CN102823939B - A kind of preparation method of wild eggplant leaf extract and the application in cigarette thereof - Google Patents
A kind of preparation method of wild eggplant leaf extract and the application in cigarette thereof Download PDFInfo
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- CN102823939B CN102823939B CN201210344619.5A CN201210344619A CN102823939B CN 102823939 B CN102823939 B CN 102823939B CN 201210344619 A CN201210344619 A CN 201210344619A CN 102823939 B CN102823939 B CN 102823939B
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- wild eggplant
- eggplant leaf
- cigarette
- leaf extract
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Abstract
The present invention discloses a kind of preparation method of wild eggplant leaf extract and the application in cigarette thereof, comprise wild eggplant leaf or powder through water extraction or variable concentrations alcoholic extraction, take a certain amount of pipe tobacco, and the wild eggplant leaf extract prepared is taken by 0.01 ~ 8% of pipe tobacco weight, this dissolution homogeneity is sprayed on the pipe tobacco made, then the pipe tobacco sprayed is made cigarette.The smoking result adding wild eggplant leaf extract in test cigarette shows: wild eggplant leaf extract can harmony fragrant with cigarette, and enrich and enrich flue gas, increase a part of fragrance, fragrance stereovision is good, and aroma quality slightly improves, and have certain long sense, flue gas is preposition, elegant; Relaxation is better, and concentration strength is moderate, and stimulate, hotness declines, pleasant impression is comparatively clean, and comfortableness significantly improves, to the improvement successful of smoke behavior and relaxation.<!--1-->
Description
Technical field
The present invention relates to a kind of preparation method of wild eggplant leaf extract and the application in cigarette thereof.
Background technology
Along with smoking and healthy problem more and more receive publicity, the harmful components of sucking in security, increase health care, reduction cigarette smoke improving cigarette are the inevitable development trend of cigarette.Therefore market one has occurred, as kinds such as ginseng cigarette, peppermint cigarettes, in pipe tobacco, namely adding the material that ginseng, peppermint etc. have unique health care or taste.Domestic about research mainly wild eggplant chemical constituents determination, medical etc. in, but have no the application report of wild eggplant in tobacco.
Wild eggplant, be commonly called as Siberian cocklebur, sheep band returned, Indian Skullcap Herb, thorn, sticky certain herbaceous plants with big flowers, be composite family annual herb plant.Being widely distributed in north and south each province of China. its complete stool is close by white undercoat, stem height about 1m, and leaf alternate, has long handle; Blade star ovum shape triangular shape, long 6-10cm, wide 5 ~ 10cm.Summer-flowering.Fruit is ripe autumn, oblong or avette.Long 1.5cm, hard and tool specificity fragrant; Perverse and the fine, soft fur of the close raw hook of fruit surface, includes 1-2 pieces of obovate achenes, its leaf toil, cold. and tool dispels the wind please the multiple efficacies such as heat, removing toxic substances analgesia
[1].At present, the research of wild eggplant aspect mainly concentrates on the aspects such as grafting, cultivation and pre-preventing disease and pest
[2,3].Yet there are no its chemical composition of volatile oil and the application report in tobacco and cigarette.
By GC × GC/TOFMS, qualitative analysis is carried out to wild eggplant leaf volatile oil, to the chemical composition of similarity >=800, in conjunction with total ion current figure, anti-similarity and possibility data, identify matching degree higher chemical composition 322 kinds (table 1) altogether, comprise 40 kinds of alcohol, 41 kinds of aldehyde, 5 kinds of acid, 2 kinds of lactones, 87 kinds of alkane, 21 kinds of alkene, 67 kinds of ketone and 10 kinds of esters etc.
Table 1 wild eggplant leaf extract qualitative results summary sheet
| Alcohol | 40 |
| Phenol | 4 |
| Ether | 1 |
| Lactone | 2 |
| Aldehyde | 41 |
| Alkynes | 2 |
| Acid | 5 |
| Ketone | 67 |
| Alkane | 87 |
| Alkene | 21 |
| Ester | 10 |
| Containing N compound | 12 |
| Benzene | 17 |
| Other | 13 |
| Add up to | 322 |
Note: some chemical composition, containing multiple functional group, only arranges in a class during classification, do not compute repeatedly.
In wild eggplant leaf extract, some chemical properties has special fragrance characteristic and medicinal curative effect.A lot of composition (see table 2) such as phenmethylol, furfural, irisone, dihydroactinidiolide, furfuryl alcohol and geranyl acetone etc. are all important flavor components, and wherein, phenmethylol has special fruital breath; Furfural has stimulation, but sweet, and like bread, caramel, like the fragrance of Chinese cassia tree, apricot, persistence is poor; Dihydroactinidiolide has fruital, is that tobacco causes fragrant precursor.Therefore, wild eggplant leaf volatile oil has the fragrance characteristics such as fragrant and sweet fragrance, fruit aroma, tobacco aroma, these compositions should have humorous mediation increases cigarette cigarette perfume, abirritate, cover assorted gas, the effect of promoting or transferring cigarette Flavor, can be applied to perfuming cigarette, can use as tobacco additive agent, give the odor characteristic of cigarette uniqueness.
Table 2 wild eggplant leaf volatile oil some chemical properties fragrance characteristic
Bibliography:
1. Zhu Xi scholar, Zhang Yunkai. the formation of wild eggplant Callus of Leaf, differentiation and Transplantation of Regenerated Plantlets [J]. GUIHAIA, 2001,21(1): 59-62.
2. Liu Chang is fragrant. R and D progress [J] of papaya. and Yunnan hotwork science and technology, 1999,22 (4): 27-31.
3. yellow precious, Sun Weilin. fruit type papaya Analysis of Development Prospect [J]. market analysis, 2007:31-32.
Summary of the invention
The invention provides a kind of preparation method of wild eggplant leaf extract and the application in cigarette thereof.Obtained cigarette aroma quality slightly improves, and concentration strength is moderate, and comfortableness significantly improves, to the improvement successful of smoke behavior and relaxation.
The present invention adopts following technical scheme:
A kind of preparation method of wild eggplant leaf extract and the application in cigarette thereof, it is characterized in that: wild eggplant leaf gets through water extraction or the alcohol extract wild eggplant leaf of variable concentrations obtains extract, in pipe tobacco weight 0.01 ~ 8% ratio take wild eggplant leaf extract, evenly be sprayed on pipe tobacco, make cigarette.
The usefulness of technique scheme is:
The wild eggplant leaf extract that the present invention adopts can harmony fragrant with cigarette, and enrich and enrich flue gas, increase a part of fragrance, fragrance stereovision is good, and aroma quality slightly improves, and have certain long sense, flue gas is preposition, elegant; Relaxation is better, and concentration strength is moderate, and stimulate, hotness declines, pleasant impression is comparatively clean, and comfortableness significantly improves, to the improvement successful of smoke behavior and relaxation.
Accompanying drawing explanation
Nothing
Detailed description of the invention
The present invention is set forth further below in conjunction with specific embodiment.These embodiments are only not used in for illustration of the present invention and limit the scope of the invention.
The preparation method of wild eggplant leaf extract and the application in cigarette thereof, its detailed description of the invention is as follows:
Embodiment one, first grinds wild eggplant leaf, gets the ground wild eggplant leaf of 20g and loads in 500mL flask, add the ethanol of 120g50%, ultrasonic extraction 6h in 60 DEG C of waters bath with thermostatic control.Then by after centrifugal for extract supercentrifuge, be condensed into paste by after extracting liquid filtering, and it is for subsequent use to be transferred to Brown Glass Brown glass bottles and jars only sealing.
First weigh 100g pipe tobacco, then 0.04g above-mentioned wild eggplant leaf paste concentrate (it is 0.04% of pipe tobacco weight that wild eggplant leaf paste concentrate applies ratio) is taken, and be dissolved into wild eggplant leaf extract dilute solution with 70% ethanol, this dilute solution is evenly sprayed on the pipe tobacco made, then the pipe tobacco sprayed is placed on and balances 48h in the climatic chamber of temperature 22 DEG C ± 1 DEG C and RH60% ± 2% and namely can be made into cigarette.
Embodiment two, first takes 50g wild eggplant leaf and loads in 2L flask, adding the ethanol of 400g60%, stirs and extract 9h in 70 DEG C of waters bath with thermostatic control.Wild eggplant leaf extract will be obtained after extracting liquid filtering, be then transferred to Brown Glass Brown glass bottles and jars only sealing for subsequent use.
First weigh 100g pipe tobacco, then the above-mentioned wild eggplant leaf extract of 3.5g (it is 3.5% of pipe tobacco weight that wild eggplant leaf extract applies ratio) is taken, and this extract is evenly sprayed on the pipe tobacco that takes, then the pipe tobacco sprayed is placed on and balances 48h in the climatic chamber of temperature 22 DEG C ± 1 DEG C and RH60% ± 2% and namely can be made into cigarette.
Embodiment three, first takes 100g wild eggplant leaf and loads in 2L flask, adding 1000g water, stirs and extract 8h in 80 DEG C of waters bath with thermostatic control.Wild eggplant leaf extract will be obtained after extracting liquid filtering, be then transferred to Brown Glass Brown glass bottles and jars only sealing for subsequent use.
First weigh 100g pipe tobacco, then the above-mentioned wild eggplant leaf extract of 7.5g (it is 7.5% of pipe tobacco weight that wild eggplant leaf extract applies ratio) is taken, and this dilute solution is evenly sprayed on the pipe tobacco that takes, then the pipe tobacco sprayed is placed on and balances 48h in the climatic chamber of temperature 22 DEG C ± 1 DEG C and RH60% ± 2% and namely can be made into cigarette.
Embodiments of the invention one, embodiment two and the difference of embodiment three are that wild eggplant leaf sample size is different, extracting mode is different, extraction time is different, but sample is wild eggplant leaf.
Above are only three specific embodiments of the present invention, but design concept of the present invention is not limited thereto, all changes utilizing this design the present invention to be carried out to unsubstantiality, all should belong to the behavior of invading scope.
Claims (1)
1. wild eggplant leaf extract is preparing the application in cigarette, wherein, wild eggplant leaf gets through water extraction or the alcohol extract of variable concentrations obtains wild eggplant leaf extract, in pipe tobacco weight 0.01 ~ 8% ratio take wild eggplant leaf extract, evenly be sprayed on pipe tobacco, make cigarette;
Wherein,
Described wild eggplant leaf is wild eggplant leaf powder or whole leaf;
Described extracting method is adopt water extraction to get or the alcohol extract of variable concentrations, and during extraction, the weight ratio of the ethanol of wild eggplant leaf and water or different concentration is 1:3-50;
The ethanol of described variable concentrations refers to that the weight ratio of ethanol and water is 1-90:99-10;
Described wild eggplant leaf extract can directly use or be condensed into paste and use.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210344619.5A CN102823939B (en) | 2012-09-17 | 2012-09-17 | A kind of preparation method of wild eggplant leaf extract and the application in cigarette thereof |
| JP2013169231A JP5781573B2 (en) | 2012-09-17 | 2013-08-16 | Method for producing cigarette using onamomi leaf extract |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201210344619.5A CN102823939B (en) | 2012-09-17 | 2012-09-17 | A kind of preparation method of wild eggplant leaf extract and the application in cigarette thereof |
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| Publication Number | Publication Date |
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| CN102823939A CN102823939A (en) | 2012-12-19 |
| CN102823939B true CN102823939B (en) | 2016-03-30 |
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| CN201210344619.5A Active CN102823939B (en) | 2012-09-17 | 2012-09-17 | A kind of preparation method of wild eggplant leaf extract and the application in cigarette thereof |
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| JP (1) | JP5781573B2 (en) |
| CN (1) | CN102823939B (en) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113545509A (en) * | 2021-08-12 | 2021-10-26 | 深圳波顿香料有限公司 | Strengthening agent for electronic cigarette oil |
| CN114523121B (en) * | 2022-02-09 | 2024-04-05 | 上海市农业技术推广服务中心 | Method for preparing nano silver particles by using eggplant leaf extract, product and application |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1124603A (en) * | 1995-09-04 | 1996-06-19 | 付耀华 | Buttercup root health cigarette and producing process thereof |
| CN1686254A (en) * | 2005-03-28 | 2005-10-26 | 中国人民解放军第二军医大学 | Use of cocklebur fruit total glucoside extract in preparing anti inflammation reaction product |
| CN101731748A (en) * | 2008-11-05 | 2010-06-16 | 湖北中烟工业有限责任公司 | Method for extracting Dendranthema indium leaves and application of extractive thereof in cigarettes |
| CN102090712A (en) * | 2010-12-29 | 2011-06-15 | 华宝食用香精香料（上海）有限公司 | Method for preparing coarse extract of peanut shell total flavones and application thereof in cigarettes |
| US8011373B2 (en) * | 2004-08-24 | 2011-09-06 | Japan Tobacco Inc. | Method of treating tobacco extract solution to reduce magnesium ions and method of manufacturing a treated tobacco material |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH09188671A (en) * | 1996-01-09 | 1997-07-22 | Alps Yakuhin Kogyo Kk | Xanthatin-containing antitumor medicinal composition |
| CN102283434A (en) * | 2010-06-18 | 2011-12-21 | 福建中烟工业公司 | Preparation method of morinda officinalis regenerated thin tablet and application of morinda officinalis regenerated thin tablet prepared by the preparation method in tobacco product |
-
2012
- 2012-09-17 CN CN201210344619.5A patent/CN102823939B/en active Active
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- 2013-08-16 JP JP2013169231A patent/JP5781573B2/en not_active Expired - Fee Related
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1124603A (en) * | 1995-09-04 | 1996-06-19 | 付耀华 | Buttercup root health cigarette and producing process thereof |
| US8011373B2 (en) * | 2004-08-24 | 2011-09-06 | Japan Tobacco Inc. | Method of treating tobacco extract solution to reduce magnesium ions and method of manufacturing a treated tobacco material |
| CN1686254A (en) * | 2005-03-28 | 2005-10-26 | 中国人民解放军第二军医大学 | Use of cocklebur fruit total glucoside extract in preparing anti inflammation reaction product |
| CN101731748A (en) * | 2008-11-05 | 2010-06-16 | 湖北中烟工业有限责任公司 | Method for extracting Dendranthema indium leaves and application of extractive thereof in cigarettes |
| CN102090712A (en) * | 2010-12-29 | 2011-06-15 | 华宝食用香精香料（上海）有限公司 | Method for preparing coarse extract of peanut shell total flavones and application thereof in cigarettes |
Non-Patent Citations (1)
| Title |
|---|
| 新疆野生苍耳叶中总黄酮的超声波提取工艺研究;阿布力克木 等;《食品科学》;20090815;第30卷(第16期);第131页至第134页 * |
Also Published As
| Publication number | Publication date |
|---|---|
| JP5781573B2 (en) | 2015-09-24 |
| JP2014057574A (en) | 2014-04-03 |
| CN102823939A (en) | 2012-12-19 |
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