CN109156866A - A kind of additive with tongue fur note style and features and include the cigarette of the additive - Google Patents
A kind of additive with tongue fur note style and features and include the cigarette of the additive Download PDFInfo
- Publication number
- CN109156866A CN109156866A CN201811233887.3A CN201811233887A CN109156866A CN 109156866 A CN109156866 A CN 109156866A CN 201811233887 A CN201811233887 A CN 201811233887A CN 109156866 A CN109156866 A CN 109156866A
- Authority
- CN
- China
- Prior art keywords
- cigarette
- additive
- tongue fur
- features
- fur note
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- General Chemical & Material Sciences (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The present invention relates to a kind of additives with tongue fur note style and features, are based on mass percent comprising: 2, the 4- dihydroxy -6- methyl toluate of 0.05%-15.5%；The 3,5- dihydroxytoluene of 0.01%-0.2%.The additive further includes the pregelatinized starch of solvent, the beta-cyclodextrin of 10%-20% or 10%-20%.The invention further relates to a kind of cigarette comprising the additive with tongue fur note style and features, the additive is added into cigarette, cigarette flavor amount can be increased, the apparent tongue fur note of cigarette is assigned, has the function of increasing rich cigarette flavor, reduction stimulation, increases tongue fur note, promotes cigarette suction comfort and satisfaction.
Description
Technical field
The invention belongs to technical field of tobacco, and in particular to a kind of additive with tongue fur note style and features and include this
The cigarette of additive.
Background technique
As international smoking ban cry rises from all around and cigarette consumption person is to the growing interest of own health, Less harmful cigarette will be at
For the mainstream of future world cigarette, but cigarette flavor loss is necessarily accompanied with while harm reduction and comfort level is deteriorated, and cigarette adds
Perfume, which feeds, to be set off, added volume cigarette perfume taste, increase flue gas concentration, and improvement is jealous, removes and cover miscellaneous gas, reduce irritation, also
The characteristic chicken flavor of product grace can be assigned, the personalized style of prominent cigarette product, the research and development and application of perfuming cigarette charging are just
As one of the most key technology for keeping cigarette flavor and taste in lowering harm and decreasing coking work.Promote cigarette sucks satisfaction and pleased
Happy degree, becomes technical problem urgently to be resolved in current cigarette flavouring humectation technology.
Natural tongue fur note fragrance mainly includes the medicinal extract and absolute oil product of tree moss or oak moss in the market, and there are soil, gas
The difference factor such as time, growing environment brings the difference of raw material variety, and stable product quality cannot ensure；Simultaneously as it is made
Standby process is more or less mingled in obtained product mainly by separation and concentrations means such as organic solvent extraction, steam distillations
Influence the invalid components such as pigment and the vegetable wax of aroma quality；In addition also often lead to human body containing some in medicinal extract and absolute oil
The ingredient and heavy metal of allergy, the Product quality and safety for food and daily use chemicals industry have buried security risk.
Currently, being also prepared by the method that various ingredients compound in the prior art some special with tongue fur note style
The additive of sign.
CN103333743A discloses the tongue fur faint scent essence of a kind of 17 kinds of standard items and 2 kinds of solvents composition, has tongue fur faint scent
Gas style, however wherein invalid ingredient is contributed containing some pairs of fragrance.
CN107354007A, CN107616547A and CN107510092A disclose 2,4- dihydroxy -3,6- dimethyl benzene
The tree moss note additive of methyl formate, 2,4-, 2 kinds of standard items of dihydroxy -6- benzyl Ethyl formate and solvent composition, wherein
2 kinds of standard items being related to all have apparent tree moss note.
Synthetic perfume technical manual (see " synthetic perfume technical manual ", Liu Shuwen etc., China Light Industry Press, 2009
January in year, page 136) list " 25 parts of orcin monomethyl ether and 75 parts of 2,4- dihydroxy -3,6- dimethylbenzoate methyl ester
Fit over and be used together, the compound fragrance of preparation has natural oak moss fragrance true to nature ", however 2 kinds of marks with oak moss note
The compound fragrance that quasi- product are prepared only has the style of similar oak moss fragrance, and fragrance is coarse, there is dense chemical breath.
Although the additive with tongue fur note style and features has also been prepared in above-mentioned technical proposal, its preparation process
Complexity, be by multiple standards product and solvent complex, wherein containing obviously invalid ingredient is contributed to fragrance and what is obtained have
The additive fragrance of tongue fur note style and features is coarse, there is dense chemical breath.
Detailed description of the invention
Nothing.
Summary of the invention
To solve the above-mentioned problems, the present invention is proposed.
First aspect present invention provides a kind of additive with tongue fur note style and features, is based on weight percent, packet
It includes:
2,4- dihydroxy -6- the methyl toluate of 0.05%-15.5%；
The 3,5- dihydroxytoluene of 0.01%-0.2%.
Preferably, the additive further includes solvent, and the solvent is selected from ethyl alcohol, glyceryl triacetate or propylene glycol and third
The mixture of triol.
Preferably, the volumetric concentration of the ethyl alcohol is 50%-65%；The propylene glycol and the volume ratio of the glycerine are
3:1-1:1。
Preferably, the additive further includes the beta-cyclodextrin of 10%-20% or the pregelatinized starch of 10%-20%.
Preferably, the additive with tongue fur note style and features the preparation method comprises the following steps: press the additive composition
Content takes 2, the 4- dihydroxy -6- methyl toluate and 3, the 5- dihydroxytoluene, the solvent is added, in room
Under the conditions of temperature vibrate 10-20min dissolve raw material sufficiently, be configured to barrelling after uniform solution, be placed in be protected from light, shady place, save
12-48h obtains the additive with tongue fur note style and features.If solid spice to be made, β-can also be added
The substances such as cyclodextrin or pregelatinized starch adsorb aforesaid liquid fragrance and become solid form.
Second aspect of the present invention provides a kind of cigarette comprising the additive with tongue fur note style and features.
Preferably, it is added in cigarette filter by the dosage of 1-3 μ L/ branch filter tip, using cloud and mist (purple) leaf group rolling cigarette sample
Product, remaining auxiliary material and additive remain unchanged, and cigarette sample is prepared.
Preferably, it is sprayed into cigarette bobbin paper surface by the dosage of 1.0-3.0mL/ hectogram obbbin, using Hongta (1956)
Leaf group rolling cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample is prepared.
Preferably, it is sprayed into cigarette shreds surface by the dosage of 0.05-3.00mL/ hectogram pipe tobacco, it is (classical using Hongta
100) leaf group rolling cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample is prepared.
Preferably, cigarette heating is sprayed by the dosage that 0.03-2.00mL/ hectogram heats the cigarette shreds that do not burn or not
Cigarette shreds surface heats the cigarette X pipe tobacco that do not burn in production using cigarette in Yunnan and rolls cigarette sample, remaining auxiliary material and additive
It remains unchanged, cigarette sample is prepared.
Compared with prior art, the invention has the following advantages:
1, of the invention by 2,4- dihydroxy -6- methyl toluate, the 3,5- bis- with pungent perfume with fertile soil taste
Hydroxy-methylbenzene and solvent combination, are prepared the additive with tongue fur note style and features, and the additive has apparent tongue fur
Note, fragrance are abundant.
2, the additive with tongue fur note style and features of the invention, is added in cigarette, can increase cigarette perfume
Tolerance assigns the apparent tongue fur note of cigarette, has and increases rich cigarette flavor, reduction stimulation, increase tongue fur note, promote cigarette
Aspirate the effect of comfort and satisfaction.
3, the additive with tongue fur note style and features of the invention, most simple formula is only by 2 kinds of standard items and a kind of solvent group
At constituent is simple, does not contribute fragrance invalid ingredient, and low in cost, preparation method is simple, is suitble to scale
Production, has a good application prospect.
Specific embodiment
Below with reference to embodiment, the present invention is described in further detail, but is not limitation of the present invention, based on this
Any transformation or improvement that invention training centre is done, each fall within protection scope of the present invention.Be not specified in embodiment particular technique or
Condition person described technology or conditions or carries out according to the literature in the art according to product description.Agents useful for same or
Production firm person is not specified in instrument, is the conventional products that can be obtained by purchase.
Comparative example 1
Take 0.05% 2,4- dihydroxy -6- methyl toluate and 99.95% triacetic acid sweet by mass percentage
Grease mixing, vibrating 10min at room temperature dissolves raw material sufficiently, is configured to barrelling after uniform solution, is placed in and is protected from light, is negative
Liang Chu stores 12 hours, obtains additive A.
By the additive A, it is added in cigarette filter by the dosage of 1 μ L/ branch filter tip, is rolled using cloud and mist (purple) leaf group
Cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample 1 is prepared, and compare and comment with cloud and mist (purple) product
Inhale discovery: fertile soil taste increases by 10%, and irritation reduces by 0.2%, and tongue fur note increases by 0%.
Comparative example 2
0.01% 3,5- dihydroxytoluene and the mixing of 99.99% glyceryl triacetate are taken by mass percentage, in room
10min is vibrated under the conditions of temperature dissolves raw material sufficiently, is configured to barrelling after uniform solution, be placed in be protected from light, shady place, storage is 12 small
When, obtain additive B.
By the additive B, it is added in cigarette filter by the dosage of 1 μ L/ branch filter tip, is rolled using cloud and mist (purple) leaf group
Cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample 2 is prepared, and compare and comment with cloud and mist (purple) product
Inhale discovery: Xin Xiang increases by 4%, and irritation reduces by 0.5%, and tongue fur note increases by 0%.
Embodiment 1
0.05% 2,4- dihydroxy -6- methyl toluate, 0.01% 3,5- dihydroxy are taken by mass percentage
Toluene, 99.94% glyceryl triacetate mixing, at room temperature vibrate 10min dissolve raw material sufficiently, be configured to uniform
Barrelling after solution, be placed in be protected from light, shady place, store 12 hours, obtain addition of C.
By the addition of C, it is added in cigarette filter by the dosage of 1 μ L/ branch filter tip, is rolled using cloud and mist (purple) leaf group
Cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample 3 is prepared, and compare and comment with cloud and mist (purple) product
Inhale discovery: fragrance is rich to increase by 2%, and irritation reduces by 1%, and tongue fur note increases by 3%.
Embodiment 2
0.2% 2,4- dihydroxy -6- methyl toluate, 0.05% 3,5- dihydroxy first are taken by mass percentage
Benzene, 99.75% 60% alcohol of volumetric concentration mixing, at room temperature vibrate 10min dissolve raw material sufficiently, be configured to
Barrelling after one solution, be placed in be protected from light, shady place, store 24 hours, obtain additive D.
By the additive D, it is sprayed into cigarette bobbin paper surface by the dosage of 1.0mL/ hectogram obbbin, using Hongta
(1956) leaf group rolling cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample 4 is prepared, with Hongta
(1956) product compares discovery of smokeing panel test: fragrance is rich to increase by 3%, and irritation reduces by 3%, and tongue fur note increases by 5%, flue gas
Comfort promotes 1%.
Embodiment 3
10% 2,4- dihydroxy -6- methyl toluate, 0.1% 3,5- dihydroxy first are taken by mass percentage
Benzene, 89.9% volume ratio be 3:1 glycol/propane triol mix, at room temperature vibrate 20min keep raw material sufficiently molten
Solution, be configured to barrelling after uniform solution, be placed in be protected from light, shady place, store 24 hours, obtain additive E.
By the additive E, it is sprayed into cigarette shreds surface by the dosage of 3.00mL/ hectogram pipe tobacco, using Hongta (warp
Allusion quotation 100) leaf group rolling cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample 5 is prepared, with Hongta
(classics 100) product compares discovery of smokeing panel test: fragrance is rich to increase by 5%, and irritation reduces by 5%, and tongue fur note increases by 7%.
Embodiment 4
15.5% 2,4- dihydroxy -6- methyl toluate, 0.2% 3,5- dihydroxy first are taken by mass percentage
Benzene, 64.3% volume ratio 3:1 glycol/propane triol, 20% pregelatinized starch mixing, stir at room temperature
25min dissolves raw material sufficiently, is configured to barrelling after uniform solution, be placed in be protected from light, shady place, store 24 hours, added
Agent F.
By the additive F, it is non-ignitable that cigarette heating is sprayed by the dosage that 2.00mL/ hectogram heats the cigarette shreds that do not burn
Cigarette shreds surface is burnt, which is simultaneously rolled cigarette sample by certain, remaining auxiliary material and additive remain unchanged, and volume is prepared
Cigarette sample 6, compare discovery of smokeing panel test with the sample before applying the fragrance: fragrance is rich to increase by 7%, and irritation reduces
5%, tongue fur note increases by 9%.
Claims (5)
1. a kind of additive with tongue fur note style and features, which is characterized in that be based on mass percent comprising:
2,4- dihydroxy -6- the methyl toluate of 0.05%-15.5%；
The 3,5- dihydroxytoluene of 0.01%-0.2%.
2. the additive according to claim 1 with tongue fur note style and features, which is characterized in that it further includes solvent,
The solvent is selected from the mixture of ethyl alcohol, glyceryl triacetate or propylene glycol and glycerine.
3. the additive according to claim 2 with tongue fur note style and features, which is characterized in that the volume of the ethyl alcohol
Concentration is 50%-65%；The propylene glycol and the volume ratio of the glycerine are 3:1-1:1.
4. the additive according to claim 1 with tongue fur note style and features, which is characterized in that it further includes 10%-
20% beta-cyclodextrin or the pregelatinized starch of 10%-20%.
5. a kind of cigarette comprising the additive described in claim 2 or 4 with tongue fur note style and features.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811233887.3A CN109156866A (en) | 2018-10-23 | 2018-10-23 | A kind of additive with tongue fur note style and features and include the cigarette of the additive |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811233887.3A CN109156866A (en) | 2018-10-23 | 2018-10-23 | A kind of additive with tongue fur note style and features and include the cigarette of the additive |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN109156866A true CN109156866A (en) | 2019-01-08 |
Family
ID=64879028
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811233887.3A Pending CN109156866A (en) | 2018-10-23 | 2018-10-23 | A kind of additive with tongue fur note style and features and include the cigarette of the additive |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109156866A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111165873A (en) * | 2019-12-26 | 2020-05-19 | 云南恩典科技产业发展有限公司 | Solid filter stick particles applying solid essence and spice and preparation method thereof |
| CN111713740A (en) * | 2020-06-28 | 2020-09-29 | 云南中烟工业有限责任公司 | Additive with angelica sinensis aroma style characteristics, preparation method thereof and cigarette containing additive |
| CN111728261A (en) * | 2020-06-28 | 2020-10-02 | 云南中烟工业有限责任公司 | Additive with raspberry flavor style characteristics, preparation method thereof and cigarette containing additive |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107510092A (en) * | 2017-09-12 | 2017-12-26 | 云南中烟工业有限责任公司 | A kind of cigarette shreds additive of tree moss note and its preparation method and application |
| CN108669622A (en) * | 2018-06-15 | 2018-10-19 | 云南中烟工业有限责任公司 | A kind of volume cigarette additive and its preparation method and application of cool fragrant and sweet rhythm |
-
2018
- 2018-10-23 CN CN201811233887.3A patent/CN109156866A/en active Pending
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107510092A (en) * | 2017-09-12 | 2017-12-26 | 云南中烟工业有限责任公司 | A kind of cigarette shreds additive of tree moss note and its preparation method and application |
| CN108669622A (en) * | 2018-06-15 | 2018-10-19 | 云南中烟工业有限责任公司 | A kind of volume cigarette additive and its preparation method and application of cool fragrant and sweet rhythm |
Non-Patent Citations (1)
| Title |
|---|
| 朱怀远等: "分子蒸馏和同时蒸馏萃取法分析树苔浸膏的化学成分", 《食品科学》 * |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111165873A (en) * | 2019-12-26 | 2020-05-19 | 云南恩典科技产业发展有限公司 | Solid filter stick particles applying solid essence and spice and preparation method thereof |
| CN111165873B (en) * | 2019-12-26 | 2022-01-28 | 云南恩典科技产业发展有限公司 | Solid filter stick particles applying solid essence and spice and preparation method thereof |
| CN111713740A (en) * | 2020-06-28 | 2020-09-29 | 云南中烟工业有限责任公司 | Additive with angelica sinensis aroma style characteristics, preparation method thereof and cigarette containing additive |
| CN111728261A (en) * | 2020-06-28 | 2020-10-02 | 云南中烟工业有限责任公司 | Additive with raspberry flavor style characteristics, preparation method thereof and cigarette containing additive |
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| PB01 | Publication | ||
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Application publication date: 20190108 |