CN115844050A - Mixed alcohol electronic cigarette atomized liquid and preparation method thereof - Google Patents
Mixed alcohol electronic cigarette atomized liquid and preparation method thereof Download PDFInfo
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- CN115844050A CN115844050A CN202211638488.1A CN202211638488A CN115844050A CN 115844050 A CN115844050 A CN 115844050A CN 202211638488 A CN202211638488 A CN 202211638488A CN 115844050 A CN115844050 A CN 115844050A
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Abstract
The application relates to a mixed alcohol electronic cigarette atomized liquid and a preparation method thereof, wherein the atomized liquid comprises the following raw materials in parts by weight: 5-10 parts of tobacco extract, 5-7 parts of plant softener, 1-3 parts of cool feeling agent, 0.5-0.7 part of stabilizer, 3-5 parts of essence material and 45-55 parts of mixed alcohol; wherein the plant softening agent comprises flos Lonicerae juice, fructus Rosae Normalis juice, green tea juice, mannan and pectin; the mixed alcohol comprises 1, 2-propylene glycol, glycerol and polyethylene glycol. The preparation method of the atomized liquid comprises the following steps: s1, adding mixed alcohol, a plant softening agent, a tobacco extract and a cooling agent into a matrix solvent, and uniformly mixing; and S2, adding a stabilizer and the essence, and uniformly mixing to obtain the mixed alcohol electronic cigarette atomized liquid. This application has the taste of sucking that promotes electron smog spinning disk atomiser, reduces the effect of irritability.
Description
Technical Field
The application relates to the field of electronic cigarettes, in particular to a mixed alcohol electronic cigarette atomized liquid and a preparation method thereof.
Background
Electronic cigarettes, also known as electronic nicotine delivery systems, are products or devices that inhale into the lungs a chemical mixture (usually a hydraulic mixture) that is heated and vaporized electronically. Most electronic cigarettes contain tobacco or nicotine components, but also a few electronic cigarettes do not contain tobacco or nicotine components. The electronic cigarette is a novel tobacco product which is developed most rapidly in recent years, people can obtain a satisfactory smoking feeling by smoking the electronic cigarette, the requirement of tobacco consumers can be met, the harm of smoking to the environment can be avoided, and the possibility that non-smoking people inhale second-hand smoke is reduced.
Propylene glycol and glycerol (glycerin) are commonly used in the existing electronic cigarette atomized liquid, the glycerin and the propylene glycol are pyrolyzed in the atomization process to form some irritant gases, and the irritations of the gases on throat, oral mucosa and the like are easily caused, and the influence on the smoking taste of the atomized liquid is also caused.
Aiming at the problems, the inventor thinks that the existing electronic cigarette atomized liquid has the defects of poor smoking taste and strong irritation.
Disclosure of Invention
In order to promote the smoking taste of the electronic cigarette atomized liquid and reduce the irritation, the application provides the mixed alcohol electronic cigarette atomized liquid and the preparation method thereof.
First aspect, the application provides a mix alcohol electron smog spinning disk atomiser adopts following technical scheme:
the mixed alcohol electronic cigarette atomized liquid comprises the following raw materials in parts by weight:
5-10 parts of tobacco extract, 5-7 parts of plant softener, 1-3 parts of cool feeling agent, 0.5-0.7 part of stabilizer, 3-5 parts of essence material and 45-55 parts of mixed alcohol;
the plant softener comprises honeysuckle juice, roxburgh rose juice, green tea juice, mannan and pectin; the mixed alcohol comprises 1, 2-propylene glycol, glycerol and polyethylene glycol (PEG 400).
By adopting the technical scheme, the atomized liquid is heated into a gaseous state at the moment of electronic cigarette suction, the temperature of the atomized liquid is rapidly reduced after the components in the atomized liquid are gasified through the suction channel, and a large number of small-particle liquid drops are formed; the components such as honeysuckle juice, roxburgh rose juice, green tea juice, mannan and the like doped in the plant softener in the atomized liquid can play a role in protecting and moistening when irritant gas generated by alcohol solvents stimulates the throat of a user, alleviate the irritant feeling caused by the irritant gas and further bring fresh and moist comfort to the throat of the user;
this application is through selecting for use multiple mellow wine to mix the complex formulation, has reduced the pungent gas that alcohol solvent produced from the root, and the active ingredient in the gentle agent of rethread plant further softly alleviates amazing for the atomized liquid atomizing effect that this application made is better, and the taste is soft sweet, and has strengthened the protection to the person's throat, and is safe more healthy.
Preferably, the mixed alcohol consists of polyethylene glycol 38-48% wt, 1, 2-propylene glycol 25-30% wt and glycerol balance.
By adopting the technical scheme, the compatibility of various alcohols in the mixed alcohol is better, the good capacity-increasing dispersion of each component in the atomized liquid is facilitated, the generation of irritant gas can be reduced when the atomized liquid is gasified, after the gas is condensed into small liquid drops, the particle size of the small liquid drops is mostly concentrated in the range of 0.02-0.05 mu m by the matching of the mixed alcohol component, the particles are not easy to agglomerate, and then the atomized liquid is less irritant when being sucked, and the taste is mild and fine.
Preferably, the plant softening agent consists of honeysuckle juice 30-35 wt%, green tea juice 20-30 wt%, mannan 5-7 wt%, pectin 3-5 wt% and roxburgh rose juice balance.
By adopting the technical scheme, the honeysuckle has the effects of clearing throat and reducing internal heat, the moisturizing performance of the roxburgh rose fruits is better, tea polyphenol and caffeine in green tea are used for refreshing and restoring consciousness, honeysuckle juice, roxburgh rose juice and green tea juice are adopted in the application, compared with extract powder, the juice can keep the activity of plant active ingredients better, and can be better matched with mannan and pectin, so that the prepared plant softener is mild and stable in performance, and is easier to atomize in the atomizing liquid atomizing process, the grain size after atomization is smaller, the retention of the active ingredients is better, and the effect of moisturizing and protecting is achieved.
Preferably, the preparation method of the plant softener comprises the following steps:
step 1, adding fresh honeysuckle into water, boiling the juice and removing residues to obtain honeysuckle juice;
step 2, selecting golden yellow mature fresh roxburgh rose fruits, cleaning, draining, squeezing, and taking the supernatant after standing to obtain roxburgh rose juice; step 3, selecting fresh green tea, boiling in boiling water for 10min, and filtering to obtain green tea juice;
and 4, uniformly mixing the honeysuckle juice, the roxburgh rose juice, the green tea juice, the mannan and the pectin according to the limited mass percentage to obtain the plant softener.
By adopting the technical scheme, the preparation process is simple, the components are uniformly mixed, the plant softener with a stable system can be obtained, and the plant softener is added into an atomized liquid system, can play a better protective and moistening role when a smoker takes the food, relieves irritation and improves the taste of the atomized liquid.
Preferably, the stabilizer is prepared by mixing xanthan gum and pectin according to a mass ratio of 1.2.
By adopting the technical scheme, the stabilizer prepared by compounding the xanthan gum and the pectin can be added into the atomized liquid to realize good bonding of all components in the system, and the pectin in the stabilizer can be compatible with the pectin in the plant softener, so that the fusibility and stability of the plant softener in the atomized liquid system are further improved, a better stable and soft effect is achieved, the mouthfeel of the atomized liquid is improved, and the irritation is alleviated.
Preferably, the cooling agent is one or two of menthol and menthyl lactate.
By adopting the technical scheme, the cooling agent selects the mint components, so that a good cooling and refreshing effect can be achieved, the mint cooling effect can slow down stimulation to a certain extent, the cooling and moistening effect of the plant softening agent on throat is further amplified, and the effect is stable and lasting.
Preferably, the essence is prepared from the following raw materials in parts by mass: 1-3 parts of ethyl vanillin, 1-3 parts of isomalt, 0.5-0.7 part of dihydroactinidiolide, 0.3-0.5 part of maltol, 0.1-0.3 part of ethyl benzoate, 8-10 parts of water and 10-20 parts of propylene glycol.
Through adopting above-mentioned technical scheme, the essence material that is prepared by the complex formulation of above-mentioned multiple component on the one hand can be better melt in the atomized liquid system, for the atomized liquid provides better fragrance, and on the other hand, the essence material that this application was prepared through above-mentioned component can cooperate the stabilizer to a certain extent, and then promotes the stability of atomized liquid system, reduces the segregation phenomenon of atomized liquid storage in-process.
In a second aspect, the preparation method of the mixed alcohol electronic cigarette atomized liquid provided by the application adopts the following technical scheme:
a preparation method of mixed alcohol electronic cigarette atomized liquid comprises the following steps:
s1, adding mixed alcohol, a plant softening agent, a tobacco extract and a cooling agent into a matrix solvent, and uniformly mixing;
and S2, adding a stabilizer and the essence, and uniformly mixing to obtain the mixed alcohol electronic cigarette atomized liquid.
By adopting the technical scheme, the main active components in the atomized liquid are added firstly, so that the plant softener, the tobacco extract and the mixed alcohol are uniformly mixed, and finally the stabilizer and the essence are added to regulate and control the viscosity performance and the fragrance of the atomized liquid basic system, so that the prepared atomized liquid has the effects of soft and smooth mouthfeel.
In summary, the present application includes at least one of the following beneficial technical effects:
1. according to the electronic cigarette atomizing liquid, the plant softener is added into the electronic cigarette atomizing liquid, the mixed alcohol is selected, and the various alcohols in the mixed alcohol are well matched, so that on one hand, the generation of irritant gas can be reduced, on the other hand, aerosol particles formed by the atomized liquid have small particle size and are not easy to aggregate, the atomizing effect of the atomized liquid is further refined, and the fine taste of the atomized liquid is improved; the components such as honeysuckle juice, roxburgh rose juice, green tea juice, mannan and the like doped in the plant softener in the atomized liquid can play a role in protecting and moistening when irritant gas generated by alcohol solvents stimulates the throat of a user, alleviate the irritant feeling caused by the irritant gas and further bring fresh and moist comfort to the throat of the user; by the matching of the mixed alcohol and the plant softener, the stimulation of the alcohol solvent to the throat of a user is reduced fundamentally, and the throat is further moistened and softened, so that the atomized liquid prepared by the method is soft and sweet in taste, and is safer and healthier;
2. adopted in this application plant softener is honeysuckle juice, roxburgh rose juice and green tea juice, compare in the extract powder, the juice more can keep plant active ingredient's activity to the cooperation of realization and mannan and pectin that can be better, thereby make the mild stability of plant softener performance that makes, at atomizing liquid atomizing in-process, atomize more easily, the particle diameter after the atomizing is less, and active ingredient retentivity is better, plays the effect of moisturizing protection more.
Detailed Description
The present application will be described in further detail with reference to examples and comparative examples.
Preparation example
Preparation example 1
Preparation example 1 discloses a preparation method of a plant softener, which specifically comprises the following steps:
step 1, adding fresh honeysuckle into water, wherein the ratio of material to water is 1:10, boiling for 15min at 70-80 ℃, and filtering the honeysuckle to obtain honeysuckle juice;
step 2, selecting golden yellow mature roxburgh rose fruit, cleaning, draining, juicing, standing and layering juice, and taking supernatant to obtain roxburgh rose juice;
step 3, selecting fresh green tea, boiling the green tea in boiling water for 10min at a material-water ratio of 1;
and 4, uniformly mixing 3g of honeysuckle juice, 4.2g of roxburgh rose juice, 2g of green tea juice, 0.5g of mannan and 0.3g of pectin to obtain the plant softening agent.
Preparation example 2
Preparation example 2 discloses a preparation method of a plant softener, which is different from preparation example 1 in that: in the step 4, 3.5g of honeysuckle juice, 2.3g of roxburgh rose juice, 3g of green tea juice, 0.7g of mannan and 0.5g of pectin are uniformly mixed to obtain the plant softening agent.
Preparation example 3
Preparation example 3 discloses a preparation method of a plant softener, which is different from preparation example 1 in that: in the step 4, 3.3g of honeysuckle juice, 3.2g of roxburgh rose juice, 2.5g of green tea juice, 0.6g of mannan and 0.4g of pectin are uniformly mixed to obtain the plant softening agent.
Preparation example 4
Preparation example 4 discloses a preparation method of a plant softener, which is different from preparation example 1 in that: in step 4, replacing mannan and pectin with equal amount of Sucus Rosae Normalis.
Preparation example 5
Preparation example 5 discloses a preparation method of a plant softener, which is different from preparation example 1 in that: in step 4, replacing the green tea juice, mannan and pectin with the same amount of roxburgh rose juice.
Preparation example 6
Preparation example 6 discloses a preparation method of a plant softener, which is different from preparation example 1 in that: in the step 4, the honeysuckle juice, the green tea juice, the mannan and the pectin are replaced by the same amount of the roxburgh rose juice.
Preparation example 7
Preparation example 7 discloses a preparation method of mixed alcohol, specifically comprising: 3.8g of polyethylene glycol, 2.5g of 1, 2-propylene glycol and 3.7g of glycerol were mixed and added to the flask, and the mixture was stirred by magnetic force to obtain a mixed alcohol.
Preparation example 8
Preparation example 8 discloses a preparation method of a mixed alcohol, specifically comprising: 4.8g of polyethylene glycol, 3g of 1, 2-propylene glycol and 2.2g of glycerol are mixed and added into a flask, and the mixture is stirred uniformly by magnetic force to obtain mixed alcohol.
Preparation example 9
Preparation example 9 discloses a preparation method of a mixed alcohol, specifically: 4.3g of polyethylene glycol, 2.7g of 1, 2-propylene glycol and 3g of glycerol are mixed and added into a flask, and the mixture is stirred uniformly by magnetic force to obtain mixed alcohol.
Preparation example 10
Preparation example 10 discloses a method for preparing a mixed alcohol, specifically: 5g of polyethylene glycol and 5g of glycerol are mixed and added into a flask, and the mixture is stirred uniformly by magnetic force to obtain mixed alcohol.
Preparation example 11
Preparation example 11 discloses a preparation method of mixed alcohol, specifically: 5g of 1, 2-propylene glycol and 5g of glycerol were mixed and added to the flask, and the mixture was stirred by magnetic force to obtain a mixed alcohol.
Preparation example 12
Preparation example 12 discloses a preparation method of a spice, specifically comprising: mixing ethyl vanillin 1g, isomalt 1g, dihydroactinidiolide 0.5g, maltol 0.3g, ethyl benzoate 0.1g, water 8g and propylene glycol 10g, and stirring at 100r/min for 10min to obtain essence.
Preparation example 13
Preparation example 13 discloses a preparation method of a spice, specifically comprising: mixing 3g ethyl vanillin, 3g isomalt, 0.7g dihydroactinidiolide, 0.5g maltol, 0.3g ethyl benzoate, 10g water and 20g propylene glycol, and stirring at 100r/min for 10min to obtain essence.
Preparation example 14
Preparation example 14 discloses a preparation method of a spice, specifically comprising: mixing 2g ethyl vanillin, 2g isomalt, 0.6g dihydroactinidiolide, 0.4g maltol, 0.2g ethyl benzoate, 9g water and 15g propylene glycol, and stirring at 100r/min for 10min to obtain essence.
Examples
Examples 1 to 3
Embodiment 1-3 discloses a mixed alcohol electronic cigarette aerosol comprising the following raw materials in parts by weight:
5-10 parts of tobacco extract, 5-7 parts of plant softener, 1-3 parts of cool feeling agent, 0.5-0.7 part of stabilizer, 3-5 parts of essence material and 45-55 parts of mixed alcohol; wherein, the plant softening agent, the mixed alcohol and the essence are prepared by the preparation examples.
Embodiments 1-3 also disclose a method for preparing the above mixed alcohol electronic cigarette aerosol, comprising the steps of:
s1, mixing the mixed alcohol, the plant softener, the tobacco extract and the cool feeling agent, and stirring for 5min at the speed of 1000 r/min;
and S2, adding the stabilizer and the essence, and continuously stirring for 5min at the speed of 1000r/min to obtain the mixed alcohol electronic atomized liquid.
The amounts (unit: g) of the feed components added in examples 1 to 3 are specified in Table 1.
TABLE 1
Comparative example
Comparative examples 1 to 3
Comparative examples 1 to 3 disclose a method for preparing a mixed alcohol electronic atomized liquid, which is different from example 3 in that: the plant softening agent prepared in preparation examples 4-6 is selected correspondingly.
Comparative examples 4 to 5
Comparative examples 4 to 5 disclose a method for preparing a mixed alcohol electronic atomized liquid, which is different from example 3 in that: the mixed alcohols obtained in preparation examples 10 and 11 were used as the mixed alcohols, respectively.
Comparative example 6
Comparative example 6 discloses a method for producing a mixed alcohol electronic atomization liquid, which is different from example 3 in that: the plant softening agent is replaced by equal amount of mixed alcohol.
Performance test
Experiment 1, aerosol particle size detection of atomized liquid: simulated smoking of the electronic cigarette aerosol prepared in the examples and the comparative examples is performed by using a Smoking Cycle Simulator (SCS) (Cambustion, cambridge, UK), and then the particle size of the exhaled smoke is detected by using a DMS500 rapid particle size spectrometer (Cambustion, cambridge, UK) analysis system, and the particle size distribution range (nm), the median (nm) of the particle size and the unit volume number concentration (per cm/cm) of the aerosol are measured 3 )。
Experiment 2, sensory evaluation: 45 male smokers, which were 25 to 35 years old and randomly divided into 9 groups of 5 persons, were selected, the electronic atomization liquids prepared in the examples and comparative examples of the present application were respectively smoked using the same type of electronic cigarette, and the feeling of the test samples after use was evaluated by scoring, with the scoring criteria shown in table 2 below; wherein the first gear is 8-10 points, the second gear is 6-8 points, the third gear is 4-6 points, the fourth gear is 2-4 points, the fifth gear is 0-2 points, and the 0 point is 0 point (the score of each gear does not contain a left end point value); and after the scores are scored, taking an average value, and calculating a total score by using the average value to obtain a final score.
TABLE 2
The performance testing data for experiments 1-2 are detailed in tables 3-4.
TABLE 3
TABLE 4
According to the performance test data of the examples 1-3 in the tables 3-4, the aerosol particles of the atomized liquid prepared in the examples 1-3 of the present application have a small median diameter, and most of the particle diameters are concentrated in the range of 10-55nm, so that the atomized liquid prepared in the examples 1-3 of the present application has a fine and dense atomized particle and a good atomization effect, and the atomized liquid prepared in the examples 1-3 is evaluated by sensory tests, the total evaluation score of the sensory evaluation of the atomized liquid prepared in the examples 1-3 is over 140, and the atomized liquid prepared in the examples 1-3 of the present application has high evaluation on the irritation sensation, taste and smoke amount, and further, the atomized liquid of the electronic cigarette prepared in the examples 1-3 of the present application has a clear and moist taste, no irritation, moderate smoke amount and good flavor.
Honeysuckle juice, roxburgh rose juice, green tea juice, these components of mannan and pectin have been added to the plant softener in this application, honeysuckle and roxburgh rose fruit can play the protection effect of moisturizing to the larynx throat, tea polyphenol and caffeine in the green tea can the refreshing brain, the cooperation of these plant active ingredient in addition mannan and pectin, thereby make the mild stability of plant softener performance that makes, in the atomizing liquid atomization process, it atomizes more easily, slow down the stimulation of alcohol solvent to the larynx throat, play the effect of more outstanding protection of moisturizing. The plant softener prepared in preparation examples 4 to 6 is used in comparative examples 1 to 3 respectively, honeysuckle juice, green tea juice, mannan and pectin in the plant softener are replaced by roxburgh rose juice in preparation examples 4 to 6 respectively, the replaced plant softener lacks related components, the effect of mutual cooperation of various plant active ingredients in example 3 is difficult to achieve, and further the atomized liquid prepared in comparative examples 1 to 3 has reduced overall performance evaluation in sensory performance tests, and particularly has obvious astringent taste.
Compared with the common atomized liquid, the atomized liquid adopts a mixed alcohol design, the mixed alcohol is formed by mixing 1, 2-propylene glycol, glycerol and polyethylene glycol according to a specific proportion, on one hand, the addition of the mixed alcohol can be beneficial to the good capacity-increasing dispersion of all components in the atomized liquid, and the generation of irritant gas can be reduced during the gasification of the atomized liquid, on the other hand, the particle size of aerosol formed after the mixed alcohol is gasified and condensed is in a small range, and the particles are not easy to agglomerate, so that the atomized liquid is small in irritation when being sucked, and the mouth feel is fine and mild. The mixed alcohols obtained in production examples 10 and 11 were selected in comparative examples 4 to 5, and one component of the mixed alcohols was removed from production examples 10 and 11, so that the above-mentioned good synergistic effect was hardly formed between the components of the mixed alcohols obtained in production examples 10 and 11, and the atomization effect and irritation to the throat were directly affected, and the atomized liquids obtained in comparative examples 4 to 5 were low in sensory evaluation.
Compared with the prior art, the plant softener is replaced by the equal amount of mixed alcohol, the atomization effect is mainly controlled by mixing the mixed alcohol and the plant softener together, the stimulation is reduced, the mouth feeling flavor of the atomized liquid is improved, the atomized liquid without the plant softener is obviously reduced in mouth feeling, and the integral sensory evaluation of the atomized liquid is lower due to the fact that the throat irritation is larger.
The above embodiments are preferred embodiments of the present application, and the protection scope of the present application is not limited by the above embodiments, so: all equivalent changes made according to the structure, shape and principle of the present application shall be covered by the protection scope of the present application.
Claims (8)
1. The utility model provides a mixed alcohol electron smog liquid which characterized in that: the feed comprises the following raw materials in parts by weight:
5-10 parts of tobacco extract, 5-7 parts of plant softener, 1-3 parts of cool feeling agent, 0.5-0.7 part of stabilizer, 3-5 parts of essence material and 45-55 parts of mixed alcohol;
the plant softener comprises honeysuckle juice, roxburgh rose juice, green tea juice, mannan and pectin; the mixed alcohol comprises 1, 2-propylene glycol, glycerol and polyethylene glycol.
2. The mixed alcohol electronic cigarette aerosol of claim 1, wherein: the mixed alcohol is composed of polyethylene glycol 38-48 wt%, 1, 2-propylene glycol 25-30 wt% and glycerol balance.
3. The mixed alcohol electronic cigarette aerosol according to claim 1 or 2, characterized in that: the plant softening agent comprises 30-35 wt% of flos Lonicerae juice, 20-30 wt% of green tea juice, 5-7 wt% of mannan, 3-5 wt% of pectin and the balance of fructus Rosae Normalis juice.
4. The mixed alcohol electronic cigarette aerosol of claim 3, wherein: the preparation method of the plant softener comprises the following steps:
step 1, taking fresh honeysuckle, adding the fresh honeysuckle into water, boiling the juice, and removing residues to obtain honeysuckle juice;
step 2, selecting golden yellow mature fresh roxburgh rose fruits, cleaning, draining, squeezing, and taking the supernatant after standing to obtain roxburgh rose juice;
step 3, selecting fresh green tea, boiling in boiling water for 10min, and filtering to obtain green tea juice;
and 4, uniformly mixing the honeysuckle juice, the roxburgh rose juice, the green tea juice, the mannan and the pectin according to the limited mass percentage to obtain the plant softener.
5. The mixed alcohol electronic cigarette aerosol according to claim 1 or 2, characterized in that: the stabilizer is prepared by mixing xanthan gum and pectin according to the mass ratio of 1.
6. The mixed alcohol electronic cigarette aerosol according to claim 1 or 2, characterized in that: the cooling agent is one or two of menthol and menthyl lactate.
7. The mixed alcohol electronic cigarette aerosol according to claim 1 or 2, characterized in that: the essence is prepared from the following raw materials in parts by mass:
1-3 parts of ethyl vanillin, 1-3 parts of isomalt, 0.5-0.7 part of dihydroactinidiolide, 0.3-0.5 part of maltol, 0.1-0.3 part of ethyl benzoate, 8-10 parts of water and 10-20 parts of propylene glycol.
8. A method for preparing the mixed alcohol electronic cigarette atomized liquid of any one of claims 1 to 7, wherein the method comprises the following steps: the method comprises the following steps:
s1, adding mixed alcohol, a plant softening agent, a tobacco extract and a cooling agent into a matrix solvent, and uniformly mixing;
and S2, adding a stabilizer and a essence, and uniformly mixing to obtain the mixed alcohol electronic cigarette atomized liquid.
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| CN202211638488.1A CN115844050A (en) | 2022-12-19 | 2022-12-19 | Mixed alcohol electronic cigarette atomized liquid and preparation method thereof |
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| CN202211638488.1A CN115844050A (en) | 2022-12-19 | 2022-12-19 | Mixed alcohol electronic cigarette atomized liquid and preparation method thereof |
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