CN110506984A - A kind of tobacco particle and preparation method thereof, low temperature fuming liquids and preparation method thereof - Google Patents

A kind of tobacco particle and preparation method thereof, low temperature fuming liquids and preparation method thereof Download PDF

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Publication number
CN110506984A
CN110506984A CN201810486784.1A CN201810486784A CN110506984A CN 110506984 A CN110506984 A CN 110506984A CN 201810486784 A CN201810486784 A CN 201810486784A CN 110506984 A CN110506984 A CN 110506984A
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CN
China
Prior art keywords
tobacco
particle
low temperature
preparation
bulk
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Granted
Application number
CN201810486784.1A
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Chinese (zh)
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CN110506984B (en
Inventor
陈潜
金勇�
李克
杜文
尹新强
易建华
谭新良
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China Tobacco Hunan Industrial Co Ltd
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China Tobacco Hunan Industrial Co Ltd
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Application filed by China Tobacco Hunan Industrial Co Ltd filed Critical China Tobacco Hunan Industrial Co Ltd
Priority to CN201810486784.1A priority Critical patent/CN110506984B/en
Priority to JP2020563970A priority patent/JP7029553B2/en
Priority to KR1020207036581A priority patent/KR102583754B1/en
Priority to PCT/CN2019/078652 priority patent/WO2019223411A1/en
Priority to US17/057,598 priority patent/US20210401030A1/en
Priority to EP19808374.3A priority patent/EP3797602A4/en
Publication of CN110506984A publication Critical patent/CN110506984A/en
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Publication of CN110506984B publication Critical patent/CN110506984B/en
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/24Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • A24B15/26Use of organic solvents for extraction

Abstract

The present invention relates to a kind of tobacco particles and preparation method thereof, low temperature fuming liquids and preparation method thereof.The tobacco particle, including particle bulk, the particle bulk include carrier, tobacco extract and Alevaire;The particle bulk is coated with coatings.Tobacco particle atomized inside agent provided by the invention and tobacco extract are evenly distributed, and smoke stability and uniformity are more preferable;Tobacco particle granulation process has carried out powder package and Cotton seeds respectively, has largely blocked particle internal component and external contact, has more conducively stored, while largely having solved liquid object leakage problems;Tobacco particle uses, and there is adhesive force material to be coated, its isolation capacity and adhesive force is cleverly utilized very much, and subsequent processing is not necessarily to be glued again, more conducively industrialized mass production;A large amount of non-tobacco materials have been used in tobacco particle, the release of nicotine when sucking can be greatly reduced, and reduce irritation.

Description

A kind of tobacco particle and preparation method thereof, low temperature fuming liquids and preparation method thereof
Technical field
The present invention relates to a kind of tobacco particles and preparation method thereof, low temperature fuming liquids and preparation method thereof, belong to low temperature volume Cigarette field.
Background technique
Generally raising with scientific and technological progress and people to health perception, new tobacco products present blowout hair Exhibition.The low temperature cigarette that do not burn is particularly subject to the attention of major research institution and enterprise as one type major product.Currently, city Low temperature on field do not burn cigarette product mainly using in special electric heater unit fill tobacco-containing material such as cigarette, pipe tobacco or Smoked sheet etc. evaporates the flue gas in tobacco fill material by electric heating, so that obtaining smoker is similar to conventional smoke The suction impression of grass.And the generally existing amount of smoke of low temperature fuming liquids of this form is insufficient, and front and back is uneven and suction oral account is few etc. Problem.
Chinese patent CN201610232919 provides a kind of column of smoke suitable for low temperature cigarette, by tobacco particle, thermally conductive Component is molded with after mixing with adhesive, tobacco essence and humectant, which has smoke amount speed fast and more, is taken out Inhale smooth advantage, even if defect be the column of smoke be dried after it is still more damp, be unfavorable for storing, the strong easy to leak of hygroscopicity, sternly Ghost image rings its availability, its smoke stability and front and back homogeneity is all poor, while nicotine content excessively high irritation when sucking It is larger.
Summary of the invention
Present invention solves the technical problem that being, low temperature does not burn in the prior art, and cigarette smoke amount is insufficient, and puff number is few, Smoke stability and front and back homogeneity are poor, and the excessively high irritation of nicotine content is larger when sucking, and permeability phenomenon easily occur in fuming liquids.
In order to solve the above-mentioned technical problem, technical scheme is as follows: a kind of tobacco particle, including particle bulk, The particle bulk includes carrier, tobacco extract and Alevaire;The particle bulk is coated with coatings.
In the present invention, tobacco extract and Alevaire are carried on carrier, so that being evenly distributed cigarette in particle bulk Careless extract and Alevaire guarantee smoke amount, promote puff number;It, can be by tobacco extract, atomization by the setting of coatings Agent is effectively isolated from the outside, and solves leakage problems.
Further, the carrier includes tobacco material and/or non-tobacco material.
Further, carrier, tobacco extract, Alevaire mass ratio be 120-200:1-15:5-30.
Further, the carrier includes tobacco material and non-tobacco material, further, tobacco material, non-tobacco Material, tobacco extract, Alevaire mass ratio be 100:20-100:1-15:5-30.
Further, the non-tobacco material include microcrystalline cellulose, tealeaves, ramie pulp fiber, bamboo fibre, cocoanut fiber, At least one of starch, coffee shell, dried peppermint leaf.The use of non-tobacco material can be played the role of diluting tobacco material, make to inhale Nicotine content is greatly reduced when food, reduces irritation;The use of some materials facilitates the control or tax of granulation process simultaneously It gives tobacco particle and particularly sucks flavor.
Further, the particle bulk also includes wetting agent, it is preferable that the wetting agent includes water and/or alcohol.Into One step, wetting agent and tobacco material mass ratio are 5-30:100, to guarantee that tobacco particle preferably forms.
Further, offal layer is additionally provided between the particle bulk and coatings, it is preferable that offal layer and particle bulk Mass ratio be 100:5-25.After offal layer is wrapped up on particle bulk surface, may make particle bulk color it is more attractive, close to cigarette Draft color, while offal layer can partially block the agent of particle atomized inside and tobacco extract externally leaks.
Further, the coatings are made of the material with adhesive force.
Further, the coatings include hydroxypropyl methyl cellulose, hydroxypropyl cellulose, povidone, carboxymethyl fibre Tie up one of plain sodium, microcrystalline cellulose, polyethylene glycol, polyvinyl alcohol or a variety of.
Further, on the one hand coatings can partially block the agent of particle atomized inside and tobacco extract externally leaks, and Making particle has better appearance and mobility, while itself has an adhesive force, and when subsequent processing can make fast between tobacco particle Fast molding bonded.
Further, the mass ratio of the coatings and tobacco particle gross weight is 0.1-5:100, to guarantee tobacco particle Can smoothly mutual molding bonded while, reduce influence of the coatings to flavor is sucked.
Further, the Alevaire includes glycerol, propylene glycol, glycerine, mass ratio 0-10:0-20:0-30, Preferably 2-8:4-16:5-25.
Further, the tobacco particle is spherical or subsphaeroidal particle.
Further, the partial size of the tobacco particle is 10-30 mesh, moisture content 10-25%.Partial size is too small, then is made After low temperature fuming liquids, fuming liquids internal breathability is inadequate, influences smoke and sucks feeling;Partial size is excessive, then fuming liquids appearance is not Enough beauties, while fuming rate is slack-off.The control of moisture content is conducive to excite tobacco particle surface coatings layer when subsequent processing Adhesive force, enable quick molding bonded.
The preparation method of tobacco particle as described above, includes the following steps:
(1) carrier, tobacco extract, Alevaire are uniformly mixed, are granulated, whole grain, obtain particle bulk;
(2) coatings are prepared in the particle bulk surface that step (1) obtains, i.e. acquisition tobacco particle finished product.
Further, in step (1), wetting agent and tobacco material, non-tobacco material, tobacco extract, Alevaire are mixed It closes uniformly, then is granulated, wherein the mass ratio of tobacco material, non-tobacco material, tobacco extract, Alevaire and wetting agent is 100: 20-100:1-15:5-30:0-25.
Further, before step (1), further include the steps that crushing carrier, further, carrier is crushed to 100-200 mesh, wherein crushing process temperature is no more than 60 DEG C.Suitable treatment temperature can guarantee that the aroma quality of raw material obtains most The reservation of big degree.
Further, between step (1) and step (2), further include the steps that preparing offal layer on particle bulk surface, i.e., After offal is wrapped up on particle bulk surface, low temperature drying obtains tobacco particle semi-finished product.Further, the partial size of the offal For 150-200 mesh.
Further, the temperature of the low temperature drying is 40-60 DEG C.
A kind of low temperature fuming liquids, the tobacco prepared including tobacco particle as described above or preparation method as described above Grain.
The preparation method of low temperature fuming liquids as described above, the tobacco particle is placed in molding die, curing molding, Obtain low temperature fuming liquids finished product.
Further, the low temperature fuming liquids are loose ventilative cylinder, water chestnut cylinder, square or other specific shapes Shape, to meet different application demand.
Preferably, effecive porosity is 65-95% inside the low temperature fuming liquids.Effecive porosity appropriate can guarantee hair Smoke internal breathability keeps its suction more easily smooth, and smoke is more rapidly.
Further, moisture content is 5-13wt% in the low temperature fuming liquids.
Further, the curing molding includes microwave curing molding or heat cure molding.Microwave or heat cure processing make Tobacco particle internal moisture is quickly volatilized, on the one hand, and fuming liquids moisture content can be made to be down to reasonable level, on the other hand, moisture Meeting excitating surface coatings adhesive force, makes good bond between tobacco particle be shaped to suitable shape during volatilization exudation Fuming liquids.
Low temperature fuming liquids of the invention can be used for low temperature smoking set or tobacco pipe fast and stable smoke.
Low temperature fuming liquids provided by the invention belong to a kind of low temperature cigarette, i.e., produce cigarette by heating in incombustible situation Gas.
Compared with prior art, the beneficial effects of the present invention are:
1, tobacco particle atomized inside agent of the invention and tobacco extract are evenly distributed, and smoke stability and uniformity are more preferable.
2, the present invention successively carries out tobacco powder package and Cotton seeds to particle bulk, can largely block Grain internal component and external contact form dual antiseepage protection, more conducively store, effectively solve liquid object leakage problems.
3, tobacco particle of the invention uses, and there is adhesive force material to be coated, its isolation is cleverly utilized very much Ability and adhesive force, subsequent processing are not necessarily to be glued again, more conducively industrialized mass production.
4, a large amount of non-tobacco materials have been used in tobacco particle of the invention, the release of nicotine when sucking can be greatly reduced, Reduce irritation;Part non-tobacco material can assign special aroma simultaneously, meet individual requirements.
Specific embodiment
Following embodiment is intended to illustrate summary of the invention, rather than further limits to the scope of the present invention.
Embodiment 1
In the present embodiment, the preparation method of low temperature fuming liquids includes the following steps:
1) mass parts are pressed, the tobacco powder of 100 parts of 100-200 mesh, the microcrystalline cellulose of 50 parts of 100-200 mesh are weighed;Weigh 6 parts Tobacco extract, 5 parts of glycerol, 10 parts of glycerine, 12 part of 95% alcohol, are sprayed on above-mentioned tobacco powder and crystallite after mixing In cellulose, and be uniformly mixed, extruding pelletization obtains soft profit tobacco particle;2) tobacco powder and step of 10 parts of 150-200 mesh are weighed Suddenly the soft profit tobacco particle mixing obtained in (1) is round as a ball, and sieving takes 10-40 mesh particle, dries under the conditions of 50 DEG C, obtains cigarette Grass particle semi-finished product;3) it takes 0.3 part of sodium carboxymethylcellulose to be dissolved in 20 parts of water, place is coated to aforementioned tobaccos pellet product Reason, and finished particle moisture 15% is controlled, tobacco particle needed for obtaining;4) tobacco particle for weighing certain mass is placed in special circle In cylindrical cavity mold, suitably presses and be brought rapidly up to 100 DEG C, it is 10% left that held for some time, which controls particle internal moisture, The right side, quickly cooling to room temperature, tobacco particle has been bonded to stick in mold, takes out up to required low temperature fuming liquids.
Fillable be used as in corresponding low temperature cigarette smoking set or tobacco pipe of the low temperature fuming liquids sucks material, also can cigarette At cigarette shape for sucking, fuming rate is fast when sucking, and amount of smoke is sufficient and front and back uniformity is good, and puff number is more, aroma quality Good, the moderate irritation of nicotine content is reduced.
Embodiment 2
In the present embodiment, the preparation method of low temperature fuming liquids includes the following steps:
1) mass parts are pressed, the tobacco powder of 100 parts of 120-200 mesh, the tea-leaf power of 20 parts of 100-200 mesh are taken;Take 12 portions of tobaccos Extract, 10 parts of glycerol, 5 parts of propylene glycol, 10 parts of glycerine, 15 parts of water are sprayed on above-mentioned tobacco powder after being mixed uniformly In tea-leaf power, and be uniformly mixed, extruding pelletization obtains soft profit tobacco particle;2) take the tobacco powders of 20 parts of 150-200 mesh with The soft profit tobacco particle mixing obtained in step (1) is round as a ball, sieving takes 10-40 mesh particle, 50 DEG C dry tobacco particle half at Product;3) it takes 1 part of povidone, 0.5 part of polyethylene glycol to be dissolved in 20 parts of water, processing is coated to aforementioned tobaccos pellet product, and Finished particle moisture 18% is controlled, tobacco particle needed for obtaining;4) tobacco particle for weighing certain mass is placed in special cylindrical cavity In mold, suitably press simultaneously microwave treatment 45s, quickly cooling to room temperature, and tobacco particle has been bonded to stick in mold, takes out up to institute Need low temperature fuming liquids.
Fillable be used as in corresponding low temperature cigarette smoking set or tobacco pipe of the low temperature fuming liquids sucks material, also can cigarette At cigarette shape for sucking, fuming rate is fast when sucking, and amount of smoke is sufficient and front and back uniformity is good, and puff number is more, aroma quality Well and there is light tea perfume, the moderate irritation of nicotine content is reduced.
Embodiment 3
In the present embodiment, the preparation method of low temperature fuming liquids includes the following steps:
1) mass parts are pressed, the tobacco powder of 100 parts of 120-200 mesh, the ramie pulp fiber of 30 parts of 100-200 mesh, 20 part of 150 purpose are taken Starch;12 parts of tobacco extracts, 10 parts of glycerol, 5 parts of propylene glycol, 10 parts of glycerine, 15 parts of water are taken, sprinkling after being mixed uniformly In above-mentioned tobacco powder and ramie pulp fiber, and be uniformly mixed, extruding pelletization obtains soft profit tobacco particle;2) 20 parts of 150-200 are taken Purpose tobacco powder mixes round as a ball, sieving with the soft profit tobacco particle and takes 10-40 mesh particle, and 50 DEG C dry to obtain tobacco particle half Finished product;3) it takes 1 part of povidone, 0.5 part of polyethylene glycol to be dissolved in 20 parts of water, processing is coated to aforementioned tobaccos pellet product, And control tobacco particle needed for finished particle moisture 18% obtains;4) tobacco particle for weighing certain mass is placed in special cylindrical cavity In mold, suitably press simultaneously microwave treatment 45s, quickly cooling to room temperature, and tobacco particle has been bonded to stick in mold, takes out up to institute Need low temperature fuming liquids.
Fillable be used as in corresponding low temperature cigarette smoking set or tobacco pipe of the low temperature fuming liquids sucks material, also can cigarette At cigarette shape for sucking, fuming rate is fast when sucking, and amount of smoke is sufficient and front and back uniformity is good, and puff number is more, aroma quality Good, the moderate irritation of nicotine content is reduced.
The content that above-described embodiment illustrates should be understood as that these embodiments are only used for being illustrated more clearly that the present invention, without For limiting the scope of the invention, after the present invention has been read, those skilled in the art are to various equivalent forms of the invention Modification each fall within the application range as defined in the appended claims.

Claims (10)

1. a kind of tobacco particle, which is characterized in that including particle bulk, the particle bulk include carrier, tobacco extract and Alevaire;The particle bulk is coated with coatings.
2. tobacco particle according to claim 1, which is characterized in that the carrier includes tobacco material and/or non-tobacco Material.
3. tobacco particle according to claim 2, which is characterized in that the non-tobacco material includes microcrystalline cellulose, tea At least one of leaf, ramie pulp fiber, bamboo fibre, cocoanut fiber, starch, coffee shell, dried peppermint leaf.
4. tobacco particle according to claim 1, which is characterized in that the quality of the carrier, tobacco extract, Alevaire Than for 120-200:1-15:5-30.
5. tobacco particle according to claim 1, which is characterized in that be additionally provided with cigarette between the particle bulk and coatings Last layer, it is preferable that the mass ratio of offal layer and particle bulk is 100:5-25.
6. tobacco particle according to claim 1, which is characterized in that the coatings include hydroxypropyl methyl cellulose, One of hydroxypropyl cellulose, povidone, sodium carboxymethylcellulose, microcrystalline cellulose, polyethylene glycol, polyvinyl alcohol are more Kind.
7. the preparation method of tobacco particle as claimed in any one of claims 1 to 6, which comprises the steps of:
Carrier, tobacco extract, Alevaire are uniformly mixed, are granulated, whole grain, particle bulk is obtained;
Coatings are prepared in the particle bulk surface that step (1) obtains, i.e. acquisition tobacco particle finished product.
8. preparation method according to claim 7, which is characterized in that between step (1) and step (2), further include The step of grain body surface prepares offal layer, i.e., after offal is wrapped up on particle bulk surface, low temperature drying obtains tobacco particle half Finished product.
9. a kind of low temperature fuming liquids, which is characterized in that including tobacco particle as claimed in any one of claims 1 to 6 or such as right It is required that the tobacco particle of the preparation of preparation method described in 7 or 8.
10. the preparation method of low temperature fuming liquids as claimed in claim 9, which is characterized in that the tobacco particle to be placed in into In pattern tool, curing molding obtains low temperature fuming liquids finished product;Preferably, effecive porosity is 65- inside the low temperature fuming liquids 95%。
CN201810486784.1A 2018-05-21 2018-05-21 Tobacco particles and preparation method thereof, low-temperature smoke body and preparation method thereof Active CN110506984B (en)

Priority Applications (6)

Application Number Priority Date Filing Date Title
CN201810486784.1A CN110506984B (en) 2018-05-21 2018-05-21 Tobacco particles and preparation method thereof, low-temperature smoke body and preparation method thereof
JP2020563970A JP7029553B2 (en) 2018-05-21 2019-03-19 Low temperature smoker and its manufacturing method
KR1020207036581A KR102583754B1 (en) 2018-05-21 2019-03-19 Low-temperature smoking body and method of manufacturing the same
PCT/CN2019/078652 WO2019223411A1 (en) 2018-05-21 2019-03-19 Low-temperature smoking body and preparation method therefor
US17/057,598 US20210401030A1 (en) 2018-05-21 2019-03-19 Low-temperature smoking body and preparation method thereof
EP19808374.3A EP3797602A4 (en) 2018-05-21 2019-03-19 Low-temperature smoking body and preparation method therefor

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CN110506984B CN110506984B (en) 2021-08-27

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111449271A (en) * 2020-04-09 2020-07-28 安徽中烟工业有限责任公司 Smoke release particle material containing biomass fibers and preparation method thereof
WO2021135583A1 (en) * 2019-12-31 2021-07-08 广东省金叶科技开发有限公司 Granular cigarette core material and preparation method therefor
CN113208146A (en) * 2021-04-02 2021-08-06 汉觅科技(福建)有限公司 Atomized smoking material for heating non-combustible product and preparation method thereof
CN114027541A (en) * 2021-11-02 2022-02-11 江苏大亚滤嘴材料有限公司 Preparation method of tobacco fragrant granules
CN114532618A (en) * 2022-02-28 2022-05-27 山东国瓷功能材料股份有限公司 Porous ceramic tape-casting slurry, porous ceramic atomizing core and preparation method

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CN104790264A (en) * 2015-05-05 2015-07-22 云南中烟工业有限责任公司 Functional low-gram-weight cigarette paper and preparation method thereof
CN106666811A (en) * 2016-07-18 2017-05-17 张秀勇 Novel cigarette and preparation method thereof
CN107307466A (en) * 2017-05-27 2017-11-03 浙江中烟工业有限责任公司 A kind of graininess heats incombustible tobacco matrixes and preparation method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN202385718U (en) * 2011-07-11 2012-08-22 湖北中烟工业有限责任公司 Novel coated perfuming sustained-release pellet
CN104790264A (en) * 2015-05-05 2015-07-22 云南中烟工业有限责任公司 Functional low-gram-weight cigarette paper and preparation method thereof
CN106666811A (en) * 2016-07-18 2017-05-17 张秀勇 Novel cigarette and preparation method thereof
CN107307466A (en) * 2017-05-27 2017-11-03 浙江中烟工业有限责任公司 A kind of graininess heats incombustible tobacco matrixes and preparation method thereof

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2021135583A1 (en) * 2019-12-31 2021-07-08 广东省金叶科技开发有限公司 Granular cigarette core material and preparation method therefor
CN111449271A (en) * 2020-04-09 2020-07-28 安徽中烟工业有限责任公司 Smoke release particle material containing biomass fibers and preparation method thereof
CN113208146A (en) * 2021-04-02 2021-08-06 汉觅科技(福建)有限公司 Atomized smoking material for heating non-combustible product and preparation method thereof
CN114027541A (en) * 2021-11-02 2022-02-11 江苏大亚滤嘴材料有限公司 Preparation method of tobacco fragrant granules
CN114532618A (en) * 2022-02-28 2022-05-27 山东国瓷功能材料股份有限公司 Porous ceramic tape-casting slurry, porous ceramic atomizing core and preparation method
CN114532618B (en) * 2022-02-28 2023-01-31 山东国瓷功能材料股份有限公司 Porous ceramic tape-casting slurry, porous ceramic atomizing core and preparation method

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