CN104489906A - Electronic cigarette liquid with China spirits aroma - Google Patents
Electronic cigarette liquid with China spirits aroma Download PDFInfo
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- CN104489906A CN104489906A CN201410788700.1A CN201410788700A CN104489906A CN 104489906 A CN104489906 A CN 104489906A CN 201410788700 A CN201410788700 A CN 201410788700A CN 104489906 A CN104489906 A CN 104489906A
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- tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/241—Extraction of specific substances
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- A24F47/002—
Abstract
The invention provides electronic cigarette liquid with China spirits aroma. The electronic cigarette liquid with the China spirits aroma comprises, by weight, 1-30% of tobacco extracts, 0.5-10% of tobacco essence, 0.5-15% of Maotai spirits, 0.5-10% of taste aroma regulators, 1-15% of deionized water, 1-25% of edible glycerol and the balance propylene glycol. The electronic cigarette liquid with the China spirits aroma has the advantages that the extracts of tobacco subjected to cellaring in a Maotai spirits cellar serve as raw materials and are added with the Maotai spirits, so that the cigarette liquid has not only unique intrinsic aroma but also the intense China spirits aroma; the electronic cigarette liquid can meet the requirements of consumers on taste and aroma, the taste and the aroma of existing electronic cigarette liquid are improved, the gap between the electronic cigarette liquid and traditional cigarettes in taste and aroma is narrowed, and the demands of the consumers for smoking electronic cigarettes are further met.
Description
Technical field
The invention belongs to electronic cigarette technical field, be specifically related to a kind of state aroma tobacco juice for electronic smoke.
Background technology
The relation of " smoking with healthy " becomes the problem that people receive much concern for a long time.Scientific research shows, the main source be detrimental to health in cigarette is the cigarette smoke because tobacco product is produced by a series of process such as high-temp combustion, cracking, distillation, enters caused by human body by sucking.Therefore the mode the most direct reducing harmfulness of smoking eliminates cigarette smoke exactly.The Application and Development of Novel smokeless gas tobacco product had both met WHO and fitness-for-all requirement, can meet again the demand of smoking consumer to smoking property of cigarette.Smoke-free tobacco product mainly contains hot type smoke-free tobacco product, containing cigarette, chewing tobacco, snuff and electronic cigarette etc.At present, electronic cigarette international market increases Novel smokeless gas tobacco product the most rapidly.
Electronic cigarette is the electronic atomized utensil copying traditional cigarette to be convenient for carrying, and by atomization utensil, the solution mist containing nicotine is changed into particulate, directly sucks human body.Its basic structure is generally made up of battery rod, atomizer and cigarette bullet three part.Electronic cigarette does not in use participate in burning, does not produce tar, carbon monoxide and other harmful substances, does not produce " second-hand-cigarette " yet, do not pollute public's environment, do not have disaster hidden-trouble, have profound significance to public health and environmental protection.Usual electronic cigarette does not adopt tobacco material itself, and therefore it is located in once emerging " substitute of tobacco " and " smoking cessation product ", thus has attracted the eyeball of numerous smoking cessation consumer to a certain extent, and has guided the consumer psychology of consumer.
But current commercially available electronic cigarette smoke agent majority is the dilute solution only containing nicotine, and its taste, fragrance can not meet the demand that consumer sucks completely, especially fragrance problem, have investigation display, domestic electronic cigarette market presents atrophy trend.Therefore be necessary the mouthfeel and the fragrance that improve existing tobacco juice for electronic smoke, shorten the gap of tobacco juice for electronic smoke in mouthfeel and fragrance and traditional cigarette, meet consumer further to the demand of sucking electronic cigarette.
Summary of the invention
The shortcoming of prior art in view of the above, the object of the present invention is to provide a kind of state aroma tobacco juice for electronic smoke, for solving the problem of existing tobacco juice for electronic smoke deficiency in mouthfeel and fragrance in prior art.
For achieving the above object and other relevant objects, the invention provides a kind of state aroma tobacco juice for electronic smoke, its raw materials by weight meter, comprises following component:
Leaf tobacco extract: 1-30%;
Flavouring essence for tobacco: 0.5-10%;
Maotai: 0.5-15%;
Mouthfeel fragrance conditioning agent: 0.5-10%;
Deionized water: 1-15%;
Edible glycerol: 1-25%;
Propane diols: surplus.
Preferably, a kind of state aroma tobacco juice for electronic smoke, its raw materials by weight meter, comprises following component:
Leaf tobacco extract: 1-30%;
Flavouring essence for tobacco: 0.5-10%;
Maotai: 0.5-15%;
Mouthfeel fragrance conditioning agent: 0.5-10%;
Deionized water: 1-15%;
Edible glycerol: 1-25%;
Propane diols: 30-70%.
Optimally, a kind of state aroma tobacco juice for electronic smoke, its raw materials by weight meter, comprises following component:
Leaf tobacco extract: 8-20%;
Flavouring essence for tobacco: 1.5-6%;
Maotai: 5-10%;
Mouthfeel fragrance conditioning agent: 1.5-6%;
Deionized water: 1-5%;
Edible glycerol: 10-20%;
Propane diols: 40-60%.
Leaf tobacco extract described in the present invention can adopt method conventional in prior art to obtain.
Preferably, described leaf tobacco extract is selected from any one or a few mixing in flue-cured tobacco, burley tobaccos, Turkish tobaccos or Sun cured tobacco extract.Further, described leaf tobacco extract is that cured tobacco leaf is through extracting the extract obtained.
Preferably, the extracting method of described leaf tobacco extract is: get tobacco leaf pulverizing, screening from Maotai wine cellar after, with extraction, then after carrying out ultrasonic extraction, through sedimentation, filtration and reduced pressure concentration, i.e. obtained leaf tobacco extract.
Preferably, the raw tobacco material of described leaf tobacco extract stores sth. in a cellar alcoholization in Maotai wine cellar.The flavor matter of aroma is infiltrated in tobacco leaf equably, the quality making its tobacco leaf more alcohol and.
Preferably; described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3; 5; 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine, 2; any multiple combination in 3,5-trimethylpyrazine.
Further, the total content of described flavouring essence for tobacco with percentage by weight shared by flavouring essence for tobacco in described state aroma tobacco juice for electronic smoke for benchmark.
Further, described flavouring essence for tobacco is selected from 1-8% Ethyl vanillin, 1-5% benzyl acetate, 1-8% furfural, 4-20% dorinone, 2-15% β-damascone, 10-30% Megastigmatrienone, 2-9% dihydroactinidiolide, 1-8% dimethyl succinate, 1-5%2, 6, 6-trimethyl-2-cyclohexene-1, 4-diketone, 1-5%2-hydroxyl-3, 5, 5-trimethyl-2-cyclonene, 3-15% geranyl acetone, 5-30% alpha, beta-lonone, 3-15% phenmethylol, 2-7% palmitic acid, 1-4% isovaleric acid, 1-4%2-methylvaleric acid, 1-3% indoles, 1-3% pyridine, 1-3%3-acetylpyridine, 1-5%2, 3, any multiple combination in 5-trimethylpyrazine.Above-mentioned tobacco flavor components content with 100% weight percent meter.
More preferably, described flavouring essence for tobacco comprises 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Described component mixes in vortex oscillator.Above-mentioned tobacco flavor components content with 100% weight percent meter.
More preferably, described flavouring essence for tobacco comprises 15% dorinone, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol.Component mixes in vortex oscillator.Above-mentioned tobacco flavor components content with 100% weight percent meter.
Preferably, described Maotai is the product of Kweichow Moutai Co., Ltd..Described Maotai is that market is bought.
Preferably, described mouthfeel fragrance conditioning agent is selected from any multiple combination in normal propyl alcohol, ethyl acetate, 2-methyl isophthalic acid-propyl alcohol, 3-methyl-butanal, 2-methyl-1-butene aldehyde, ethyl propionate, acetal, 2-methvl-propionic acid ethvl ester, ethyl butyrate, ethyl lactate, ethyl 2-methylbutyrate, 3 Methylbutanoic acid ethyl ester, furfuryl alcohol, ethyl valerate, benzaldehyde, ethyl hexanoate, phenmethylol, cognac oil, ethyl caprilate.
Further, the formula (weight percent meter) of described mouthfeel fragrance conditioning agent is selected from normal propyl alcohol 1.5-3.0%, ethyl acetate 5.5-7.0%, 2-methyl isophthalic acid-propyl alcohol 1.0-2.0%, 3-methyl-butanal 1.0-2.0%, 2-methyl-1-butene aldehyde 1.5-2.5%, ethyl propionate 1.0-2.5%, acetal 9.0-14.0%, 2-methvl-propionic acid ethvl ester 0.1-1.0%, ethyl butyrate 4.0-5.5%, ethyl lactate 1.0-2.5%, ethyl 2-methylbutyrate 0.3-1.5%, 3 Methylbutanoic acid ethyl ester 1.0-2.0%, furfuryl alcohol 3.5-5.0%, ethyl valerate 2.0-3.0%, benzaldehyde 2.0-3.0%, ethyl hexanoate 15-20%, phenmethylol 25-35%, cognac oil 2.0-3.0%, any multiple combination in ethyl caprilate 3.5-5.0%.
More preferably, described mouthfeel fragrance conditioning agent is the following stated formula (weight percent meter with 100%):
Formula one: normal propyl alcohol 2.0%, ethyl acetate 6.0%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 2.0%, acetal 10.0%, 2-methvl-propionic acid ethvl ester 0.5%, ethyl butyrate 4.5%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.7%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.2%, ethyl valerate 2.5%, benzaldehyde 2.5%, ethyl hexanoate 18.0%, phenmethylol 32.7%, cognac oil 2.5%, ethyl caprilate 4.5%.
Formula two: normal propyl alcohol 2.4%, ethyl acetate 6.5%, 2-methyl isophthalic acid-propyl alcohol 1.4%, 3-methyl-butanal 1.3%, 2-methyl-1-butene aldehyde 2.1%, ethyl propionate 1.9%, acetal 12.0%, 2-methvl-propionic acid ethvl ester 0.6%, ethyl butyrate 4.9%, ethyl lactate 1.3%, ethyl 2-methylbutyrate 0.8%, 3 Methylbutanoic acid ethyl ester 1.6%, furfuryl alcohol 4.3%, ethyl valerate 2.4%, benzaldehyde 2.6%, ethyl hexanoate 17.5%, phenmethylol 29.2%, cognac oil 2.6%, ethyl caprilate 4.6%.
Formula three: normal propyl alcohol 2.2%, ethyl acetate 6.4%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 1.8%, acetal 11.5%, 2-methvl-propionic acid ethvl ester 0.6%, ethyl butyrate 4.7%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.6%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.0%, ethyl valerate 2.2%, benzaldehyde 2.7%, ethyl hexanoate 17.8%, phenmethylol 31.8%, cognac oil 2.3%, ethyl caprilate 4.0%.Preferably, described propane diols is food grade propane diols.Described food grade propane diols is that market is bought.
The preparation method of a kind of state of the present invention aroma tobacco juice for electronic smoke, comprises the following steps:
1) get tobacco leaf pulverizing, screening from Maotai wine cellar after, with extraction, then after carrying out ultrasonic extraction, through sedimentation, filtration and reduced pressure concentration, i.e. obtained leaf tobacco extract;
Preferably, described tobacco leaf is the tobacco leaf being cooled to room temperature after drying.
Further, described drying condition is: oven temperature: 40 ± 2 DEG C; Drying time 3 ± 0.1h.Preferably, described pulverizing adopts pulverizer to pulverize.
Preferably, the fineness of described screening offal is 40-100 order.Further, the fineness of described screening offal is 40-60 order.
Preferably, described solvent is selected from the one in deionized water or ethanol.
Preferably, described lixiviate and ultrasonic extraction condition are: the mass ratio of tobacco leaf and solvent is: 1:2-5; Ultrasonic extraction temperature: 30-60 DEG C; The ultrasonic extraction time: 2-5h.
Further, described lixiviate and ultrasonic extraction condition are: the mass ratio of tobacco leaf and solvent is: 1:2.5-3.5; Ultrasonic extraction temperature: 40-60 DEG C; The ultrasonic extraction time: 3.5-4.5h.
Preferably, described sedimentation time >=4h.
Preferably, described filtration adopts sand core funnel filter type.Further, described sand core funnel adopts the sand core funnel of conventional aperture.
Preferably, described concentrating is revolved through decompression by tobacco leaf extract to desolventize.Further, described thickening temperature is 60-80 DEG C.
2), after selecting component to mix in proportion, flavouring essence for tobacco, mouthfeel fragrance conditioning agent is made into;
3) by step 1) in preparation leaf tobacco extract, step 2) in flavouring essence for tobacco, mouthfeel fragrance conditioning agent, mix with after other components based on weight percentage amount, fully stir and evenly mix, Ji get state aroma tobacco juice for electronic smoke.
Preferably, described mixing time is 30 ± 5min.Further, described mixing time is 30 ± 2min.
The invention also discloses the application of a kind of state's aroma tobacco juice for electronic smoke in electronic cigarette.
As mentioned above, a kind of state provided by the invention aroma tobacco juice for electronic smoke, compared with prior art, the present invention has following beneficial effect: the extract adopting Maotai wine cellar to store sth. in a cellar tobacco leaf is raw material, and add Maotai, thus make tobacco juice not only have unique this perfume of tobacco, there is again the perfume (or spice) of strong national wine simultaneously.The national wine note of its uniqueness and this fragrant ingenious combination of pure and sweet natural tobacco, make flue gas exquisiteness mellow and full, aftertaste Tianjin is sweet long, can satisfy the demands of consumers on taste and fragrance, improve mouthfeel and the fragrance of existing tobacco juice for electronic smoke, shorten the gap of tobacco juice for electronic smoke in mouthfeel and fragrance and traditional cigarette, meet consumer further to the demand of sucking electronic cigarette.
Detailed description of the invention
The invention provides a kind of state aroma tobacco juice for electronic smoke, its raw materials by weight meter, comprises following component: leaf tobacco extract: 1-30%; Flavouring essence for tobacco: 0.5-10%; Maotai: 0.5-15%; Mouthfeel fragrance conditioning agent: 0.5-10%; Deionized water: 1-15%; Edible glycerol: 1-25%; Propane diols: surplus.Concrete constituent content is: leaf tobacco extract: 1-30%; Flavouring essence for tobacco: 0.5-10%; Maotai: 0.5-15%; Mouthfeel fragrance conditioning agent: 0.5-10%; Deionized water: 1-15%; Edible glycerol: 1-25%; Propane diols: 30-70%.Preferred scope is: leaf tobacco extract: 8-20%; Flavouring essence for tobacco: 1.5-6%; Maotai: 5-10%; Mouthfeel fragrance conditioning agent: 1.5-6%; Deionized water: 1-5%; Edible glycerol: 10-20%; Propane diols: 40-60%.In an embodiment of the present invention, the mass concentration of described raw material components can be specially certain the concrete numerical value in above-mentioned scope.
The leaf tobacco extract used in the present invention, if flue-cured tobacco, burley tobaccos, Turkish tobaccos or Sun cured tobacco extract are manufacturer's self-control; Tobacco flavor components, mouthfeel fragrance conditioning agent component also can adopt commercial goods; Maotai, edible glycerol, propane diols also can be commercially.Deionized water is that manufacturer adopts water purification machine self-control.The equipment used in the present invention and reagent needed for other are all commercially available.
Present invention also offers the preparation method of a kind of state aroma tobacco juice for electronic smoke, first, tobacco leaf is got at the oven drying 2.9-3.1h of 38-42 DEG C from Maotai wine cellar, after being cooled to room temperature, pulverize, after offal screening is 40-100 order (preferred 40-60 order) with pulverizer, with solvent deionized water or alcohol steep, wherein the solid-to-liquid ratio of tobacco leaf and solvent is 1:2-5 (preferred 1:2.5-3.5).Carry out ultrasonic extraction again, ultrasonic extraction temperature is 30-60 DEG C (preferred 40-60 DEG C), and the ultrasonic extraction time is 2-5h (preferred 3.5-4.5h).Then through standing sedimentation >=4h, sand core funnel filters to obtain tobacco leaf extract, and 60-80 DEG C of vacuum rotary steam concentrates and obtain leaf tobacco extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3; 5; any multiple combination in 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine, 2,3,5-trimethylpyrazines.The total content of described flavouring essence for tobacco with percentage by weight shared by flavouring essence for tobacco in described state aroma tobacco juice for electronic smoke for benchmark.
Further, described flavouring essence for tobacco is selected from 1-8% Ethyl vanillin, 1-5% benzyl acetate, 1-8% furfural, 4-20% dorinone, 2-15% β-damascone, 10-30% Megastigmatrienone, 2-9% dihydroactinidiolide, 1-8% dimethyl succinate, 1-5%2, 6, 6-trimethyl-2-cyclohexene-1, 4-diketone, 1-5%2-hydroxyl-3, 5, 5-trimethyl-2-cyclonene, 3-15% geranyl acetone, 5-30% alpha, beta-lonone, 3-15% phenmethylol, 2-7% palmitic acid, 1-4% isovaleric acid, 1-4%2-methylvaleric acid, 1-3% indoles, 1-3% pyridine, 1-3%3-acetylpyridine, 1-5%2, 3, any multiple combination in 5-trimethylpyrazine.Above-mentioned tobacco flavor components content with 100% weight percent meter.
More preferably, described flavouring essence for tobacco comprises 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Described component mixes in vortex oscillator.Above-mentioned tobacco flavor components content with 100% weight percent meter.
More preferably, described flavouring essence for tobacco comprises 15% dorinone, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol.Component mixes in vortex oscillator.Above-mentioned tobacco flavor components content with 100% weight percent meter.
Preferably, described mouthfeel fragrance conditioning agent is selected from any multiple combination in normal propyl alcohol, ethyl acetate, 2-methyl isophthalic acid-propyl alcohol, 3-methyl-butanal, 2-methyl-1-butene aldehyde, ethyl propionate, acetal, 2-methvl-propionic acid ethvl ester, ethyl butyrate, ethyl lactate, ethyl 2-methylbutyrate, 3 Methylbutanoic acid ethyl ester, furfuryl alcohol, ethyl valerate, benzaldehyde, ethyl hexanoate, phenmethylol, cognac oil, ethyl caprilate.
Further, the total content of described mouthfeel fragrance conditioning agent with percentage by weight shared by mouthfeel fragrance conditioning agent in described Maotai-flavor tobacco juice for electronic smoke for benchmark, described mouthfeel fragrance conditioning agent is selected from normal propyl alcohol 1.5-3.0%, ethyl acetate 5.5-7.0%, 2-methyl isophthalic acid-propyl alcohol 1.0-2.0%, 3-methyl-butanal 1.0-2.0%, 2-methyl-1-butene aldehyde 1.5-2.5%, ethyl propionate 1.0-2.5%, acetal 9.0-14.0%, 2-methvl-propionic acid ethvl ester 0.1-1.0%, ethyl butyrate 4.0-5.5%, ethyl lactate 1.0-2.5%, ethyl 2-methylbutyrate 0.3-1.5%, 3 Methylbutanoic acid ethyl ester 1.0-2.0%, furfuryl alcohol 3.5-5.0%, ethyl valerate 2.0-3.0%, benzaldehyde 2.0-3.0%, ethyl hexanoate 15-20%, phenmethylol 25-35%, cognac oil 2.0-3.0%, any multiple combination in the fragrance conditioning agents such as ethyl caprilate 3.5-5.0%.Above-mentioned mouthfeel fragrance conditioning agent constituent content with 100% weight percent meter.
More preferably, described mouthfeel fragrance conditioning agent includes normal propyl alcohol 2.0%, ethyl acetate 6.0%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 2.0%, acetal 10.0%, 2-methvl-propionic acid ethvl ester 0.5%, ethyl butyrate 4.5%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.7%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.2%, ethyl valerate 2.5%, benzaldehyde 2.5%, ethyl hexanoate 18.0%, phenmethylol 32.7%, cognac oil 2.5%, ethyl caprilate 4.5%.Above-mentioned mouthfeel fragrance conditioning agent constituent content with 100% weight percent meter.
More preferably, described mouthfeel fragrance conditioning agent includes normal propyl alcohol 2.4%, ethyl acetate 6.5%, 2-methyl isophthalic acid-propyl alcohol 1.4%, 3-methyl-butanal 1.3%, 2-methyl-1-butene aldehyde 2.1%, ethyl propionate 1.9%, acetal 12.0%, 2-methvl-propionic acid ethvl ester 0.6%, ethyl butyrate 4.9%, ethyl lactate 1.3%, ethyl 2-methylbutyrate 0.8%, 3 Methylbutanoic acid ethyl ester 1.6%, furfuryl alcohol 4.3%, ethyl valerate 2.4%, benzaldehyde 2.6%, ethyl hexanoate 17.5%, phenmethylol 29.2%, cognac oil 2.6%, ethyl caprilate 4.6%.Above-mentioned mouthfeel fragrance conditioning agent constituent content with 100% weight percent meter.
More preferably, described mouthfeel fragrance conditioning agent includes normal propyl alcohol 2.2%, ethyl acetate 6.4%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 1.8%, acetal 11.5%, 2-methvl-propionic acid ethvl ester 0.6%, ethyl butyrate 4.7%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.6%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.0%, ethyl valerate 2.2%, benzaldehyde 2.7%, ethyl hexanoate 17.8%, phenmethylol 31.8%, cognac oil 2.3%, ethyl caprilate 4.0%.Above-mentioned mouthfeel fragrance conditioning agent constituent content with 100% weight percent meter.
Finally, leaf tobacco extract, flavouring essence for tobacco, mouthfeel fragrance conditioning agent are mixed by above-mentioned percentage by weight with other component, fully stirs 25-35min, Ji get state aroma tobacco juice for electronic smoke.
In an embodiment of the present invention, the related data of described preparation method's conditional can specific to the concrete numerical value of certain in the condition and range of said method.
Set forth the present invention further below in conjunction with specific embodiment, should be understood that these embodiments are only not used in for illustration of the present invention and limit the scope of the invention.
Below by way of specific instantiation, embodiments of the present invention are described, those skilled in the art the content disclosed by this description can understand other advantages of the present invention and effect easily.The present invention can also be implemented or be applied by detailed description of the invention different in addition, and the every details in this description also can based on different viewpoints and application, carries out various modification or change not deviating under spirit of the present invention.
Embodiment 1
A kind of state aroma tobacco juice for electronic smoke, comprise following raw material components by weight percentage: cured tobacco leaf extract 20%, flavouring essence for tobacco 3%, Maotai 6%, mouthfeel fragrance conditioning agent 3%, deionized water 3%, edible glycerol 8%, surplus 57% is propane diols.
Wherein, get cured tobacco leaf dry 3h in 40 DEG C of baking ovens that alcoholization is stored sth. in a cellar in Maotai wine cellar, be cooled to room temperature, pulverize with pulverizer, screen to 40-100 order.Then, use solvent deionized water lixiviate, wherein the mass ratio of tobacco leaf and water is 1:3, takes the conical flask that 100g offal is placed in 1L, adds 300ml deionized water, then carry out ultrasonic extraction, and ultrasonic extraction temperature is 40 DEG C, and the ultrasonic extraction time is 4h.Then standing sedimentation 4h, filters to obtain tobacco leaf extract with sand core funnel, is concentrated into 3ml through vacuum rotary steam, obtain cured tobacco leaf extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco mainly comprises: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Above-mentioned tobacco flavor components content with 100% weight percent meter.Said components is mixed in vortex oscillator.
Suitable component is selected to be made into mouthfeel fragrance conditioning agent again.Described mouthfeel fragrance conditioning agent comprises: normal propyl alcohol 2.0%, ethyl acetate 6.0%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 2.0%, acetal 10.0%, 2-methvl-propionic acid ethvl ester 0.5%, ethyl butyrate 4.5%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.7%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.2%, ethyl valerate 2.5%, benzaldehyde 2.5%, ethyl hexanoate 18.0%, phenmethylol 32.7%, cognac oil 2.5%, ethyl caprilate 4.5%.Above-mentioned mouthfeel fragrance conditioning agent constituent content with 100% weight percent meter.Said components is mixed in vortex oscillator.Finally, cured tobacco leaf extract, flavouring essence for tobacco, mouthfeel fragrance conditioning agent are mixed by above-mentioned percentage by weight with other component, fully stirs 30min, each component is fully mixed, Ji get state aroma tobacco juice for electronic smoke 1#.
Embodiment 2
A kind of state aroma tobacco juice for electronic smoke, comprise following raw material components by weight percentage: Sun cured tobacco leaf tobacco extract 22%, flavouring essence for tobacco 2.5%, Maotai 7%, mouthfeel fragrance conditioning agent 3%, deionized water 2.5%, edible glycerol 6%, surplus 57% is propane diols.
Wherein, get Sun cured tobacco tobacco leaf dry 3h in 40 DEG C of baking ovens that alcoholization is stored sth. in a cellar in Maotai wine cellar, be cooled to room temperature, pulverize with pulverizer, screen to 40-60 order, with alcohol steep, wherein the mass ratio of tobacco leaf and ethanol is 1:3, take the conical flask that 100g offal is placed in 1L, add 300ml ethanol, then carry out ultrasonic extraction, ultrasonic extraction temperature is 60 DEG C, and the ultrasonic extraction time is 4h.Then standing sedimentation 4h, filters to obtain tobacco leaf extract with sand core funnel, is concentrated into 3ml through vacuum rotary steam, obtain Sun cured tobacco leaf tobacco extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco mainly comprises: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Above-mentioned tobacco flavor components content with 100% weight percent meter.Said components is mixed in vortex oscillator.
Suitable component is selected to be made into mouthfeel fragrance conditioning agent again.Described mouthfeel fragrance conditioning agent comprises: normal propyl alcohol 2.2%, ethyl acetate 6.4%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 1.8%, acetal 11.5%, 2-methvl-propionic acid ethvl ester 0.6%, ethyl butyrate 4.7%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.6%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.0%, ethyl valerate 2.2%, benzaldehyde 2.7%, ethyl hexanoate 17.8%, phenmethylol 31.8%, cognac oil 2.3%, ethyl caprilate 4.0%.Above-mentioned mouthfeel fragrance conditioning agent constituent content with 100% weight percent meter.Said components is mixed in vortex oscillator.Finally, Sun cured tobacco leaf tobacco extract, flavouring essence for tobacco, mouthfeel fragrance conditioning agent are mixed by above-mentioned percentage by weight with other component, fully stirs 30min, each component is fully mixed, Ji get state aroma tobacco juice for electronic smoke 2#.
Embodiment 3
A kind of state aroma tobacco juice for electronic smoke, comprise following raw material components by weight percentage: burley tobaccos leaf tobacco extract 18%, flavouring essence for tobacco 2%, Maotai 5%, mouthfeel fragrance conditioning agent 3%, deionized water 3%, edible glycerol 9%, surplus 60% is propane diols.
Wherein, get burley tobaccos tobacco leaf dry 3h in 40 DEG C of baking ovens that alcoholization is stored sth. in a cellar in Maotai wine cellar, be cooled to room temperature, pulverize with pulverizer, screen to 40-100 order, use solvent deionized water lixiviate, wherein the solid-liquid mass ratio of tobacco leaf and water is 1:3.5, take the conical flask that 100g offal is placed in 1L, add 350ml deionized water, then carry out ultrasonic extraction, ultrasonic extraction temperature is 50 DEG C, and the ultrasonic extraction time is 4h.Then standing sedimentation 4h, filters to obtain tobacco leaf extract with sand core funnel, is concentrated into 3ml through vacuum rotary steam, obtain burley tobaccos leaf tobacco extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco mainly comprises: 15% dorinone, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol.Above-mentioned tobacco flavor components content with 100% weight percent meter.Said components is mixed in vortex oscillator.
Suitable component is selected to be made into mouthfeel fragrance conditioning agent again.Described mouthfeel fragrance conditioning agent comprises: normal propyl alcohol 2.4%, ethyl acetate 6.5%, 2-methyl isophthalic acid-propyl alcohol 1.4%, 3-methyl-butanal 1.3%, 2-methyl-1-butene aldehyde 2.1%, ethyl propionate 1.9%, acetal 12.0%, 2-methvl-propionic acid ethvl ester 0.6%, ethyl butyrate 4.9%, ethyl lactate 1.3%, ethyl 2-methylbutyrate 0.8%, 3 Methylbutanoic acid ethyl ester 1.6%, furfuryl alcohol 4.3%, ethyl valerate 2.4%, benzaldehyde 2.6%, ethyl hexanoate 17.5%, phenmethylol 29.2%, cognac oil 2.6%, ethyl caprilate 4.6%.Above-mentioned mouthfeel fragrance conditioning agent constituent content with 100% weight percent meter.Said components is mixed in vortex oscillator.Finally, burley tobaccos leaf tobacco extract, flavouring essence for tobacco, mouthfeel fragrance conditioning agent are mixed by above-mentioned percentage by weight with other component, fully stirs 30min, each component is fully mixed, Ji get state aroma tobacco juice for electronic smoke 3#.
Comparative example 1
A kind of tobacco juice for electronic smoke, comprise following raw material components by weight percentage: cured tobacco leaf extract 20%, flavouring essence for tobacco 3%, mouthfeel fragrance conditioning agent 3%, deionized water 2%, edible glycerol 8%, surplus 64% is propane diols.
Wherein, get cured tobacco leaf dry 3h in 40 DEG C of baking ovens, be cooled to room temperature, pulverize with pulverizer, screen to 40-100 order.Then, use deionized water lixiviate, wherein the solid-liquid mass ratio of tobacco leaf and water is 1:3, takes the conical flask that 100g offal is placed in 1L, adds 300ml deionized water, then carry out ultrasonic extraction, and ultrasonic extraction temperature is 40 DEG C, and the ultrasonic extraction time is 4h.Then standing sedimentation 4h, filters to obtain tobacco leaf extract with sand core funnel, is concentrated into 3ml through vacuum rotary steam, obtain cured tobacco leaf extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco mainly comprises: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Above-mentioned tobacco flavor components content with 100% weight percent meter.Said components is mixed in vortex oscillator.
Suitable component is selected to be made into mouthfeel fragrance conditioning agent again.Described mouthfeel fragrance conditioning agent comprises: normal propyl alcohol 2.0%, ethyl acetate 6.0%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 2.0%, acetal 10.0%, 2-methvl-propionic acid ethvl ester 0.5%, ethyl butyrate 4.5%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.7%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.2%, ethyl valerate 2.5%, benzaldehyde 2.5%, ethyl hexanoate 18.0%, phenmethylol 32.7%, cognac oil 2.5%, ethyl caprilate 4.5%.Above-mentioned mouthfeel fragrance conditioning agent constituent content with 100% weight percent meter.Said components is mixed in vortex oscillator.Finally, cured tobacco leaf extract, flavouring essence for tobacco, mouthfeel fragrance conditioning agent are mixed by above-mentioned percentage by weight with other component, fully stirs 30min, each component is fully mixed, obtains tobacco juice for electronic smoke 1*.
Comparative example 2
A kind of tobacco juice for electronic smoke, comprise following raw material components by weight percentage: Sun cured tobacco leaf tobacco extract 22%, flavouring essence for tobacco 2.5%, mouthfeel fragrance conditioning agent 3%, deionized water 2.5%, edible glycerol 6%, surplus 64% is propane diols.
Wherein, get Sun cured tobacco tobacco leaf dry 3h in 40 DEG C of baking ovens, be cooled to room temperature, pulverize with pulverizer, screen to 40-60 order, with alcohol steep, wherein the mass ratio of tobacco leaf and ethanol is 1:3, take the conical flask that 100g offal is placed in 1L, add 300ml ethanol, then carry out ultrasonic extraction, ultrasonic extraction temperature is 60 DEG C, and the ultrasonic extraction time is 4h.Then standing sedimentation 4h, filters to obtain tobacco leaf extract with sand core funnel, is concentrated into 3ml through vacuum rotary steam, obtain Sun cured tobacco leaf tobacco extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco mainly comprises: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Above-mentioned tobacco flavor components content with 100% weight percent meter.Said components is mixed in vortex oscillator.
Suitable component is selected to be made into mouthfeel fragrance conditioning agent again.Described mouthfeel fragrance conditioning agent comprises: normal propyl alcohol 2.2%, ethyl acetate 6.4%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 1.8%, acetal 11.5%, 2-methvl-propionic acid ethvl ester 0.6%, ethyl butyrate 4.7%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.6%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.0%, ethyl valerate 2.2%, benzaldehyde 2.7%, ethyl hexanoate 17.8%, phenmethylol 31.8%, cognac oil 2.3%, ethyl caprilate 4.0%.Above-mentioned mouthfeel fragrance conditioning agent constituent content with 100% weight percent meter.Said components is mixed in vortex oscillator.Finally, Sun cured tobacco leaf tobacco extract, flavouring essence for tobacco, mouthfeel fragrance conditioning agent are mixed by above-mentioned percentage by weight with other component, fully stirs 30min, each component is fully mixed, obtains tobacco juice for electronic smoke 2*.
Comparative example 3
A kind of tobacco juice for electronic smoke, comprise following raw material components by weight percentage: burley tobaccos leaf tobacco extract 18%, flavouring essence for tobacco 2%, mouthfeel fragrance conditioning agent 3%, deionized water 3%, edible glycerol 9%, surplus 65% is propane diols.
Wherein, get burley tobaccos tobacco leaf dry 3h in 40 DEG C of baking ovens, be cooled to room temperature, pulverize with pulverizer, screen to 40-100 order, use deionized water lixiviate, wherein the solid-liquid mass ratio of tobacco leaf and water is 1:3.5, take the conical flask that 100g offal is placed in 1L, add 350ml deionized water, then carry out ultrasonic extraction, ultrasonic extraction temperature is 50 DEG C, and the ultrasonic extraction time is 4h.Then standing sedimentation 4h, filters to obtain tobacco leaf extract with sand core funnel, is concentrated into 3ml through vacuum rotary steam, obtain burley tobaccos leaf tobacco extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco mainly comprises: 15% dorinone, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol.Above-mentioned tobacco flavor components content with 100% weight percent meter.Said components is mixed in vortex oscillator.
Suitable component is selected to be made into mouthfeel fragrance conditioning agent again.Described mouthfeel fragrance conditioning agent comprises: normal propyl alcohol 2.4%, ethyl acetate 6.5%, 2-methyl isophthalic acid-propyl alcohol 1.4%, 3-methyl-butanal 1.3%, 2-methyl-1-butene aldehyde 2.1%, ethyl propionate 1.9%, acetal 12.0%, 2-methvl-propionic acid ethvl ester 0.6%, ethyl butyrate 4.9%, ethyl lactate 1.3%, ethyl 2-methylbutyrate 0.8%, 3 Methylbutanoic acid ethyl ester 1.6%, furfuryl alcohol 4.3%, ethyl valerate 2.4%, benzaldehyde 2.6%, ethyl hexanoate 17.5%, phenmethylol 29.2%, cognac oil 2.6%, ethyl caprilate 4.6%.Above-mentioned mouthfeel fragrance conditioning agent constituent content with 100% weight percent meter.Said components is mixed in vortex oscillator.Finally, burley tobaccos leaf tobacco extract, flavouring essence for tobacco, mouthfeel fragrance conditioning agent are mixed by above-mentioned percentage by weight with other component, fully stirs 30min, each component is fully mixed, obtains tobacco juice for electronic smoke 3*.
Embodiment 4
Electronic cigarette sensory quality assessment method is adopted to evaluate the sample obtained in embodiment 1-3 and comparative example 1-3.Sensory quality assessment method comprises the following steps:
(1) 9 sensory quality assessment indexs are provided with, comprise excitant, satisfaction, concentration, comfort level, feature style, tobacco perfume, aroma quality, perfume quantity and the amount of being fuming, and give different score value according to the Different Effects degree of every evaluation index to tobacco juice for electronic smoke aesthetic quality.
Described excitant refers to: suck the discomfort that flue gas comprises oral cavity to sense organ, throat and nasal cavity produce that tobacco juice for electronic smoke produces through atomization and be subject to.
Described satisfaction refers to: the flue gas strength that tobacco juice for electronic smoke produces through atomization, concentration and note are to the comprehensive impression that sense organ produces.
Described concentration refers to: the impression of tobacco juice for electronic smoke oral cavity filling degree when the flue gas firm suction inlet that atomization produces.
Described comfort level refers to: the impact of flue gas on oral cavity level of comfort after sucking oral cavity and exhalation that tobacco juice for electronic smoke produces through atomization.
Described feature style refers to: a kind of tobacco juice for electronic smoke is different from the sense organ Main Differences performance of other homogeneous e cigarette tobacco juices in joyful sense.
Described tobacco perfume (or spice) refers to: in process of smokeing panel test, sensory feel is to the breath of this perfume (or spice) of tobacco.
Described aroma quality refers to: felt the good and bad degree of pleasant breath in process of smokeing panel test by sense of smell and the sense of taste.
Described perfume quantity refers to: in process of smokeing panel test by oral cavity and nasal cavity weigh pleasant breath amount number.
The described amount of being fuming refers to: tobacco juice for electronic smoke through atomization produce exhaust gas volumn number.
(2) member of smoking of 9 people is set, everyone a tobacco juice for electronic smoke sensory quality assessment table, adopt the marking mode secretly commented, adopt the overall method of smokeing panel test that circulates, tobacco juice for electronic smoke is aspirated, according to the implication of 9 sensory quality assessment index score values in table 1, adopt hundred-mark system point system to carry out comprehensive grading to the aesthetic quality of tobacco juice for electronic smoke, every evaluation index is by five points, ten point system or the scoring of ten the five-grade marking systems.The concrete meaning of the score value of tobacco juice for electronic smoke evaluation index sees the following form 1.The minimum score unit of score value is 0.5.
Described hundred-mark system point system refers to: 9 sensory quality assessment indexs respectively by five points, very or ten the five-grade marking systems mark, and the score value summation of 9 sensory quality assessment indexs is a percentage.The concrete meaning of the score value of described 9 sensory quality assessment indexs sees the following form 1.
(3) the sensory quality assessment result of member of smoking is added up.By the score value of every sensory quality assessment index of all members of smoking, remove one minimum point and a best result respectively, calculate the mean value of effective score value of every sensory quality assessment index by formula I.The mean value sum of the score value of every sensory quality assessment index is calculated by formula II.
Described formula I is:
In formula:
---the average score value of the effective sense organ quality evaluation index of certain individual event, result retains two-decimal;
---the summation of the score value of the effective sense organ quality evaluation index of certain individual event;
N---total number of persons of effectively smokeing panel test.
Described formula II is:
In formula: S---general comment score value, result retains a decimal;
---the average score value sum of every effective sense organ quality evaluation index.
The score value implication table of table 1 sensory quality assessment index
Tobacco juice for electronic smoke 1*, 2*, 3* of preparing in state aroma tobacco juice for electronic smoke 1#, 2#, the 3# and comparative example 1-3 prepared in embodiment 1-3 are added in electronic cigarette and carry out sensory quality assessment.Concrete evaluation result is in table 2, and in table 2, the scoring of every evaluation index is that the arithmetic average that 9 members of smoking effectively mark is divided.
Table 2 tobacco juice for electronic smoke sensory quality assessment result
Show from the sensory quality assessment result of table 2, state provided by the invention aroma tobacco juice for electronic smoke, less to throat irritation, fragrance fragrance, obviously can experience the perfume (or spice) of this perfume of tobacco and national wine, delicate mouthfeel is soft, wine rhythm cigarette perfume (or spice) makes us enjoying endless aftertastes, the amount of being fuming abundance, and the general comment score value of sensory quality assessment is better than the tobacco juice for electronic smoke in comparative example, its quality is good, can meet the needs of consumer.
Above-described embodiment is illustrative principle of the present invention and effect thereof only, but not for limiting the present invention.Any person skilled in the art scholar all without prejudice under spirit of the present invention and category, can modify above-described embodiment or changes.Therefore, such as have in art usually know the knowledgeable do not depart from complete under disclosed spirit and technological thought all equivalence modify or change, must be contained by claim of the present invention.
Claims (10)
1. state's aroma tobacco juice for electronic smoke, its raw materials by weight meter, comprises following component:
Leaf tobacco extract: 1-30%;
Flavouring essence for tobacco: 0.5-10%;
Maotai: 0.5-15%;
Mouthfeel fragrance conditioning agent: 0.5-10%
Deionized water: 1-15%;
Edible glycerol: 1-25%;
Propane diols: surplus.
2. a kind of state according to claim 1 aroma tobacco juice for electronic smoke, is characterized in that, described leaf tobacco extract is selected from any one or a few mixing in flue-cured tobacco, burley tobaccos, Turkish tobaccos or Sun cured tobacco extract.
3. a kind of state according to claim 1 aroma tobacco juice for electronic smoke, is characterized in that, the raw tobacco material of described leaf tobacco extract stores sth. in a cellar alcoholization in Maotai wine cellar.
4. a kind of state according to claim 1 aroma tobacco juice for electronic smoke, it is characterized in that, described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2, 6, 6-trimethyl-2-cyclohexene-1, 4-diketone, 2-hydroxyl-3, 5, 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine, 2, 3, any multiple combination in 5-trimethylpyrazine.
5. state according to claim 1 aroma tobacco juice for electronic smoke, it is characterized in that, described mouthfeel fragrance conditioning agent is selected from any multiple combination in normal propyl alcohol, ethyl acetate, 2-methyl isophthalic acid-propyl alcohol, 3-methyl-butanal, 2-methyl-1-butene aldehyde, ethyl propionate, acetal, 2-methvl-propionic acid ethvl ester, ethyl butyrate, ethyl lactate, ethyl 2-methylbutyrate, 3 Methylbutanoic acid ethyl ester, furfuryl alcohol, ethyl valerate, benzaldehyde, ethyl hexanoate, phenmethylol, cognac oil, ethyl caprilate.
6. a preparation method for state's aroma tobacco juice for electronic smoke, comprises the following steps:
1) get tobacco leaf pulverizing, screening from Maotai wine cellar after, with extraction, then after carrying out ultrasonic extraction, through sedimentation, filtration and reduced pressure concentration, i.e. obtained leaf tobacco extract;
2), after selecting component to mix in proportion, flavouring essence for tobacco, mouthfeel fragrance conditioning agent is made into;
3) by step 1) in preparation leaf tobacco extract, step 2) in flavouring essence for tobacco, mouthfeel fragrance conditioning agent, mix with after other components based on weight percentage amount, fully stir and evenly mix, Ji get state aroma tobacco juice for electronic smoke.
7. the preparation method of a kind of state according to claim 6 aroma tobacco juice for electronic smoke, is characterized in that, step 1) in, the fineness of described screening offal is 40-100 order; Described solvent is selected from the one in deionized water or ethanol.
8. the preparation method of a kind of state according to claim 6 aroma tobacco juice for electronic smoke, it is characterized in that, step 1) in, described lixiviate and ultrasonic extraction condition are: the mass ratio of tobacco leaf and solvent is: 1:2-5, ultrasonic extraction temperature: 30-60 DEG C, the ultrasonic extraction time: 2-5h; Described sedimentation time >=4h; Described filtration adopts sand core funnel filter type; Described concentrating is revolved through decompression by tobacco leaf extract to desolventize.
9. the preparation method of a kind of state according to claim 6 aroma tobacco juice for electronic smoke, is characterized in that, step 3) in, described mixing time is 25-35min.
10. according to the arbitrary described application of a kind of state's aroma tobacco juice for electronic smoke in electronic cigarette of claim 1-5.
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