CN105919154A - Blasting bead filter rod for reducing free radical in cigarette smoke - Google Patents

Blasting bead filter rod for reducing free radical in cigarette smoke Download PDF

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Publication number
CN105919154A
CN105919154A CN201610485504.6A CN201610485504A CN105919154A CN 105919154 A CN105919154 A CN 105919154A CN 201610485504 A CN201610485504 A CN 201610485504A CN 105919154 A CN105919154 A CN 105919154A
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CN
China
Prior art keywords
quick
free radical
filter stick
fried pearl
extract
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201610485504.6A
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Chinese (zh)
Inventor
吴景强
熊姗姗
何雪峰
沈靖轩
肖维毅
徐兰兰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Yunnan Reascend Tobacco Technology Group Co Ltd
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Yunnan Reascend Tobacco Technology Group Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Yunnan Reascend Tobacco Technology Group Co Ltd filed Critical Yunnan Reascend Tobacco Technology Group Co Ltd
Priority to CN201610485504.6A priority Critical patent/CN105919154A/en
Publication of CN105919154A publication Critical patent/CN105919154A/en
Pending legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/18Treatment of tobacco products or tobacco substitutes
    • A24B15/24Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/06Use of materials for tobacco smoke filters
    • A24D3/14Use of materials for tobacco smoke filters of organic materials as additive

Abstract

The invention discloses a blasting bead filter rod for reducing the free radical in cigarette smoke. The blasting bead filter rod is characterized in that a free radical reducing blasting bead is applied to the center of a cylindrical cigarette filter tow of the blasting bead filter rod. According to the blasting bead filter rod disclosed by the invention, the blasting bead which is filled with a plant extract, an animal extract, an enzymes scavenging agent and anti-oxidation powder is innovatively applied to the blasting bead filter rod, so that not only can the free radical in the cigarette smoke be reduced, but also the stability is high, and the security is high.

Description

A kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke
Technical field
The invention belongs to cigarette filter rod technical field.
Background technology
Free radical generally refers to the covalent bond in compound molecule under light, heat, high-energy ray radiation effects, or in internal metabolism Being containing the most paired free single electron by homolysis, it is quite active, easily captures the electronics on other molecule or atom, makes certainly Oneself reaches stable, thus destroys the structure of other molecule or atom.
Find about smoking and healthy research in recent years, during cigarette burning in addition to producing thousands of kinds of compounds, also produce high concentration Free radical, often suck a bite flue gas, free-radical contents therein is just more than 106Individual.Free radical in cigarette smoke is to cause The major reason of various diseases.The direct toxicity of Free Radicals In Cigarette Smoke is the materials such as coup injury cell and enzyme, and ties with DNA Conjunction makes cell transformation produce sudden change;Its indirect toxicity is can to activate and produce bigger other of a large amount of activity more high toxicity in vivo Free radical, such as superoxide radical and hydroxyl radical free radical, thus causes multiple pathological changes.Therefore, research reduces the side of flue gas free radical Method is of great significance for reducing harm of smoking tool.At present, free radical scavenger majority adds with liquid or powder type It is added in filter tip and Nicotiana tabacum L., as patent CN103626675A discloses a kind of Schiff 's base and preparation method thereof and as Medicated cigarette freedom The application of base scavenger, this invention is to be applied in cigarette shreds by free radical scavenger;Patent CN102860583A discloses The preparation method and application of a kind of natural baccy flue gas free radical scavenger, this invention is by natural baccy flue gas free radical scavenger Join Nicotiana tabacum L. or be sprayed onto in filter tip.Some have the free radical scavenger of non-oxidizability because of chemical under room temperature natural conditions Matter is more active, is directly appended in Medicated cigarette and filter stick there will be less stable, causes dropping free radical activity and reduces.
Summary of the invention
For above-mentioned the deficiencies in the prior art, it is an object of the invention to provide one and can reduce Free Radicals In Cigarette Smoke and stability Good quick-fried pearl filter stick.
The purpose of the present invention is achieved through the following technical solutions:
A kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke, is applied with fall free radical quick-fried at the cylindrical pipe tobacco center of filter stick Pearl.
The present invention can apply a fall quick-fried pearl of free radical at the cylindrical pipe tobacco center of filter stick, it is possible at the cylindrical cigarette of filter stick More than two the fall quick-fried pearls of free radical are applied centrally along being axially interrupted with tow.A diameter of 2mm of the described quick-fried pearl of fall free radical~ 5mm, is surrounded by free radical scavenger in the fall quick-fried pearl of free radical.Described free radical scavenger can reduce free radical in cigarette smoke One in plant extract, animal extracts, enzyme scavenger, non-oxidizability powder.Described plant extract is goldentop side Ear extract, Stropharia rugoso-annulata extract, JIGU extract, Liu Song mushroom extract, green tea extract, walnut shell extract, male One or more planted in peel extract, Thallus Laminariae (Thallus Eckloniae) extract, Herba Dendrobii extract, seed of Fructus Hippophae extract red.Described animal carries Taking thing is one or more in propolis, chitosan, omega-3 polybasic unsaturated fatty acid.Described enzyme scavenger is super oxygen One in compound dismutase, catalase, glutathion peroxidase.Described non-oxidizability powder is astaxanthin lyophilizing One or both in powder, freeze-dried sheep placenta extract powder.
The present invention will be equipped with plant extract, animal extracts, enzyme scavenger, non-oxidizability powder quick-fried pearl innovatively should In filter stick, in order to reduce the free radical in cigarette smoke.This addition manner is different from being sprayed by free radical scavenger of routine It is sprinkled upon in tobacco shred or cigarette filter.Additionally, enzyme scavenger and astaxanthin class non-oxidizability powder are directly appended in filter stick It is difficult to, because chemical property is more active under room temperature natural conditions, is directly appended in cigarette filter rod there will be stability Poor, cause dropping free radical activity and reduce.The present invention carries out parcel with quick-fried pearl form and is then added in filter stick the most well solve This technical problem.Stable performance when quick-fried pearl filter stick prepared by the present invention stores, has higher safety.
Detailed description of the invention
The present invention is described in detail below in conjunction with detailed description of the invention.But, protection scope of the present invention is not limited to retouch in detail below The preferred implementation stated.
Embodiment 1
Take JIGU extract 10mg, add in the minds of quick-fried pearl capsule, be prepared as the quick-fried pearl of fall free radical of a diameter of 2mm.At filter stick Apply this quick-fried pearl along location, axle center during wire-beam forming, use general filter stick formation Technology one-shot forming one meta structure Filter stick, obtains a kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke, then makes the sample Medicated cigarette containing quick-fried pearl filter stick.At Medicated cigarette Aspirate front hands to be pinched brokenly by the capsule in filter stick, can hear " " the sound, then according to standard method (GB/T19609-2004) Suction, the free radical total amount of every filter disc one cigarette cigarette of trapping, then carry out determining free radicals with ESR, with ESR signal Intensity is as the index of free radical amount, and calculates meansigma methods.Meanwhile, with the Medicated cigarette without quick-fried pearl as blank, and Free radical scavenging activity is calculated with this.Free radical scavenging efficiency is as shown in table 1.
Embodiment 2
Take Paeonia suffruticosa kind peel extract and each 10mg of pleurotus citrinopilestus, add in the minds of quick-fried pearl capsule, be prepared as a diameter of 2.5mm The quick-fried pearl of fall free radical.During filter stick wire-beam forming, apply this quick-fried pearl along location, axle center, use general filter stick formation work Technology one-shot forming one meta structure filter stick, obtains a kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke, then makes containing quick-fried pearl The sample Medicated cigarette of filter stick.With hands, the capsule in filter stick is pinched brokenly before cigarette smoking, can hear " " the sound, then according to Standard method (GB/T19609-2004) is aspirated, the free radical total amount of every filter disc one cigarette cigarette of trapping, then enters with ESR Row determining free radicals, using ESR signal intensity as the index of free radical amount, and calculates meansigma methods.Meanwhile, with without The Medicated cigarette of quick-fried pearl is blank, and calculates free radical scavenging activity with this.Free radical scavenging efficiency is as shown in table 1.
Embodiment 3
Take propolis 3mg, chitosan 8mg, add in the minds of quick-fried pearl capsule, be prepared as the quick-fried pearl of fall free radical of a diameter of 2mm.? Apply this quick-fried pearl along location, axle center during filter stick wire-beam forming, use general filter stick formation Technology one-shot forming unitary Structure filter stick, obtains a kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke, then makes the sample Medicated cigarette containing quick-fried pearl filter stick.? With hands, the capsule in filter stick is pinched brokenly before cigarette smoking, can hear " " the sound, then according to standard method (GB/T19609-2004) suction, the free radical total amount of every filter disc one cigarette cigarette of trapping, then carry out free radical with ESR Measure, using ESR signal intensity as the index of free radical amount, and calculate meansigma methods.Meanwhile, with the volume without quick-fried pearl Cigarette is blank, and calculates free radical scavenging activity with this.Free radical scavenging efficiency is as shown in table 1.
Embodiment 4
Take omega-3 polybasic unsaturated fatty acid 20mg, add in the minds of quick-fried pearl capsule, be prepared as the fall of a diameter of 3mm freely The quick-fried pearl of base.During filter stick wire-beam forming, apply this quick-fried pearl along location, axle center, use general filter stick formation Technology one Secondary molding one meta structure filter stick, obtains a kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke, then makes the sample containing quick-fried pearl filter stick Product Medicated cigarette.With hands, the capsule in filter stick is pinched brokenly before cigarette smoking, can hear " " the sound, then according to standard method (GB/T19609-2004) suction, the free radical total amount of every filter disc one cigarette cigarette of trapping, then carry out free radical with ESR Measure, using ESR signal intensity as the index of free radical amount, and calculate meansigma methods.Meanwhile, with the volume without quick-fried pearl Cigarette is blank, and calculates free radical scavenging activity with this.Free radical scavenging efficiency is as shown in table 1.
Embodiment 5
Take catalase 10mg, add in the minds of quick-fried pearl capsule, be prepared as the quick-fried pearl of fall free radical of a diameter of 3mm.At filter stick Apply two these quick-fried pearls along location, axle center during wire-beam forming, use general filter stick formation Technology one-shot forming one meta structure Filter stick, obtains a kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke, then makes the sample Medicated cigarette containing quick-fried pearl filter stick.At Medicated cigarette Aspirate front hands to be pinched brokenly by the capsule in filter stick, can hear " " the sound, then according to standard method (GB/T19609-2004) Suction, the free radical total amount of every filter disc one cigarette cigarette of trapping, then carry out determining free radicals with ESR, with ESR signal Intensity is as the index of free radical amount, and calculates meansigma methods.Meanwhile, with the Medicated cigarette without quick-fried pearl as blank, and Free radical scavenging activity is calculated with this.Free radical scavenging efficiency is as shown in table 1.
Embodiment 6
Take glutathion peroxidase 15mg, add in the minds of quick-fried pearl capsule, be prepared as the quick-fried pearl of fall free radical of a diameter of 4mm. During filter stick wire-beam forming, apply three these quick-fried pearls of fall free radical at cylindrical bundle centrally along being axially interrupted, use general Filter stick formation Technology one-shot forming one meta structure filter stick, obtains a kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke, then Make the sample Medicated cigarette containing quick-fried pearl filter stick.With hands, the capsule in filter stick is pinched brokenly before cigarette smoking, can hear " " the sound, Then according to standard method (GB/T19609-2004) suction, the free radical total amount of every filter disc one cigarette cigarette of trapping, then Carry out determining free radicals with ESR, using ESR signal intensity as the index of free radical amount, and calculate meansigma methods.Meanwhile, With the Medicated cigarette without quick-fried pearl as blank, and calculate free radical scavenging activity with this.Free radical scavenging efficiency is as shown in table 1.
Embodiment 7
Take astaxanthin 20mg, add in the minds of quick-fried pearl capsule, be prepared as the quick-fried pearl of fall free radical of a diameter of 3.5mm.In cylinder Tow applies two these quick-fried pearls of fall free radical centrally along being axially interrupted, and uses general filter stick formation Technology one-shot forming unitary to tie Structure filter stick, obtains a kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke, then makes the sample Medicated cigarette containing quick-fried pearl filter stick.At volume Cigarette aspirates front hands and is pinched brokenly by the capsule in filter stick, can hear " " the sound, then according to standard method (GB/T19609-2004) Suction, the free radical total amount of every filter disc one cigarette cigarette of trapping, then carry out determining free radicals with ESR, with ESR signal Intensity is as the index of free radical amount, and calculates meansigma methods.Meanwhile, with the Medicated cigarette without quick-fried pearl as blank, and Free radical scavenging activity is calculated with this.Free radical scavenging efficiency is as shown in table 1.
Embodiment 8
Take freeze-dried sheep placenta extract powder 10mg, add in the minds of quick-fried pearl capsule, be prepared as the quick-fried pearl of fall free radical of a diameter of 5mm.In filter Apply this quick-fried pearl in location, center during rod wire-beam forming, use general filter stick formation Technology one-shot forming one Meta structure filter stick, obtains a kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke, then makes the sample Medicated cigarette with quick-fried pearl filter stick. With hands, the capsule in filter stick is pinched brokenly before cigarette smoking, can hear " " the sound, then according to standard method (GB/T19609-2004) suction, the free radical total amount of every filter disc one cigarette cigarette of trapping, then carry out free radical with ESR Measure, using ESR signal intensity as the index of free radical amount, and calculate meansigma methods.Meanwhile, with the volume without quick-fried pearl Cigarette is blank, and calculates free radical scavenging activity with this.Free radical scavenging efficiency is as shown in table 1.
Table 1 free radical scavenging activity result
Sample Free radical scavenging activity
Embodiment 1 10.6%
Embodiment 2 13.2%
Embodiment 3 18.4%
Embodiment 4 19.3%
Embodiment 5 8.7%
Embodiment 6 20.4%
Embodiment 7 25.3%
Embodiment 8 18.7%
Above example, adds the free radical scavenger of the preparation fall quick-fried pearl of free radical in the minds of quick-fried pearl capsule to and can also is that Stropharia rugoso-annulata carries Take thing, Liu Song mushroom extract, green tea extract, walnut shell extract, Thallus Laminariae (Thallus Eckloniae) extract, Herba Dendrobii extract, seed of Fructus Hippophae The plant extracts such as extract.It can also be superoxide dismutase.

Claims (9)

1. the quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke, it is characterised in that execute at the cylindrical pipe tobacco center of filter stick Added with the fall quick-fried pearl of free radical.
A kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke the most according to claim 1, it is characterised in that at filter stick Cylindrical pipe tobacco center applies a fall quick-fried pearl of free radical.
A kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke the most according to claim 1, it is characterised in that at filter stick Cylindrical pipe tobacco applies more than two the fall quick-fried pearls of free radical centrally along being axially interrupted.
4. according to a kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke described in claim 1 or 2 or 3, it is characterised in that A diameter of 2mm~5mm of the described quick-fried pearl of fall free radical, is surrounded by free radical scavenger in the fall quick-fried pearl of free radical.
A kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke the most according to claim 4, it is characterised in that described freedom Base scavenger is to reduce the plant extract of free radical in cigarette smoke, animal extracts, enzyme scavenger, non-oxidizability powder One in end.
A kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke the most according to claim 5, it is characterised in that described plant Extract is pleurotus citrinopilestus, Stropharia rugoso-annulata extract, JIGU extract, Liu Song mushroom extract, green tea extract, core One or several in peach shell extract, Paeonia suffruticosa kind peel extract, Thallus Laminariae (Thallus Eckloniae) extract, Herba Dendrobii extract, seed of Fructus Hippophae extract Kind.
A kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke the most according to claim 5, it is characterised in that described animal Extract is one or more in propolis, chitosan, omega-3 polybasic unsaturated fatty acid.
A kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke the most according to claim 5, it is characterised in that described enzyme Scavenger is the one in superoxide dismutase, catalase, glutathion peroxidase.
A kind of quick-fried pearl filter stick reducing Free Radicals In Cigarette Smoke the most according to claim 5, it is characterised in that described antioxygen The property changed powder is one or both in astaxanthin lyophilized powder, freeze-dried sheep placenta extract powder.
CN201610485504.6A 2016-06-28 2016-06-28 Blasting bead filter rod for reducing free radical in cigarette smoke Pending CN105919154A (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108338406A (en) * 2018-02-13 2018-07-31 玉溪开元金蓝生物科技有限责任公司 A kind of quick-fried pearl of rosemary antioxidant and its application in cigarette filter rod
CN109875106A (en) * 2019-03-20 2019-06-14 福建绿色黄金生物科技有限公司 Composition, preparation method and applications

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CN104549085A (en) * 2015-01-12 2015-04-29 中国科学院化学研究所 Antioxidant enzyme nano capsules as well as preparation method and application thereof
CN105146745A (en) * 2013-10-18 2015-12-16 贵州中烟工业有限责任公司 Immobilized catalase additive for tobacco as well as preparation method and application of additive
CN105581364A (en) * 2016-03-07 2016-05-18 云南瑞升烟草技术(集团)有限公司 Preparation method of astaxanthin microcapsule and application to cigarette shreds

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CN101412945A (en) * 2007-10-16 2009-04-22 武汉烟草(集团)有限公司 Walnut shell extract and use thereof in cigarettes
CN102132953A (en) * 2010-12-29 2011-07-27 华宝食用香精香料(上海)有限公司 Method for preparing salvia miltiorrhiza extract microcapsules and use of product thereof
CN102367283A (en) * 2011-10-20 2012-03-07 广东中烟工业有限责任公司 Laminarin as well as extraction method and application thereof
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Publication number Priority date Publication date Assignee Title
CN108338406A (en) * 2018-02-13 2018-07-31 玉溪开元金蓝生物科技有限责任公司 A kind of quick-fried pearl of rosemary antioxidant and its application in cigarette filter rod
CN109875106A (en) * 2019-03-20 2019-06-14 福建绿色黄金生物科技有限公司 Composition, preparation method and applications

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Application publication date: 20160907