CN109288137B - Preparation method and application of tobacco shreds added with atomizing agent - Google Patents

Preparation method and application of tobacco shreds added with atomizing agent Download PDF

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CN109288137B
CN109288137B CN201811389054.6A CN201811389054A CN109288137B CN 109288137 B CN109288137 B CN 109288137B CN 201811389054 A CN201811389054 A CN 201811389054A CN 109288137 B CN109288137 B CN 109288137B
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tobacco
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atomizing agent
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CN109288137A (en
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王昊
张耀华
熊斌
程炳发
庞哲
杨俊鹏
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China Tobacco Hubei Industrial LLC
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Abstract

The invention provides a preparation method and application of cut tobacco added with an atomizing agent, which is characterized by comprising the following steps: the method comprises the following steps: feeding, unpacking and cutting the tobacco flakes, loosening and dampening; performing primary feeding treatment, wherein the mass percentage of the fed tobacco is 15 percent according to the mass of the added tobacco as a base number; storing the leaves for 0.5-1h, and carrying out secondary feeding treatment; storing the leaves for 0.5-1h, then baking at a hot air temperature of 110 +/-10 ℃, a tobacco sheet temperature of less than or equal to 65 ℃ and a moisture of 18 +/-2%; shredding the cured tobacco sheets, and performing expansion drying after shredding, wherein the water content is controlled to be 10 +/-1%; blending the prepared tobacco shreds added with the atomizing agent by using a tobacco blend; the blended tobacco shreds are flavored, wherein the flavoring proportion is less than or equal to 1.0 percent, and the proportion of the atomizing agent is not less than 0.8 percent. The invention solves the technical problem that the traditional tobacco shred production line can not prepare and obtain tobacco shreds with a large proportion of atomizing agents.

Description

Preparation method and application of tobacco shreds added with atomizing agent
Technical Field
The invention relates to the technical field of heating non-combustible tobacco products, in particular to a preparation method and application of tobacco shreds added with an atomizing agent.
Background
With the development of modern cigarette industry, heating non-combustible tobacco products gradually becomes a new traditional cigarette substitute. The tobacco component containing the atomizing agent such as glycerin is heated by heating the non-burning tobacco product in an electric, carbon, chemical and other modes to generate smoke containing nicotine and flavor components, so that the consumption experience similar to that of the traditional cigarette is realized.
Because the non-combustion mode is adopted, the harmful components generated by heating the non-combustion tobacco product are greatly reduced compared with the traditional cigarette, and the tobacco product has rapid development and popularity in international markets such as Japan and Korean.
In the new type of heat not burn tobacco products that are marketed, the tobacco component is mainly constituted by a thick-paste tobacco reconstituted tobacco, such as the electrically heated cigarette of patent 200580036230.2, filed by the company fizeau, the tobacco material (tobacco mat) of which is preferably formed by a paper-making type process. Volatile substances such as glycerin and propylene glycol are atomized by heating to generate smoke similar to cigarette combustion, so that the smoking experience of a consumer is closer to that of a traditional cigarette. The products on the market at present comprise IQOS, GLO, PLOOM and other products and matched cigarettes, and the market development is rapid.
The tobacco material in the cigarettes of the product is generally reconstituted tobacco with a regular structure or an analogue thereof, for example, patent 201710984517.2 needs to be newly matched with a brand-new tobacco material preparation device and cigarette processing equipment, the tobacco material cannot be prepared by adopting the traditional cigarette shredding and cigarette wrapping processing technology, and related methods of tobacco substances for manufacturing novel tobacco products by adopting the traditional cigarette technology are not applied and reported.
In Liuxin et al (Nanchang university journal (Rickett) No. 27, No. 2 of 2003), the adsorption process of glycerol to tobacco leaves increases with time. After the tobacco is crushed, the adsorption effect is better than that of the cut tobacco, and the cut tobacco has a certain limit on the adsorption of the glycerol.
In the reports of Tang baking and the like (tobacco science and technology, 3 months in 2015, 3 rd period in volume 48), the influence of glycerin on the thermal performance and the smoke release in a heating state of tobacco leaves shows that when the addition amount of glycerin in tobacco shreds is more than 10%, the tar release amount is not obviously increased under the heating condition at a certain temperature (350 ℃), and the proportion of the glycerin added in the tobacco shreds is more than 10%, so that the atomization effect cannot be better realized, and tar is released.
In order to fully utilize the traditional cigarette processing process equipment and realize the preparation of the cigarette which is not burnt by heating on the conventional cigarette making and rolling process equipment, the process and the tobacco formula design are carried out in a targeted manner by combining the characteristics of the novel tobacco product which is not burnt by heating, thereby realizing the aim.
In the traditional tobacco shred production line of flue-cured cigarettes, the proportion of sugar-added materials is generally about 3.5 percent, the large-proportion addition of an atomizing agent cannot be realized, the large-proportion addition of 10-20 percent of material liquid can be realized in a burley tobacco curing line, and the mixture is processed at high temperature and then mixed with formulated tobacco leaves for feeding.
Meanwhile, as the tobacco leaves have low absorption performance on the atomizing agents such as glycerin and the like, the independently added large-proportion atomizing agents cannot be fully absorbed by the tobacco leaves, so that most of applied atomizing agents are adsorbed on the surfaces of the tobacco leaves, and the atomizing agents attached to the surfaces of the tobacco shreds are easy to absorb moisture to block tobacco strips and tobacco shred conveying devices by utilizing traditional cigarette equipment.
Disclosure of Invention
Aiming at the defects in the prior art, the invention utilizes the existing burley tobacco processing process route, and adds the atomizing agent such as glycerol and the like in the lining material adding process, adjusts the process control conditions, produces the tobacco shreds which have the atomizing agent adding proportion of more than 8 percent and can be used for heating the non-burning tobacco products, and then mixes and mixes the tobacco shreds with other tobacco raw materials to form mixed tobacco shreds.
The technical scheme of the invention is as follows:
a preparation method of cut tobacco added with an atomizing agent is characterized by comprising the following steps: the method comprises the following steps:
the method comprises the following steps: feeding, unpacking and cutting tobacco flakes, loosening and dampening the tobacco flakes, wherein the moisture content of the tobacco flakes is 20-25%, and the temperature is 40-80 ℃;
step two: performing primary feeding treatment, wherein the mass percent of the fed tobacco is 15 percent, the temperature of the feed liquid is 80 +/-10 ℃, the mass percent of the atomizing agent in the feed liquid is less than or equal to 10 percent, and the water content of tobacco flakes is 25-30 percent according to the mass of the added tobacco leaves as a base number;
step three: storing the tobacco leaves for 0.5-1h, and performing secondary feeding treatment, wherein the feeding mass percent is 15%, the feed liquid temperature is 80 +/-10 ℃, the mass percent of a fogging agent in the feed liquid is less than or equal to 10%, and the water content of tobacco flakes is 30-35%;
step four: storing the leaves for 0.5-1h, then baking at a hot air temperature of 110 +/-10 ℃, a tobacco sheet temperature of less than or equal to 65 ℃ and a moisture of 18 +/-2%;
step five: shredding the cured tobacco sheets, and performing expansion drying after shredding, wherein the water content is controlled to be 10 +/-1%;
step six: blending the prepared tobacco shreds added with the atomizing agent by using a tobacco blend, wherein a sheet in the tobacco blend is common reconstituted tobacco or reconstituted tobacco added with the atomizing agent in a certain proportion, the proportion of the atomizing agent is 15 +/-5%, cut stems in the tobacco blend are common expanded cut stems, reconstituted cut stems or cut stems added with the atomizing agent in a certain proportion, and the proportion of the atomizing agent is 15 +/-5%;
step seven: the blended tobacco shreds are flavored, wherein the flavoring proportion is less than or equal to 1.0 percent, and the proportion of the atomizing agent is not less than 0.8 percent.
The material liquid added in the second step and the third step is a mixture consisting of an atomizing agent, invert sugar, a tobacco extract and water, wherein the proportion of the atomizing agent to the tobacco leaves is 5-10%, the proportion of the invert sugar to the tobacco leaves is 3-5%, and the proportion of the tobacco extract to the tobacco leaves is 1-2%.
The atomizing agent is glycerin or propylene glycol or a combination of the glycerin and the propylene glycol.
And in the fifth step, the shredding width is 1.0 +/-0.2 mm.
The tobacco shreds added with the atomizing agent are matched with a composite filter stick capable of cooling on a conventional cigarette making machine, and cigarettes are coiled through binary or multi-element composite to be used for electrically heating or carbon heating cigarettes.
Compared with the prior art, the invention has the beneficial effects that:
1. the method of the invention utilizes traditional cigarette technology to prepare cut tobacco equipment to a greater extent, redesigns the technology method, utilizes mixed cut tobacco burley tobacco baking technology equipment, adds the atomizing agent by one step or multiple steps, gradually increases the tobacco leaf adsorption atomizing dosage, and obtains cut tobacco added with the atomizing agent by two steps or multiple steps of drying, wherein the content of the atomizing agent is 8-15%, thus solving the technical problem that the traditional cut tobacco preparation production line can not prepare cut tobacco with a large proportion of atomizing agent.
2. According to the invention, the tobacco shreds added with the atomizing agent and the blends thereof are blended by different materials, and the processing performance and the filling value of the mixed tobacco shreds are adjusted, so that the tobacco shreds containing the atomizing agent in a larger proportion can be rolled by the traditional cigarette rolling equipment, and the technical problem that the traditional rolling equipment cannot prepare the tobacco shreds containing the atomizing agent in a large proportion is solved.
3. The tobacco product cigarette which is prepared by the method and is not burnt generates smoke when being heated to the temperature of 200-350 ℃, and releases nicotine and fragrant substances.
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FIG. 1 is a process flow diagram of a preparation method of cut tobacco added with an atomizing agent.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Example 1: mixing type A
The embodiment of the invention provides a preparation method of cut tobacco added with an atomizing agent, which comprises the following steps:
the method comprises the following steps: preparing 40-50% of burley tobacco, 20-30% of flue-cured tobacco and 10-20% of common reconstituted tobacco according to mass percent, feeding, unpacking, loosening and moisture regaining after cutting, wherein the moisture content of tobacco flakes is 20-25%, and the temperature is 40-80 ℃;
step two: performing primary feeding treatment, wherein the feeding mass ratio is 15%, the temperature of the feed liquid is 80 +/-10 ℃, the feed liquid contains 10% of glycerol, 3-5% of invert sugar and 25-30% of water content of tobacco flakes;
step three: storing the tobacco leaves for 0.5-1h, and performing secondary feeding treatment, wherein the feeding mass ratio is 15%, the feed liquid temperature is 80 +/-10 ℃, the mass ratio of glycerol is 8%, the mass ratio of invert sugar is 3-5%, and the water content of tobacco flakes is 30-35%;
step four: storing the leaves for 0.5-1h, then baking at a hot air temperature of 110 +/-10 ℃, a tobacco sheet temperature of less than or equal to 65 ℃ and a moisture of 18 +/-2%;
step five: slicing (width of 1.0 + -0.2 mm), swelling and drying to water content of 10 + -1%.
The mixed type A cut tobacco is obtained, the glycerin content of the cut tobacco is 8.9-10.5%, the filling value of the cut tobacco is 3.0cm3/g, the whole cut tobacco rate is 85.0%, the cut tobacco shredding rate is 1.8%, a composite filter stick capable of cooling is matched on a conventional cigarette making machine, cigarettes are made by two-element or multi-element composite rolling, cigarettes are used for electrically heating or carbon heating, and after the cigarettes are ignited or at 350 ℃, the smoke amount is medium, the physiological strength is obvious, and the taste in the oral cavity is more.
On the basis of referring to the traditional cigarette evaluation method and combining the characteristics of novel tobacco products, the cigarette made of the cut tobacco is evaluated, and the results are as follows:
TABLE 1 sensory evaluation table for novel tobacco products
Index (I) Evaluation of
Fragrance Is more sufficient
Feeling of dryness Is a little bit
Burning sensation Is a little bit
Degree of cleanliness Clean and clean
Degree of sweetness In
Stimulation of Is a little bit
Stiff head Mid value of
Concentration of Medium and high grade
Example 2: hybrid type B
The embodiment of the invention provides a preparation method of cut tobacco added with an atomizing agent, which comprises the following steps:
the method comprises the following steps: preparing 40-50% of burley tobacco, 20-30% of flue-cured tobacco and 10-20% of common reconstituted tobacco according to mass percent, feeding, unpacking, loosening and moisture regaining after cutting, wherein the moisture content of tobacco flakes is 20-25%, and the temperature is 40-80 ℃;
step two: one-time feeding treatment, wherein the feeding proportion is 15%, the feed liquid temperature is 80 +/-10 ℃, the glycerol proportion is 10%, in addition, 3-5% of invert sugar and a plurality of tobacco extracts are contained, and the water content of tobacco flakes is 25-30%;
step three: storing leaves for 0.5-1h, and performing secondary feeding treatment at feeding ratio of 15% and material liquid temperature of 80 + -10 deg.C, wherein the glycerol ratio is 10%, invert sugar 3-5% and tobacco extract are several, and tobacco flake water content is 30-35%;
step four: storing the leaves for 0.5-1h, then baking at a hot air temperature of 110 +/-10 ℃, a tobacco sheet temperature of less than or equal to 65 ℃ and a moisture of 18 +/-2%;
step five: slicing (width of 1.0 + -0.2 mm), swelling and drying to water content of 10 + -1%.
Sixthly, adding 20-30% of atomizing agent to regenerate the tobacco leaves (the proportion of the atomizing agent is 15%).
And seventhly, perfuming the blended tobacco shreds, wherein the perfuming proportion is less than or equal to 1.0 percent, and the proportion of propylene glycol is not less than 0.8 percent.
The mixed type B tobacco shreds are obtained, the glycerin content of the tobacco shreds is 13.5-14.8%, the filling value of the tobacco shreds is 3.6cm3/g, the whole tobacco shred rate is 84.0%, the shredded tobacco shred rate is 1.4%, a composite filter stick capable of reducing the temperature is matched on a conventional cigarette making machine, cigarettes are coiled through two-element or multi-element composite, the cigarettes are used for electrically heating or carbon heating cigarettes, and after the cigarettes are ignited or at 350 ℃, the smoke amount is medium, the physiological strength is obvious, and the taste in the oral cavity is more.
TABLE 2 sensory evaluation table for novel tobacco products
Index (I) Evaluation of
Fragrance Sufficient (sufficient)
Feeling of dryness Is a little bit
Burning sensation Is a little bit
Degree of cleanliness Is clean and clean
Degree of sweetness In general
Stimulation of Is a little bit
Stiff head Is larger
Concentration of Medium and high grade
Example 3: flue-cured tobacco type C
The embodiment of the invention provides a preparation method of cut tobacco added with an atomizing agent, which comprises the following steps:
the method comprises the following steps: preparing 40-50% of burley tobacco, 20-30% of flue-cured tobacco and 10-20% of common reconstituted tobacco according to mass percent, feeding, unpacking, loosening and moisture regaining after cutting, wherein the moisture content of tobacco flakes is 20-25%, and the temperature is 40-80 ℃;
step two: one-time feeding treatment, wherein the feeding proportion is 15%, the feed liquid temperature is 80 +/-10 ℃, the glycerol proportion is 10%, in addition, 3-5% of invert sugar and a plurality of tobacco extracts are contained, and the water content of tobacco flakes is 25-30%;
step three: storing leaves for 0.5-1h, and performing secondary feeding treatment at feeding ratio of 15% and material liquid temperature of 80 + -10 deg.C, wherein the glycerol ratio is 10%, invert sugar 3-5% and tobacco extract are several, and tobacco flake water content is 30-35%;
step four: storing the leaves for 0.5-1h, then baking at a hot air temperature of 110 +/-10 ℃, a tobacco sheet temperature of less than or equal to 65 ℃ and a moisture of 18 +/-2%;
step five: cutting into shreds (width of 1.0 + -0.2 mm), swelling and drying to water content of 10 + -1%;
step six, blending 10-20% of expanded cut stems;
and seventhly, perfuming the blended tobacco shreds, wherein the perfuming proportion is less than or equal to 1.0 percent, and the proportion of propylene glycol is not less than 0.8 percent.
The baked tobacco type C cut tobacco is obtained, the glycerin content of the cut tobacco is 10.5-12.3%, the filling value of the cut tobacco is 3.5cm3/g, the whole cut tobacco rate is 83.0%, the cut tobacco shredding rate is 1.8%, a composite filter stick capable of cooling is matched on a conventional cigarette making machine, cigarettes are coiled through two-element or multi-element composite, the cigarettes are used for electrically heating or carbon heating, the smoke amount is medium, the physiological strength is moderate, the smoke is elegant, and the oral cavity is clean after the cigarettes are ignited or at 350 ℃.
TABLE 3 sensory evaluation table for novel tobacco products
Index (I) Evaluation of
Fragrance Is elegant
Feeling of dryness Is a little bit
Burning sensation Is a little bit
Degree of cleanliness Clean and clean
Degree of sweetness Is relatively sweet and moist
Stimulation of Is a little bit
Stiff head Medium and high grade
Concentration of Medium and high grade
Example 4: flue-cured tobacco type D
The embodiment of the invention provides a preparation method of cut tobacco added with an atomizing agent, which comprises the following steps:
the method comprises the following steps: preparing 40-50% of burley tobacco, 20-30% of flue-cured tobacco and 10-20% of common reconstituted tobacco according to mass percent, feeding, unpacking, loosening and moisture regaining after cutting, wherein the moisture content of tobacco flakes is 20-25%, and the temperature is 40-80 ℃;
step two: one-time feeding treatment, wherein the feeding proportion is 15%, the feed liquid temperature is 80 +/-10 ℃, the glycerol proportion is 10%, in addition, 3-5% of invert sugar and a plurality of tobacco extracts are contained, and the water content of tobacco flakes is 25-30%;
step three: storing leaves for 0.5-1h, and performing secondary feeding treatment at feeding ratio of 15% and material liquid temperature of 80 + -10 deg.C, wherein the glycerol ratio is 10%, invert sugar 3-5% and tobacco extract are several, and tobacco flake water content is 30-35%;
step four: storing the leaves for 0.5-1h, then baking at a hot air temperature of 110 +/-10 ℃, a tobacco sheet temperature of less than or equal to 65 ℃ and a moisture of 18 +/-2%;
step five: cutting into shreds (width of 1.0 + -0.2 mm), swelling and drying to water content of 10 + -1%;
step six, blending 10% of reconstituted cut stems and 20% of tobacco leaves reconstituted by adding an atomizing agent (the proportion of the atomizing agent is 15%);
and seventhly, perfuming the blended tobacco shreds, wherein the perfuming proportion is less than or equal to 1.0 percent, and the proportion of propylene glycol is not less than 0.8 percent.
The obtained D-type cut tobacco of the flue-cured tobacco has the glycerin content of 13.2-14.3 percent, the filling value of the cut tobacco is 3.9cm3/g, the whole cut tobacco rate is 82.0 percent, the broken cut tobacco rate is 1.4 percent, a composite filter stick capable of reducing the temperature is matched on a conventional cigarette making machine, the cigarette is coiled by two-element or multi-element composite to be used for electrically heating or carbon heating the cigarette, and the cigarette has moderate smoke amount, moderate physiological strength, elegant smoke and clean oral cavity at 350 ℃ or after being ignited.
TABLE 4 sensory evaluation table for novel tobacco products
Figure BDA0001873617330000081
Figure BDA0001873617330000091
Although embodiments of the present invention have been shown and described, it will be appreciated by those skilled in the art that changes, modifications, substitutions and alterations can be made in these embodiments without departing from the principles and spirit of the invention, the scope of which is defined in the appended claims and their equivalents.

Claims (5)

1. A preparation method of cut tobacco added with an atomizing agent is characterized by comprising the following steps: the method comprises the following steps:
the method comprises the following steps: feeding, unpacking and cutting tobacco leaves, loosening and dampening the tobacco leaves, wherein the moisture content of the tobacco leaves is 20-25%, and the temperature is 40-80 ℃;
step two: performing primary feeding treatment, wherein the mass percent of the fed tobacco is 15 percent based on the mass of the added tobacco, the temperature of the feed liquid is 80 +/-10 ℃, the mass percent of the atomizing agent in the feed liquid relative to the mass of the added tobacco is less than or equal to 10 percent, and the moisture content of the tobacco is 25-30 percent;
step three: storing the tobacco leaves for 0.5-1h, and performing secondary feeding treatment, wherein the feeding mass percent is 15%, the temperature of the feed liquid is 80 +/-10 ℃, the mass percent of a fogging agent in the feed liquid relative to the mass of the added tobacco leaves is less than or equal to 10%, and the water content of the tobacco leaves is 30-35%;
step four: storing the tobacco leaves for 0.5-1h, and then performing baking treatment, wherein the hot air temperature is 110 +/-10 ℃, the tobacco leaf temperature is less than or equal to 65 ℃, and the moisture content of the tobacco leaves is 18 +/-2%;
step five: shredding the cured tobacco leaves, and performing expansion drying after shredding, wherein the moisture content of the tobacco leaves is controlled to be 10 +/-1%;
step six: blending the prepared tobacco shreds added with the atomizing agent by using a tobacco blend, wherein a sheet in the tobacco blend is common reconstituted tobacco or reconstituted tobacco added with the atomizing agent in a certain proportion, the proportion of the atomizing agent is 15 +/-5%, cut stems in the tobacco blend are common expanded cut stems, reconstituted cut stems or cut stems added with the atomizing agent in a certain proportion, and the proportion of the atomizing agent is 15 +/-5%;
step seven: perfuming the blended tobacco shreds, wherein the proportion of the perfuming perfume relative to the mass of the blended tobacco shreds is less than or equal to 1.0 percent, and the proportion of the atomizing agent in the perfume relative to the mass of the blended tobacco shreds is not less than 0.8 percent.
2. The method for preparing the cut tobacco added with the atomizing agent according to claim 1, is characterized in that: the feed liquid added in the second step and the third step is a mixture consisting of an atomizing agent, invert sugar, a tobacco extract and water, wherein the proportion of the atomizing agent to the mass of the added tobacco leaves is 5-10%, the proportion of the invert sugar to the mass of the added tobacco leaves is 3-5%, and the proportion of the tobacco extract to the mass of the added tobacco leaves is 1-2%.
3. The method for preparing the cut tobacco added with the atomizing agent according to claim 2, is characterized in that: the atomizing agent is glycerin or propylene glycol or a combination of the glycerin and the propylene glycol.
4. The method for preparing the cut tobacco added with the atomizing agent according to claim 2, is characterized in that: and in the fifth step, the shredding width is 1.0 +/-0.2 mm.
5. Use of a cut tobacco with added atomizing agent according to any one of claims 1 to 4, characterized in that: the prepared tobacco shreds added with the atomizing agent are matched with a composite filter stick capable of cooling on a conventional cigarette making machine, and cigarettes are coiled through binary or multi-element composite for electrically heating or carbon heating cigarettes.
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