CN109512015B - Heating non-combustion solid essence for cigarettes and preparation method thereof - Google Patents
Heating non-combustion solid essence for cigarettes and preparation method thereof Download PDFInfo
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- CN109512015B CN109512015B CN201811267270.3A CN201811267270A CN109512015B CN 109512015 B CN109512015 B CN 109512015B CN 201811267270 A CN201811267270 A CN 201811267270A CN 109512015 B CN109512015 B CN 109512015B
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
Abstract
The invention relates to a heating non-combustion solid essence and a preparation method thereof, wherein the heating non-combustion solid essence contains natural extracts, microcrystalline cellulose, sodium carboxymethylcellulose and a smoke agent.
Description
[ technical field ] A method for producing a semiconductor device
The invention belongs to the technical field of tobacco processing. More particularly, the invention relates to a heating non-combustion solid essence for cigarettes and a preparation method of the heating non-combustion solid essence for cigarettes.
[ background of the invention ]
The cigarette which is heated without burning tobacco substances is a cigarette which heats tobacco substances through electronic equipment, does not generate open fire and cigarette ash in the smoking process of the cigarette, is environment-friendly, enables consumers to feel the fragrance of the tobacco when smoking the cigarette through the electronic heating equipment, reduces harmful substances generated by high-temperature pyrolysis in the burning of the conventional cigarette, provides an effective way for the healthy smoking of the consumers, and the smoking mode is more and more popular at home and abroad, and forms a consumer group with a considerable scale.
At present, materials such as paper-making thin sheets, dry thin sheets, thick paste thin sheets, coated forming paper and the like are mainly used in the heating and non-burning aroma-producing section sold in the market, the base materials of the materials are paper fibers, miscellaneous gas is brought when the materials are heated, the smoking quality is influenced, and less aroma substances are reduced and removed, so that the requirements of consumption on aroma and physiological satisfaction are difficult to meet.
Therefore, the present inventors have conducted a great deal of experiments and analyses to solve the technical drawbacks of the prior art, and finally completed the present invention.
[ summary of the invention ]
[ problem to be solved ]
The invention aims to provide a solid essence which is not burnt when being heated for cigarettes.
The invention also aims to provide a preparation method of the heating non-burning solid essence for cigarettes.
[ solution ]
The invention is realized by the following technical scheme.
The invention relates to a solid essence which is used for cigarettes and does not burn when being heated.
The invention relates to a solid essence which is not burnt when being heated, which comprises the following components: in parts by weight
The natural extract is a mixture of yunyan extract, a cocoa extract, a liquorice extract, a tree moss extract, a jujube extract, a plum extract and a fig extract;
the smoke agent is a mixture of propylene glycol, glycerol and glycerol diacetate.
According to a preferred embodiment of the present invention, the composition of the non-burning solid flavor is as follows: in parts by weight
According to another preferred embodiment of the present invention, in the natural extract, the weight ratio of yunyan extract, cocoa extract, licorice extract, tree moss extract, jujube extract, plum extract and fig extract is 50-70: 10-20: 5-10: 1-3: 3-9: 2-8: 5 to 10.
According to another preferred embodiment of the present invention, in the natural extract, the weight ratio of yunyan extract, cocoa extract, licorice extract, tree moss extract, jujube extract, plum extract and fig extract is 55-65: 12-18: 6-8: 1.6-2.4: 4-8: 3-6: 6-8.
According to another preferred embodiment of the present invention, in the smoking agent, the weight ratio of propylene glycol, glycerol and glycerol diacetate is 10 to 30: 20-40: 50-80 parts.
According to another preferred embodiment of the present invention, in the smoking agent, the weight ratio of propylene glycol, glycerol and glycerol diacetate is 14 to 26: 24-36: 58 to 72.
The invention also relates to a preparation method of the solid essence which is not burnt by heating.
The method comprises the following steps:
A. preparation of natural extracts
Mixing Yunyan extract, cocoa extract, licorice extract, tree moss extract, jujube extract, plum extract and fig extract according to a weight ratio of 50-70: 10-20: 5-10: 1-3: 3-9: 2-8: 5-10, mixing to obtain the natural extract;
B. preparation of a fuming agent
Mixing propylene glycol, glycerol and glycerol diacetate according to the weight ratio of 10-30: 20-40: 50-80 to obtain the smoke agent;
C. mixing
And (2) adding 0.08-2.6 parts by weight of microcrystalline cellulose and 0.08-1.0 part by weight of sodium carboxymethylcellulose into 76-130 parts by weight of the natural extract obtained in the step (A), uniformly mixing, injecting the obtained mixture into a mold, placing the mold into a drying oven, drying at 105-115 ℃ until the water content is below 5% by weight, spraying 0.8-1.6 parts by weight of smoke generating agent obtained in the step (B), and drying to obtain the solid essence which can not be burnt by heating.
According to a preferred embodiment of the present invention, the weight ratio of yunyan extract, cocoa extract, licorice extract, tree moss extract, jujube extract, plum extract and fig extract is 55-65: 12-18: 6-8: 1.6-2.4: 4-8: 3-6: 6-8.
According to another preferred embodiment of the present invention, the weight ratio of propylene glycol, glycerol and glycerol diacetate is 14-26: 24-36: 58 to 72.
According to another preferred embodiment of the invention, the mold has a cylindrical, pentagonal, rhombohedral, spherical, rectangular or cubic shape.
The present invention will be described in more detail below.
The invention relates to a solid essence which is used for cigarettes and does not burn when being heated.
The invention relates to a heating non-combustion solid essence for cigarettes, which comprises the following components: in parts by weight
The natural extract is a mixture of yunyan extract, a cocoa extract, a liquorice extract, a tree moss extract, a jujube extract, a plum extract and a fig extract;
the Yunyan tobacco extract is an additive which is prepared by scientifically extracting and processing high-quality Yunnan tobacco, does not contain any additive, can effectively improve the quality of cigarettes, increases the natural feeling of tobacco sheets and improves the Yunyan tobacco flavor of the cigarettes. The yunyan extract used in the present invention is a product currently marketed, for example, by kaifei spring flavor and fragrance limited company under the trade name yunyan alcohol extract. The basic function of the yunyan tobacco extract used in the invention in heating the non-burning solid essence is to provide the original fragrance of tobacco. When the other components in the natural extract are in the weight ratio range, if the weight ratio of the yunyan tobacco extract is lower than 50, the tobacco fragrance is thinner; if the weight ratio of the Yunyan tobacco extract is higher than 70, the smoke burred feeling is increased, and the throat choking phenomenon occurs, so that the weight ratio of the Yunyan tobacco extract is reasonable to be 50-70.
The cocoa extract used in the invention has the basic functions of increasing the thickness of smoke and increasing the smoke concentration in the solid essence which is not burnt by heating. The cocoa extract used in the present invention is a product currently marketed, for example, by kauri spring flavor and fragrance limited under the trade name of cocoa alcohol extract. In the natural extract, when other components are in the weight ratio range, if the weight ratio of the cocoa extract is lower than 10, smoke is empty, and the smoke concentration is reduced; if the weight ratio of cocoa extract is higher than 20, smoke is emitted and the lumping property is poor; therefore, the weight ratio of the cocoa extract is preferably 10 to 20.
The licorice extract used in the invention has the basic function of increasing the sweet note of smoke in the solid essence which is not burnt by heating. The licorice extract used in the present invention is a product currently marketed, for example, by kauri spring essence and flavor ltd under the trade name of licorice extract. In the natural extract, when other components are in the weight ratio range, if the weight ratio of the licorice extract is lower than 5, the smoke is bitter, and the sweet and charming feeling is poor; if the weight ratio of the licorice extract is higher than 10, the licorice green smell in the smoke is heavier; therefore, the weight ratio of the licorice extract is preferably 5 to 10.
The tree moss extract used in the invention has the basic function of enriching moss fragrance in smoke and increasing elegant smoke in the solid essence without burning during heating. The moss extract used in the present invention is a product currently marketed, for example, by kauri spring flavor and fragrance limited under the trade name of moss water extract. In the natural extract, when other components are in the weight ratio range, if the weight ratio of the tree moss extract is lower than 1, the richness of smoke is poor; if the weight ratio of the tree moss extract is higher than 3, the moss fragrance is too heavy and is not harmonious with smoke; therefore, the weight ratio of the tree moss extract is reasonable to be 1-3.
The basic function of the jujube extract used in the invention in the solid essence which is not burnt by heating is to increase the sweet smell of the jujube and cover up the miscellaneous gas. The jujube extract used in the present invention is a product currently marketed, for example, by kauri spring essence and flavor ltd under the trade name of jujube alcohol extract. When the weight ratio of other components in the natural extract is within the weight ratio range, if the weight ratio of the jujube extract is lower than 3, the miscellaneous gas is obvious, and the residue in the oral cavity is heavier; if the weight ratio of the jujube extract is higher than 9, the jujube has obvious sweet smell and is pressed to smoke; therefore, the weight ratio of the jujube extract is 3-9.
The basic functions of the plum extract used in the invention in heating the non-burning solid essence are to increase the sweet and sour taste of smoke, reduce stimulation and soften smoke. The ume extract used in the present invention is a product currently marketed, for example, by kauri spring essence and flavor ltd under the trade name ume alcohol extract. In the natural extract, when other components are in the weight ratio range, if the weight ratio of the plum extract is lower than 2, the smoke stimulation is enhanced, and the smoke is more explosive; if the weight ratio of the plum extract is higher than 8, the smoke is sour, and the taste is affected; therefore, the weight ratio of the plum extract is reasonable to be 2-8.
The fig extract used in the invention has the basic functions of increasing the sweetness of smoke and reducing the residue in the oral cavity in the solid essence which is not burnt by heating. The fig extract used in the present invention is a product currently marketed, for example, by kauri spring flavor and fragrance limited under the trade name fig alcohol extract. In the natural extract, when other components are in the weight ratio range, if the weight ratio of the fig extract is lower than 5, the residual weight of the oral cavity is heavy; if the weight ratio of the fig extract is higher than 10, the tobacco fragrance is pressed, and the smoke penetrability is poor; therefore, the weight ratio of fig extract is preferably 5 to 10.
According to the invention, in the natural extracts, the weight ratio of the yunyan extract, the cocoa extract, the licorice extract, the tree moss extract, the jujube extract, the plum extract and the fig extract is 50-70: 10-20: 5-10: 1-3: 3-9: 2-8: 5 to 10.
Preferably, in the natural extracts, the weight ratio of the yunyan extract, the cocoa extract, the licorice extract, the tree moss extract, the jujube extract, the plum extract and the fig extract is 55-65: 12-18: 6-8: 1.6-2.4: 4-8: 3-6: 6-8.
In the heating non-combustion solid essence, the main function of the smoke agent is to provide the smoke amount and the smoke moistening feeling during smoking. The smoke agent is a mixture of propylene glycol, glycerol and glycerol diacetate, wherein the propylene glycol is used for moistening smoke; the glycerol plays a role in atomization; the glycerol diacetate plays a role in fuming. The propylene glycol, glycerin and glyceryl diacetate used in the present invention are all commercially available products, such as glyceryl diacetate sold under the trade name diacetate by Shanghai Kanglang Biotech Co., Ltd.
In the smoke agent, when other components are in the weight ratio range, if the weight ratio of the propylene glycol is lower than 10, smoke is dried, and if the weight ratio of the propylene glycol is higher than 30, water vapor in the smoke is obvious and influences the smoking taste, so that the weight ratio of the propylene glycol is 10-30, which is suitable. Similarly, when the other components are within the above weight ratio range, if the weight ratio of glycerin is less than 20, the atomization effect is poor and the amount of smoke is small; if the weight ratio of the glycerol is higher than 40, the moisture in the smoke is increased, so that the smoking taste is poor; therefore, the weight ratio of the glycerol is 20-40. When the other components are in the weight ratio range, if the weight ratio of the glyceryl diacetate is lower than 50, the smoke generation amount is less, and if the weight ratio of the glyceryl diacetate is higher than 80, the smoke generation amount is too high, and the smoking experience is poor; therefore, the weight ratio of the glycerol diacetate is between 50 and 80.
Therefore, the weight ratio of the propylene glycol, the glycerol and the glycerol diacetate in the smoke agent is 10-30: 20-40: 50-80 parts.
Preferably, in the smoke agent, the weight ratio of the propylene glycol, the glycerol and the glycerol diacetate is 14-26: 24-36: 58 to 72.
In the heating non-combustion solid essence, the microcrystalline cellulose mainly plays a role as a bonding agent in the heating non-combustion solid essence to bond the essences together. The microcrystalline cellulose used in the present invention is a product currently marketed, for example, by Shandong Ningheng cellulose Co., Ltd under the trade name microcrystalline cellulose. The main function of the sodium carboxymethyl cellulose in the non-combustible solid essence is as a curing agent to play a role in curing. The sodium carboxymethylcellulose used in the present invention is also a product currently marketed, for example, by Shandong Yuheng cellulose Co., Ltd under the trade name sodium carboxymethylcellulose.
In the solid essence which is not combusted during heating and used for the cigarette, when other components are in the content range, if the content of the natural extract is lower than 76, the texture of smoke is poor, and the smoke is empty; if the content of the natural extract is higher than 130, the smoke concentration is higher, the oral cavity irritation is larger, and the smoking taste is influenced; therefore, the content of the natural extract is 76-130. Similarly, when the other components are in the content range, if the content of the microcrystalline cellulose is lower than 0.08, the solid essence is loose and is not beneficial to pumping; if the content of the microcrystalline cellulose is higher than 2.6, the miscellaneous gas is heavier during suction; therefore, the content of microcrystalline cellulose is preferably 0.08 to 2.6. When the other components are in the content range, if the content of the sodium carboxymethyl cellulose is lower than 0.08, the solid essence is soft in texture, fragile and difficult to pump; if the content of the sodium carboxymethylcellulose is higher than 1.0, the solid essence is hard in texture and is not beneficial to smoking; therefore, the content of sodium carboxymethylcellulose is preferably 0.08 to 1.0. When the other components are within the content range, if the content of the smoking agent is less than 0.8, the amount of smoke is small, and it is difficult to satisfy the psychological expectation of consumers; if the content of the smoke agent is higher than 1.6, the smoke is larger, and the smoking experience is influenced; therefore, the content of the smoke generating agent is preferably 0.8 to 1.6.
Therefore, the heating non-combustion solid essence for the cigarette comprises the following components: in parts by weight
Preferably, the heating non-combustion solid essence for the cigarette comprises the following components: in parts by weight
The invention also relates to a preparation method of the solid essence which is not burnt by heating.
The method comprises the following steps:
A. preparation of natural extracts
Mixing Yunyan extract, cocoa extract, licorice extract, tree moss extract, jujube extract, plum extract and fig extract according to a weight ratio of 50-70: 10-20: 5-10: 1-3: 3-9: 2-8: 5-10, mixing to obtain the natural extract;
B. preparation of a fuming agent
Mixing propylene glycol, glycerol and glycerol diacetate according to the weight ratio of 10-30: 20-40: 50-80 to obtain the smoke agent;
C. mixing
And (2) adding 0.08-2.6 parts by weight of microcrystalline cellulose and 0.08-1.0 part by weight of sodium carboxymethylcellulose into 76-130 parts by weight of the natural extract obtained in the step (A), uniformly mixing, injecting the obtained mixture into a mold, placing the mold into a drying oven, drying at 105-115 ℃ until the water content is below 5% by weight, spraying 0.8-1.6 parts by weight of smoke generating agent obtained in the step (B), and drying to obtain the solid essence which can not be burnt by heating.
Preferably, the weight ratio of the yunyan extract, the cocoa extract, the licorice extract, the tree moss extract, the jujube extract, the plum extract and the fig extract is 55-65: 12-18: 6-8: 1.6-2.4: 4-8: 3-6: 6-8.
Preferably, the weight ratio of the propylene glycol, the glycerol and the glycerol diacetate is 10-30: 20-40: 50-80 parts.
Details of the natural extract, microcrystalline cellulose, sodium carboxymethylcellulose and the smoke generator have been described above and are not described herein.
The mold used in the invention has a cylindrical, pentagonal, rhombohedral, spherical, cuboid or cubic shape. Of course, other shapes of the mold can be selected according to the actual needs, without any technical difficulties for the person skilled in the art.
The drying box used in the invention is sold on the market at present and is a commonly used drying box product at present.
In the invention, the water content is detected according to a method for detecting the moisture of GB/T23357-.
In the examples, a heating chamber suction device of different shape produced by Balanophora yunnanensis was used, the heating temperature was 300 ℃, the heating time was 3 minutes and 30 seconds, in contrast to an IUOC suction device sold by Shenzhen Yuanzhi Intelligent science and technology Limited, a photoelectric smoke sensor sold under the trade name of smoke alarm by Beijing Xinglong sensor science and technology development Limited was used, a closed three-way tube was made, 35ml of smoke was injected by an injector every time, and the detection was performed by using the photoelectric smoke sensor sold under the trade name of alarm by Beijing Xinglong sensor science and technology development Limited. The smoke amount is divided into three levels, namely low level (one bright lamp), middle level (two bright lamps) and high level (three bright lamps); sensory evaluation is carried out on cigarettes according to the GB5606.4-2005 standard, and the results are shown in the following table 1.
[ advantageous effects ]
The invention has the beneficial effects that:
the heating non-combustion aroma-producing section sold in the market at present mainly comprises materials such as paper-making sheets, dry-process sheets, thick pulp sheets, coated molding paper and the like, the main base materials of the materials are paper fibers, the paper fibers can bring offensive odor during heating, the smoking quality is influenced, and less aroma substances are reduced and removed, so that the requirements of consumers on aroma and physiological satisfaction are difficult to meet. The solid spice is directly heated, the aroma layering sense is rich and thick, compared with the commercially available non-burning heating cigarette bomb, the miscellaneous gas is obviously weakened, the process is simple, the solid spice can be suitable for non-burning heating devices with different specifications and shapes, the appearance and the shape are novel, and the psychological and physiological requirements of consumers are met.
[ detailed description ] embodiments
The invention will be better understood from the following examples.
Example 1: preparation of the invention heating non-combustion solid essence
The implementation steps of this example are as follows:
A. preparation of natural extracts
A yunyan extract sold under the trade name yunyan alcohol extract by kaihong spring flavor and fragrance limited, a cocoa extract sold under the trade name theobroma alcohol extract by kaihong spring flavor and fragrance limited, a licorice extract sold under the trade name glycyrrhizal alcohol extract by kaihong spring flavor and fragrance limited, a tree moss extract sold under the trade name water extract by kaihong spring flavor and fragrance limited, a jujube extract sold under the trade name jujube alcohol extract by kaihong spring flavor and fragrance limited, a plum extract sold under the trade name plum alcohol extract by kaihong spring flavor and fragrance limited, and a fig extract sold under the trade name fig alcohol extract by kaihong spring flavor and fragrance limited, are mixed in a weight ratio of 50: 12: 5: 1.6: 3: 3: 5, mixing to obtain the natural extract:
B. preparation of a fuming agent
Propylene glycol sold by shanghai kang biotechnology limited under the trade name PG, glycerol sold by shanghai kang biotechnology limited under the trade name glycerin, and glycerol diacetate sold by shanghai kang biotechnology limited under the trade name diacetate were mixed in a weight ratio of 10: 24: 50, mixing to obtain the smoke agent;
C. mixing
Adding 0.08 weight part of microcrystalline cellulose and 0.2 weight part of sodium carboxymethylcellulose into 88 weight parts of the natural extract prepared in the step A, uniformly mixing, injecting the obtained mixture into a cylindrical mold with the circumference of 25.0mm and the height of 50mm, placing the cylindrical mold into a drying oven, drying at 105 ℃ until the water content is 4.8 percent by weight, and spraying 0.8 weight part of the smoke agent prepared in the step B to obtain the solid essence which can not be burnt by heating.
The non-combustible solid essence prepared in this example was added to a cylindrical heating chamber of a non-combustible smoking set, and then subjected to sensory evaluation according to the method described in the specification of the present application, and the results thereof are listed in table 1 below.
Example 2: preparation of the invention heating non-combustion solid essence
The implementation steps of this example are as follows:
A. preparation of natural extracts
A yunyan extract sold under the trade name yunyan alcohol extract by kaihong spring flavor and fragrance limited, a cocoa extract sold under the trade name theobroma alcohol extract by kaihong spring flavor and fragrance limited, a licorice extract sold under the trade name glycyrrhizal alcohol extract by kaihong spring flavor and fragrance limited, a tree moss extract sold under the trade name water extract by kaihong spring flavor and fragrance limited, a jujube extract sold under the trade name jujube alcohol extract by kaihong spring flavor and fragrance limited, a plum extract sold under the trade name plum alcohol extract by kaihong spring flavor and fragrance limited, and a fig extract sold under the trade name fig alcohol extract by kaihong spring flavor and fragrance limited, are mixed in a weight ratio of 70: 18: 10: 2.4: 9: 6: 10 mixing to obtain the natural extract:
B. preparation of a fuming agent
Propylene glycol sold by shanghai kang biotechnology limited under the trade name PG, glycerol sold by shanghai kang biotechnology limited under the trade name glycerin, and glycerol diacetate sold by shanghai kang biotechnology limited under the trade name diacetate were mixed in a weight ratio of 14: 36: 80 to obtain the smoke agent;
C. mixing
Adding 2.6 parts by weight of microcrystalline cellulose and 0.8 part by weight of sodium carboxymethylcellulose into 112 parts by weight of the natural extract prepared in the step A, uniformly mixing, injecting the obtained mixture into a cuboid mold with a long side length of 50.0mm and a short side length of 18.0mm, placing the cuboid mold in a drying oven, drying at the temperature of 110 ℃ until the water content is 4.5 percent by weight, and spraying 1.0 part by weight of the smoke agent prepared in the step B to obtain the solid essence which can not be burnt by heating.
The solid essence prepared in this example and heated without combustion is added to a smoking set heated with a heating cavity in a rectangular parallelepiped shape and then subjected to sensory evaluation according to the method described in the specification of the application, and the results are listed in table 1 below.
Example 3: preparation of the invention heating non-combustion solid essence
The implementation steps of this example are as follows:
A. preparation of natural extracts
Yunyan extract sold under the trade name yunyan alcohol extract by kaihong spring flavor and fragrance limited, cacao extract sold under the trade name cacao alcohol extract by kaihong spring flavor and fragrance limited, glycyrrhiza extract sold under the trade name glycyrrhizal alcohol extract by kaihong spring flavor and fragrance limited, tree moss extract sold under the trade name tree moss water extract by kaihong spring flavor and fragrance limited, jujube extract sold under the trade name jujube alcohol extract by kaihong spring flavor and fragrance limited, plum extract sold under the trade name plum alcohol extract by kaihong spring flavor and fragrance limited, and fig extract sold under the trade name fig alcohol extract by kaihong spring flavor and fragrance limited, fig extracts are sold according to a weight ratio of 55: 10: 6: 1: 4: 2: 6, mixing to obtain the natural extract:
B. preparation of a fuming agent
Propylene glycol sold by shanghai kang biotechnology limited under the trade name PG, glycerol sold by shanghai kang biotechnology limited under the trade name glycerin, and glycerol diacetate sold by shanghai kang biotechnology limited under the trade name diacetate were mixed in a weight ratio of 26: 20: 58 to obtain the smoke agent;
C. mixing
And (2) adding 0.2 part by weight of microcrystalline cellulose and 0.08 part by weight of sodium carboxymethylcellulose into 76 parts by weight of the natural extract prepared in the step (A), uniformly mixing, injecting the obtained mixture into a diamond mould with the side length of 20.0mm and the height of 20.0mm, placing the diamond mould into a drying box, drying at the temperature of 115 ℃ until the water content is 4.9 percent by weight, and spraying 1.5 parts by weight of the smoke agent prepared in the step (B) to obtain the solid essence which can not be burnt by heating.
The non-combustible heating solid flavor prepared in this example was added to a non-combustible heating smoking set having a rhombic heating cavity, and then sensory evaluation was performed according to the method described in the specification of the present application, and the results are listed in table 1 below.
Example 4: preparation of the invention heating non-combustion solid essence
The implementation steps of this example are as follows:
A. preparation of natural extracts
A yunyan extract sold under the trade name yunyan alcohol extract by kaihong spring flavor and fragrance limited, a cocoa extract sold under the trade name theobroma alcohol extract by kaihong spring flavor and fragrance limited, a licorice extract sold under the trade name glycyrrhizal alcohol extract by kaihong spring flavor and fragrance limited, a tree moss extract sold under the trade name water extract by kaihong spring flavor and fragrance limited, a jujube extract sold under the trade name jujube alcohol extract by kaihong spring flavor and fragrance limited, a plum extract sold under the trade name plum alcohol extract by kaihong spring flavor and fragrance limited, and a fig extract sold under the trade name fig alcohol extract by kaihong spring flavor and fragrance limited, the fig extracts are sold according to a weight ratio of 65: 20: 8: 3: 8: 8: 8, mixing to obtain the natural extract:
B. preparation of a fuming agent
Propylene glycol sold by Shanghai Kanglang Biotech Co., Ltd under the trade name PG, glycerin sold by Shanghai Kanglang Biotech Co., Ltd under the trade name glycerin, and glyceryl diacetate sold by Shanghai Kanglang Biotech Co., Ltd under the trade name diacetate were mixed in a weight ratio of 30: 40: 72 mixing to obtain the smoke agent;
C. mixing
And (2) adding 2.0 parts by weight of microcrystalline cellulose and 1.0 part by weight of sodium carboxymethylcellulose into 130 parts by weight of the natural extract prepared in the step (A), uniformly mixing, injecting the obtained mixture into a cube mold with the side length of 20.0mm, placing the cube mold in a drying box, drying at the temperature of 110 ℃ until the water content is 4.2% by weight, and spraying 1.6 parts by weight of the smoke agent prepared in the step (B) to obtain the solid essence which is not burnt by heating.
The non-combustible heating solid essence prepared in this example was added to a non-combustible heating smoking set with a cube heating cavity, and then sensory evaluation was performed according to the method described in the specification of the present application, and the results are listed in table 1 below.
The samples prepared in examples 1 to 4 were designated as the sample of example 1, the sample of example 2, the sample of example 3 and the sample of example 4, respectively, sample B was a reconstituted tobacco heat non-combustible sample sold by fizeau international under the trade name IQOS cartridge, and sample C was a tobacco purple cloud sample sold by yunnan central tobacco industry ltd.
Table 1: smoke quantity and sensory evaluation results of different cigarette samples
The test results in table 1 show that: the cigarette which is prepared by the invention and is not burnt has greatly improved aroma, after the smoke agent is added, the smoke amount is superior to that of the existing reconstituted tobacco sheet and the conventional cigarette, the taste is comfortable, the aroma is beautiful, and the cigarette meets the psychological and physiological requirements of consumers.
Claims (8)
1. A solid essence which is used for cigarettes and does not burn when being heated is characterized by comprising the following components: in parts by weight
The natural extract is a mixture of yunyan extract, a cocoa extract, a liquorice extract, a tree moss extract, a jujube extract, a plum extract and a fig extract, and the weight ratio of the natural extract to the jujube extract is 50-70: 10-20: 5-10: 1-3: 3-9: 2-8: 5-10;
the smoke agent is a mixture of propylene glycol, glycerol and glycerol diacetate, and the weight ratio of the smoke agent is 10-30: 20-40: 50-80 parts.
2. A solid fragrance which does not burn on heating according to claim 1, characterized in that it consists of: in parts by weight
3. The solid essence not burning by heating according to claim 1, wherein in the natural extracts, the weight ratio of yunyan extract, cacao extract, licorice extract, tree moss extract, jujube extract, plum extract and fig extract is 55-65: 12-18: 6-8: 1.6-2.4: 4-8: 3-6: 6-8.
4. The solid essence capable of not being combusted by heating as claimed in claim 1, wherein in the smoking agent, the weight ratio of propylene glycol, glycerol and glycerol diacetate is 14-26: 24-36: 58 to 72.
5. The method for preparing the solid essence which is not burnt by heating according to claim 1 is characterized by comprising the following steps:
A. preparation of natural extracts
Mixing Yunyan extract, cocoa extract, licorice extract, tree moss extract, jujube extract, plum extract and fig extract according to a weight ratio of 50-70: 10-20: 5-10: 1-3: 3-9: 2-8: 5-10, mixing to obtain the natural extract;
B. preparation of a fuming agent
Mixing propylene glycol, glycerol and glycerol diacetate according to the weight ratio of 10-30: 20-40: 50-80 to obtain the smoke agent;
C. mixing
And (2) adding 0.08-2.6 parts by weight of microcrystalline cellulose and 0.08-1.0 part by weight of sodium carboxymethylcellulose into 76-130 parts by weight of the natural extract obtained in the step (A), uniformly mixing, injecting the obtained mixture into a mold, placing the mold into a drying oven, drying at 105-115 ℃ until the water content is below 5% by weight, spraying 0.8-1.6 parts by weight of smoke generating agent obtained in the step (B), and drying to obtain the solid essence which can not be burnt by heating.
6. The method for preparing the solid essence not burning by heating according to claim 5, wherein the weight ratio of the yunyan extract, the cocoa extract, the licorice extract, the tree moss extract, the jujube extract, the plum extract and the fig extract is 55-65: 12-18: 6-8: 1.6-2.4: 4-8: 3-6: 6-8.
7. The preparation method of the solid essence not burning by heating according to claim 5, wherein the weight ratio of the propylene glycol, the glycerol and the glycerol diacetate is 14-26: 24-36: 58 to 72.
8. The method for preparing the solid flavor without burning by heating as claimed in claim 5, wherein the mold has a shape of cylinder, pentagonal body, rhombohedral body, sphere, cuboid or cube.
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| CN107752122B (en) * | 2017-09-18 | 2020-04-07 | 四川三联卷烟材料有限公司 | Interlayer aroma-producing material for cigarette heated without burning and preparation method thereof |
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