperature range and the spraying of the powdered essence in the low-temperature drying area can effectively avoid the loss of volatile essence components with low boiling points.
The processing method of the flavor type reconstituted tobacco provided by the application has the following advantages:
in the production process of the reconstituted tobacco, the loss of volatile aroma substances with low boiling points is reduced, the energy consumption in the drying process is reduced, and the production cost of the reconstituted tobacco is reduced;
the product characteristics of the flavor reconstituted tobacco are stable, after heating, the release of the aroma substances is relatively stable, and the integrity of different essence components is reserved;
in the production process of the flavor reconstituted tobacco, the production environment is improved, and the influence on the production environment smell is reduced; the influence between the production of reconstituted tobaccos with different flavors is reduced, and the process maintenance requirement is lowered;
in the production of reconstituted tobacco, on one hand, the original flavor and the original fragrance of tobacco are maintained in the drying process, the baking fragrance is better maintained, and the influence of different spices on the forming of the reconstituted tobacco is reduced; on the other hand, the method is suitable for showing the characteristics of different flavor products.
For further understanding of the present invention, the following examples are provided to illustrate the processing method of flavored reconstituted tobacco provided by the present invention, and the scope of the present invention is not limited by the following examples.
Example 1 mint-flavored reconstituted tobacco
a: according to the design of mint type reconstituted tobacco essence, selecting tobacco raw materials (one or a mixture of tobacco leaves, fragments and the like) with the proportion of 15 wt% (relative to the final reconstituted tobacco finished product), and treating with CO2Performing expansion treatment (soaking time is 60s, hot air temperature is 310 ℃), grinding the mixture into powder (water content is 10%), and crushing the powder to be below 150 meshes at normal temperature;
b: mixing the powder as adsorption substance of liquid essence with liquid mint flavor essence (mixture of L-menthol and mint oil, 80 wt% and ethanol as solvent) containing microcapsule adjuvant (one or more of modified starch, guar gum and sodium alginate), drying under reduced pressure at low temperature (less than 30 deg.C), homogenizing, and making into powder essence; wherein the mass ratio of the expanded tobacco powder to the essence to the microcapsule auxiliary agent is (80: 18: 2);
c: mixing, homogenizing and molding reconstituted tobacco raw materials: crushing tobacco raw materials (the residual proportion, tobacco stems, tobacco leaf fragments and the like, 85 wt% (relative to the final reconstituted tobacco finished product, the same below)) to be less than 150 meshes, adding a solid auxiliary agent (a mixture of carboxymethyl cellulose and sodium alginate, 2.0 wt%) and a liquid auxiliary agent (an atomizing agent, glycerol and propylene glycol, the proportion is 20 wt%, cellulose is 0.5 wt%, a proper amount of water and the water content of a homogeneous material is 60% +/-5%), mixing, stirring, homogenizing, pulping, molding, casting, and performing multistage drying (the highest process temperature is less than 100 +/-5 ℃);
d: spraying and perfuming: the mint essence has stronger volatility, and the weight loss still exists at lower temperature when the mint essence is heated at a certain heating rate, so that the prepared mint essence tobacco solid powder (25 percent) is uniformly sprayed in the running direction of the reconstituted tobacco sheet before the process of shredding/rolling at a low-temperature drying area (less than 50 ℃), and can be sprayed for multiple times and on the front and back sides when necessary;
e, subsequent steps: and (4) carrying out subsequent shredding or coiling process after spraying to finish the production of the mint-type flavor reconstituted tobacco.
Preparing a heating cigarette from the reconstituted tobacco according to a certain specification product standard of a COO brand, and performing sensory evaluation; and adding the mint type reconstituted tobacco in a liquid essence form at the mixing, homogenizing and forming stage of the reconstituted tobacco raw materials, performing multistage drying to obtain the control mint type reconstituted tobacco, performing cigarette heating preparation, and performing sensory evaluation. The results are shown in table 1:
TABLE 1 sensory evaluation index of the whole quality of electrically heated cigarette
Figure BDA0003649665210000061
Through comparison and evaluation, the heated cigarette sample prepared by the process has good performance in the aspects of fragrance and uniformity, and the strength of mint cool feeling and the uniformity before and after smoking are good; compared with the mint type sample cigarette, the mint flavor intensity of the mint type sample cigarette is weakened after 8 mouths according to the standard smoking mouth number (12 mouths), and the mint type sample cigarette has slight burning sensation of wood fibers.
Fig. 1 is a comparison graph of the weight loss under heat, specifically, the weight loss ratio of the mint-type reconstituted tobacco sample cigarette (red) of the invention and the mint-type sample cigarette (black) of the comparison process at a certain temperature rise rate in the range from room temperature to 105 ℃, and it can be seen from the graph that the weight loss of the sample of the invention is larger than that of the comparison sample, which shows that the volatilization loss of the essence applied in the production process is less, and a large amount of essence is volatilized in the subsequent heating process of heating the cigarette, so that more flavor substances are provided.
Example 2 fruit-flavored reconstituted tobacco
a: according to the design of the fruity reconstituted tobacco essence, selecting tobacco raw materials (one or a mixture of tobacco leaves, fragments and the like) with a proportion of 25 wt% (relative to the final reconstituted tobacco finished product), and subjecting the tobacco raw materials to CO treatment2Performing expansion treatment (soaking time is 30s, hot air temperature is 300 ℃), grinding (water content is 8%), and crushing to below 150 meshes at normal temperature;
b: mixing the above powder as adsorbent of liquid essence with liquid fruit flavor essence (sweet orange oil, menthol, raspberry ketone, etc. 60 wt%, ethanol as solvent) added with microcapsule adjuvant (one or more of modified starch, guar gum, sodium alginate, etc.), drying under reduced pressure at low temperature (less than 30 deg.C), homogenizing, and making into powder essence; wherein the mass ratio of the expanded tobacco powder to the essence to the microcapsule auxiliary agent is 75: 24: 1;
c: mixing, homogenizing and molding reconstituted tobacco raw materials: crushing tobacco raw materials (the residual proportion, tobacco stems, tobacco leaf fragments and the like, 75 wt% (relative to the final reconstituted tobacco finished product, the same below)) to be less than 150 meshes, adding a solid auxiliary agent (a mixture of carboxymethyl cellulose and sodium alginate, 1.5 wt%) and a liquid auxiliary agent (an atomizing agent, glycerol and propylene glycol, the total proportion is 20 wt%, cellulose is 1.5 wt%, a proper amount of water, and the water content of a homogenized material is 30% +/-5%), mixing, stirring, homogenizing, performing multi-stage rolling, and performing multi-stage drying (the highest process temperature is less than 100 +/-5 ℃);
d: spraying and perfuming: the volatility of the fruit flavor essence is strong, and the weight loss still exists at a lower temperature when the fruit flavor essence is heated at a certain heating rate, so that the prepared mint flavor tobacco solid powder (20 wt%) is uniformly sprayed in the running direction of the reconstituted tobacco sheet before the processes of shredding/rolling at a low-temperature drying area (less than 60 ℃), and can be sprayed for multiple times and on the front side and the back side when necessary;
e, subsequent: and (4) carrying out subsequent shredding or coiling process after spraying to finish the production of the fruit-type flavor reconstituted tobacco.
Preparing a heating cigarette from the reconstituted tobacco according to a certain specification product standard of a COO brand, and performing sensory evaluation; and (3) adding the fruit-flavor reconstituted tobacco in a liquid essence form at the mixing, homogenizing and forming stage of the reconstituted tobacco raw materials in contrast to the processing technology, then performing multistage drying to obtain the fruit-flavor reconstituted tobacco, and performing heated cigarette preparation and sensory evaluation. The results are shown in table 2:
TABLE 2 sensory evaluation index of the whole quality of electrically heated cigarette
Figure BDA0003649665210000081
Through comparison and evaluation, the heated cigarette sample prepared by the process has good aroma and uniformity, the fruit flavor intensity and the uniformity before and after smoking are good, and the good uniformity is kept in the front 8 mouths according to the standard number of smoking mouths (12 mouths); the intensity of the fruit aroma of the control fruit flavor sample cigarette is weakened after 6 mouths according to the standard number of suction mouths (12 mouths).
The above description of the embodiments is only intended to facilitate the understanding of the method of the invention and its core idea. It should be noted that, for those skilled in the art, it is possible to make various improvements and modifications to the present invention without departing from the principle of the present invention, and those improvements and modifications also fall within the scope of the claims of the present invention.
The previous description of the disclosed embodiments is provided to enable any person skilled in the art to make or use the present invention. Various modifications to these embodiments will be readily apparent to those skilled in the art, and the generic principles defined herein may be applied to other embodiments without departing from the spirit or scope of the invention. Thus, the present invention is not intended to be limited to the embodiments shown herein but is to be accorded the widest scope consistent with the principles and novel features disclosed herein.

Claims (10)

1. A processing method of flavor type reconstituted tobacco comprises the following steps:
grinding part of tobacco raw materials after expansion treatment to obtain tobacco powder; drying and homogenizing the tobacco powder and the liquid essence under reduced pressure at low temperature to obtain powder essence;
crushing the residual tobacco raw materials, mixing the crushed residual tobacco raw materials with a solid auxiliary agent and a liquid auxiliary agent, homogenizing, forming, and performing multi-stage drying to obtain a tobacco material;
and spraying the powdered essence onto the surface of the tobacco material from a low-temperature drying area to a post-treatment stage, and performing post-treatment to obtain the flavor reconstituted tobacco.
2. The process according to claim 1, characterized in that the mass ratio of the partial tobacco raw material to the residual tobacco raw material is (10% to 25%): (75% to 90%).
3. The process of claim 1, wherein the liquid fragrance comprises a microencapsulation aid selected from one or more of modified starch, guar gum and sodium alginate.
4. The processing method according to claim 3, wherein the mass ratio of the tobacco powder, the liquid essence and the microcapsule auxiliary agent is (75-95): (5-25): (1-2).
5. The process according to claim 1, wherein in the step of obtaining a powdered flavour, the temperature of the low temperature is < 20 ℃.
6. The processing method as claimed in claim 1, wherein the solid auxiliary agent is selected from one or two of hydroxymethyl cellulose and sodium alginate, and the liquid auxiliary agent comprises atomizing agent, cellulose and water.
7. The process of claim 6, wherein the solid additive comprises 0.5 to 3.0 wt% of the blended material, the atomizing agent comprises 10 to 25 wt% of the blended material, and the cellulose comprises 0.5 to 3.0 wt% of the blended material.
8. The process of claim 1, wherein in the step of obtaining tobacco material, the temperature of the multistage drying is less than 110 ℃, and the moisture content of the homogenized material is 25-65%.
9. The process of claim 1, wherein the temperature in the low temperature drying zone is no higher than the maximum temperature of thermal weight loss of the powdered flavor.
10. A process according to any one of claims 1 to 9, wherein the post-treatment comprises shredding and coiling in sequence.
CN202210539474.8A 2022-05-18 2022-05-18 Processing method of flavor type reconstituted tobacco Pending CN114680363A (en)

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CN1565285A (en) * 2003-06-13 2005-01-19 广东省金叶烟草薄片技术开发有限公司 Remaking tobacco leaf applying reduction process using paper making method
CN105996111A (en) * 2016-07-20 2016-10-12 湖北中烟工业有限责任公司 Fragrance-keeping method for increasing quality of tobacco leaves reprocessed through paper-making process
CN114009826A (en) * 2021-12-06 2022-02-08 云南中烟新材料科技有限公司 Heating cigarette core material and preparation method thereof
CN114287655A (en) * 2022-02-23 2022-04-08 云南景立新材料科技有限公司 Preparation method of aroma-retaining slow-release smoking material for heating cigarettes

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2023221441A1 (en) * 2022-05-18 2023-11-23 湖北中烟工业有限责任公司 Method for processing flavored reconstituted tobacco

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