CN103666764B - A kind of cold taste essence for peppermint type cigarette composition - Google Patents
A kind of cold taste essence for peppermint type cigarette composition Download PDFInfo
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- CN103666764B CN103666764B CN201310744007.XA CN201310744007A CN103666764B CN 103666764 B CN103666764 B CN 103666764B CN 201310744007 A CN201310744007 A CN 201310744007A CN 103666764 B CN103666764 B CN 103666764B
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Abstract
The present invention relates to a kind of cold taste essence for peppermint type cigarette composition.Existing cigarette coolant agent, or adopt traditional peppermint, easily volatilizees, or adopts the derivative of peppermint but taste is not good.The cool taste essence combination of mint type provided by the invention comprises following ingredients and weight ratio: metatitanic acid three peppermint one ethyl ester 65--85; Gaultherolin 1--3; Lemon oil 0--0.5; Peppermint oil dementholized 0.2-0.3; Essence 6-11.Adopt the mint type cigarette that essence of the present invention is made, the cross pollution do not caused because of peppermint distillation in production process and problem of environmental pollution; In transport and storing process, can not, overlong time too high because of temperature and cause peppermint cool feeling to decline; In aspiration procedure, cool taste is lasting and even, and remains the vegetalitas note of peppermint.
Description
Technical field
The present invention relates to a kind of cool taste type cigarette flavoring essence, particularly a kind of mint type cigarette essence.
Background technology
Existing mint type cigarette essence main component is menthol, or the chemical derivative of menthol, and these mint type cigarette essence exist some defects, mainly:
1, in production process, peppermint distillation causes cross pollution and problem of environmental pollution.Menthol has character of strongly volatilizing, and penetration is extremely strong, and the menthol volatilization gas of high concentration has strong impulse and corrosion function to the skin of people and mucous membrane, pollutes cigarette production line and working environment;
2, the cigarette products igniting and sucking quality difference of menthol perfuming is adopted and shelf life is short.The cigarette products of simple employing menthol perfuming, when burning and sucking, minty note (cool) taste weakens rapidly with the increase of puff number, arrive cigarette end, minty note (cool) taste is very thin, the suction sensation that minty note (cool) taste evenly discharges can not be obtained, there is great igniting and sucking quality defect; And the shelf life of cigarette is relatively short, the long menthol that causes volatilized and affected its stability the resting period
3, in order to overcome the defect of above-mentioned menthol flavored cigarette product, the applicant discloses a kind of metatitanic acid three peppermint one ethyl ester (CN102321116A).This menthol derivative can well keep cool taste, but adopts the cigarette products of menthol derivative perfuming when sucking, and the distinctive plant note of menthol slightly feels not enough.Although menthol derivative can increase the stability of mentholated cigarette, extend the cigarette resting period, there is cool feeling in the suction time, loses the distinctive plant note of menthol.
Summary of the invention
The object of the present invention is to provide a kind of cool taste essence of mint type cigarette, solve the above-mentioned defect of existing mint type cigarette, the cool taste of mentholated cigarette can be made even lastingly, and the resting period is long, and retains menthol distinctive plant note when aspirating.
For achieving the above object, this invention takes following technical scheme:
The cool taste essence of a kind of mint type cigarette of the present invention, it comprise following composition and weight ratio as follows:
Metatitanic acid three peppermint one ethyl ester 65--85;
Gaultherolin 1--3;
Lemon oil 0--5;
Peppermint oil dementholized 0.2-0.3;
Essence 6-11.
Can also add protective agent in above-mentioned cold taste essence for peppermint type cigarette composition provided by the invention, be 1-4 with the weight ratio of other components.Described protective agent is low-carbon alcohols.Protectant effect prevents in titanate esters technical process, absorbs the moisture in air and decompose, discharging solid-state peppermint, like this, can cause the blocking of spray gun when giving tobacco flavoring.Preferred alcohol in the present invention is or/and propane diols.
When adopting the cool taste essence of a kind of mint type cigarette of the present invention to prepare cigarette; after weighing by above-mentioned percentage by weight; metatitanic acid three peppermint one ethyl ester, peppermint oil dementholized, spearmint base, gaultherolin, lemon oil, perfume base raw material are added in container; and add protective agent, stir and obtain the cool taste fragrance solution of the present invention.Then described cool taste fragrance solution is evenly sprayed in pipe tobacco, then pipe tobacco is made cigarette, namely make mint type cigarette.
The preferred spearmint base of described essence is or/and perfume base.
The cool taste essence of a kind of mint type cigarette of the present invention compared with prior art, possesses following advantage:
1, the cool taste essence preparation technology of a kind of mint type cigarette of the present invention is simple, and in preparation process, menthol volatilization is few, on production operation personnel and production of cigarettes environment without impact.When producing mint type cigarette, the cross pollution do not caused because of peppermint distillation and problem of environmental pollution.
2, the cool taste essence of a kind of mint type cigarette of the present invention, main component is metatitanic acid three peppermint one ethyl ester, utilize active hydroxyl groups in menthol, by the method for chamical binding, menthol is fixed on inorganic group, form metastable peppermint derivative, when cigarette is burnt, peppermint derivative decomposes, thus discharges menthol equably.The cigarette made from the present invention is when 50 DEG C of high temperature are deposited, and the menthol half-life is about 130 days, is more than 2 times of traditional pure menthol cigarette half-life; Deposit under normal operation, the half-life was more than 8 months, and traditional pure menthol cigarette is 2 months.In the mint type cigarette transport adopting essence of the present invention and storing process, can not, overlong time too high because of temperature and cause peppermint cool feeling to decline.
3, the cool taste essence of a kind of mint type cigarette of the present invention, also include gaultherolin, lemon oil, perfume base, peppermint oil dementholized, spearmint base in composition, compensate for simple metatitanic acid three peppermint one ethyl ester that adopts and lack the defect of menthol endemic plant note as the cigarette products of essence.By to main component metatitanic acid three peppermint one ethyl ester and auxiliary element gaultherolin, lemon oil, essence, peppermint oil dementholized and protectantly to distribute rationally, make cool taste essence of the present invention.Adopt the cigarette products that essence of the present invention is made, during suction, cool taste is evenly lasting, and has the plant note of pleasant.
Accompanying drawing explanation
Fig. 1 prepares the cigarette essence attenuation curve after cold taste essence for peppermint type cigarette compositions-treated by the embodiment of the present invention.
Illustrate: A is that the embodiment of the present invention 2 is filled a prescription mentholated cigarette sample, and B is conventional formulation mentholated cigarette sample, two samples are all that two samples were the capsule packaging do not broken a seal 50 DEG C of oven-baked 5,12,24,32,40 days.
Detailed description of the invention
Embodiment 1
Add metatitanic acid three peppermint one ethyl ester 65g, gaultherolin 3g, peppermint oil dementholized 0.2g, lemon oil 0.5g, ethanol 4g, perfume base 10g, spearmint base 0.8g in a reservoir, stir, be then evenly sprayed in 10Kg pipe tobacco, make light mint flavored cigarette.
Embodiment 2
Add metatitanic acid three peppermint one ethyl ester 85g, gaultherolin 1g, peppermint oil dementholized 0.3g, propane diols 1g, perfume base 5g, spearmint base 1g in a reservoir, stir, be then evenly sprayed in 10Kg pipe tobacco, make dense mint flavored cigarette.
Embodiment 3
The mentholated cigarette adopting essence combination of the present invention (composition of embodiment 2) to make and conventional formulation mentholated cigarette are put into 50 DEG C of oven-baked, the attenuation of test essence.Draw essence attenuation curve as shown in Figure 1.
According to Fig. 1, estimate and to deposit at 50 DEG C of temperature, the half-life of conventional formulation mentholated cigarette Mint Essence is about 50 days, and the half-life of this patent formula mentholated cigarette Mint Essence is about 130 days.
Embodiment 4:
On October 15th, 2009, the mentholated cigarette that present invention applicant engages the essence combination of some tobacco business sensory evaluating smoking experts to the employing embodiment of the present invention 1 to make and conventional formulation mentholated cigarette carry out contrast and smoke panel test.
The conclusion of smokeing panel test of expert is as follows:
Wherein 1# is traditional Mint Essence cigarette, and 2# is the cigarette adding essence of the present invention.
The applicant also to the sucking of the cool taste composition that existing coolant agent and the application provide, to prepare and security is appraised through comparison, result is as following table:
Claims (4)
1. a cold taste essence for peppermint type cigarette composition, is characterized in that it is made up of following ingredients and weight ratio:
Metatitanic acid three peppermint one ethyl ester 65-85;
Gaultherolin 1-3;
Lemon oil 0-0.5;
Peppermint oil dementholized 0.2-0.3;
Essence 6-11;
Protective agent 1-4;
Low-carbon alcohols selected by described protective agent.
2. cold taste essence for peppermint type cigarette composition according to claim 1, is characterized in that described low-carbon alcohols is that ethanol is or/and propane diols.
3. cold taste essence for peppermint type cigarette composition according to claim 1 and 2, is characterized in that:
Metatitanic acid three peppermint one ethyl ester 65;
Gaultherolin 3;
Lemon oil 0.5;
Peppermint oil dementholized 0.2;
Essence 6-11;
Protective agent 1-4.
4. cold taste essence for peppermint type cigarette composition according to claim 1 and 2, is characterized in that:
Metatitanic acid three peppermint one ethyl ester 85;
Gaultherolin 1;
Peppermint oil dementholized 0.3;
Essence 6-11;
Protective agent 1-4.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310744007.XA CN103666764B (en) | 2013-12-30 | 2013-12-30 | A kind of cold taste essence for peppermint type cigarette composition |
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| Application Number | Priority Date | Filing Date | Title |
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| CN201310744007.XA CN103666764B (en) | 2013-12-30 | 2013-12-30 | A kind of cold taste essence for peppermint type cigarette composition |
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| CN103666764A CN103666764A (en) | 2014-03-26 |
| CN103666764B true CN103666764B (en) | 2016-01-20 |
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Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104161303B (en) * | 2014-07-16 | 2018-11-30 | 广西中烟工业有限责任公司 | A kind of cool taste mint type cigarette filter stick additive preparation method and applications |
| CN106753787B (en) * | 2016-11-29 | 2020-07-24 | 湖北中烟工业有限责任公司 | Bead-blasting lemon mint essential oil for cigarettes as well as preparation method and application thereof |
| CN110477440B (en) * | 2019-07-09 | 2022-03-22 | 河南中烟工业有限责任公司 | Mint essence for heating non-combustible cigarette, tobacco sheet and non-combustible cigarette |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101808541A (en) * | 2007-06-08 | 2010-08-18 | 菲利普莫里斯生产公司 | Has the smoking article that controlled flavor discharges |
| CN102321116A (en) * | 2011-06-07 | 2012-01-18 | 湖南中烟工业有限责任公司 | Triple refined peppermint titanate-ethyl ester, and preparation and application methods thereof |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103351949B (en) * | 2013-06-28 | 2014-12-10 | 湖北中烟工业有限责任公司 | Anti-bacterium essence for cigarettes and yew paper containing same for cigarettes |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101808541A (en) * | 2007-06-08 | 2010-08-18 | 菲利普莫里斯生产公司 | Has the smoking article that controlled flavor discharges |
| CN102321116A (en) * | 2011-06-07 | 2012-01-18 | 湖南中烟工业有限责任公司 | Triple refined peppermint titanate-ethyl ester, and preparation and application methods thereof |
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Inventor after: Luo Jia Inventor after: Ren Jianxin Inventor after: Lian Wenliu Inventor after: Li Yabai Inventor after: Liu Jinyun Inventor before: Guo Xiaoyi Inventor before: Zhong Kejun Inventor before: Dai Yuangang Inventor before: Du Wen Inventor before: Zhuo Ningye Inventor before: Lian Wenliu Inventor before: Han Xing |
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Free format text: CORRECT: INVENTOR; FROM: GUO XIAOYI ZHONG KEJUN DAI YUANGANG DU WEN ZHUO NINGYE LIAN WENLIU HAN XING TO: LUO JIA REN JIANXIN LIAN WENLIU LI YABAI LIU JINYUN |
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