CN109156879A - A kind of essence highlighting tongue fur note style and features and the cigarette comprising the essence - Google Patents
A kind of essence highlighting tongue fur note style and features and the cigarette comprising the essence Download PDFInfo
- Publication number
- CN109156879A CN109156879A CN201811281594.2A CN201811281594A CN109156879A CN 109156879 A CN109156879 A CN 109156879A CN 201811281594 A CN201811281594 A CN 201811281594A CN 109156879 A CN109156879 A CN 109156879A
- Authority
- CN
- China
- Prior art keywords
- essence
- cigarette
- tongue fur
- features
- fur note
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/06—Use of materials for tobacco smoke filters
- A24D3/14—Use of materials for tobacco smoke filters of organic materials as additive
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
Abstract
The present invention relates to a kind of essence for highlighting tongue fur note style and features, are based on mass percent comprising: 2,4- dihydroxy -3,5 of 0.2%-10%, 6- trimethylbenzoic acid ethyl ester；The 3,4- xylenol of 0.05%-6%.The essence further includes the pregelatinized starch of solvent, the beta-cyclodextrin of 10%-20% or 10%-20%.The invention further relates to a kind of cigarette comprising the essence for highlighting tongue fur note style and features, the essence is added into cigarette, cigarette flavor amount can be increased, the apparent tongue fur note of cigarette is assigned, has the function of increasing rich cigarette flavor, reduction stimulation, increases tongue fur note, promotes cigarette suction comfort and satisfaction.
Description
Technical field
The invention belongs to technical field of tobacco, and in particular to a kind of essence for highlighting tongue fur note style and features and comprising the perfume
The cigarette of essence.
Background technique
As international smoking ban cry rises from all around and cigarette consumption person is to the growing interest of own health, Less harmful cigarette will be at
For the mainstream of future world cigarette, but cigarette flavor loss is necessarily accompanied with while harm reduction and comfort level is deteriorated, and cigarette adds
Perfume, which feeds, to be set off, added volume cigarette perfume taste, increase flue gas concentration, and improvement is jealous, removes and cover miscellaneous gas, reduce irritation, also
The characteristic chicken flavor of product grace can be assigned, the personalized style of prominent cigarette product, the research and development and application of perfuming cigarette charging are just
As one of the most key technology for keeping cigarette flavor and taste in lowering harm and decreasing coking work.Promote cigarette sucks satisfaction and pleased
Happy degree, becomes technical problem urgently to be resolved in current cigarette flavouring humectation technology.
Natural tongue fur note fragrance mainly includes the medicinal extract and absolute oil product of tree moss or oak moss in the market, and there are soil, gas
The difference factor such as time, growing environment brings the difference of raw material variety, and stable product quality cannot ensure；Simultaneously as it is made
Standby process is more or less mingled in obtained product mainly by separation and concentrations means such as organic solvent extraction, steam distillations
Influence the invalid components such as pigment and the vegetable wax of aroma quality；In addition also often lead to human body containing some in medicinal extract and absolute oil
The ingredient and heavy metal of allergy, the Product quality and safety for food and daily use chemicals industry have buried security risk.
Currently, being also prepared by the method that various ingredients compound in the prior art, some to highlight tongue fur note style special
The essence of sign.
CN103333743A discloses the tongue fur faint scent essence of a kind of 17 kinds of standard items and 2 kinds of solvents composition, has tongue fur faint scent
Gas style, however wherein invalid ingredient is contributed containing some pairs of fragrance.
CN107354007A, CN107616547A and CN107510092A disclose 2,4- dihydroxy -3,6- dimethyl benzene
The tree moss note essence of methyl formate, 2,4-, 2 kinds of standard items of dihydroxy -6- benzyl Ethyl formate and solvent composition, wherein relating to
And 2 kinds of standard items all have apparent tree moss note.
Synthetic perfume technical manual (see " synthetic perfume technical manual ", Liu Shuwen etc., China Light Industry Press, 2009
January in year, page 136) list " 25 parts of orcin monomethyl ether and 75 parts of 2,4- dihydroxy -3,6- dimethylbenzoate methyl ester
Fit over and be used together, the compound fragrance of preparation has natural oak moss fragrance true to nature ", however 2 kinds of marks with oak moss note
The compound fragrance that quasi- product are prepared only has the style of similar oak moss fragrance, and fragrance is coarse, there is dense chemical breath.
Although the essence for highlighting tongue fur note style and features has also been prepared in above-mentioned technical proposal, its preparation process is multiple
It is miscellaneous, it be by multiple standards product and solvent complex, wherein containing obviously invalid ingredient is contributed to fragrance and what is obtained highlight tongue fur
The essence fragrance of note style and features is coarse, there is dense chemical breath.
Summary of the invention
To solve the above-mentioned problems, the present invention is proposed.
First aspect present invention provides a kind of essence for highlighting tongue fur note style and features, is based on weight percent comprising:
2,4- dihydroxy -3,5,6- trimethylbenzoic acid the ethyl ester of 0.2%-10%；
The 3,4- xylenol of 0.05%-6%.
Preferably, the essence further includes solvent, and the solvent is selected from ethyl alcohol, glyceryl triacetate or propylene glycol and the third three
The mixture of alcohol.
Preferably, the volumetric concentration of the ethyl alcohol is 50%-65%；The propylene glycol and the volume ratio of the glycerine are
3:1-1:1。
Preferably, the essence further includes the beta-cyclodextrin of 10%-20% or the pregelatinized starch of 10%-20%.
Preferably, the essence for highlighting tongue fur note style and features the preparation method comprises the following steps: by the essence composition content,
2, the 4- dihydroxy -3,5,6- trimethylbenzoic acid ethyl ester and 3, the 4- xylenol are taken, the solvent is added, in room
Under the conditions of temperature vibrate 10-20min dissolve raw material sufficiently, be configured to barrelling after uniform solution, be placed in be protected from light, shady place, save
12-48h obtains the essence for highlighting tongue fur note style and features.If solid spice to be made, β-ring can also be added
The substances such as dextrin or pregelatinized starch adsorb aforesaid liquid fragrance and become solid form.
Second aspect of the present invention provides a kind of cigarette comprising the essence for highlighting tongue fur note style and features.
Preferably, it is added in cigarette filter by the dosage of 1-3 μ L/ branch filter tip, using cloud and mist (purple) leaf group rolling cigarette sample
Product, remaining auxiliary material and essence remain unchanged, and cigarette sample is prepared.
Preferably, it is sprayed into cigarette bobbin paper surface by the dosage of 1.0-3.0mL/ hectogram obbbin, using Hongta (1956)
Leaf group rolling cigarette sample, remaining auxiliary material and essence remain unchanged, and cigarette sample is prepared.
Preferably, it is sprayed into cigarette shreds surface by the dosage of 0.05-3.00mL/ hectogram pipe tobacco, it is (classical using Hongta
100) leaf group rolling cigarette sample, remaining auxiliary material and essence remain unchanged, and cigarette sample is prepared.
Preferably, cigarette heating is sprayed by the dosage that 0.03-2.00mL/ hectogram heats the cigarette shreds that do not burn or not
Cigarette shreds surface heats the cigarette X pipe tobacco that do not burn in production using cigarette in Yunnan and rolls cigarette sample, remaining auxiliary material and essence are equal
It remains unchanged, cigarette sample is prepared.
Compared with prior art, the invention has the following advantages:
1, the present invention by with fertile soil taste 2,4- dihydroxy -3,5,6- trimethylbenzoic acid ethyl ester, with pungent fragrant
3,4- xylenols and solvent combination, are prepared the essence for highlighting tongue fur note style and features, and the essence has apparent
Tongue fur note, fragrance are abundant.
2, the essence for highlighting tongue fur note style and features of the invention, is added in cigarette, can increase cigarette flavor
Amount assigns the apparent tongue fur note of cigarette, has rich increase cigarette flavor, reduction stimulation, increases tongue fur note, promotes cigarette pumping
Inhale the effect of comfort and satisfaction.
3, the essence for highlighting tongue fur note style and features of the invention, most simple formula is only by 2 kinds of standard items and a kind of solvent group
At constituent is simple, does not contribute fragrance invalid ingredient, and low in cost, preparation method is simple, is suitble to scale
Production, has a good application prospect.
Specific embodiment
Below with reference to embodiment, the present invention is described in further detail, but is not limitation of the present invention, based on this
Any transformation or improvement that invention training centre is done, each fall within protection scope of the present invention.Be not specified in embodiment particular technique or
Condition person described technology or conditions or carries out according to the literature in the art according to product description.Agents useful for same or
Production firm person is not specified in instrument, is the conventional products that can be obtained by purchase.
Comparative example 1
0.2% 2,4- dihydroxy -3,5,6- trimethylbenzoic acid ethyl ester and 99.8% three second are taken by mass percentage
Acid glyceride mixing, vibrating 10min at room temperature dissolves raw material sufficiently, is configured to barrelling after uniform solution, is placed in and keeps away
Light, shady place are stored 12 hours, obtain essence A.
It is added in cigarette filter, the essence A using cloud and mist (purple) leaf group rolling cigarette by the dosage of 1 μ L/ branch filter tip
Sample, remaining auxiliary material and essence remain unchanged, and cigarette sample 1 is prepared, and compare hair of smokeing panel test with cloud and mist (purple) product
Existing: fertile soil taste increases by 4%, and irritation reduces by 1%, and tongue fur note increases by 0%.
Comparative example 2
0.05% 3,4- xylenol and the mixing of 99.95% glyceryl triacetate are taken by mass percentage, in room
10min is vibrated under the conditions of temperature dissolves raw material sufficiently, is configured to barrelling after uniform solution, be placed in be protected from light, shady place, storage is 12 small
When, obtain essence B.
It is added in cigarette filter, the essence B using cloud and mist (purple) leaf group rolling cigarette by the dosage of 1 μ L/ branch filter tip
Sample, remaining auxiliary material and essence remain unchanged, and cigarette sample 2 is prepared, and compare hair of smokeing panel test with cloud and mist (purple) product
Existing: Xin Xiang increases by 6%, and irritation reduces by 0.5%, and tongue fur note increases by 0%.
Embodiment 1
0.2% 2,4- dihydroxy -3,5,6- trimethylbenzoic acid ethyl ester, 0.05% 3,4- are taken by mass percentage
Xylenol, 99.75% glyceryl triacetate mixing, at room temperature vibrate 10min dissolve raw material sufficiently, prepare
At barrelling after uniform solution, be placed in be protected from light, shady place, store 12 hours, obtain essence C.
It is added in cigarette filter, the essence C using cloud and mist (purple) leaf group rolling cigarette by the dosage of 1 μ L/ branch filter tip
Sample, remaining auxiliary material and essence remain unchanged, and cigarette sample 3 is prepared, and compare hair of smokeing panel test with cloud and mist (purple) product
Existing: fragrance is rich to increase by 2%, and irritation reduces by 3%, and tongue fur note increases by 3%.
Embodiment 2
3% 2,4- dihydroxy -3,5,6- trimethylbenzoic acid ethyl ester, 2% 3,4- dimethyl are taken by mass percentage
Phenol, 95% 60% alcohol of volumetric concentration mixing, at room temperature vibrate 10min dissolve raw material sufficiently, be configured to
Barrelling after one solution, be placed in be protected from light, shady place, store 24 hours, obtain essence D.
By the essence D, it is sprayed into cigarette bobbin paper surface by the dosage of 1.0mL/ hectogram obbbin, using Hongta
(1956) leaf group rolling cigarette sample, remaining auxiliary material and essence remain unchanged, and cigarette sample 4 is prepared, with Hongta
(1956) product compares discovery of smokeing panel test: fragrance is rich to increase by 5%, and irritation reduces by 4%, and tongue fur note increases by 5%, flue gas
Comfort promotes 3%.
Embodiment 3
8% 2,4- dihydroxy -3,5,6- trimethylbenzoic acid ethyl ester, 4% 3,4- dimethyl are taken by mass percentage
Phenol, 88% volume ratio be 3:1 glycol/propane triol mix, at room temperature vibrate 20min keep raw material sufficiently molten
Solution, be configured to barrelling after uniform solution, be placed in be protected from light, shady place, store 24 hours, obtain essence E.
By the essence E, it is sprayed into cigarette shreds surface by the dosage of 3.00mL/ hectogram pipe tobacco, it is (classical using Hongta
100) leaf group rolling cigarette sample, remaining auxiliary material and essence remain unchanged, and cigarette sample 5 is prepared, (classical with Hongta
100) product compares discovery of smokeing panel test: fragrance is rich to increase by 7%, and irritation reduces by 5%, and tongue fur note increases by 7%.
Embodiment 4
10% 2,4- dihydroxy -3,5,6- trimethylbenzoic acid ethyl ester, 6% 3,4- dimethyl are taken by mass percentage
Phenol, 64% volume ratio 3:1 glycol/propane triol, 20% pregelatinized starch mixing, stir at room temperature
25min dissolves raw material sufficiently, is configured to barrelling after uniform solution, be placed in be protected from light, shady place, store 24 hours, obtain essence
F。
By the essence F, cigarette heating is sprayed by the dosage that 2.00mL/ hectogram heats the cigarette shreds that do not burn and is not burnt
Cigarette shreds surface, which is simultaneously rolled cigarette sample by certain, remaining auxiliary material and essence remain unchanged, and cigarette sample is prepared
Product 6, compare discovery of smokeing panel test with the sample before applying the fragrance: fragrance is rich to increase by 10%, and irritation reduces by 5%,
Tongue fur note increases by 7%.
Claims (5)
1. a kind of essence for highlighting tongue fur note style and features, which is characterized in that be based on mass percent comprising:
2,4- dihydroxy -3,5,6- trimethylbenzoic acid the ethyl ester of 0.2%-10%；
The 3,4- xylenol of 0.05%-6%.
2. the essence according to claim 1 for highlighting tongue fur note style and features, which is characterized in that it further includes solvent, institute
State the mixture that solvent is selected from ethyl alcohol, glyceryl triacetate or propylene glycol and glycerine.
3. the essence according to claim 2 for highlighting tongue fur note style and features, which is characterized in that the volume of the ethyl alcohol is dense
Degree is 50%-65%；The propylene glycol and the volume ratio of the glycerine are 3:1-1:1.
4. the essence according to claim 1 for highlighting tongue fur note style and features, which is characterized in that it further includes 10%-
20% beta-cyclodextrin or the pregelatinized starch of 10%-20%.
5. a kind of cigarette comprising highlighting the essence of tongue fur note style and features described in claim 2 or 4.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811281594.2A CN109156879B (en) | 2018-10-23 | 2018-10-23 | Essence capable of highlighting moss aroma style characteristics and cigarette containing essence |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201811281594.2A CN109156879B (en) | 2018-10-23 | 2018-10-23 | Essence capable of highlighting moss aroma style characteristics and cigarette containing essence |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN109156879A true CN109156879A (en) | 2019-01-08 |
| CN109156879B CN109156879B (en) | 2021-01-29 |
Family
ID=64876249
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201811281594.2A Active CN109156879B (en) | 2018-10-23 | 2018-10-23 | Essence capable of highlighting moss aroma style characteristics and cigarette containing essence |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN109156879B (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103333743A (en) * | 2013-07-10 | 2013-10-02 | 江苏中烟工业有限责任公司 | Essence with moss faint scent and applications thereof |
| CN107354007A (en) * | 2017-09-12 | 2017-11-17 | 云南中烟工业有限责任公司 | A kind of cigarette bobbin paper additive of tree moss note and its preparation method and application |
| CN107432496A (en) * | 2016-05-25 | 2017-12-05 | 浙江中烟工业有限责任公司 | One kind is applied to heating non-combustion-type tobacco product and its perfuming method |
| CN107510092A (en) * | 2017-09-12 | 2017-12-26 | 云南中烟工业有限责任公司 | A kind of cigarette shreds additive of tree moss note and its preparation method and application |
| CN108669622A (en) * | 2018-06-15 | 2018-10-19 | 云南中烟工业有限责任公司 | A kind of volume cigarette additive and its preparation method and application of cool fragrant and sweet rhythm |
-
2018
- 2018-10-23 CN CN201811281594.2A patent/CN109156879B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103333743A (en) * | 2013-07-10 | 2013-10-02 | 江苏中烟工业有限责任公司 | Essence with moss faint scent and applications thereof |
| CN107432496A (en) * | 2016-05-25 | 2017-12-05 | 浙江中烟工业有限责任公司 | One kind is applied to heating non-combustion-type tobacco product and its perfuming method |
| CN107354007A (en) * | 2017-09-12 | 2017-11-17 | 云南中烟工业有限责任公司 | A kind of cigarette bobbin paper additive of tree moss note and its preparation method and application |
| CN107510092A (en) * | 2017-09-12 | 2017-12-26 | 云南中烟工业有限责任公司 | A kind of cigarette shreds additive of tree moss note and its preparation method and application |
| CN108669622A (en) * | 2018-06-15 | 2018-10-19 | 云南中烟工业有限责任公司 | A kind of volume cigarette additive and its preparation method and application of cool fragrant and sweet rhythm |
Non-Patent Citations (1)
| Title |
|---|
| 朱怀远等: "子蒸馏和同时蒸馏萃取法分析树苔浸膏的化学成分", 《食品科学》 * |
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| Publication number | Publication date |
|---|---|
| CN109156879B (en) | 2021-01-29 |
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