CN105167190B - Cigarette is with flavones essence cigarette pearl and preparation method thereof - Google Patents
Cigarette is with flavones essence cigarette pearl and preparation method thereof Download PDFInfo
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- CN105167190B CN105167190B CN201510336913.5A CN201510336913A CN105167190B CN 105167190 B CN105167190 B CN 105167190B CN 201510336913 A CN201510336913 A CN 201510336913A CN 105167190 B CN105167190 B CN 105167190B
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- 229930003944 flavone Natural products 0.000 title claims abstract description 69
- 235000011949 flavones Nutrition 0.000 title claims abstract description 69
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 64
- 150000002213 flavones Chemical class 0.000 title claims abstract description 63
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- REFJWTPEDVJJIY-UHFFFAOYSA-N Quercetin Chemical compound C=1C(O)=CC(O)=C(C(C=2O)=O)C=1OC=2C1=CC=C(O)C(O)=C1 REFJWTPEDVJJIY-UHFFFAOYSA-N 0.000 claims abstract description 18
- 239000011122 softwood Substances 0.000 claims abstract description 16
- 239000000853 adhesive Substances 0.000 claims abstract description 13
- 230000001070 adhesive effect Effects 0.000 claims abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 11
- ZVOLCUVKHLEPEV-UHFFFAOYSA-N Quercetagetin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=C(O)C(O)=C(O)C=C2O1 ZVOLCUVKHLEPEV-UHFFFAOYSA-N 0.000 claims abstract description 9
- HWTZYBCRDDUBJY-UHFFFAOYSA-N Rhynchosin Natural products C1=C(O)C(O)=CC=C1C1=C(O)C(=O)C2=CC(O)=C(O)C=C2O1 HWTZYBCRDDUBJY-UHFFFAOYSA-N 0.000 claims abstract description 9
- QUQPHWDTPGMPEX-UTWYECKDSA-N aurantiamarin Natural products COc1ccc(cc1O)[C@H]1CC(=O)c2c(O)cc(O[C@@H]3O[C@H](CO[C@@H]4O[C@@H](C)[C@H](O)[C@@H](O)[C@H]4O)[C@@H](O)[C@H](O)[C@H]3O)cc2O1 QUQPHWDTPGMPEX-UTWYECKDSA-N 0.000 claims abstract description 9
- 238000004090 dissolution Methods 0.000 claims abstract description 9
- MWDZOUNAPSSOEL-UHFFFAOYSA-N kaempferol Natural products OC1=C(C(=O)c2cc(O)cc(O)c2O1)c3ccc(O)cc3 MWDZOUNAPSSOEL-UHFFFAOYSA-N 0.000 claims abstract description 9
- 229960001285 quercetin Drugs 0.000 claims abstract description 9
- 235000005875 quercetin Nutrition 0.000 claims abstract description 9
- XDQITMCFPPPMBC-TUANDBMESA-N scutelloside Natural products OC[C@H]1O[C@@H](O[C@@H]2O[C@@H]3C[C@H]4[C@H](O)[C@@H](O)[C@@](O)(CO3)[C@@H]24)[C@H](O)[C@@H](O)[C@@H]1O XDQITMCFPPPMBC-TUANDBMESA-N 0.000 claims abstract description 9
- 238000003756 stirring Methods 0.000 claims abstract description 3
- 238000000034 method Methods 0.000 claims description 8
- 229920002134 Carboxymethyl cellulose Polymers 0.000 claims description 4
- 229920002153 Hydroxypropyl cellulose Polymers 0.000 claims description 4
- 239000001768 carboxy methyl cellulose Substances 0.000 claims description 4
- 235000010948 carboxy methyl cellulose Nutrition 0.000 claims description 4
- 239000008112 carboxymethyl-cellulose Substances 0.000 claims description 4
- 239000001863 hydroxypropyl cellulose Substances 0.000 claims description 4
- 235000010977 hydroxypropyl cellulose Nutrition 0.000 claims description 4
- 239000002245 particle Substances 0.000 claims description 3
- 238000001035 drying Methods 0.000 claims description 2
- 239000001866 hydroxypropyl methyl cellulose Substances 0.000 claims description 2
- 229920003088 hydroxypropyl methyl cellulose Polymers 0.000 claims description 2
- 235000010979 hydroxypropyl methyl cellulose Nutrition 0.000 claims description 2
- UFVKGYZPFZQRLF-UHFFFAOYSA-N hydroxypropyl methyl cellulose Chemical compound OC1C(O)C(OC)OC(CO)C1OC1C(O)C(O)C(OC2C(C(O)C(OC3C(C(O)C(O)C(CO)O3)O)C(CO)O2)O)C(CO)O1 UFVKGYZPFZQRLF-UHFFFAOYSA-N 0.000 claims description 2
- 150000002576 ketones Chemical class 0.000 claims description 2
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract description 35
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 abstract description 7
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 abstract description 6
- 239000000779 smoke Substances 0.000 abstract description 6
- 230000008901 benefit Effects 0.000 abstract description 4
- 239000003205 fragrance Substances 0.000 abstract description 3
- 150000002212 flavone derivatives Chemical class 0.000 abstract 1
- 229960003742 phenol Drugs 0.000 description 15
- -1 flavone compound Chemical class 0.000 description 13
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 11
- 239000003546 flue gas Substances 0.000 description 11
- 150000002989 phenols Chemical class 0.000 description 8
- 239000000126 substance Substances 0.000 description 7
- 230000000694 effects Effects 0.000 description 6
- 239000012530 fluid Substances 0.000 description 6
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 6
- 239000002304 perfume Substances 0.000 description 5
- YCIMNLLNPGFGHC-UHFFFAOYSA-N catechol Chemical compound OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 description 4
- 229930003935 flavonoid Natural products 0.000 description 4
- 235000017173 flavonoids Nutrition 0.000 description 4
- 235000013824 polyphenols Nutrition 0.000 description 4
- 150000003254 radicals Chemical class 0.000 description 4
- 238000011160 research Methods 0.000 description 4
- 238000010521 absorption reaction Methods 0.000 description 3
- 230000003064 anti-oxidating effect Effects 0.000 description 3
- 230000003078 antioxidant effect Effects 0.000 description 3
- 150000002215 flavonoids Chemical class 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- 239000001301 oxygen Substances 0.000 description 3
- 229910052760 oxygen Inorganic materials 0.000 description 3
- 230000000391 smoking effect Effects 0.000 description 3
- QIGBRXMKCJKVMJ-UHFFFAOYSA-N Hydroquinone Chemical compound OC1=CC=C(O)C=C1 QIGBRXMKCJKVMJ-UHFFFAOYSA-N 0.000 description 2
- 241000208125 Nicotiana Species 0.000 description 2
- 235000002637 Nicotiana tabacum Nutrition 0.000 description 2
- 102000019197 Superoxide Dismutase Human genes 0.000 description 2
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- 230000001093 anti-cancer Effects 0.000 description 2
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- 231100000315 carcinogenic Toxicity 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- MLUCVPSAIODCQM-NSCUHMNNSA-N crotonaldehyde Chemical compound C\C=C\C=O MLUCVPSAIODCQM-NSCUHMNNSA-N 0.000 description 2
- MLUCVPSAIODCQM-UHFFFAOYSA-N crotonaldehyde Natural products CC=CC=O MLUCVPSAIODCQM-UHFFFAOYSA-N 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 230000036541 health Effects 0.000 description 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 2
- 238000009940 knitting Methods 0.000 description 2
- 230000003647 oxidation Effects 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 description 2
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- 206010002383 Angina Pectoris Diseases 0.000 description 1
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- 206010020772 Hypertension Diseases 0.000 description 1
- 102000004882 Lipase Human genes 0.000 description 1
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- 239000004367 Lipase Substances 0.000 description 1
- WSMYVTOQOOLQHP-UHFFFAOYSA-N Malondialdehyde Chemical compound O=CCC=O WSMYVTOQOOLQHP-UHFFFAOYSA-N 0.000 description 1
- 241000124008 Mammalia Species 0.000 description 1
- WHNWPMSKXPGLAX-UHFFFAOYSA-N N-Vinyl-2-pyrrolidone Chemical group C=CN1CCCC1=O WHNWPMSKXPGLAX-UHFFFAOYSA-N 0.000 description 1
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- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 150000002240 furans Chemical class 0.000 description 1
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- 125000004356 hydroxy functional group Chemical group O* 0.000 description 1
- 235000019421 lipase Nutrition 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
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- 108010071584 oxidized low density lipoprotein Proteins 0.000 description 1
- IWDCLRJOBJJRNH-UHFFFAOYSA-N p-cresol Chemical class CC1=CC=C(O)C=C1 IWDCLRJOBJJRNH-UHFFFAOYSA-N 0.000 description 1
- 150000002978 peroxides Chemical class 0.000 description 1
- KHUXNRRPPZOJPT-UHFFFAOYSA-N phenoxy radical Chemical compound O=C1C=C[CH]C=C1 KHUXNRRPPZOJPT-UHFFFAOYSA-N 0.000 description 1
- 235000013855 polyvinylpyrrolidone Nutrition 0.000 description 1
- 229920000036 polyvinylpyrrolidone Polymers 0.000 description 1
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Abstract
The invention discloses a kind of cigarettes with flavones essence cigarette pearl and preparation method thereof, weigh the adhesive that weight is flavones essence weight 0.1%~1%, it is added in flavones essence after adhesive water dissolution, it stirs evenly and softwood is made, then by extrusion-spheronizator on softwood, flavones essence cigarette pearl is obtained after dry；The weight percentages of components of the wherein described flavones essence includes cyanidenon 30%~60%, scutelloside 15%~40%, Quercetin 15%~40%, aurantiamarin 10%~25%.There is the flavones essence cigarette pearl of the present invention significant advantage, phenol reduced rate can reach 15~45% in terms of reducing phenol in smoke；There is the plant flavone essence of the present invention excellent natural breath, addition unique, strong additional fragrance can be brought to cigarette at cigarette filter tip position.
Description
Technical field
The invention belongs to technical field of cigarettes, and in particular to a kind of cigarette is with flavones essence cigarette pearl and preparation method thereof.
Background technology
Natural plants are widely used in tobacco aromaticss, wherein being much containing Flavonoid substances.According to Flavonoid substances
Molecular characterization and interelectric active force power, Primary Study find the substance burning crack after will produce
Furans and its derivative, these substances are the main aroma components in flue gas, can be brought camerlsed to flue gas, it is fragrant and sweet,
Roasting perfume, increases perfume quantity and aroma quality.Therefore in the allotment of essence spice for cigarette, there is the use of many flavonoids perfume materials.
Many researchs also indicate that, flavone compound has multiple biological activities, except using its antibacterial, anti-inflammatory, anti-mutation,
Outside the effects that decompression, clearing heat and detoxicating, calm, diuresis, in anti-oxidant, anticancer, anti-cancer, inhibits lipase etc. and also have notable effect
Fruit.It is the scavenger of most of oxygen radicals, thus the vigor of energy increased SOD (superoxide dismutase), reduces MDA (fat
Matter peroxide malonaldehyde) and OX-LDL (OxLDL ELISA) generation.It can increase coronary flow, to experiment
Myocardial inyaretion has antagonism；There is protective effect to acute myocardial ischemia；Have to treatment coronary heart diseases and angina pectoris, hypertension etc.
Remarkable result；To reducing diastolic pressure, prevention arrhythmia cordis, cardiovascular disease and promoting blood circulation and removing blood stasis also play an important role.
Phenolic compound is a kind of compound common in nature, in water, fuel, vehicle exhaust, air, wine and cigarette
There is the presence of phenolic compound in flue gas.The phenolic compounds in cigarette smoke reported has more than 50 kinds, wherein most important phenol
Class compound includes phenol, catechol, resorcinol, hydroquinone, o, m, 7 kinds of ingredients such as p- cresols.
Phenolic compound can cause protein denaturation, thin by being directly entered blood circulation with the contact of skin, mucous membrane
Born of the same parents destroy and lose vigor.And induced by alkyl hydroxybenzene has endocrine disrupting activity, sends out the reproduction of mammal and aquatile
It educates and impacts, be referred to as phenols environmental estrogens, there is part phenols component genotoxicity and carcinogenic or promotion mutagenesis to make
With.Above 7 kinds of phenols components are put into EPA harmful components lists, and catechol is classified as 2B grades of carcinogenic components by IARC.Zheng
State Bureau's key research project " cigarette harmfulness Research on Index System " project that state tobacco research institute undertakes is harmful by studying
The relationship of ingredient burst size and flue gas biological activity finds that phenol is that influence cigarette mainstream flue gas harmfulness is most important harmful
One of ingredient.
Currently, the method for phenol is mainly using the method for absorption in reduction flue gas, because phenol is present in flue gas
In granule phase substance, it can be retained down from flue gas by the method for physical absorption.The adsorbent of prior art application is mainly table
The larger porous material of area can also adsorb the aroma component of part and flue gas water in flue gas while absorption, retention phenol
Point, cause to easy to produce stimulation, perfume quantity deficiency, aroma quality decline when cigarette smoking, seriously affects cigarette smoking quality.
The cigarette pearl containing essence and flavoring agent is put into filter tip in the prior art, which can make cigarette in aspiration procedure
In it is more raw fragrant, strengthen fragrance or characteristic, smoker made to obtain more comfortably experiencing.This cigarette pearl can only simply make cigarette
It is raw fragrant in aspiration procedure, the harmful substance for reducing and being generated when smoking cigarette cannot be played.
Invention content
In view of the deficiencies of the prior art, the present invention provides a kind of cigarette flavones blocking phenol generation using antioxidation
Essence cigarette pearl and preparation method thereof has the function that reduce phenol in smoke.
Technical solution is used by the present invention solves above-mentioned technical problem：Preparation side of the cigarette with flavones essence cigarette pearl is provided
Method, the preparation method are as follows：
The adhesive that weight is flavones essence weight 0.1%~1% is weighed, flavones perfume is added to after adhesive water dissolution
It in essence, stirs evenly and softwood is made, then by extrusion-spheronizator on softwood, first pass through extruder and be extruded into elongated strip, so
It is round as a ball by spheronizator afterwards, obtain the Huang that particle size range is 0.5mm~4mm, heap density is 1.2g/ml~1.8g/ml after dry
Ketone essence cigarette pearl；
Wherein：The weight percentages of components of the flavones essence is as follows：
Further, the DNA purity of the cyanidenon, scutelloside, Quercetin and aurantiamarin is 80~95%.
Further, described adhesive is povidone, hydroxypropyl cellulose, hydroxypropyl methyl cellulose and carboxymethyl cellulose
It is one or more in element.It is not only convenient for the molding of cigarette pearl using these adhesives and does not influence judging parameter.
Further, the particle size range of the cigarette pearl is 0.8mm~1.5mm, and heap density is 1.4g/ml~1.6g/ml.
Further, the drying is 4~6 hours dry under the conditions of temperature is 60 DEG C~80 DEG C.
A kind of flavones essence cigarette that cigarette is prepared with flavones essence cigarette pearl, the flavones essence cigarette pearl for method described above
Pearl.
It is analyzed according to organic chemistry basic theories, influences to be most importantly hydroxyl in the oxidation resistant factor of flavone compound
Change degree and hydroxy position, phenolic hydroxyl group are the chief active group of flavone compound antioxidation, while finding flavonoids
Hydroxyl activity difference on each ring is larger, is mainly manifested in：B rings are the main work of flavone compound oxidation and removing free radicals
Property position, when the ring is there are when ortho-phenolic hydroxyl structure, antioxidant activity greatly enhances；When hydroxyl on c rings and unsaturated double-bond phase
Lian Shi, c ring also have stronger antioxidant activity；The phenolic hydroxyl group of A rings is most weak.Phenolic hydroxyl group in flavones structure is lived with hydrogen supply
Property, hydrogen atom can be supplied to active oxygen radical, form the Phenoxy radical of stable low activity, to avoid these activity
Oxygen radical generates phenolic compound to the attack of aromatic rings.Phenolic hydroxyl group number in flavones molecule is more, it is possible to provide to
The hydrogen atom combined with living radical is more, and therefore, flavone compound can utilize the life of antioxidation blocking phenol
At to have the function of preferably reducing phenol release amount in flue gas.
The present invention has the following advantages：
1, there is flavones essence cigarette pearl of the invention significant advantage, phenol reduced rate can reach in terms of reducing phenol in smoke
To 15~45%, natural, environmental protection meets requirement of the consumer to health, low evil；
2, flavones essence of the invention has excellent natural breath, adds at cigarette filter tip position, can give cigarette band
Carry out unique, strong additional fragrance, and be not involved in cigarette burning, because without generating new undesirable substance because of cracking, meeting
Requirement of the consumer to health, low evil；
3, flavones flavor of raw material of the present invention derives from a wealth of sources, of low cost, easy to utilize.
Specific implementation mode
In order to make the purpose , technical scheme and advantage of the present invention be clearer, with reference to embodiments, to the present invention
It is further elaborated.The specific embodiments described herein are merely illustrative of the present invention, is not used to limit this hair
It is bright.
Embodiment 1
Flavones essence is mixed according to ratio in table 1, it is fine to weigh the hydroxypropyl methyl that weight is flavones essence weight 0.1%
The plain adhesive of dimension is stirred evenly and softwood is made with being added in flavones essence after 400ml water dissolutions, then will be squeezed on softwood
Go out-spheronizator, first pass through extruder and be extruded into elongated strip, then round as a ball by spheronizator, upper fluid bed is 60 DEG C in temperature
Under the conditions of obtain the flavones essence cigarette pearl that grain size is 0.5mm, heap density is 1.8g/ml after dry 6 hours.
Table 1
| Flavones type | Cyanidenon | Scutelloside | Quercetin | Aurantiamarin |
| Weight percent | 30% | 25% | 30% | 15% |
Embodiment 2
Flavones essence is mixed according to ratio in table 2, it is fine to weigh the hydroxypropyl methyl that weight is flavones essence weight 0.5%
The plain adhesive of dimension is stirred evenly and softwood is made with being added in flavones essence after 450ml water dissolutions, then will be squeezed on softwood
Go out-spheronizator, first pass through extruder and be extruded into elongated strip, then round as a ball by spheronizator, upper fluid bed is 65 DEG C in temperature
Under the conditions of obtain the flavones essence cigarette pearl that grain size is 0.8mm, heap density is 1.6g/ml after dry 5.5 hours.
Table 2
| Flavones type | Cyanidenon | Scutelloside | Quercetin | Aurantiamarin |
| Weight percent | 40% | 25% | 30% | 15% |
Embodiment 3
Flavones essence is mixed according to ratio in table 3, weighs the carboxymethyl cellulose that weight is flavones essence weight 0.8%
Adhesive is stirred evenly and softwood is made with being added in flavones essence after 500ml water dissolutions, then by extrusion-rolling on softwood
Circular knitting machine first passes through extruder and is extruded into elongated strip, then round as a ball by spheronizator, and upper fluid bed is under the conditions of temperature is 70 DEG C
The flavones essence cigarette pearl that grain size is 1.0mm, heap density is 1.6g/ml is obtained after 6 hours dry.
Table 3
| Flavones type | Cyanidenon | Scutelloside | Quercetin | Aurantiamarin |
| Weight percent | 50% | 20% | 20% | 10% |
Embodiment 4
Flavones essence is mixed according to ratio in table 4, weighs the carboxymethyl cellulose that weight is flavones essence weight 0.8%
Adhesive is stirred evenly and softwood is made with being added in flavones essence after 500ml water dissolutions, then by extrusion-rolling on softwood
Circular knitting machine first passes through extruder and is extruded into elongated strip, then round as a ball by spheronizator, and upper fluid bed is under the conditions of temperature is 75 DEG C
The flavones essence cigarette pearl that grain size is 1.5mm, heap density is 1.4g/ml is obtained after 6 hours dry.
Table 4
| Flavones type | Cyanidenon | Scutelloside | Quercetin | Aurantiamarin |
| Weight percent | 60% | 15% | 15% | 10% |
Embodiment 5
Flavones essence is mixed according to ratio in table 5, it is viscous to weigh the hydroxypropyl cellulose that weight is flavones essence weight 1%
Mixture is stirred evenly and softwood is made with being added in flavones essence after 550ml water dissolutions, then will be squeezed out on softwood-round as a ball
Machine first passes through extruder and is extruded into elongated strip, then round as a ball by spheronizator, and upper fluid bed is dry under the conditions of temperature is 70 DEG C
The flavones essence cigarette pearl that grain size is 1.5mm, heap density is 1.4g/ml is obtained after dry 5 hours.
Table 5
| Flavones type | Cyanidenon | Scutelloside | Quercetin | Aurantiamarin |
| Weight percent | 50% | 30% | 15% | 15% |
Embodiment 6
Flavones essence is mixed according to ratio in table 6, it is viscous to weigh the hydroxypropyl cellulose that weight is flavones essence weight 1%
Mixture is stirred evenly and softwood is made with being added in flavones essence after 550ml water dissolutions, then will be squeezed out on softwood-round as a ball
Machine first passes through extruder and is extruded into elongated strip, then round as a ball by spheronizator, and upper fluid bed is dry under the conditions of temperature is 80 DEG C
The flavones essence cigarette pearl that grain size is 1.5mm, heap density is 1.4g/ml is obtained after dry 4 hours.
Table 6
| Flavones type | Cyanidenon | Scutelloside | Quercetin | Aurantiamarin |
| Weight percent | 40% | 20% | 15% | 25% |
Flavones essence cigarette pearl prepared in above 6 embodiments is added in cigarette filter stick, then to manufactured
Cigarette carries out detection of exhaust gas compositions, and carries out phenol reduced rate and compare, and is specifically shown in the following table 7
Table 7
The smoke components mainly reduced have phenol, crotonaldehyde, free radical, while smoke hazard index is also in decline
Gesture, specific reduced rate result see the table below 8
Table 8
| Sample number into spectrum | Phenol | Crotonaldehyde | Index | Free radical |
| Embodiment 1 | 15.5% | 18.2% | 12.8% | 5.6% |
| Embodiment 2 | 20.9% | 17.3% | 10.3% | 12.6% |
| Embodiment 3 | 24.8% | 16.5% | 12.8% | 13.7% |
| Embodiment 4 | 45.0% | 36.2% | 17.9% | 19.6% |
| Embodiment 5 | 42.6% | 34.5% | 15.4% | 20.9% |
| Embodiment 6 | 40.3% | 31.6% | 14.1% | 17.5% |
Flavones essence cigarette pearl prepared in above 6 embodiments is added in cigarette filter stick, then to manufactured
Cigarette carries out sensory evaluation, as a result such as table 9
Table 9
The above description is merely a specific embodiment, but scope of protection of the present invention is not limited thereto, any
Belong to those skilled in the art in the technical scope disclosed by the present invention, the change or replacement that can be readily occurred in all are answered
It is included within the scope of the present invention.Therefore, protection scope of the present invention should be subject to the protection scope in claims.
Claims (4)
1. a kind of cigarette preparation method of flavones essence cigarette pearl, it is characterised in that：The preparation method is as follows：
The adhesive that weight is flavones essence weight 0.1%~1% is weighed, flavones essence is added to after adhesive water dissolution
In, it stirs evenly and softwood is made, then by extrusion-spheronizator on softwood, first pass through extruder and be extruded into elongated strip, then
It is round as a ball by spheronizator, obtain the flavones that particle size range is 0.5mm~4mm, heap density is 1.2g/ml~1.8g/ml after dry
Essence cigarette pearl；
Wherein：The weight percentages of components of the flavones essence is as follows：
The cyanidenon, scutelloside, Quercetin and aurantiamarin DNA purity be 80~95%, described adhesive is poly- dimension
It is one or more in ketone, hydroxypropyl cellulose, hydroxypropyl methyl cellulose and carboxymethyl cellulose.
2. the cigarette according to claim 1 preparation method of flavones essence cigarette pearl, it is characterised in that：The grain size of the cigarette pearl
Ranging from 0.8mm~1.5mm, heap density are 1.4g/ml~1.6g/ml.
3. the cigarette according to claim 1 preparation method of flavones essence cigarette pearl, it is characterised in that：The drying is in temperature
Degree is 4~6 hours dry under the conditions of being 60 DEG C~80 DEG C.
4. a kind of cigarette is with flavones essence cigarette pearl, it is characterised in that：The flavones essence cigarette pearl prepares for claim 1 the method
Flavones essence cigarette pearl.
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| CN107400107B (en) * | 2017-07-26 | 2020-06-16 | 云南中烟工业有限责任公司 | Flavonoid compound in rose waste residue and preparation method and application thereof |
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| CN109259308A (en) * | 2018-09-25 | 2019-01-25 | 云南中烟工业有限责任公司 | The coffee for reducing flue gas free-radical contents toasts cigarette with quick-fried pearl and preparation method thereof |
| KR102288257B1 (en) * | 2019-10-25 | 2021-08-10 | 주식회사 케이티앤지 | Functional cigarette filter comprising natural plant material, cigarette containing the same, and method for producing the same |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4600026A (en) * | 1985-03-14 | 1986-07-15 | Qu Dong Fen | Tobacco composition with bluish dogbane and a process for the preparation thereof |
| CN101731747A (en) * | 2008-11-06 | 2010-06-16 | 张晓红 | Cigarette medicament capable of lowering tar, reducing harm and preventing diseases |
| CN102106606A (en) * | 2009-12-25 | 2011-06-29 | 湖北中烟工业有限责任公司 | Filter rod with visual perfumed beads as well as production process and equipment thereof |
| CN102342583A (en) * | 2010-08-02 | 2012-02-08 | 南通烟滤嘴有限责任公司 | Filter stick containing tobacco particles and preparation method thereof |
| CN103689802A (en) * | 2013-12-03 | 2014-04-02 | 红云红河烟草(集团)有限责任公司 | Tobacco porous particle and application thereof in cigarette |
| CN103876286A (en) * | 2014-03-04 | 2014-06-25 | 湖南中烟工业有限责任公司 | Filter rod particle additive with coffee or cocoa flavor and preparation method and application thereof |
| CN104068467A (en) * | 2014-07-01 | 2014-10-01 | 安徽中烟工业有限责任公司 | Electronic cigarette liquid rich in plant flavone |
| CN104336776A (en) * | 2013-08-05 | 2015-02-11 | 贵州中烟工业有限责任公司 | Slow release aromatic base material, particles as well as preparation method and application thereof |
| EP2517584B1 (en) * | 2009-12-23 | 2015-09-02 | China Tobacco Chuanyu Industrial Co., Ltd | Composite filter comprising biological composition |
-
2015
- 2015-06-17 CN CN201510336913.5A patent/CN105167190B/en active Active
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4600026A (en) * | 1985-03-14 | 1986-07-15 | Qu Dong Fen | Tobacco composition with bluish dogbane and a process for the preparation thereof |
| CN101731747A (en) * | 2008-11-06 | 2010-06-16 | 张晓红 | Cigarette medicament capable of lowering tar, reducing harm and preventing diseases |
| EP2517584B1 (en) * | 2009-12-23 | 2015-09-02 | China Tobacco Chuanyu Industrial Co., Ltd | Composite filter comprising biological composition |
| CN102106606A (en) * | 2009-12-25 | 2011-06-29 | 湖北中烟工业有限责任公司 | Filter rod with visual perfumed beads as well as production process and equipment thereof |
| CN102342583A (en) * | 2010-08-02 | 2012-02-08 | 南通烟滤嘴有限责任公司 | Filter stick containing tobacco particles and preparation method thereof |
| CN104336776A (en) * | 2013-08-05 | 2015-02-11 | 贵州中烟工业有限责任公司 | Slow release aromatic base material, particles as well as preparation method and application thereof |
| CN103689802A (en) * | 2013-12-03 | 2014-04-02 | 红云红河烟草(集团)有限责任公司 | Tobacco porous particle and application thereof in cigarette |
| CN103876286A (en) * | 2014-03-04 | 2014-06-25 | 湖南中烟工业有限责任公司 | Filter rod particle additive with coffee or cocoa flavor and preparation method and application thereof |
| CN104068467A (en) * | 2014-07-01 | 2014-10-01 | 安徽中烟工业有限责任公司 | Electronic cigarette liquid rich in plant flavone |
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