CN110522083A - A kind of new tobacco products Alevaire and its preparation method and application - Google Patents
A kind of new tobacco products Alevaire and its preparation method and application Download PDFInfo
- Publication number
- CN110522083A CN110522083A CN201810513494.1A CN201810513494A CN110522083A CN 110522083 A CN110522083 A CN 110522083A CN 201810513494 A CN201810513494 A CN 201810513494A CN 110522083 A CN110522083 A CN 110522083A
- Authority
- CN
- China
- Prior art keywords
- alevaire
- parts
- electronic cigarette
- cyclopentene
- hydroxyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- MDYZKJNTKZIUSK-UHFFFAOYSA-N tyloxapol Chemical compound O=C.C1CO1.CC(C)(C)CC(C)(C)C1=CC=C(O)C=C1 MDYZKJNTKZIUSK-UHFFFAOYSA-N 0.000 title claims abstract description 33
- 235000019505 tobacco product Nutrition 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims abstract description 39
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims abstract description 18
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 18
- 238000010438 heat treatment Methods 0.000 claims abstract description 16
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 13
- WOPKYMRPOKFYNI-UHFFFAOYSA-N 2-hydroxycyclopent-2-en-1-one Chemical compound OC1=CCCC1=O WOPKYMRPOKFYNI-UHFFFAOYSA-N 0.000 claims abstract description 11
- 238000000889 atomisation Methods 0.000 claims abstract description 6
- 150000001875 compounds Chemical class 0.000 claims abstract description 4
- 150000002148 esters Chemical class 0.000 claims abstract description 3
- 241000208125 Nicotiana Species 0.000 claims description 33
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 33
- 239000003571 electronic cigarette Substances 0.000 claims description 19
- 239000000758 substrate Substances 0.000 claims description 18
- 239000000779 smoke Substances 0.000 claims description 10
- 238000005507 spraying Methods 0.000 claims description 8
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 claims description 5
- 229960002715 nicotine Drugs 0.000 claims description 5
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 claims description 5
- 239000000341 volatile oil Substances 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 3
- 238000007710 freezing Methods 0.000 claims description 3
- 230000008014 freezing Effects 0.000 claims description 3
- 238000007598 dipping method Methods 0.000 claims description 2
- 238000007639 printing Methods 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims 2
- BZKFMUIJRXWWQK-UHFFFAOYSA-N Cyclopentenone Chemical compound O=C1CCC=C1 BZKFMUIJRXWWQK-UHFFFAOYSA-N 0.000 claims 1
- 235000010358 acesulfame potassium Nutrition 0.000 claims 1
- 239000003595 mist Substances 0.000 claims 1
- 239000003921 oil Substances 0.000 claims 1
- 235000019504 cigarettes Nutrition 0.000 abstract description 8
- 238000012795 verification Methods 0.000 abstract description 2
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 7
- 239000003546 flue gas Substances 0.000 description 7
- 238000000034 method Methods 0.000 description 6
- 239000002304 perfume Substances 0.000 description 6
- 238000000576 coating method Methods 0.000 description 4
- 239000000284 extract Substances 0.000 description 4
- 239000011248 coating agent Substances 0.000 description 3
- 239000000243 solution Substances 0.000 description 3
- 206010067484 Adverse reaction Diseases 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- 230000006838 adverse reaction Effects 0.000 description 2
- 235000009508 confectionery Nutrition 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- 239000003205 fragrance Substances 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 230000008569 process Effects 0.000 description 2
- -1 traditional Alevaire Chemical compound 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- 206010013789 Dry throat Diseases 0.000 description 1
- 208000027418 Wounds and injury Diseases 0.000 description 1
- 239000012752 auxiliary agent Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- NWZXFAYYQNFDCA-UHFFFAOYSA-N cyclopenten-1-ol Chemical compound OC1=CCCC1 NWZXFAYYQNFDCA-UHFFFAOYSA-N 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 210000004919 hair shaft Anatomy 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 208000014674 injury Diseases 0.000 description 1
- 150000002576 ketones Chemical class 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 239000011259 mixed solution Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 210000001533 respiratory mucosa Anatomy 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 230000004936 stimulating effect Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 235000019605 sweet taste sensations Nutrition 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
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- Manufacture Of Tobacco Products (AREA)
Abstract
The present invention relates to a kind of new tobacco products Alevaires and its preparation method and application.The Alevaire contains 2- hydroxyl -2- cyclopentene-1-one；The volume fraction of the 2- hydroxyl -2- cyclopentene-1-one is between 10%-100%.The Alevaire also contains one of ester type compound, ethylene glycol, propylene glycol, glycerol or water or a variety of.By experimental verification, new tobacco products Alevaire provided by the present invention can adjust its state and atomization temperature at room temperature, improve heating and do not burn the organoleptic attribute of cigarette.
Description
Technical field
The present invention relates to a kind of new tobacco products Alevaires and its preparation method and application, belong to electronic cigarette technology neck
Domain.
Background technique
In recent years, the new tobacco productses such as low temperature cigarette, electronic cigarette are just in rapid rising.These new tobacco productses are full
While sufficient people's tobacco habit, the injury to human body is reduced, such as: it does not 1. need to burn, avoids the generation of tar, phase
It is smaller for conventional tobacco products harmfulness；2. reducing the burst size of PM2.5, the influence to public environment generation is relatively
It is small；3. the consumption feature with conventional tobacco products, adapts to and meets to a certain extent the tobacco consumption demand of consumer.
For new tobacco products in aspiration procedure, the fragrance of tobacco or cigarette is by the heating atomization to pipe tobacco or tobacco tar
And discharge.Alevaire is essential component part in new tobacco products.
Currently, Alevaire used in new tobacco products is mainly made of water, propylene glycol, glycerol, the content of three is logical
Often it is higher than 90%.Since propylene glycol and glycerol are all hygroscopic thick liquids, and there is apparent sweet taste, they are as Alevaire
When being widely used, in addition to stimulating respiratory mucosa, causes throat dry outer, also easily cause the adverse reactions such as sweet sense, reduce
The consumption experience of new tobacco products.
Summary of the invention
In order to solve the above technical problem, the present invention provides a kind of new tobacco products Alevaires.Compared to it is existing with
Water, glycerol, propylene glycol are the theme the Alevaire of ingredient, and advantage is mainly reflected in: being 1. solid under room temperature, can be improved heating
Do not burn the external appearance characteristic of tobacco product；2. atomization temperature is relatively low, the energy consumption in sucking process is reduced；3. alternative
The usage amount of traditional Alevaire such as traditional Alevaire, or reduction glycerol, ethylene glycol improves throat hair shaft, thorn in aspiration procedure
Swash the adverse reactions such as property and sweet sense.
The technical solution adopted in the present invention is as follows.
A kind of Alevaire, containing 2- hydroxyl -2- cyclopentene-1-one, volume fraction is between 10%-100%.
In the Alevaire, in addition to 2- hydroxyl -2- cyclopentene-1-one, can also contain other auxiliary agents, as ester type compound,
Ethylene glycol, propylene glycol, glycerol and water.
Preferably, the Alevaire includes the component of following parts by weight: 9-11 parts of -2- cyclopentene-1-one of 2- hydroxyl, glycerol
1-3 parts, 0.8-1.2 parts of water.
Preferably, the Alevaire includes the component of following parts by weight: 4-6 parts of -2- cyclopentene-1-one of 2- hydroxyl, second two
4-6 parts of alcohol, 9-11 parts of glycerol, 4-6 parts of water, can be 0.4-0.5 parts of nicotine, 0.7-0.9 parts of essential oil of tobaccos.
The source of the compound 2- hydroxyl -2- cyclopentene-1-one: from leaf tobacco extract extract to or chemical synthesis obtain
It arrives.
The freezing point of the Alevaire is unrestricted, and boiling point is lower than 250 DEG C.When for heating do not burn cigarette and atomization electricity
When sub- cigarette, freezing point is higher than 40 DEG C, and boiling point is lower than 250 DEG C.
The present invention also provides application of the above-mentioned Alevaire in tobacco product；The tobacco product is to heat the electronics that do not burn
Cigarette or Atmized electronic cigarrette.
The heating is not burnt electronic cigarette, includes: the substrate as made from pipe tobacco or reconstituted tobacoo, and be overlying on substrate surface,
The atomizing layer formed by above-mentioned Alevaire.
The load capacity of the atomizing layer can reach 0.1-2g/g substrate, i.e. mass percent 10%-200%；Preferably
1.5-2g/g substrate, i.e. mass percent 150%-200%.
The heating electronic cigarette that do not burn be superimposed with multilayer atomizing layer by multi-layer substrate and forms, and preferably replaces superposition；Wherein
The substrate number of plies is 2-6 layers, is preferred with 3-4 layers.Adhesion with higher between the atomizing layer and substrate.
The atomizing layer forms dotted, strip in substrate surface or other forms the shape to match according to actual needs.
It does not burn the preparation method of electronic cigarette the present invention also provides above-mentioned heating, comprising: Alevaire is passed through into spraying, leaching
Stain, the mode of printing are carried on substrate surface, are cooled to room temperature, and form atomizing layer, it is dry to get.
The spraying specifically: Alevaire is heated, substrate surface is sprayed at, is cooled to room temperature, atomizing layer is formed；It is described
Spraying temperature is 50-85 DEG C；It is preferred that 60-65 DEG C.
The dipping specifically: substrate is impregnated in Alevaire, room temperature is dried after taking-up, and it is dry, form atomizing layer.
The Atmized electronic cigarrette includes tobacco tar, above-mentioned Alevaire in smoke grenade.
The conventional tobacco tar that the tobacco tar is grasped by those skilled in the art, such as nicotine, essential oil of tobaccos.
One of preferably, following parts by weight of component: 2- hydroxyl -2- cyclopentene -1- is contained in the smoke grenade
4-6 parts of ketone, 4-6 parts of water, 9-11 parts of glycerol, 4-6 parts of ethylene glycol, 0.4-0.5 parts of nicotine, 0.7-0.9 parts of essential oil of tobaccos.
The specifically used method of the Alevaire, comprising: Alevaire is mixed with tobacco tar in proportion, by atomizer plus
Heat generates the dense flue gas of fragrance.
Experimental verification, when the heating for loading Alevaire do not burn temperature in electronic cigarette rise to 42-55 DEG C when, substrate surface is opened
Beginning becomes sticky, gets wet；When temperature rises to 240 DEG C, flue gas generates more obvious；When temperature rises to 260 DEG C, smoke perfume is dense in smog
It is thick.
When temperature rises to 35 DEG C in Atmized electronic cigarrette, tobacco tar viscosity is substantially reduced, and when being warming up to 230 DEG C, flue gas is generated
More obvious, when being warming up to 250 DEG C, smoke perfume is dense in smog.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the present invention for heating the electronic cigarette that do not burn.
Fig. 2 is the preparation principle schematic diagram of the present invention for heating the electronic cigarette that do not burn.
Specific embodiment
The following examples are used to illustrate the present invention, but are not intended to limit the scope of the present invention..
Embodiment 1 heats the preparation for the electronic cigarette that do not burn
5.0 grams of 2- hydroxyl -2- cyclopentene-1-ones extracted from tobacco leaf are taken, 60 DEG C is heated to, is sprayed at 2.5 grams of conventional smokes
Silk table face, is cooled to room temperature, and pipe tobacco surface forms 0.5-1 millimeters of thick coatings, at room temperature dry tack free, shape of the coating to pipe tobacco
Looks, color, flexibility etc. are without influence.
After tested, when the pipe tobacco temperature after spraying rises to 55 DEG C, surface starts to become sticky, get wet；Temperature rises to 240 DEG C
When, flue gas generates more obvious；When temperature rises to 260 DEG C, smoke perfume is dense in smog.
Embodiment 2 heats the preparation for the electronic cigarette that do not burn
It takes 5.0 grams to be dissolved in 10 grams of water from the 2- hydroxyl -2- cyclopentene-1-one that tobacco leaf extracts, takes 2.5 grams of conventional smokes
Silk, is soaked in above-mentioned 2- hydroxyl -2- cyclopentene-1-one solution 30 minutes, room temperature is dried after taking-up, pipe tobacco dry tack free.Cigarette
The variation such as pattern, color, flexibility of silk is unobvious.
Through detecting, heating atomization process is similar to Example 1, and when temperature rises to 55 DEG C, pipe tobacco becomes sticky, gets wet；Temperature liter
When to 240 DEG C, flue gas generates obvious；When temperature rises to 260 DEG C, smoke perfume is dense in smog.
Embodiment 3 heats the preparation for the electronic cigarette that do not burn
5.0 grams of chemically synthesized 2- hydroxyl -2- cyclopentene-1-ones are taken, are heated to 60 DEG C after 0.5 gram of water, 1 gram of glycerol is added
It dissolves, is cooled to room temperature solution spraying in 2.5 grams of pipe tobacco surfaces at 60 DEG C, pipe tobacco surface forms and has become 0.6-1.2 millimeters thick
Coating, dry tack free, coating are on the pattern of pipe tobacco, color, flexibility etc. without influence at room temperature.
When pipe tobacco temperature after spraying rises to 42 DEG C, surface starts to become sticky, get wet；When temperature rises to 245 DEG C, flue gas is generated
It is more obvious；When temperature rises to 260 DEG C, smoke perfume is dense in smog.
The preparation of 4 Atmized electronic cigarrette of embodiment
5.0 grams are taken to be dissolved in 5 grams of water, 10 grams of glycerol and 5 grams of second two from the 2- hydroxyl -2- cyclopentene-1-one that tobacco leaf extracts
In the mixed solution of alcohol composition, it is added tobacco tar (0.42 gram of nicotine, 0.8 gram of essential oil of tobaccos), stirs evenly, the cigarette of electronic cigarette is added
In bullet, seals and stand 24 hours at room temperature.
Smoke grenade is heated, when being heated to 35 DEG C, tobacco tar viscosity is substantially reduced, when being heated to 230 DEG C, flue gas generate compared with
To be obvious, when temperature rises to 250 DEG C, smoke perfume is dense in smog.
Although above the present invention is described in detail with a general description of the specific embodiments,
On the basis of the present invention, it can be made some modifications or improvements, this will be apparent to those skilled in the art.Cause
This, these modifications or improvements, fall within the scope of the claimed invention without departing from theon the basis of the spirit of the present invention.
Claims (10)
1. a kind of Alevaire, which is characterized in that contain 2- hydroxyl -2- cyclopentene-1-one；2- hydroxyl -2- the cyclopentene-1-one
Volume fraction between 10%-100%.
2. Alevaire according to claim 1, which is characterized in that also contain ester type compound, ethylene glycol, propylene glycol, sweet
One of oil or water are a variety of；
Preferably, the Alevaire includes the component of following parts by weight: 9-11 parts of -2- cyclopentene-1-one of 2- hydroxyl, glycerol 1-3
Part, 0.8-1.2 parts of water；
Alternatively,
Preferably, the Alevaire includes the component of following parts by weight: 4-6 parts of -2- cyclopentene-1-one of 2- hydroxyl, ethylene glycol 4-6
Part, it 9-11 parts of glycerol, 4-6 parts of water, can be 0.4-0.5 parts of nicotine, 0.7-0.9 parts of essential oil of tobaccos.
3. Alevaire according to claim 1 or 2, which is characterized in that the freezing point of the Alevaire is higher than 40 DEG C, boiling point
Lower than 250 DEG C.
4. application of any Alevaire of claim 1-3 in tobacco product；Preferably, the tobacco product is to heat not
Burn electronic cigarette or Atmized electronic cigarrette.
5. a kind of heating does not burn electronic cigarette, characterized by comprising: the substrate as made from pipe tobacco or reconstituted tobacoo, and is overlying on
Substrate surface, the atomizing layer formed by any Alevaire of claim 1-3.
The electronic cigarette 6. heating according to claim 5 is not burnt, which is characterized in that the load capacity of the atomizing layer is quality
Percentage 10%-200%；It is preferred that 150%-200%.
The electronic cigarette 7. heating according to claim 5 or 6 is not burnt, which is characterized in that described to heat the electronic cigarette that do not burn
It is superimposed and is formed with multilayer atomizing layer by multi-layer substrate, is preferably alternately superimposed；Wherein the substrate number of plies is 2-6 layers, preferably 3-4 layers.
8. not burnt electronic cigarette according to any heating of claim 5-7, which is characterized in that the atomizing layer is in substrate table
Face forms dotted, strip or other forms the shape to match according to actual needs.
The preparation method of electronic cigarette 9. a kind of heating is not burnt characterized by comprising by any mist of claim 1-3
Agent is carried on substrate surface by way of spraying, dipping, printing, is cooled to room temperature, and forms atomizing layer, it is dry to get；
The spraying temperature is 50-85 DEG C.
10. a kind of Atmized electronic cigarrette, which is characterized in that include tobacco tar, any atomization of claim 1-3 in its smoke grenade
Agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810513494.1A CN110522083A (en) | 2018-05-25 | 2018-05-25 | A kind of new tobacco products Alevaire and its preparation method and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201810513494.1A CN110522083A (en) | 2018-05-25 | 2018-05-25 | A kind of new tobacco products Alevaire and its preparation method and application |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN110522083A true CN110522083A (en) | 2019-12-03 |
Family
ID=68657001
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201810513494.1A Pending CN110522083A (en) | 2018-05-25 | 2018-05-25 | A kind of new tobacco products Alevaire and its preparation method and application |
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| Country | Link |
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| CN (1) | CN110522083A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110946320A (en) * | 2019-12-12 | 2020-04-03 | 河南卷烟工业烟草薄片有限公司 | Damp-proof heating non-combustion reconstituted tobacco, preparation method and application |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102499432A (en) * | 2011-10-14 | 2012-06-20 | 湖南中烟工业有限责任公司 | Method of improving process-bearing property of volatile sweet spice in tobacco slice flavoring |
| CN104256888A (en) * | 2014-08-07 | 2015-01-07 | 江苏中烟工业有限责任公司 | Heat-sensitivity electronic tobacco juice and preparation of heat-sensitivity electronic tobacco juice |
| CN208550023U (en) * | 2018-05-25 | 2019-03-01 | 中国科学院理化技术研究所 | A kind of new tobacco products |
-
2018
- 2018-05-25 CN CN201810513494.1A patent/CN110522083A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102499432A (en) * | 2011-10-14 | 2012-06-20 | 湖南中烟工业有限责任公司 | Method of improving process-bearing property of volatile sweet spice in tobacco slice flavoring |
| CN104256888A (en) * | 2014-08-07 | 2015-01-07 | 江苏中烟工业有限责任公司 | Heat-sensitivity electronic tobacco juice and preparation of heat-sensitivity electronic tobacco juice |
| CN208550023U (en) * | 2018-05-25 | 2019-03-01 | 中国科学院理化技术研究所 | A kind of new tobacco products |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110946320A (en) * | 2019-12-12 | 2020-04-03 | 河南卷烟工业烟草薄片有限公司 | Damp-proof heating non-combustion reconstituted tobacco, preparation method and application |
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