CN104068467B - A kind of tobacco juice for electronic smoke being rich in plant flavone - Google Patents

A kind of tobacco juice for electronic smoke being rich in plant flavone Download PDF

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CN104068467B
CN104068467B CN201410312006.2A CN201410312006A CN104068467B CN 104068467 B CN104068467 B CN 104068467B CN 201410312006 A CN201410312006 A CN 201410312006A CN 104068467 B CN104068467 B CN 104068467B
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extract
flavone
tobacco
plant
root
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CN104068467A (en
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宁敏
周顺
何庆
徐迎波
张亚平
王孝峰
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China Tobacco Anhui Industrial Co Ltd
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China Tobacco Anhui Industrial Co Ltd
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Abstract

The invention discloses a kind of tobacco juice for electronic smoke being rich in plant flavone, its raw material is configured to by mass percentage: propane diols 50-70%, glycerine 5-10%, deionized water 5-15%, natural flavone extract 5-15%, tobacco extract 4-8%, flavouring essence for tobacco 2-6%, thickener 2-6%.Wherein natural flavone extract is the extract obtained by steam distillation or ethanol extraction plant mixture, and in general flavone, general flavone content is 20-50%; Described plant mixture is made up of Chu chrysanthemum, orrisroot, propolis, orange peel, grape, peanut skin, lily, the root of kudzu vine, the root of large-flowered skullcap, Rosa roxburghii, green tea.Tobacco juice for electronic smoke of the present invention can not only meet the smoking demand of smoker, and the plant flavone be simultaneously rich in has effect that is anti-oxidant, anti-aging, immunity moderation power, and also has certain health-care effect to cardiovascular and cerebrovascular.

Description

A kind of tobacco juice for electronic smoke being rich in plant flavone
One, technical field
The present invention relates to a kind of tobacco juice for electronic smoke, specifically a kind of tobacco juice for electronic smoke being rich in plant flavone.
Two, background technology
At present, under the macroeconomic situation that various countries' Tobacco use control continues reinforcement and economic growth continued downturn, World tobacco industry development is faced with abnormal severe risk and challenge.Particularly due to smoking and healthy relation, tobacco endures social disputes to the fullest extent always.For smoking and the health demand of satisfied different consumer, novel tobacco goods achieve in recent years and develop comparatively fast, mainly comprise smoke-free tobacco product, low temperature cigarette and electronic cigarette.
Electronic cigarette and electronics nicotine delivery device, invented by Chinese the earliest and create.It is not containing tobacco, main by the vaporous thing of tobacco juice atomization formation is sucked oral cavity.Electronic cigarette generally by tobacco juice, atomizer and battery rod three part form.Atomizer is powered by battery rod, tobacco juice in cigarette bullet can be transformed into fog, thus allows user have a kind of sensation of similar smoking when inhaling, and realizes " swallowing clouds and blowing out fog ".Electronic cigarette does not produce the harmful components such as tar, and in addition, the tobacco juice through atomization is diluted rapidly in atmosphere, does not have side-stream smoke, and can not form second-hand-cigarette harm, be a kind of cigarette substitute popular gradually.
Research proves, smoking can accelerate the aging of people, reduces the immunity of people.Although electronic cigarette reduces the harm of passive smoking, but still do not solve these problems of active smoker.
Flavone compound refers to the compounds general name that two phenyl ring are connected by the ring that three carbochains are formed.At first, the semifinished product of this kind of material only as application, the twenties in 20th century, abroad Quercetin, rutin be used for clinical after, just cause the concern of people.At the end of the sixties, it is found that flavone compound has anti-inflammatory, antiviral, cholagogic, cardiac stimulant, the effect such as calmness and analgesia.To the seventies, find that again they have anti-oxidant, anti-ageing, immunological regulation and the effect such as antitumor.All contain a certain amount of flavone compound in the leaf of many plants, skin, root and fruit, these natural flavone molecular weights, can be absorbed rapidly by human body, all obtain utilization at present in the industry such as cosmetics, health products.The plant of abundant flavone content comprises chrysanthemum, propolis, the root of kudzu vine, oranges and tangerines, grape, tealeaves etc.Such as, research proves, the rutin be rich in chrysanthemum, Quercetin and Isoquercitrin have very strong scavenging activated oxygen (O 2-) and the effect of hydroxy radical (OH); Scullcap total-flavonoid has removing O 2-prevent the snperoxiaized effect of biomembrane with OH, also can significantly suppress OH to the damaging action of DNA, be the main component of root of large-flowered skullcap antioxidation; In addition, some other flavone compound such as oldenlandia diffusa flavones, licoflavone, total seabuckthorn flavone, blumea flavanones etc. all have scavenging free radicals or lipoid peroxidization resistant.
Tobacco juice for electronic smoke is the key factor affecting suction quality, tobacco juice of the present invention is made up of the natural plant extracts being rich in plant flavone, while meeting smoker's smoking demand, ensureing flue gas mouthfeel, there is effect that is anti-oxidant, anti-aging, immunity moderation power, and also have certain health-care effect to cardiovascular and cerebrovascular.
Three, summary of the invention
The present invention aims to provide a kind of tobacco juice for electronic smoke being rich in plant flavone, can either meet the smoking demand of smoker, can remove human free radical again, and anti-oxidant, anti-aging, immunity moderation power, also has certain health-care effect to cardiovascular and cerebrovascular.
The composition that the tobacco juice for electronic smoke of plant flavone is rich in the present invention is configured to by mass percentage:
Propane diols 50-70%, glycerine 5-10%, deionized water 5-15%, natural flavone extract 5-15%, tobacco extract 4-8%, flavouring essence for tobacco 2-6%, thickener 2-6%.
Each raw material is uniformly mixed at normal temperatures and obtains tobacco juice for electronic smoke above.
Described natural flavone extract adds in flask by plant mixture and distilled water, the quality of distilled water is 20 times of plant mixture quality, be heated to reflux and be incubated 2 hours, collect distillate, gained distillate filtered and obtains after being concentrated into 1/10th of original volume; Or plant mixture and absolute ethyl alcohol are added in flask, the quality of absolute ethyl alcohol is 20 times of plant mixture quality, is heated to reflux extraction 2 hours, and extract filters and to obtain after being concentrated into 1/10th of original volume.
In natural flavone extract, flavones content calculates with general flavone, and general flavone content is 20-50%; Assay method reference literature [1], take rutin as standard, in general flavone extract, add Al (NO 3) 3solution, makes chromocor compound and aluminium salt form stable colored complex, measures absorbance, calculate general flavone content with calibration curve method at wavelength 510nm place.
In described plant mixture, each component is configured to by mass percentage: Chu chrysanthemum 8-15%, mythical bird like the phoenix root of the tail 8-15%, propolis 8-15%, orange peel 6-10%, grape pip 8-15%, peanut skin 4-8%, lily 4-8%, root of kudzu vine 6-10%, root of large-flowered skullcap 4-8%, Rosa roxburghii 4-8%, green tea 2-6%.
Described tobacco extract is preferably Zimbabwe's leaf tobacco extract.
Tobacco extract in raw material of the present invention is commercial, purchased from Guangzhou Huabao Flavor Co., Ltd..
Described thickener is selected from one or more in guar gum, carragheen, sodium alginate, agar, sodium carboxymethylcellulose, network protein acid sodium.
Zhang Guangcheng etc. [2]by kudzuvine root isoflavone, lipid peroxidation product (LPO) content in animal tissue and superoxide dismutase (SOD) activity are studied, inquire into the anti-radical action of kudzuvine root isoflavone compounds.Experiment in vitro shows, kudzuvine root isoflavone 0.01-1.0g/L can obviously suppress Mouse Liver, nephridial tissue and too the even spring of white rabbit brain tissue raise at the LPO that causes under rose incubation conditions of shaking, and have dose-effect relationship.Zhang Erxian etc. [3]by chrysanthemum extract to Fe 2+bring out the inhibitory action of lipovitellinin PuFA peroxidating system, TBAs generation structure and pyrogallol-Luminol luminescence system, have studied the antioxidation activity of the different extracts of chrysanthemum.Result shows. Chrysan Yellow ketone compounds has removes OH, O 2-deng the ability of free radical, and there is stronger antioxidation activity, and find that chrysanthemum antioxidation activity is relevant to flavonoid content.
The harm of tobacco juice for electronic smoke without second-hand-cigarette of plant flavone is rich in the present invention, therefore also can use completely in public, can not only meet smoker's smoking demand, and can not affect other people health.Meanwhile, be rich in plant flavone composition in natural flavone extract, can be absorbed rapidly by human body, thus have the effect of very strong anti-oxidant and scavenging free radicals, this antioxidation can stop degeneration, the aging of cell, also can stop the generation of cancer.
In addition, flavones can also improve blood circulation, can reduce cholesterol, reduces the incidence of disease of cardiovascular and cerebrovascular disease, also can improve the symptom of cardiovascular and cerebrovascular disease.
Bibliography:
[1] Zhang Zhiliang, the Zhai Wei mountain valley with clumps of trees and bamboo. plant physiology experiment instructs [M]. Beijing: Higher Education Publishing House, 2003,173-175
[2] Zhang Guangcheng, Fang Si ring. the antioxidation of kudzuvine root isoflavone, Tongji Medical Univ's journal, 1997,26 (5), 340-342
[3] Zhang Erxian, Fang Li etc. the antioxidation activity research of chrysanthemum extract, Food Science, 2000,21 (10), 6-8
Four, detailed description of the invention
Below in conjunction with embodiment, the solution of the present invention is described further.
The tobacco extract used in the embodiment of the present invention is purchased from Zimbabwe of Guangzhou Huabao Flavor Co., Ltd. leaf tobacco extract.
Embodiment 1:
The composition being rich in the tobacco juice for electronic smoke of plant flavone in the present embodiment is configured to by mass percentage:
Propane diols 70%, glycerine 5%, deionized water 5%, natural flavone extract 10%, tobacco extract 4%, flavouring essence for tobacco 4%, thickener 2%.
Described natural flavone extract adds in flask by plant mixture and 20 quality distilled water doubly, be heated to reflux and be incubated 2 hours, collecting distillate, gained distillate is filtered and be concentrated into do after obtain.In natural flavone extract, flavones content calculates with general flavone, is 27%.
In described plant mixture, each component is configured to by mass percentage: Chu chrysanthemum 8%, mythical bird like the phoenix root of the tail 15%, propolis 15%, orange peel 10%, grape pip 8%, peanut skin 4%, lily 8%, the root of kudzu vine 10%, the root of large-flowered skullcap 8%, Rosa roxburghii 8%, green tea 6%.
Described thickener by guar gum and carragheen in mass ratio 1:1 form.
Embodiment 2:
The composition being rich in the tobacco juice for electronic smoke of plant flavone in the present embodiment is configured to by mass percentage:
Propane diols 50%, glycerine 8%, deionized water 15%, natural flavone extract 15%, tobacco extract 8%, flavouring essence for tobacco 2%, thickener 2%.
Described natural flavone extract adds in flask by plant mixture and 20 quality distilled water doubly, be heated to reflux and be incubated 2 hours, collecting distillate, gained distillate is filtered and be concentrated into do after obtain.In natural flavone extract, flavones content calculates with general flavone, is 39%.
In described plant mixture, each component is configured to by mass percentage: Chu chrysanthemum 15%, mythical bird like the phoenix root of the tail 13%, propolis 15%, orange peel 10%, grape pip 15%, peanut skin 8%, lily 8%, the root of kudzu vine 6%, the root of large-flowered skullcap 4%, Rosa roxburghii 4%, green tea 2%.
Described thickener by sodium alginate, agar, sodium carboxymethylcellulose and network protein acid sodium in mass ratio 1:1:1:1 form.
Embodiment 3:
The composition being rich in the tobacco juice for electronic smoke of plant flavone in the present embodiment is configured to by mass percentage:
Propane diols 58%, glycerine 10%, deionized water 12%, natural flavone extract 5%, tobacco extract 5%, flavouring essence for tobacco 6%, thickener 4%.
Described natural flavone extract adds in flask by plant mixture and 20 quality absolute ethyl alcohol doubly, be heated to reflux extraction 2 hours, extract filters and be concentrated into do after obtain.In natural flavone extract, flavones content calculates with general flavone, is 32%.
In described plant mixture, each component is configured to by mass percentage: Chu chrysanthemum 10%, mythical bird like the phoenix root of the tail 7%, propolis 12%, orange peel 8%, grape pip 15%, peanut skin 8%, lily 8%, the root of kudzu vine 10%, the root of large-flowered skullcap 8%, Rosa roxburghii 8%, green tea 6%.
Described thickener is guar gum.
Embodiment 4:
The composition being rich in the tobacco juice for electronic smoke of plant flavone in the present embodiment is configured to by mass percentage:
Propane diols 67%, glycerine 8%, deionized water 8%, natural flavone extract 5%, tobacco extract 4%, flavouring essence for tobacco 2%, thickener 6%.
Described natural flavone extract adds in flask by plant mixture and 20 quality absolute ethyl alcohol doubly, be heated to reflux extraction 2 hours, extract filters and be concentrated into do after obtain.In natural flavone extract, flavones content calculates with general flavone, is 46%.
In described plant mixture, each component is configured to by mass percentage: Chu chrysanthemum 15%, mythical bird like the phoenix root of the tail 15%, propolis 8%, orange peel 6%, grape pip 15%, peanut skin 8%, lily 8%, the root of kudzu vine 10%, the root of large-flowered skullcap 6%, Rosa roxburghii 4%, green tea 5%.
Described thickener is configured to by mass percentage: guar gum 30%, sodium carboxymethylcellulose 45%, agar 18%, network protein acid sodium 7%.

Claims (1)

1. be rich in a tobacco juice for electronic smoke for plant flavone, it is characterized in that its raw material is configured to by mass percentage:
Propane diols 50-70%, glycerine 5-10%, deionized water 5-15%, natural flavone extract 5-15%, tobacco extract 4-8%, flavouring essence for tobacco 2-6%, thickener 2-6%;
Described natural flavone extract adds in flask by plant mixture and distilled water, the quality of distilled water is 20 times of plant mixture quality, be heated to reflux and be incubated 2 hours, collect distillate, gained distillate filtered and obtains after being concentrated into 1/10th of original volume; Or described natural flavone extract adds in flask by plant mixture and absolute ethyl alcohol, the quality of absolute ethyl alcohol is 20 times of plant mixture quality, is heated to reflux extraction 2 hours, and extract filters and to obtain after being concentrated into 1/10th of original volume;
In described plant mixture, each component is configured to by mass percentage: Chu chrysanthemum 8-15%, mythical bird like the phoenix root of the tail 8-15%, propolis 8-15%, orange peel 6-10%, grape pip 8-15%, peanut skin 4-8%, lily 4-8%, root of kudzu vine 6-10%, root of large-flowered skullcap 4-8%, Rosa roxburghii 4-8%, green tea 2-6%;
Described tobacco extract is Zimbabwe's leaf tobacco extract;
Described thickener is selected from one or more in guar gum, carragheen, sodium alginate, agar, sodium carboxymethylcellulose, network protein acid sodium.
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