CN108669622A - A kind of volume cigarette additive and its preparation method and application of cool fragrant and sweet rhythm - Google Patents
A kind of volume cigarette additive and its preparation method and application of cool fragrant and sweet rhythm Download PDFInfo
- Publication number
- CN108669622A CN108669622A CN201810618554.6A CN201810618554A CN108669622A CN 108669622 A CN108669622 A CN 108669622A CN 201810618554 A CN201810618554 A CN 201810618554A CN 108669622 A CN108669622 A CN 108669622A
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- Prior art keywords
- cigarette
- additive
- fragrant
- cool
- sweet rhythm
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
- Fats And Perfumes (AREA)
Abstract
The present invention relates to a kind of volume cigarette additives and its preparation method and application of cool fragrant and sweet rhythm, belong to Field of Tobacco.The additive is mixed by mass percentage by the deionized water of 20% 35% menthyl acetate, 20% 50% beta cyclodextrin or pregelatinized starch, 30% 45%, 14 hours are ground at room temperature to paste, be placed in be protected from light, shady place, opening place 12 36 hours after be made.The present invention can increase cigarette flavor amount, assign cigarette apparent cool fragrant and sweet rhythm, fragrance is abundant, reduces stimulation, improve cigarette sucks satisfaction and pleasure degree.
Description
Technical field
The present invention relates to a kind of volume cigarette additives, and in particular to a kind of volume cigarette additive of cool fragrant and sweet rhythm further relates to
Preparation method and application, belong to Field of Tobacco.
Background technology
In recent years, with the variation of the progress and tobacco consumption idea of science and technology, harm reduction has become World tobacco industry
Established developing direction, novel tobacco product are able to occur and develop.Novel tobacco product is divided into heating not combustion products, electronics
Cigarette and smoke-free tobacco product heat pipe tobacco using special heat source wherein heating not burning type cigarette, pipe tobacco it is heated but
Do not burn, sucking impression and mode etc. close to traditional cigarette, provided compared with electronic cigarette and smoke-free tobacco product compared with
High satisfaction, tobacco consumer are easier to receive, and are the important directions of tobacco business future development.
Burning type cigarette is not compared with traditional combustion type cigarette for heating, and heating temperature is generally at 500 DEG C hereinafter, be usually
It is 300 DEG C, different with the mechanism of generation fragrance to the effect of the aroma-producing substance in cigarette.Essence and flavoring agent can play raising and inhale in cigarette
Gravitation stimulates the effect consumed, thus is also a part indispensable in new cigarette.But suitable for the essence of new cigarette
Exploitation lag, only continues to use traditional flavouring essence for tobacco product.Since fragrance material is largely for molecular weight is relatively low, low boiling point, waves
The stronger compound of hair property, loses in high temperature working processes serious, causes to release fragrant non-uniform phenomenon, or even because waving during storage
Hair loses fragrance or unstable chemcial property easily by oxidation deterioration.
Menthyl acetate, colourless or light yellow clear liquid, there is soft peppermint and rose fragrance;Being added in cigarette can assign
The cool fragrant and sweet rhythm of cigarette is given, however, since it is with certain volatility, is easy there are different journeys in cigarette burning and aspiration procedure
The loss of degree causes the stability of cigarette product quality that cannot ensure.The present invention develop it is a kind of have can make cool fragrant and sweet rhythm
The cigarette additive of slow release, fragrance is abundant, reduces stimulation, and suck satisfaction and the pleasure degree of cigarette get a promotion.
Since menthyl acetate has certain volatility, existing cigarette extract addition of C N20161117074.2
Menthyl acetate cigarette additive is not suitable for it using techniques such as composite extract preparation method, supercritical carbon dioxide extractings
It prepares;The technique that the heating, drying or spray drying process that CN201710647631.6 is related to prepare overlapping glue addition additive is same
Sample is not suitable for the preparation of menthyl acetate cigarette additive.
Invention content
In order to solve the above-mentioned technical problem, the purpose of the present invention is to provide a kind of volume cigarette additive of cool fragrant and sweet rhythm,
Another is designed to provide the preparation method of the volume cigarette additive, also resides in the application for providing the volume cigarette additive.This
The technical solution of invention is specially:
A kind of volume cigarette additive of cool fragrant and sweet rhythm, is made of the raw material of following mass percents:The acetic acid peppermint of 20%-35%
The deionized water of ester, the beta-cyclodextrin of 20%-50% or pregelatinized starch and 30%-45%.
The preparation method of above-mentioned volume cigarette additive of the present invention, is carried out as follows:
It is the menthyl acetate of 20%-35%, the beta-cyclodextrin of 20%-50% or pregelatinized starch and 30%- by mass percent
45% deionized water mixing grinds 1-4 hour to paste at room temperature, be placed in be protected from light, shady place, open placement 12-36 is small
When, you can obtain the volume cigarette additive.
The application of above-mentioned volume cigarette additive of the present invention, the additive is heated by 3-20 mg/ hectograms
The dosage of cigarette shreds of not burning is added heating and does not burn in cigarette shreds.
The application of above-mentioned volume cigarette additive of the present invention, 3-15 mg/ hectogram obbbins are pressed by the additive
Dosage be added cigarette bobbin paper in.
Compared with prior art, the invention has the advantages that:
(1), the present invention it is of low cost, preparation method is easy, and without adding other reagents, the reaction time shortens, for heating not
When in burning cigarette shreds, cigarette flavor amount can be increased, assign cigarette apparent cool fragrant and sweet rhythm, and cool fragrant and sweet rhythm can be made slow
Release, fragrance is abundant, reduces stimulation, improve cigarette sucks satisfaction and pleasure degree, wherein and aroma quality promotes 3-4%,
Irritation reduces 2-7%, and cool fragrant and sweet rhythm increases 2-8%, has preferable suction consistency, has a good application prospect.
(2), the present invention additive be used for cigarette bobbin paper when, cigarette can be increased and smell perfume (or spice), promote the comfortable of side-stream smoke
Property, meanwhile, it is capable to increase cigarette flavor amount, assign cigarette apparent cool fragrant and sweet rhythm, and cool fragrant and sweet rhythm slow release can be made, fragrance
It is abundant, stimulation is reduced, improve cigarette sucks satisfaction and pleasure degree, wherein fragrance is rich or quality increases 2-5%, thorn
Swashing property reduces 1-8%, and cool fragrant and sweet rhythm increases 1-8%.
Specific implementation mode
With reference to embodiment, the present invention is described in further detail, but is not limitation of the present invention, based on this
Any transformation or improvement that invention training centre is done, each fall within protection scope of the present invention.Be not specified in embodiment particular technique or
Condition person carries out according to technology or condition described in document in the art or according to product description.Agents useful for same or
Production firm person is not specified in instrument, and being can be by buying the conventional products obtained.
Embodiment 1
The preparation method of the volume cigarette additive of the cool fragrant and sweet rhythm of the present embodiment, is carried out as follows:
Pipette the menthyl acetate of mass percent 20%, 50% beta-cyclodextrin, 30% deionized water mixing, grind at room temperature
Mill 1 hour to paste, be placed in be protected from light, shady place, opening place 12 hours, the cigarette shreds additive that do not burn must be heated.
The heating is not burnt cigarette shreds additive, the dosage for the cigarette shreds that do not burn by the heating of 3mg/ hectograms
It is added and heats in the cigarette shreds that do not burn, using Hongta (1956) leaf group rolling cigarette sample, remaining auxiliary material and additive
It remains unchanged, cigarette sample A is prepared, carry out comparing discovery of smokeing panel test with Hongta (1956) product:Aroma quality is promoted
3%, irritation reduces by 3%, and cool fragrant and sweet rhythm increases by 2%, has preferable suction consistency.
The additive that will be prepared by CN20161117074.2, the dosage that the cigarette shreds that do not burn are heated by 3 mg/ hectograms add
Enter to heat in the cigarette shreds that do not burn, using Hongta (1956) leaf group rolling cigarette sample, remaining auxiliary material and additive are equal
It remains unchanged, cigarette sample A is prepared, carry out comparing discovery of smokeing panel test with Hongta (1956) product:Aroma quality is promoted
1%, irritation reduces by 0.5%, when suction before 2 mouthfuls of cool fragrant and sweet rhythms increase by 0.5%, fragrant and sweet rhythm cool later disappears.
Embodiment 2
The preparation method of the volume cigarette additive of the cool fragrant and sweet rhythm of the present embodiment, is carried out as follows:
Pipette the menthyl acetate of mass percent 30%, 40% pregelatinized starch, 30% deionized water mixing, at room temperature
Grinding 4 hours to paste, be placed in be protected from light, shady place, opening place 36 hours, the cigarette shreds additive that do not burn must be heated.
The heating is not burnt cigarette shreds additive, the use for the cigarette shreds that do not burn by the heating of 6 mg/ hectograms
Amount, which is added, to be heated in the cigarette shreds that do not burn, using Hongta (1956) leaf group rolling cigarette sample, remaining auxiliary material and additive
It remains unchanged, cigarette sample B is prepared, carry out comparing discovery of smokeing panel test with Hongta (1956) product:The rich increasing of fragrance
Add 4%, irritation reduces by 7%, and cool fragrant and sweet rhythm increases by 5%, has preferable suction consistency.
The additive that will be prepared by CN20161117074.2, the dosage that the cigarette shreds that do not burn are heated by 6 mg/ hectograms add
Enter to heat in the cigarette shreds that do not burn, using Hongta (1956) leaf group rolling cigarette sample, remaining auxiliary material and additive are protected
It holds constant, cigarette sample B is prepared, carrying out comparison with Hongta (1956) product smokes panel test discovery:Aroma quality promotes 2%,
Irritation reduces by 1%, when suction before 4 mouthfuls of cool fragrant and sweet rhythms increase by 1%, fragrant and sweet rhythm cool later disappears.
Embodiment 3
The preparation method of the volume cigarette additive of the cool fragrant and sweet rhythm of the present embodiment, is carried out as follows:
Pipette the menthyl acetate of mass percent 35%, 20% beta-cyclodextrin, 45% deionized water mixing, grind at room temperature
Mill 2 hours to paste, be placed in be protected from light, shady place, opening place 24 hours, the cigarette shreds additive that do not burn must be heated.
The heating is not burnt cigarette shreds additive, the use for the cigarette shreds that do not burn by the heating of 20 mg/ hectograms
Amount, which is added, to be heated in the cigarette shreds that do not burn, using Hongta (1956) leaf group rolling cigarette sample, remaining auxiliary material and additive
It remains unchanged, cigarette sample C is prepared, carry out comparing discovery of smokeing panel test with Hongta (1956) product:The rich increasing of fragrance
Add 3%, irritation reduces by 2%, and cool fragrant and sweet rhythm increases by 8%, has preferable suction consistency.
The additive that will be prepared by CN201710647631.6, the dosage for the cigarette shreds that do not burn by the heating of 15 mg/ hectograms
It is added and heats in the cigarette shreds that do not burn, using Hongta (1956) leaf group rolling cigarette sample, remaining auxiliary material and additive are equal
It remains unchanged, cigarette sample C is prepared, carry out comparing discovery of smokeing panel test with Hongta (1956) product:The rich increase of fragrance
1%, irritation reduces by 0.5%, when suction before 5 mouthfuls of cool fragrant and sweet rhythms increase by 2%, fragrant and sweet rhythm cool later disappears.
Embodiment 4
The preparation method of the volume cigarette additive of the cool fragrant and sweet rhythm of the present embodiment, is carried out as follows:
Pipette the menthyl acetate of mass percent 22%, 50% beta-cyclodextrin, 35% deionized water mixing, grind at room temperature
Mill 1 hour to paste, be placed in be protected from light, shady place, opening place 12 hours, obtain cigarette bobbin paper additive.
It is added in cigarette bobbin paper, the cigarette bobbin paper additive using Hongta by the dosage of 3 mg/ hectogram obbbins
Mountain (1956) leaf group rolling cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample A is prepared, and red
The Tashan Mountain (1956) product carries out comparing discovery of smokeing panel test:Aroma quality promotes 2%, and irritation reduces by 2%, and cool fragrant and sweet rhythm increases by 1%, tool
There is preferable suction consistency.
The additive that will be prepared by CN20161117074.2 is added by the dosage of 3 mg/ hectogram obbbins in cigarette bobbin paper,
Using Hongta (1956) leaf group rolling cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample is prepared
A carries out comparing discovery of smokeing panel test with Hongta (1956) product:Aroma quality promotes 1.5%, and irritation reduces by 0.4%, when suction before
2 mouthfuls of cool fragrant and sweet rhythms increase by 0.3%, and fragrant and sweet rhythm cool later disappears.
Embodiment 5
The preparation method of the volume cigarette additive of the cool fragrant and sweet rhythm of the present embodiment, is carried out as follows:
Pipette the menthyl acetate of mass percent 20%, 40% pregelatinized starch, 40% deionized water mixing, at room temperature
Grinding 4 hours to paste, be placed in be protected from light, shady place, opening place 36 hours, obtain cigarette bobbin paper additive.
It is added in cigarette bobbin paper, the cigarette bobbin paper additive using Hongta by the dosage of 6 mg/ hectogram obbbins
Mountain (1956) leaf group rolling cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample B are prepared, with Hongta
Mountain (1956) product carries out comparing discovery of smokeing panel test:Fragrance is rich to increase by 5%, and irritation reduces by 8%, and cool fragrant and sweet rhythm increases by 6%, tool
There is preferable suction consistency.
The additive that will be prepared by CN20161117074.2 is added by the dosage of 6 mg/ hectogram obbbins in cigarette bobbin paper,
Using Hongta (1956) leaf group rolling cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample is prepared
B carries out comparing discovery of smokeing panel test with Hongta (1956) product:Aroma quality promotes 2%, and irritation reduces by 1.5%, when suction before 4
The cool fragrant and sweet rhythm of mouth increases by 1%, and fragrant and sweet rhythm cool later disappears.
Embodiment 6
The preparation method of the volume cigarette additive of the cool fragrant and sweet rhythm of the present embodiment, is carried out as follows:
Pipette the menthyl acetate of mass percent 35%, 20% beta-cyclodextrin, 45% deionized water mixing, grind at room temperature
Mill 2 hours to paste, be placed in be protected from light, shady place, opening place 24 hours, obtain cigarette bobbin paper additive.
By the cigarette bobbin paper additive, it is added in cigarette bobbin paper by the dosage of 15 mg/ hectogram obbbins, use is red
The Tashan Mountain (1956) leaf group rolling cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample C is prepared, and red
The Tashan Mountain (1956) product carries out comparing discovery of smokeing panel test:Fragrance is rich to increase by 3%, and irritation reduces by 1%, and cool fragrant and sweet rhythm increases by 8%,
With preferable suction consistency.
Cigarette bobbin paper is added by the dosage of 15 mg/ hectogram obbbins in the additive that will be prepared by CN201710647631.6
In, using Hongta (1956) leaf group rolling cigarette sample, remaining auxiliary material and additive remain unchanged, and cigarette sample is prepared
Product C carries out comparing discovery of smokeing panel test with Hongta (1956) product:Fragrance is rich to increase by 0.4%, and irritation reduces by 0.5%, suction
When before 5 mouthfuls of cool fragrant and sweet rhythms increase by 1.5%, fragrant and sweet rhythm cool later disappears.
The basic principles, main features and advantages of the present invention have been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the above embodiments and description only describe this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and improvements may be made to the invention, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (4)
1. a kind of volume cigarette additive of cool fragrant and sweet rhythm, it is characterised in that:It is made of the raw material of following mass percents:20%-
The deionized water of 35% menthyl acetate, the beta-cyclodextrin of 20%-50% or pregelatinized starch and 30%-45%.
2. the preparation method of volume cigarette additive described in claim 1, it is characterised in that:It is carried out as follows:
It is the menthyl acetate of 20%-35%, the beta-cyclodextrin of 20%-50% or pregelatinized starch and 30%- by mass percent
45% deionized water mixing grinds 1-4 hour to paste at room temperature, be placed in be protected from light, shady place, open placement 12-36 is small
When, you can obtain the volume cigarette additive.
3. the application of volume cigarette additive as claimed in claim 1 or 2, it is characterised in that:The additive is pressed into 3-20
The dosage addition that mg/ hectograms heat the cigarette shreds that do not burn is heated in the cigarette shreds that do not burn.
4. the application of volume cigarette additive as claimed in claim 1 or 2, it is characterised in that:The additive is pressed into 3-15
The dosage of mg/ hectogram obbbins is added in cigarette bobbin paper.
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Cited By (18)
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CN109156870A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of additive with tongue fur note style and features and include the cigarette of the additive |
CN109156867A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence with tongue fur note style and features and include the cigarette of the essence |
CN109156879A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence highlighting tongue fur note style and features and the cigarette comprising the essence |
CN109156875A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of additive highlighting tongue fur note style and features and the cigarette comprising the additive |
CN109156868A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence with tongue fur note style and features and include the cigarette of the essence |
CN109156873A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence highlighting tongue fur note style and features and the cigarette comprising the essence |
CN109156876A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence with tongue fur note style and features and include the cigarette of the essence |
CN109156878A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of additive highlighting tongue fur note style and features and the cigarette comprising the additive |
CN109156872A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of additive highlighting tongue fur note style and features and the cigarette comprising the additive |
CN109156874A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence highlighting tongue fur note style and features and the cigarette comprising the essence |
CN109156877A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of additive highlighting tongue fur note style and features and the cigarette comprising the additive |
CN109156871A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence with tongue fur note style and features and include the cigarette of the essence |
CN109156880A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of additive with tongue fur note style and features and include the cigarette of the additive |
CN109156869A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence highlighting tongue fur note style and features and the cigarette comprising the essence |
CN109156866A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of additive with tongue fur note style and features and include the cigarette of the additive |
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CN109156869A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence highlighting tongue fur note style and features and the cigarette comprising the essence |
CN109156870A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of additive with tongue fur note style and features and include the cigarette of the additive |
CN109156875A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of additive highlighting tongue fur note style and features and the cigarette comprising the additive |
CN109156868A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence with tongue fur note style and features and include the cigarette of the essence |
CN109156873A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence highlighting tongue fur note style and features and the cigarette comprising the essence |
CN109156876A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence with tongue fur note style and features and include the cigarette of the essence |
CN109156878A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of additive highlighting tongue fur note style and features and the cigarette comprising the additive |
CN109156879A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence highlighting tongue fur note style and features and the cigarette comprising the essence |
CN109156874A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence highlighting tongue fur note style and features and the cigarette comprising the essence |
CN109156871A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence with tongue fur note style and features and include the cigarette of the essence |
CN109156877A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of additive highlighting tongue fur note style and features and the cigarette comprising the additive |
CN109156880A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of additive with tongue fur note style and features and include the cigarette of the additive |
CN109156867A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of essence with tongue fur note style and features and include the cigarette of the essence |
CN109156866A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of additive with tongue fur note style and features and include the cigarette of the additive |
CN109156865A (en) * | 2018-10-23 | 2019-01-08 | 云南中烟工业有限责任公司 | A kind of additive with tongue fur note style and features and include the cigarette of the additive |
CN110477440A (en) * | 2019-07-09 | 2019-11-22 | 河南中烟工业有限责任公司 | For heating the Mint Essence and reconstituted tobacoo and the cigarette that do not burn of the cigarette that do not burn |
CN110477440B (en) * | 2019-07-09 | 2022-03-22 | 河南中烟工业有限责任公司 | Mint essence for heating non-combustible cigarette, tobacco sheet and non-combustible cigarette |
CN110714367A (en) * | 2019-09-20 | 2020-01-21 | 河南中烟工业有限责任公司 | Cool and sweet gloss oil, preparation method and tipping paper for cigarettes |
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Application publication date: 20181019 |