CN106072750A - A kind of compound flavouring essence for tobacco, Preparation Method And The Use - Google Patents
A kind of compound flavouring essence for tobacco, Preparation Method And The Use Download PDFInfo
- Publication number
- CN106072750A CN106072750A CN201610454434.8A CN201610454434A CN106072750A CN 106072750 A CN106072750 A CN 106072750A CN 201610454434 A CN201610454434 A CN 201610454434A CN 106072750 A CN106072750 A CN 106072750A
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- China
- Prior art keywords
- tobacco
- flavouring essence
- wall material
- core
- compound
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Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention belongs to the technical field that compound flavouring essence for tobacco is applied in Medicated cigarette field, the invention discloses a kind of compound flavouring essence for tobacco, including wall material, core and emulsifying agent；Described wall material is the mixture of modified starch and arabic gum；Described core is Trilobatin, geraniol and the mixture of geraniol glucosides；Described emulsifying agent is one of sucrose fatty acid ester or distillation monoglyceride.The invention also discloses the preparation method of compound flavouring essence for tobacco and for the purposes to Medicated cigarette flavouring, compound flavouring essence for tobacco can keep the stability of cigarette flavor, persistency and fragrance release uniformity consistency in time.
Description
Technical field
The invention belongs to the technical field that compound flavouring essence for tobacco is applied in Medicated cigarette field, be specifically related to a kind of composite smoke and use
Essence, its preparation method and the application in Medicated cigarette.
Background technology
Tobacco product generally will use perfuming method, reaches to improve cigarette fragrance characteristic, cover miscellaneous taste and give medicated cigarette
The purpose of individual style, thus become a part indispensable in tobacco industry.Updating formula, exploitation Novel tobacco is used
While essence, the stability of cigarette flavor and persistent problem, especially Research Center's enterprise scientific research personnel focus of attention in one's power.
The boiling point of most of perfume materials is relatively low, highly volatile, and during long-term storage, loss is serious, and burns and sucks owing to medicated cigarette belongs to high temperature
Handling characteristics, the flue gas of heat can make the spice in medicated cigarette discharge in advance, cause early stage strong, and it is fragrant uneven that what the later stage was boring release
Phenomenon, reduces product consumption quality.
Microcapsule technology is to improve the important means of essence stability, uses naturally occurring or synthetic macromolecular compound to constitute
Perfume material to be protected (core or internal phase) is coated with by continuous film (wall or foreign minister) completely, can effectively stop fragrant composition
Volatilization scatter and disappear, isolation simultaneously contacts with extraneous, and also slow down that chemical change causes goes bad, and improves the steady of fragrance material
Qualitative.But microcapsule embedded essence product, during the burning and sucking of medicated cigarette, owing to flue-gas temperature is higher, still can not prevent perfume (or spice)
The release in advance of gas composition, releases fragrant homogeneity question and still cannot solve.
Summary of the invention
The present invention, for overcoming loss in fragrance material high temperature working processes serious, causes releasing fragrant non-uniform phenomenon, even exists
Losing fragrance because of volatilization during storage, or unstable chemcial property is easy to be oxidized rotten and propose, the present invention uses compound
Flavouring essence for tobacco, and flavouring in Medicated cigarette, can keep the uniform of the stability of cigarette flavor, persistency and/or fragrance release
Concordance.
A first aspect of the present invention relates to a kind of compound flavouring essence for tobacco, including wall material, core and emulsifying agent；Described wall material is
Modified starch and the mixture of arabic gum；Described core is Trilobatin, geraniol and the mixture of geraniol glucosides；Described breast
Agent is one of sucrose fatty acid ester or distillation monoglyceride (i.e. glyceryl monostearate).
In the preferred version of a first aspect of the present invention, described modified starch is described wall material 30wt%～40wt%,
Described arabic gum is described wall material 60wt%～70wt%.
Described Trilobatin is 0.5wt%～5.0wt% of described core, and described geraniol is described core
44.5wt%～74.5wt%, described geraniol glucosides is 25wt%～55wt% of described core.
Described wall material is 1:1～1:1.5 with the mass ratio of described core；
Emulsifying agent is wall material and 1wt%～2wt% of core total amount.
A second aspect of the present invention relates to the preparation method of described compound flavouring essence for tobacco, comprises the steps:
(1) it is mixed to get mixture after weighing described wall material, described core and described emulsifying agent in proportion；
(2) add water stirring by the mixture that step (1) obtains, and is configured to 30wt%～40wt% aqueous dispersions；
(3) aqueous dispersions step (2) obtained homogenizing under 60～70 DEG C and 25～35MPa, obtains uniform moisture
Dissipate liquid；
(4) uniform aqueous dispersions step (3) obtained is spray-dried and i.e. obtains described compound flavouring essence for tobacco.Preferably
Ground, the inlet temperature of described spray drying is 150～250 DEG C, and outlet temperature is 60～90 DEG C.
A third aspect of the present invention relates to described compound flavouring essence for tobacco for the purposes to Medicated cigarette flavouring.
A fourth aspect of the present invention relates to described compound flavouring essence for tobacco for keeping the stability of cigarette flavor, persistency
And/or the purposes of the uniformity consistency that fragrance release is in time
Beneficial effects of the present invention:
1, the stable type flavouring essence for tobacco using the present invention to produce, adds in cigarette shreds, with the Medicated cigarette adding geraniol
Comparing, during the long-term storage of medicated cigarette, fragrance last is permanent, and flavouring essence quality does not occur the change of perceptibility, stability
Good.During burning and sucking, from start to end, fragrance is the most uniform and stable, releases fragrant uniform.And the medicated cigarette adding geraniol is deposited
During volatile aroma loss, occur flavouring essence quality to deteriorate, during burning and sucking, owing to flue-gas temperature is high, make essence quickly wave
Send out, give off a strong fragrance before formation, after the boring phenomenon of fragrance.
2, the present invention with the addition of novel sweetener Trilobatin, brings pure and fresh sweet taste to flue gas, improves flue gas product
Matter, has again clearing away lung-heat, the effect of preventing pharyngitis.
4, the present invention uses complex technique to combine with glucosides fragrance precursor stabilization technology, has both improve fragrance in medicated cigarette
The stability of composition, long-term storage does not change flavouring essence quality, during burning and sucking, can control again the rate of release of fragrance component,
Because glucosides fragrance precursor be heated to 300 DEG C and above time just thermal cracking release fragrance, conform exactly to during medicated cigarette burns and sucks,
Along with the movement of cigarette end, progressively discharging the feature of fragrance, improve consumption impression during burning and sucking, the present invention will be to improving medicated cigarette
Quality, sets up Premium Brands, significant.
Detailed description of the invention
The compound flavouring essence for tobacco using the present invention adds in cigarette shreds, with the Medicated cigarette phase adding common flavouring essence for tobacco
Ratio, chooses 6 professionals and carries out scoring of smokeing panel test, and appraisal result is as shown in table 2, and standards of grading are as shown in table 1.
Table 1 Score index and standards of grading
Table 2 appraisal result
As can be seen from Table 2, compared with the control, the present invention is combined the fragrance value that flavouring essence for tobacco adds in cigarette shreds
High, perfume quantity foot, almost without miscellaneous QI, pleasant impression is comfortable.During burning and sucking, from lighting medicated cigarette suction, to last after-flame, fragrance is lasting
Uniformly, the equal melancholy of each item rating, in matched group, achieves unexpected effect.
Using the compound flavouring essence for tobacco of the present invention, during medicated cigarette long-term storage, fragrance is still stable lasting, deposits for a long time
The medicated cigarette put, during burning and sucking, fragrance is uniform and stable from the beginning to the end, releases fragrant uniform.Common flavouring essence for tobacco is then deposited medicated cigarette
During putting, volatile aroma loss, forms above fragrance dense during burning and sucking, after the boring phenomenon of fragrance, and burning and sucking
During, owing to flue-gas temperature is high, makes essence volatilization loss fast, there is also above fragrance dense, after the boring phenomenon of fragrance.
Use the compound flavouring essence for tobacco of the present invention, compound essence ratio uniform can be made, also to a certain degree improve perfume (or spice)
The stability of essence.Significantly improve the aroma quality of medicated cigarette.The present invention will promote sending out of tobacco business to improving cigarette quality
Exhibition, significant.
Claims (5)
1. a compound flavouring essence for tobacco, including wall material and core；It is characterized in that, described wall material is modified starch and arabic gum
Mixture；Described core is Trilobatin, geraniol and the mixture of geraniol glucosides.
Compound flavouring essence for tobacco the most according to claim 1, it is characterised in that described modified starch accounts for described wall material
30wt%～40wt%, described arabic gum accounts for 60wt%～70wt% of described wall material；
Described Trilobatin accounts for 0.5wt%～5.0wt% of described core, described geraniol account for described core 44.5wt%～
74.5wt%, described geraniol glucosides accounts for 25wt%～55wt% of described core；
Described wall material is 1:1～1:1.5 with the mass ratio of described core.
The preparation method of a kind of compound flavouring essence for tobacco the most according to claim 2, it is characterised in that comprise the steps:
(1) weigh described wall material and described core in proportion, and be mixed to get mixture, wherein said emulsifying agent after emulsifying agent
For one of sucrose fatty acid ester or distillation monoglyceride, the amount of emulsifying agent accounts for wall material and 1wt%～2wt% of core gross mass；
(2) add water stirring by the mixture that step (1) obtains, and is configured to 30wt%～40wt% aqueous dispersions；
(3) aqueous dispersions step (2) obtained homogenizing under 60～70 DEG C and 25～35MPa, obtains uniform aqueous dispersions；
(4) uniform aqueous dispersions step (3) obtained is spray-dried and i.e. obtains described compound flavouring essence for tobacco.
Compound flavouring essence for tobacco the most according to claim 1 is for the purposes of Medicated cigarette flavouring.
Compound flavouring essence for tobacco the most according to claim 1 is for keeping the stability of cigarette flavor, persistency and/or fragrance
The purposes of release uniformity consistency in time.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610454434.8A CN106072750A (en) | 2016-06-22 | 2016-06-22 | A kind of compound flavouring essence for tobacco, Preparation Method And The Use |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610454434.8A CN106072750A (en) | 2016-06-22 | 2016-06-22 | A kind of compound flavouring essence for tobacco, Preparation Method And The Use |
Publications (1)
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|---|---|
| CN106072750A true CN106072750A (en) | 2016-11-09 |
Family
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| Application Number | Title | Priority Date | Filing Date |
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| CN201610454434.8A Pending CN106072750A (en) | 2016-06-22 | 2016-06-22 | A kind of compound flavouring essence for tobacco, Preparation Method And The Use |
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| CN (1) | CN106072750A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106666822A (en) * | 2016-11-29 | 2017-05-17 | 将军烟草集团有限公司 | Cigarette blast bead and preparation method thereof |
| CN107779262A (en) * | 2017-10-20 | 2018-03-09 | 云南中烟工业有限责任公司 | One kind heats the special flores aurantii flavor essence of cigarette and preparation method thereof that do not burn |
| CN107802026A (en) * | 2017-10-20 | 2018-03-16 | 云南中烟工业有限责任公司 | A kind of flores aurantii flavor heats the preparation method for the new cigarette core that do not burn |
| CN107822197A (en) * | 2017-10-20 | 2018-03-23 | 云南中烟工业有限责任公司 | A kind of peppermint flavor heats the preparation method for the new cigarette core that do not burn |
| CN108244693A (en) * | 2016-12-29 | 2018-07-06 | 广州华芳烟用香精有限公司 | A kind of preparation method of cloud and mist extract powder fragrance and its application in cigarette |
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| JPS53133697A (en) * | 1977-04-20 | 1978-11-21 | Japan Tobacco Inc | Microcapsule containing flavor as core substance, and tobacco product containing the same |
| CN103451019A (en) * | 2013-09-04 | 2013-12-18 | 湖北中烟工业有限责任公司 | Microcapsule essence perfume for cigarettes as well as preparation method of microcapsule essence perfume |
| CN103865650A (en) * | 2014-03-20 | 2014-06-18 | 中国热带农业科学院农产品加工研究所 | Temperature sensibility liquor-fragrance essence microcapsule for cigarette and preparation method thereof |
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| CN104711120A (en) * | 2015-03-31 | 2015-06-17 | 川渝中烟工业有限责任公司 | Essential oil micro-capsule prepared by using tobacco wastes as well as preparation method and application thereof |
-
2016
- 2016-06-22 CN CN201610454434.8A patent/CN106072750A/en active Pending
Patent Citations (6)
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| JPS53133697A (en) * | 1977-04-20 | 1978-11-21 | Japan Tobacco Inc | Microcapsule containing flavor as core substance, and tobacco product containing the same |
| CN103451019A (en) * | 2013-09-04 | 2013-12-18 | 湖北中烟工业有限责任公司 | Microcapsule essence perfume for cigarettes as well as preparation method of microcapsule essence perfume |
| CN103865650A (en) * | 2014-03-20 | 2014-06-18 | 中国热带农业科学院农产品加工研究所 | Temperature sensibility liquor-fragrance essence microcapsule for cigarette and preparation method thereof |
| CN103861537A (en) * | 2014-03-20 | 2014-06-18 | 中国热带农业科学院农产品加工研究所 | Preparation method of essential oil microcapsule |
| CN104178343A (en) * | 2014-09-05 | 2014-12-03 | 南京泽朗生物科技有限公司 | Preparation method of perilla arguta microcapsules and application of perilla arguta microcapsules in tobaccos |
| CN104711120A (en) * | 2015-03-31 | 2015-06-17 | 川渝中烟工业有限责任公司 | Essential oil micro-capsule prepared by using tobacco wastes as well as preparation method and application thereof |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106666822A (en) * | 2016-11-29 | 2017-05-17 | 将军烟草集团有限公司 | Cigarette blast bead and preparation method thereof |
| CN108244693A (en) * | 2016-12-29 | 2018-07-06 | 广州华芳烟用香精有限公司 | A kind of preparation method of cloud and mist extract powder fragrance and its application in cigarette |
| CN107779262A (en) * | 2017-10-20 | 2018-03-09 | 云南中烟工业有限责任公司 | One kind heats the special flores aurantii flavor essence of cigarette and preparation method thereof that do not burn |
| CN107802026A (en) * | 2017-10-20 | 2018-03-16 | 云南中烟工业有限责任公司 | A kind of flores aurantii flavor heats the preparation method for the new cigarette core that do not burn |
| CN107822197A (en) * | 2017-10-20 | 2018-03-23 | 云南中烟工业有限责任公司 | A kind of peppermint flavor heats the preparation method for the new cigarette core that do not burn |
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Application publication date: 20161109 |
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| RJ01 | Rejection of invention patent application after publication |