CN109953367A - A kind of Herba Cistanches extracting solution and preparation method thereof, composition and application - Google Patents
A kind of Herba Cistanches extracting solution and preparation method thereof, composition and application Download PDFInfo
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- CN109953367A CN109953367A CN201910224107.7A CN201910224107A CN109953367A CN 109953367 A CN109953367 A CN 109953367A CN 201910224107 A CN201910224107 A CN 201910224107A CN 109953367 A CN109953367 A CN 109953367A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/20—Biochemical treatment
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
- A24D3/00—Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
- A24D3/02—Manufacture of tobacco smoke filters
- A24D3/0204—Preliminary operations before the filter rod forming process, e.g. crimping, blooming
- A24D3/0212—Applying additives to filter materials
- A24D3/0216—Applying additives to filter materials the additive being in the form of capsules, beads or the like
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Fats And Perfumes (AREA)
- Cigarettes, Filters, And Manufacturing Of Filters (AREA)
Abstract
The present invention provides a kind of Herba Cistanches extracting solution and preparation method thereof, composition and applications, and wherein the preparation method of Herba Cistanches extracting solution includes: extraction Herba Cistanches dry matter to obtain Herba Cistanches extract liquor, are concentrated after enzyme preparation is added into Herba Cistanches extract liquor；The present invention also provides the applications of a kind of composition rich in Herba Cistanches extracting solution and its promotion cigarette sensory quality.Cigarette provided by the invention containing the quick-fried pearl of Herba Cistanches extracting solution, there is higher sensory quality assessment in suction, flue gas exquisiteness sense improves, entrance is submissive, it is fragrant and sweet with unique sauce, pleasant impression is still net, while the physical and chemical index content of cigarette smoke decreases, and has the function of mitigating smoking property of cigarette harm.
Description
Technical field
This application involves technical field of cigarette production more particularly to a kind of Herba Cistanches extracting solution and preparation method thereof, contain
The composition of Herba Cistanches extracting solution and the application in raising cigarette quality.
Background technique
More concern with people to smoking and healthy relationship, improves the interior quality and safety of cigarette, while auxiliary
It helps and increases centainly with the harmful components in healthcare function ingredient, reduction cigarette smoke, will be a main trend of cigarette development.And
By smoking and healthy deepening continuously for research and constantly bringing forth new ideas for cigarette industry technology, world wide inner wrap strip is burnt
Oil mass is presented the trend gradually decreased and keeps the aroma quality of cigarette smoke how during tar content in cigarette persistently reduces
Amount is one of the focal issue of Cigarette Industrial Enterprise common concern.
In traditional cigarette production process, spice liquid is often added in the tobacco, and spice liquid added by this mode is normal
Often it is lost during cigarette burning, simultaneously because the reaction of complex material system is difficult to be expected under high temperature, part fragrance
Liquid can also generate some bad organoleptic effects.
Quick-fried pearl is as emerging material a kind of in cigarette, due to the special delivery mode of its content, supplement, improvement,
The function of coordinating smoking property of cigarette quality and promotion, change, cigarette product style etc. is more and more prominent.Although currently on the market
There are a certain number of quick-fried pearl cigarette, but the fragrance in this quick-fried pearl is due to being lack of pertinence design, thus with flue gas harmony
It is relatively poor, and be affected to the odor characteristic of cigarette itself, thus affect the sucking quality of quick-fried pearl cigarette.
Herba Cistanches are the fleshy stems of the dry zone scale leaf for orobanchaceae plant cistanche or Cistanche tubulosa, and main product is in China
There is the title of " desert ginseng " on the ground such as the Inner Mongol, Gansu.Herba Cistanches nature and flavor are sweet, salty, warm, return kidney, with kidney-replenishing, benefiting essence-blood,
The effect of relax bowel and defecation, for treating the insufficiency of the kidney yang, blood and essence asthenia, the functions such as dry constipation of intestines.Compendium of Material Medica is recorded: Shi Zhen
This object of Yue ︰ is mended without high, therefore has calm number.Calmly, gentle looks.The chemical component of Herba Cistanches identified at present is main
There are benzyl carbinol glycoside, polysaccharide, iridoids etc.；Pharmacological research show Herba Cistanches have neuroprotection, immunological regulation,
It is antifatigue, adjust hormonal balance, it is anti-oxidant the effects of.
At present both at home and abroad to Herba Cistanches research be mostly its effective component desert cistanche polysaccharide chemical constituents determination and curing
Medicine, field of food it is medical etc., extracting method be mostly after using distilled water immersion ethyl alcohol extract, not yet occur related using compound
The method of processing with enzyme preparation Herba Cistanches extract liquor, or cigarette is placed in by quick-fried pearl is made after the appropriate blending of Herba Cistanches extracting solution progress
In filter stick, or the relevant report being applied in production of cigarettes.
Summary of the invention
The present invention is intended to provide a kind of applied to irritation can be significantly reduced in tobacco, promote cigarette fragrance and sense organ
Quality, while can reduce the Herba Cistanches extracting solution of tar, nicotine and carbon monoxide content in the main flume of cigarette.
On the one hand, the present invention provides a kind of preparation methods of Herba Cistanches extracting solution, and the method includes extracting Herba Cistanches
After dry matter obtains Herba Cistanches extract liquor, into Herba Cistanches extract liquor the step of addition enzyme preparation.
Wherein, in terms of dry matter, the amount that enzyme preparation is added in every gram of Herba Cistanches dry matter is 3,000-3 ten thousand U.The enzyme preparation choosing
From one of cellulase, beta-glucosidase, lignoenzyme and pectase or a variety of.
It is preferred that enzyme preparation and Herba Cistanches extract liquor dosage volume ratio are 1-2:100, preferably 1.1-1.8:100, more preferably
1.3-1.7:100。
In one embodiment, Herba Cistanches dry matter can be the fresh herba cistanches after drying, be also possible to Herba Cistanches
The Herba Cistanches block or Herba Cistanches powder being ground into after drying.
Further, the enzyme preparation is including at least cellulase, beta-glucosidase, lignoenzyme and pectase
Complex enzyme, cellulase, beta-glucosidase, lignoenzyme and pectase enzyme activity ratio be (2~5): (1~7): (3~
6): (1~9), preferably 4:1:3:5.
Preferably, the concentration of enzyme preparation is ten thousand U/ml of 10-20；It is preferred that adding cellulase in every gram of Herba Cistanches dry matter
2000-5000U, beta-glucosidase 1000-7000U, lignoenzyme 3000-6000U, pectase 1000-9000U；It is further preferred that
Add thousand U of cellulase 2-5, beta-glucosidase 1-7 thousand U of thousand U, lignoenzyme 3-6, pectin in every 100ml Herba Cistanches extract liquor
Thousand U of enzyme 1-9；Wherein, the condition of enzymolysis step is 20-25 DEG C of temperature, enzymolysis time 120-150min.
Preferably, the enzyme preparation is extracted from animal, plant and/or microorganism, it is furthermore preferred that deriving from microorganism
It extracts, such as bacterium, fungi, protist.The use of complex enzyme can sufficiently decompose cellulose, wood in Herba Cistanches extract liquor
Quality, glucose and pectin obtain the Herba Cistanches extracting solution containing small molecule effective component.
Further, the above method specifically includes the following steps:
Under 80-100 DEG C or ultrasonic wave or microwave condition, water-bath heat reflux is carried out to Herba Cistanches dry matter with 60% ethyl alcohol
Or oscillation extraction 1-12 hours, Herba Cistanches extract liquor is obtained, it is cooling, 1-2ml enzyme system is added in every 100ml Herba Cistanches extract liquor
Agent, it is (2~5): (1~7): (3~6): cellulase, the beta-glucosidase of (1~9) that the enzyme preparation, which is containing enzyme activity ratio,
The complex enzyme of enzyme, lignoenzyme and pectase, being further concentrated to concentration of the volume of the concentrated liquid containing dry matter is 8%-25%, that is, is obtained
The Herba Cistanches extracting solution.
In a preferred embodiment, water-bath heat reflux or oscillation extraction 1-10 hours, preferably 2-8 hours, more preferable 4-7
Hour；The solid-liquid ratio of Herba Cistanches powder and ethyl alcohol is 1g:7-10ml, preferably 1g:7ml, 1g:8ml, 1g:9ml, 1g:10ml；It is described
Enzyme preparation preferably comprises the compound of the cellulase that enzyme activity ratio is 4:1:3:5, beta-glucosidase, lignoenzyme and pectase
Enzyme；Before enzyme preparation is added, Herba Cistanches extract liquor is cooled to 15-25 DEG C, preferably 15 DEG C, 20 DEG C, 22 DEG C, 25 DEG C；It is preferred that concentration
It is inactivated 5 minutes at 100 DEG C afterwards, so set, inactivation treatment can be carried out to the biological enzyme of addition.
Further, the above method further includes carrying out pretreated step to Herba Cistanches, is specifically included:
By Herba Cistanches washing, removal impurity, sunning, is dried at 30-60 DEG C, directly crush or be crushed in liquid nitrogen
40-100 mesh.
In one embodiment, the step of can using above-mentioned pre-processing, is by fresh herba cistanches or Herba Cistanches dry-cure
After the Herba Cistanches powder of 40-100 mesh, then extracted；In another embodiment, Herba Cistanches block, particle can directly be bought
Or powder, then crushed, until partial size is 40-100 mesh.
On the other hand, it the present invention also provides a kind of Herba Cistanches extracting solution, is prepared using the above method.
On the other hand, the present invention also provides a kind of composition, the Herba Cistanches including using the above method to prepare are mentioned
Take liquid, wherein the quality accounting of the Herba Cistanches extracting solution in composition is 16%-98%, preferably 50-80%, more preferable 55%-
75%.
Further, above-mentioned composition further includes any one or a few in following component: Glycerin, mixed triester with caprylic acid capric acid, three second
Acid glyceride, maltol, menthyl acetate, vanillic aldehyde, Ethyl vanillin, ethyl caprilate, orange limonene, γ-terpinene, β-pinane
Alkene, australene, D- pyroglutamic acid ethyl ester, 5- hydroxyl maltol, nerol, geraniol.
In one embodiment, by mass percentage, the preferred following components of above-mentioned composition and proportion: 16%-
98% Herba Cistanches extracting solution, 15%-30% Glycerin, mixed triester with caprylic acid capric acid, 1%-2% glyceryl triacetate, 0.3%-2.5% malt
Phenol, 0.1%-2.3% menthyl acetate, 0.2%-1.8% vanillic aldehyde, 1%-3% Ethyl vanillin, 0.7%-1.4% octanoic acid
Ethyl ester, 0.1%-1.2%D- limonene, 0.1%-1.1% γ-terpinene, 0.2%-1.5% nopinene, 0.2%-1.8% australene
Alkene, 0.1%-2.0%D- pyroglutamic acid ethyl ester, 0.1%-2.1%5- hydroxyl maltol, 0.3%-3.0% nerol, 0.3%-
1.4% geraniol.
On the other hand, the present invention also provides a kind of quick-fried pearl, the quick-fried pearl contains above-mentioned composition；It is preferred that the quick-fried pearl
Contain 10-30 microlitres of composition；It is further preferred that the diameter of the quick-fried pearl is 2-4mm, weight is 10-25mg/, and circularity is less than
0.15mm, cracking pressure value are 1-1.5kgf.
In a preferred embodiment, the content of composition is 10-25ul/ in above-mentioned quick-fried pearl；The diameter of the quick-fried pearl
For 2.5-3.5mm, more preferable 2.5mm, 2.6mm, 3.0mm, 3.45mm, 3.5mm, weight is preferably 10.5-24.2mg/, is broken
Broken pressure value is preferably 1.3kgf.In actual production operation, shape, size, specification, cracking pressure value of quick-fried pearl etc. are specific
Parameter can be adjusted according to the specification for the cigarette filter rod that add the quick-fried pearl, and can also use the corresponding rule of production
The preparation such as tooling, equipment or machine of lattice.
On the other hand, the present invention also provides a kind of above-mentioned Herba Cistanches extracting solutions, and/or are prepared using the above method
Herba Cistanches extracting solution and/or above-mentioned composition and/or above-mentioned quick-fried pearl promoting the application in cigarette sensory quality.
Wherein, the organoleptic quality of cigarette of the present invention refers to " the 4th part of GB 5606.4-2005 cigarette: sense organ technology
It is required that " in Sensory Quality of Cigarette judgment criteria, comprising: gloss, fragrance, harmony, miscellaneous gas, irritation and pleasant impression.
In one embodiment, it is mentioned using the Herba Cistanches that above-mentioned Herba Cistanches extracting solution and/or the above method prepare
Liquid and/or above-mentioned composition are taken, can directly add in pipe tobacco, filter stick, cigarette paper, forming paper and/or is connect in mouth glue；Another
In kind embodiment, the Herba Cistanches extracting solution and/or above-mentioned composition also be can be injected in quick-fried pearl, be then added to the filter of cigarette
In stick.
In one embodiment, the quick-fried pearl can add rolls up in regular-size cigarette, binary composite cigarette and/or tri compound
In cigarette；Position of the quick-fried pearl in cigarette filter rod is unlimited, preferably apart from lip end 12-16mm, more preferable 15mm；Every cigarette
One or more quick-fried pearls can be added.
On the other hand, the present invention also provides a kind of cigarette, the meat desert that is prepared in the cigarette containing the above method
Rong's extracting solution, and/or contain above-mentioned composition, and/or contain an at least above-mentioned quick-fried pearl.Preferably, the specification of the cigarette
It is unlimited, it can be ramuscule, middle branch or conventional branch, be also possible to regular-size cigarette, binary composite cigarette and/or tri compound cigarette,
The circumference of the cigarette preferred 15-30mm, more preferable 16mm, 17mm, 20mm, 22mm, 24mm, 24.1mm, 27mm.
It can be brought the following benefits by the application:
1, the preparation method of Herba Cistanches extracting solution provided by the invention, by using the complex enzyme formulation suitably matched to the winter
Worm summer grass extract liquor is digested, and the Herba Cistanches extracting solution suitable for cigarette can be obtained, which is applied to
Fragrance can be promoted in cigarette, irritation is reduced, is obviously improved the organoleptic quality of cigarette, and also there is health-care efficacy, it is particularly suitable
In high-quality cigarette.
2, the composition provided by the invention rich in Herba Cistanches extracting solution can be made into quick-fried pearl applied to cigarette, so that cigarette
Have sauce fragrant and sweet in suction, note is dense；Smoking result shows: using the volume for being rich in Herba Cistanches extracting solution provided by the invention
After cigarette quick-fried pearl suction, the rich of fragrance in flue gas can be significantly improved, enhance the satiety of flue gas by and pleasant feeling, Jin Erti
The harmony for rising fragrance and product sensory quality, increases the interest of cigarette smoking, while can also reduce the mainstream of cigarette
Total granules, tar, smoking nicotine, carbon monoxide equal size in the physical and chemical index of flue gas reduce the harm to human health.
3, the cigarette provided by the invention containing the quick-fried pearl of composition provided by the invention has more preferable sense organ matter in suction
Amount evaluation, is mainly reflected in rich, the fine and smooth sense of flue gas, solid sense has and is obviously improved, and cigarette perfume is stronger, saturating hair,
Degrees of fusion is more preferable, toast perfume, Jiao Tian, spicy fragrance, enrich cigarette flavor, significantly improve flue gas aroma quality, plumpness,
The interest of suction reduces the cognitive stimulatory of flue gas, and exquisiteness sense improves, and entrance is submissive, returns sweet tea sense and is remarkably reinforced, pleasant impression is still
Only, while the physical and chemical index content of cigarette smoke decreases, and has the function of mitigating smoking property of cigarette harm to a certain degree.
Specific embodiment
For the clearer general idea for illustrating the application, it is described in detail by way of examples below.Under
In the description of text, gives a large amount of concrete details and more thoroughly understand in order to provide to the application.However, for this field
It is readily apparent that the application may not need one or more of these details and be carried out for technical staff.In others
In example, in order to avoid obscuring with the application, some technical characteristics well known in the art are not described.
Such as non-specified otherwise, in the following embodiments, Herba Cistanches are purchased from three Shen Niu commerce and trade Co., Ltd of Qinghai, and following groups
Remaining each component in object in addition to Herba Cistanches extracting solution is closed to buy by commercial sources；Cellulase, pectin in enzyme preparation
Enzyme, lignoenzyme and beta-glucosidase are purchased from letter (China) Bioisystech Co., Ltd, Novi；Using the precious biology of Shanghai China
The cigarette capsule pill dripping machine for the model MSM-06 that Science and Technology Ltd. provides, is made quick-fried pearl；Using the positive light industry strain formula of South Korea
The model JK-S1 flavored capsules that company, commercial firm provides put into device, and quick-fried pearl is placed in cigarette filter rod；Using Changde tobacco machine
The rolling up and connecting machine for the model ZJ17 that tool Co., Ltd provides, prepares cigarette；Flue gas inspection test, using full-automatic smoking machine
It is tested.
In a preferred embodiment, the preparation method of the Herba Cistanches extracting solution, specifically comprises the following steps:
S1, herba cistanches washing, removal impurity, sunning pre-processing after, dried at 30-60 DEG C, directly crushing or
It is crushed to 40-100 mesh in liquid nitrogen, obtains Herba Cistanches powder；
S2 carries out water-bath heat reflux to Herba Cistanches powder with 60% ethyl alcohol under 80-100 DEG C or ultrasonic wave or microwave condition
Or oscillation extraction 1-12 hours, wherein the solid-liquid ratio of Herba Cistanches powder and ethanol solution are as follows: Herba Cistanches powder: ethyl alcohol=1g:7-
10ml；
S3 after liquid to be extracted is cooled to 15-25 DEG C, is added contains cellulase, beta-glucosidase, lignin thereto
The complex enzyme formulation of enzyme, pectase, 20-25 DEG C of hydrolysis temperature, enzymolysis time 120-150min；
S4, it is 8-25% that the extract liquor that a variety of enzyme preparations are added, which is concentrated into concentration of the volume of the concentrated liquid containing dry matter, dense
It is inactivated 5 minutes at 100 DEG C after contracting, the Herba Cistanches extracting solution can be obtained.
In the following embodiments, the quick-fried pearl of the cigarette preferably uses drop method in shunting-liquid to be prepared, including the use of cold
But after the shearing force cutting rubber column gel column that oil liquidates the step of dripping, it specifically may is that the cooling oil different using two incident angles
Shearing force is formed in solenoid, by the wall material and the cutting of core liquid during lower drop, and by surface tension in cooling oil
Effect condensation balling-up, then quick-fried pearl finished product is made after the programs such as deoiled, dried, sieved.
Embodiment 1
A kind of Herba Cistanches extracting solution, is prepared via a method which:
After herba cistanches washing, removal impurity, sunning, is dried at 60 DEG C, 100 mesh are crushed in liquid nitrogen, obtain meat desert
Rong's powder；At 100 DEG C, with Herba Cistanches powder: ethyl alcohol=1g:10ml solid-liquid ratio carries out oscillation extraction 10 hours, is cooled to 25 DEG C
Afterwards, the complex enzyme 1.7ml that concentration is 100,000 U/ml is added in every 100ml Herba Cistanches extract liquor, i.e. every gram of Herba Cistanches dry matter adds
1.7 ten thousand U of enzyme preparation, wherein complex enzyme is by cellulase, beta-glucosidase, lignoenzyme and pectase in enzyme activity ratio 2:
6:5:4 is formed, i.e., adds cellulase 2000U, beta-glucosidase 6000U, lignoenzyme in every 100ml Herba Cistanches extract liquor
5000U, pectase 4000U；After enzymatic hydrolysis, it is 20% that concentration of the volume of the concentrated liquid containing dry matter is concentrated under reduced pressure at 70kPa, dense
It is inactivated 5 minutes at 100 DEG C after contracting, obtains Herba Cistanches extracting solution.
A kind of composition comprising above-mentioned Herba Cistanches extracting solution, it is based on mass fraction, composed of the following components: 55% meat
Desert cistanche extracting solution, 25% Glycerin, mixed triester with caprylic acid capric acid, 2% glyceryl triacetate, 2.1% maltol, 1.5% menthyl acetate, 1.8%
Vanillic aldehyde, 1% Ethyl vanillin, 1.2% ethyl caprilate, 0.9%D- limonene, 0.8% γ-terpinene, 1.4% nopinene,
1.5% australene, 1.5%D- pyroglutamic acid ethyl ester, 1.1%5- hydroxyl maltol, 2.2% nerol, 1% geraniol.
A kind of quick-fried pearl comprising above-mentioned composition is obtained using drop method preparation in above-mentioned shunting-liquid.Wherein, above-mentioned group
Closing content of the object in quick-fried pearl is 24.2 μ l/, and the diameter of quick-fried pearl is 3.4mm, and weight is 24.2mg/, and circularity is less than
0.15mm, cracking pressure value are 1.3kgf.
A kind of cigarette comprising above-mentioned quick-fried pearl, prepares according to existing cigarette producing process.Wherein, the cigarette is general
Flow-through cigarette, circumference 24.1mm place a quick-fried pearl in cigarette filter rod, which is placed in the middle section position of the cigarette filter rod, have
Body is apart from lip end 15.0mm.
The flue gas inspection result and suction evaluation score value of the embodiment cigarette are shown in Table 2 and table 3.
Wherein, by the feedback of suction evaluation result it is found that the cigarette that obtains of the embodiment be added to it is above-mentioned rich in meat
After the quick-fried pearl of desert cistanche extracting solution, the rich tool of cigarette sample flue gas has a certain upgrade, and baking is fragrant and the fragrant and sweet note of sauce is prominent
Out, non-stimulated, without miscellaneous gas, flue gas exquisiteness sense is improved, and is returned sweet tea sense and is remarkably reinforced, pleasant impression is comfortable.
Embodiment 2
A kind of Herba Cistanches extracting solution, is prepared via a method which:
After herba cistanches washing, removal impurity, sunning, is dried at 50 DEG C, be directly crushed to 80 mesh, obtain Herba Cistanches powder；
Under ultrasonic conditions, with Herba Cistanches powder: ethyl alcohol=1g:8ml solid-liquid ratio carries out the hot reflux extraction of water-bath 8 hours, is cooled to
The complex enzyme 1.5ml that concentration is 100,000 U/ml, i.e. every gram of Herba Cistanches dry are added after 20 DEG C, in every 100ml Herba Cistanches extract liquor
Enzyme 1.2 ten thousand U of preparation in matter, wherein complex enzyme presses enzyme activity by cellulase, beta-glucosidase, lignoenzyme and pectase
Ratio 3:2:4:6 is formed, i.e., adds 3,000 U of cellulase, 2,000 U of beta-glucosidase, lignin in every 100ml Herba Cistanches extract liquor
400,000 U of enzyme, 600,000 U of pectase；After enzymatic hydrolysis, it is 25% that concentration of the volume of the concentrated liquid containing dry matter is concentrated under reduced pressure at 50kPa,
It is inactivated 5 minutes at 100 DEG C after concentration, obtains Herba Cistanches extracting solution.
A kind of composition comprising above-mentioned Herba Cistanches extracting solution, it is based on mass fraction, composed of the following components: 65% meat
Desert cistanche extracting solution, 20% Glycerin, mixed triester with caprylic acid capric acid, 1.4% glyceryl triacetate, 1.6% maltol, 0.8% menthyl acetate,
1.2% vanillic aldehyde, 1.5% Ethyl vanillin, 1% ethyl caprilate, 0.9%D- limonene, 0.8% γ-terpinene, 1.0% β-pinane
Alkene, 0.9% australene, 1.0%D- pyroglutamic acid ethyl ester, 0.9%5- hydroxyl maltol, 1.2% nerol, 0.8% geraniol.
A kind of quick-fried pearl comprising above-mentioned composition is obtained using drop method preparation in above-mentioned shunting-liquid.Wherein, above-mentioned group
Closing content of the object in quick-fried pearl is 14.0 μ l/, and the diameter of quick-fried pearl is 3.0mm, and weight is 14.0mg/, and circularity is less than
0.15mm, cracking pressure value are 1.3kgf.
A kind of cigarette comprising above-mentioned quick-fried pearl, prepares according to existing cigarette producing process.Wherein, the cigarette is two
First composite cigarette, circumference 22.0mm place a quick-fried pearl in cigarette filter rod, which is placed in the middle section position of the cigarette filter rod,
Specially apart from lip end 15.0mm.
The flue gas inspection result and suction evaluation score value of the embodiment cigarette are shown in Table 2 and table 3.
Wherein, by the feedback of suction evaluation result it is found that the embodiment is being added to rich in above-mentioned Herba Cistanches extracting solution
Quick-fried pearl after, the rich tool of cigarette sample flue gas has a certain upgrade, this perfume of tobacco and the fragrant and sweet note of sauce are prominent, harmony
Preferably, the sense of flue gas exquisiteness improves, and cigarette perfume is sent out more thoroughly, returns sweet tea sense and is remarkably reinforced, pleasant impression is still net.
Embodiment 3
A kind of Herba Cistanches extracting solution, is prepared via a method which:
After herba cistanches washing, removal impurity, sunning, is dried at 40 DEG C, 90 mesh are crushed in liquid nitrogen, obtain Herba Cistanches
Powder；Under microwave condition, with Herba Cistanches powder: ethyl alcohol=1g:10ml solid-liquid ratio carries out the hot reflux extraction of water-bath 6 hours, cooling
The complex enzyme 1.3ml that concentration is 100,000 U/ml is added to after 15 DEG C, in every 100ml Herba Cistanches extract liquor, i.e. every gram of Herba Cistanches are dry
Enzyme 1.3 ten thousand U of preparation in substance, wherein complex enzyme presses enzyme by cellulase, beta-glucosidase, lignoenzyme and pectase
Ratio 4:1:3:5 composition living, i.e., in every 100ml Herba Cistanches extract liquor plus 4,000 U of cellulase, beta-glucosidase 1,000 U is wooden
Plain 3,000 U of enzyme, 5,000 U of pectase；After enzymatic hydrolysis, it is 15% that concentration of the volume of the concentrated liquid containing dry matter is concentrated under reduced pressure at 60kPa,
It is inactivated 5 minutes at 100 DEG C after concentration, obtains Herba Cistanches extracting solution.
A kind of composition comprising above-mentioned Herba Cistanches extracting solution, it is based on mass fraction, composed of the following components: 75% meat
Desert cistanche extracting solution, 16% Glycerin, mixed triester with caprylic acid capric acid, 1% glyceryl triacetate, 0.5% maltol, 0.4% menthyl acetate, 0.4%
Vanillic aldehyde, 1.2% Ethyl vanillin, 0.8% ethyl caprilate, 0.7%D- limonene, 0.3% γ-terpinene, 0.75% nopinene,
0.25% australene, 0.35%D- pyroglutamic acid ethyl ester, 0.75%5- hydroxyl maltol, 0.95% nerol, 0.65% spiceleaf
Alcohol.
A kind of quick-fried pearl comprising above-mentioned composition is obtained using drop method preparation in above-mentioned shunting-liquid.Wherein, above-mentioned group
Closing content of the object in quick-fried pearl is 10.5 μ l/, and the diameter of the quick-fried pearl is 2.60mm, and weight is 10.5mg/, and circularity is less than
0.15mm, cracking pressure value are 1.3kgf.
A kind of cigarette comprising above-mentioned quick-fried pearl, prepares according to existing cigarette producing process.Wherein, the cigarette is three
First composite cigarette, circumference 17.0mm place a quick-fried pearl in cigarette filter rod, which is placed in the middle section position of the cigarette filter rod,
Specially apart from lip end 15.0mm.
The flue gas inspection result and suction evaluation score value of the embodiment cigarette are shown in Table 2 and table 3.
Wherein, by the feedback of suction evaluation result it is found that the embodiment be added to it is quick-fried rich in Herba Cistanches extracting solution
After pearl, cigarette sample cigarette perfume is stronger, and herbal and the fragrant and sweet note of sauce are prominent, and cigarette perfume degrees of fusion is preferable, flue gas solid sense
Preferably, entrance is submissive, pleasant impression Hui Tian.
The detection of 4 physicochemical property of embodiment and sensory quality assessment
Comparative example 1: the quick-fried pearl of blank cigarette is obtained using drop method preparation in above-mentioned shunting-liquid and (is free of any content
Object), and the quick-fried pearl of the blank is placed in the filter stick middle section position with 1 specification of embodiment and the identical plain edition cigarette of ingredient,
Specially apart from lip end 15.0mm.
Comparative example 2: the preparation method is the same as that of Example 1 for Herba Cistanches extracting solution, and difference is directly to be concentrated after extracting, not enzyme
Preparation.Gained Herba Cistanches extracting solution is directly injected into same embodiment 1 24.2 μ l/ in the identical quick-fried pearl of specification, then be placed in
In the cigarette of 1 same size of embodiment.
Comparative example 3: the preparation method is the same as that of Example 1 for Herba Cistanches extracting solution, after difference is extraction, every 100ml Herba Cistanches
Complex enzyme 2.5ml is added in extract liquor, wherein the enzyme activity ratio of cellulase, beta-glucosidase, lignoenzyme and pectase
For 4:1:3:5.Gained Herba Cistanches extracting solution is directly injected into same embodiment 3 10.50 μ l/ in the identical quick-fried pearl of specification, then
It is placed in the cigarette of specification same as Example 3.
Conventional specifications parameter is carried out to embodiment 1-3 and comparative example 1-3 quick-fried pearl obtained and cigarette respectively to detect,
Acquired results are as shown in table 1.
The specifications parameter of quick-fried pearl and cigarette obtained by each example of table 1
According to the detection in " GB/T 19609-2004 cigarette conventional analysis smoking machine measures total granules and tar "
Method carries out the detection of physicochemical property to above-mentioned each obtained cigarette of example, is not pinching brokenly quick-fried pearl to measure each exemplary cigarette
It is preceding and in the case where pinching brokenly after quick-fried pearl, total granules, tar, smoking nicotine and carbon monoxide content in main flume, institute
The results are shown in Table 2.
The physicochemical property of cigarette obtained by each example of table 2
By the data in table 2 it is found that the cigarette of embodiment 1-3 pinches brokenly front and back in quick-fried pearl, the total granules in main flume
Downward trend is presented in amount, tar content, nicotine content in smoke and CO content.Since Herba Cistanches extract liquor contains in each embodiment
Amount is different, therefore the reduction amount of the main stream flue gas index of each embodiment is not also identical, but is above unused processing with enzyme preparation
The quick-fried pearl of cigarette of Herba Cistanches extract liquor (comparative example 2) pinches brokenly the reduction amount of front and back main stream flue gas index.Thus, compared to existing
There is the method for technology, can effectively reduce the content of harmful substance in cigarette by the Herba Cistanches extracting solution that complex enzyme formulation is handled.
Wherein, total granules amount of the embodiment 3 after quick-fried pearl pinches brokenly is 6.01mg/ branch, and tar content is 4.9mg/ branch, and nicotine content in smoke is
0.50mg/ branch, CO content are 4.8mg/ branch, and main stream flue gas index decline is the most significant.
Meanwhile embodiment 3 after quick-fried pearl is pinched brokenly compared with comparative example 3, total granules amount, tar content in main flume,
Nicotine content in smoke and CO content are remarkably decreased, and thus can be illustrated, the Herba Cistanches of suitable complex enzyme formulation processing are extracted
Effect of the liquid in promotion cigarette quality is more preferable.
Above-mentioned conclusion shows containing with the cigarette of Herba Cistanches extracting solution composition as main component provided by the invention,
It can effectively reduce total granules amount, tar content, nicotine content in smoke and the CO content of result of combustion of tobacco main flume in suction,
Cigarette quality is promoted, the harm to human health is reduced.
Random selection 33 professional sensory evaluation personnel, carry out sensory quality assessment to each example cigarette obtained.Its
In, the organoleptic quality of cigarette of the present invention is with reference to the volume in " the 4th part of GB 5606.4-2005 cigarette: sense organ technical requirements "
Cigarette aesthetic quality's judgment criteria, comprising: gloss, fragrance, harmony, miscellaneous gas, irritation and pleasant impression, specific judgment criteria such as 3 institute of table
Show.
3 Sensory Quality of Cigarette judgment criteria of table
According to the Sensory Quality of Cigarette judgment criteria in table 3, by professional sensory evaluation personnel to the sense organ of each example cigarette
Quality score, then be averaged as final score, the sensory quality assessment appraisal result of each example cigarette of gained such as 4 institute of table
Show.
The sensory quality assessment of cigarette obtained by each example of table 4
It can be obtained by the data in table 4, the sensory quality assessment score of cigarette obtained by embodiment 1-3 is above comparative example 1-3,
Illustrate that the aesthetic quality of cigarette of the embodiment of the present invention is obviously improved.It is retouched by the specific feedback of professional sensory evaluation personnel
It states it is found that sensory experience of the resulting cigarette of embodiment 1-3 in suction, is mainly reflected in: rich, the fine and smooth sense of flue gas,
Solid sense, which has, to be obviously improved, and cigarette perfume is stronger, saturating hair, and degrees of fusion is more preferable, the note that baking is fragrant, herbal and sauce are fragrant and sweet
Prominent, non-stimulated, without miscellaneous gas, harmony is fine, and flue gas exquisiteness sense improves, and entrance is submissive, returns sweet tea sense and is remarkably reinforced, pleasant impression is still
Only.
Above-mentioned conclusion shows containing with the cigarette of Herba Cistanches extracting solution composition as main component provided by the invention,
It can significantly improve organoleptic quality in suction, promote fragrance, hence it is evident that improve pleasant impression, significantly reduce the irritation of tobacco and miscellaneous
Gas.
In conclusion the preparation method of Herba Cistanches extracting solution provided by the invention, by using the complex enzyme suitably matched
Preparation is digested, and use can promote fragrance in cigarette, also has health-care efficacy, especially suitable for high-quality cigarette.
It is provided by the invention to be shown with Herba Cistanches extracting solution composition as main component when being applied in cigarette
Strong and unique sauce is fragrant and sweet and herbal, this is the cigarette containing other additives or only the cigarette institute containing Herba Cistanches is not
Have, while the total granules amount of cigarette mainstream flue gas, tar content, nicotine content in smoke, CO content can also be reduced etc.
Physical and chemical index reduces the harm to human health.
Quick-fried pearl provided by the invention containing above-mentioned composition, is applicable to the cigarette of different size type, improves volume
Interest when cigarette aspirates.Cigarette containing the quick-fried pearl, has in main stream flue gas index and sensory quality assessment and significantly mentions
It rises.
Quick-fried pearl by targetedly designing specific fragrance is formulated, and after being applied to cigarette, can be obviously improved volume
Impression is sucked in the interior quality that cigarette is sucked, abundant and raising.Simultaneously as Herba Cistanches have certain simple tonic effect, it can
Cigarette harm is reduced to a certain extent.Therefore, Herba Cistanches extracting solution provided herein and combinations thereof, quick-fried pearl, in cigarette
There is certain application value in careless industry.
The above description is only an example of the present application, is not intended to limit this application.For those skilled in the art
For, various changes and changes are possible in this application.All any modifications made within the spirit and principles of the present application are equal
Replacement, improvement etc., should be included within the scope of the claims of this application.
Claims (10)
1. a kind of preparation method of Herba Cistanches extracting solution, which is characterized in that the method includes extraction Herba Cistanches dry matters to obtain
Herba Cistanches extract liquor, and in Herba Cistanches extract liquor the step of addition enzyme preparation；
In terms of dry matter, the amount that enzyme preparation is added in every gram of Herba Cistanches dry matter is 3,000-3 ten thousand U；
The enzyme preparation is selected from one of cellulase, beta-glucosidase, lignoenzyme and pectase or a variety of.
2. the method according to claim 1, wherein the enzyme preparation is to include cellulase, beta-glucosidase
The complex enzyme of enzyme, lignoenzyme and pectase, the complex enzyme cellulase, beta-glucosidase, lignoenzyme and pectin
The enzyme activity ratio of enzyme is (2~5): (1~7): (3~6): (1~9), preferably 4:1:3:5；It is preferred that in every gram of Herba Cistanches dry matter
Add cellulase 2000-5000U, beta-glucosidase 1000-7000U, lignoenzyme 3000-6000U, pectase 1000-
9000U；It is further preferred that the enzyme preparation is extracted from animal, plant and/or microorganism.
3. method according to claim 1 or 2, which is characterized in that the method specifically includes the following steps:
Under 80-100 DEG C or ultrasonic wave or microwave condition, the reflux of water-bath heat or vibration are carried out to Herba Cistanches dry matter with 60% ethyl alcohol
Extraction 1-12 hours is swung, Herba Cistanches extract liquor is obtained, it is cooling, 1-2ml enzyme preparation, institute are added in every 100ml Herba Cistanches extract liquor
Enzyme preparation is stated to be (2~5): (1~7): (3~6): cellulase, beta-glucosidase, the wood of (1~9) containing enzyme activity ratio
The complex enzyme of quality enzyme and pectase, being further concentrated to concentration of the volume of the concentrated liquid containing dry matter is 8%-25%, i.e., described in acquisition
Herba Cistanches extracting solution；
It is preferred that the solid-liquid ratio of the Herba Cistanches powder and ethyl alcohol is 1g:7-10ml；It is preferred that Herba Cistanches are extracted before enzyme preparation is added
Liquid is cooled to 15-25 DEG C；It is preferred that being inactivated 5 minutes at 100 DEG C after concentration.
4. according to the method described in claim 3, it is characterized in that, the method also includes carrying out pretreated step to Herba Cistanches
Suddenly, it specifically includes:
It by Herba Cistanches washing, removal impurity, sunning, is dried at 30-60 DEG C, directly crushes or be crushed in liquid nitrogen 40-100
Mesh.
5. a kind of Herba Cistanches extracting solution, which is characterized in that prepared using the method as described in claim 1-4 is any.
6. a kind of composition, which is characterized in that including the meat desert for using the method as described in claim 1-4 is any to prepare
Rong's extracting solution, the quality accounting of Herba Cistanches extracting solution is 16%-98%, preferably 50%-80% in the composition.
7. composition according to claim 6, which is characterized in that the composition further include it is following any one or a few
Ingredient: Glycerin, mixed triester with caprylic acid capric acid, glyceryl triacetate, maltol, menthyl acetate, vanillic aldehyde, Ethyl vanillin, ethyl caprilate,
Orange limonene, γ-terpinene, nopinene, australene, D- pyroglutamic acid ethyl ester, 5- hydroxyl maltol, nerol, geraniol.
8. a kind of quick-fried pearl, which is characterized in that the quick-fried pearl contains composition as claimed in claims 6 or 7；It is preferred that described quick-fried
Pearl contains 10-30 microlitres of composition；It is further preferred that the diameter of the quick-fried pearl is 2-4mm, weight is 10-25mg/, and circularity is small
In 0.15mm, cracking pressure value is 1-1.5kgf.
9. Herba Cistanches extracting solution as claimed in claim 5 and/or composition as claimed in claim 6, and/or such as right
It is required that quick-fried pearl described in 8 is improving the application in cigarette sensory quality.
10. a kind of cigarette, which is characterized in that contain Herba Cistanches extracting solution as claimed in claim 5 in the cigarette, and/or
Containing composition as claimed in claim 6, and/or contain at least one quick-fried pearl as claimed in claim 8.
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