CN101103841A - Tobacco product - Google Patents
Tobacco product Download PDFInfo
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- CN101103841A CN101103841A CNA2007100623271A CN200710062327A CN101103841A CN 101103841 A CN101103841 A CN 101103841A CN A2007100623271 A CNA2007100623271 A CN A2007100623271A CN 200710062327 A CN200710062327 A CN 200710062327A CN 101103841 A CN101103841 A CN 101103841A
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- tobacco
- tobacco product
- seabuckthorn seeds
- seeds extract
- free radical
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Abstract
The invention belongs to a tobacco product technical field, substantially relates to a tobacco product comprising seabuckthorn seed extract, which displays the regional advantages of natural plant resources so as to meet the urgent needs of low free radical and safe tobacco in the cigarette industry development. The tobacco product comprising the seabuckthorn seed extract. The seabuckthorn seed extract accounts for 0.03 percent to 0.06 percent of the weight of tobacco shred in the tobacco product. The invention has the advantages that: a novel field of application for developing a new healthy purpose of the seabuckthorn seed. As a free radical scavenging agent for tobacco product, the seabuckthorn seed has obvious effect, and has a good prospect for developing low-toxicity and low free radical safe tobacco product.
Description
Technical field
The invention belongs to the technical field of tobacco product, be specifically related to a kind of tobacco product that contains the seabuckthorn seeds extract.
Background technology
People aspirate the flue gas that the tobacco product burning is produced, but exist pair cell to produce the free radical of poisoning in the flue gas.These cytotoxic molecules bring out cancer in smoker's body, particularly lung cancer.The safety-type tobacco product of Development and Production low free radical is the important R﹠D direction of tobacco product industry in recent years.
Summary of the invention
The invention provides a kind ofly with the tobacco product of seabuckthorn seeds extract as free radical scavenger, the regional advantages of its performance natural plant resource satisfy pressing for of cigarette industry exploitation low free radical safety type cigarette.
The present invention adopts following technical scheme to realize: a tobacco articles is characterized in that containing in the described tobacco product seabuckthorn seeds extract.Described seabuckthorn seeds extract accounts for 0.03%～0.06% (0.05% for best) of pipe tobacco weight in the tobacco product.Described tobacco product is cigarette, cigar or tobacco pipe pipe tobacco.
The step that described seabuckthorn seeds extract is added in the tobacco product pipe tobacco is: the seabuckthorn seeds extract is dissolved in the alcoholic solvent, the solvent that is dissolved with the seabuckthorn seeds extract is sprayed on the pipe tobacco, subsequently volatilization alcohol.Contain the seabuckthorn seeds extract in the described cigarette filter tip, account for 0.01%～0.03% (0.02% for best) of mouth rod weight, during interpolation the seabuckthorn seeds extract is dissolved in the triacetyl glycerine, become in the process to implement in the mouth clavate.
The anti-oxidant behavior of antioxidant has certain selectivity.The main component of the free radical in the flue gas is alkanes and alcoxyl type free base.Will effectively remove the free radical in the flue gas, selected antioxidant should have versatility, promptly has the ability of removing multiple free radical.The leaching liquor of the water of seabuckthorn seeds, ethanol, acetone, water-ethanol-acetone (1: 1: 1), ethyl acetate, chloroform, ether, benzinum, petroleum ether-ethyl acetate (1: 1) equal solvent, to active oxygen ultra-oxygen anion free radical and stabilized radical 1, the bitter diazanyl free radical of 1-diphenyl-2-all shows certain scavenging action, and wherein the antioxidation activity of acetone leaching liquor all is significantly higher than other solvents in two kinds of radicals scavenging tests.The concentration of each solvent leaching liquor all becomes dose-effect relationship with its clearance rate to free radical, and the concentration of leaching liquor is high more, and is strong more to measured by esr technique.Patent applicant's series of experimental research result shows that adding seabuckthorn seeds extract can be removed the free radical in the flue gas effectively when tobacco product aspirates, and promptly the seabuckthorn seeds extract meets the requirement of removing free radical in the tobacco.Add the tobacco product of seabuckthorn seeds extract and comparing of not adding, pair cell produces the molecule of the free radical of poisoning in the former flue gas, no matter is a gas phase or a phase, can both significantly be reduced.
The approach that obtains the seabuckthorn seeds extract has multiple, for example can obtain by polar solvent such as alcohol or aqueous alcohols solvent extraction.The alcohol that is used as solvent especially can be ethanol.This extract also can obtain by supercritical carbon dioxide extracting.Certainly also can carry out supercritical carbon dioxide extracting more earlier after polar solvent extracts obtains.Extract and the method for one-tenth branchs that separates the seabuckthorn seeds extract is a prior art, it was reported as 1, " seabuckthorn seeds OPC Study on Its Antioxidant Activity in Vitro " (2005 02 phases of Food Science); 2, " the anti-oxidant and antibacterial activity researchs of different seabuckthorn seeds extracts " (2006 01 phases of international sea-buckthorn research and development); 3, " research that the antioxidation activity of seabuckthorn seeds extract and phenols are formed " (2006 04 phases of research and development of natural products); 4, " seabuckthorn seeds slag and pomace flavonoid anti peroxidation of lipid, the effect of removing free radical " (2003 08 phases of Chinese patent drug); 5, " mensuration of total seabuckthorn flavone and antioxygenic property thereof " (2006 02 phases of Shanghai University Of Engineering Science's journal).
The main electron paramagnetic resonance method that adopts is tested in the process of the present invention, also uses additive method, particularly AAS simultaneously, test result has been done contrast reflected card, and the result conforms to.Used EPR spectrometer is a German BRUKER company.
1, blank test
Is the concentration adjustment of the gaseous phase free radical trapping agent DMPO in the organic solvent-benzene 20 mMs, and use 5 cigarette that are not added with the seabuckthorn seeds extract to carry out in its flue gas gas phase and grain catching of free radical mutually, carrying out free radical with ESR then measures, with the index of ESR signal strength signal intensity as the free radical amount, inferior mean value is calculated in parallel determination 5 times.
2, clearance test
Use the cigarette of seabuckthorn seeds extract to carry out in its flue gas gas phase and grain catching of free radical mutually, repetition aforesaid operations.
The double integrator quantitative result shows, adds the cigarette of seabuckthorn seeds extract and comparing of not adding, the quantity of the molecule of cytotoxin free radical in the former flue gas, and gaseous phase free radical reduces by 40～50%, and grain phase free radical reduces by 50～60%.
Fig. 1 is the paramagnetic resonance signal recording curve of certain blank test, and wherein label is 035 to be the primary signal curve of gas phase, and label is that 037 is the double integrator curve of gas phase.Label is
*038 is the primary signal curve of grain phase, and label is the 040 double integrator curves for the grain phase.The biproduct score value of 037 curve is that the biproduct score value of 66401.279562,040 curves is 48327.570587.
Fig. 2 is the paramagnetic resonance signal recording curve of certain clearance test, and wherein label is 053 to be the primary signal curve of gas phase, and label is,
*055 is the double integrator curve of gas phase.Label is the 056 primary signal curves for the grain phase, and label is the 059 double integrator curves for the grain phase.
*The biproduct score value of 055 curve is that the biproduct score value of 35856.690964,059 curves is 22230.682470.
The experimental condition that obtains Fig. 1 and 2 is: sweep the collection collection of illustrative plates slowly, central magnetic field=3385.0GS sweeps wide 200.0GS, microwave frequency=9.4800GHz.
With regard to Fig. 1 and 2, grain phase free radical reduced rate=(48327.570587-22230.682470)/48327.570587=54%; The gaseous phase free radical reduced rate=(66401.279562-35856.690964)/66401.279562=46%.
Because the inhomogeneities that extract applies, during repeatedly free radical detected, the seabuckthorn seeds extract reduced the ratio of grain phase free radical in the cigarette smoke between 50～60%, and mean value is 55%; The ratio that reduces gaseous phase free radical in the cigarette smoke is between 40～50%, and mean value is 45%.
(5) sensory quality assessment
Through specialty smoke panel test personnel to the test cigarette contrast of propping up secretly comment, consistently think that the cigarette flavor style there is not change substantially, contain seabuckthorn seeds extract cigarette and prop up being better than blank cigarette aspect dry sensation and the pleasant impression and prop up.
The invention has the beneficial effects as follows, excavated new health purpose for seabuckthorn seeds and opened up a new application.The seabuckthorn seeds extract is as the tobacco product free radical scavenger, and effect is obvious, and exploitation low toxicity safety-type tobacco product harmful, low free radical is had good application prospects.
Description of drawings
Fig. 1 is the paramagnetic resonance signal recording curve of certain blank test.
Fig. 2 is the paramagnetic resonance signal recording curve of certain clearance test.
The specific embodiment
The present invention is described further by embodiment, but scope of invention is not subjected to the limitation of illustrated embodiment.
Embodiment 1
(1) preparation of seabuckthorn seeds extract
The fresh sea-buckthorn fleshing of harvesting is got seed, cleans, and dries naturally, pulverizes, and adds ethanol (70%) in 40 ℃ of lixiviates 6 hours of vibrating down, and is centrifugal, with supernatant concentration and dry, promptly gets the seabuckthorn seeds extract.
(2) in the pipe tobacco of cigarette and filter tip, add the extract that is obtained
Extract rolled in the pipe tobacco of production of cigarettes add pipe tobacco in the process.The seabuckthorn seeds extract that is added in the pipe tobacco accounts for 0.05% of pipe tobacco weight.Concrete grammar is earlier the said extracted thing of seabuckthorn seeds to be dissolved in the ethanol, is sprayed at the ethanol that is dissolved with the seabuckthorn seeds extract on the pipe tobacco or in the filter tip, and ethanol is volatilized subsequently falls.The seabuckthorn seeds extract is added in the mouth rod, the seabuckthorn seeds extract can be dissolved in the triacetyl glycerine, become in the process to implement in the mouth clavate.Be added into the seabuckthorn seeds extract in the mouth rod, account for about 0.02% of mouth rod weight.
(3) will contain the pipe tobacco and the mouth rod of seabuckthorn seeds extract, last machine rolls into qualified cigarette and props up, usefulness to be detected.To not contain the pipe tobacco and the mouth rod of seabuckthorn seeds extract, last machine rolls into qualified cigarette and props up, and treats contrast usefulness.
(4) the removing effect of free radical in the cigarette smoke
The detection of free radical has multiple known method to adopt, electron spin resonance (ESR) for example, chromatography, chemoluminescence method, XRF, AAS etc.One of the device people such as visible Pryor that are used for holding back cigarette smoke gas phase and grain phase free radical publication " Environmengtal HealthPerspectives " (1976, vol.16, report pp161-175).
Embodiment 2
(1) preparation of seabuckthorn seeds extract
The preparation method is with embodiment 1.
(2) in the pipe tobacco of cigarette and filter tip, add the extract that is obtained
Extract rolled in the pipe tobacco of production of cigarettes add pipe tobacco in the process.The seabuckthorn seeds extract that is added in the pipe tobacco accounts for 0.06% of pipe tobacco weight.Concrete grammar is with embodiment 1.The seabuckthorn seeds extract is added in the mouth rod, and concrete grammar is with embodiment 1.Be added into the seabuckthorn seeds extract in the mouth rod, account for about 0.01% of mouth rod weight.
(3) will contain the pipe tobacco and the mouth rod of seabuckthorn seeds extract, last machine rolls into qualified cigarette and props up.
(4) the removing effect of free radical in the cigarette smoke
Detection method is with embodiment 1
Embodiment 3
(1) preparation of seabuckthorn seeds extract
The preparation method is with embodiment 1.
(2) in the pipe tobacco of cigarette and filter tip, add the extract that is obtained
Extract rolled in the pipe tobacco of production of cigarettes add pipe tobacco in the process.The seabuckthorn seeds extract that is added in the pipe tobacco accounts for 0.03% of pipe tobacco weight.Concrete grammar is with embodiment 1.The seabuckthorn seeds extract is added in the mouth rod, and concrete grammar is with embodiment 1.Be added into the seabuckthorn seeds extract in the mouth rod, account for 0.03% of mouth rod weight.
(3) will contain the pipe tobacco and the mouth rod of seabuckthorn seeds extract, last machine rolls into qualified cigarette and props up.
(4) the removing effect of free radical in the cigarette smoke
Detection method is with embodiment 1.
Claims (8)
1. a tobacco articles is characterized in that containing in the described tobacco product seabuckthorn seeds extract.
2. tobacco product according to claim 1 is characterized in that described seabuckthorn seeds extract accounts for 0.03%～0.06% of pipe tobacco weight in the tobacco product.
3. tobacco product according to claim 1, it is characterized in that the step that described seabuckthorn seeds extract adds in the tobacco product pipe tobacco being: the seabuckthorn seeds extract is dissolved in the alcoholic solvent, the solvent that is dissolved with the seabuckthorn seeds extract is sprayed on the pipe tobacco, subsequently volatilization alcohol.
4. according to claim 1 or 2 or 3 described tobacco products, it is characterized in that described seabuckthorn seeds extract accounts for 0.05% of pipe tobacco weight in the tobacco product.
5. according to claim 1 or 2 or 3 described tobacco products, it is characterized in that described tobacco product is cigarette, cigar or tobacco pipe pipe tobacco.
6. tobacco product according to claim 4 is characterized in that described tobacco product is cigarette, cigar or tobacco pipe pipe tobacco.
7. tobacco product according to claim 6, it is characterized in that containing in the described cigarette filter tip seabuckthorn seeds extract, account for 0.01%～0.03% of mouth rod weight, during interpolation the seabuckthorn seeds extract is dissolved in the triacetyl glycerine, become in the process to implement in the mouth clavate.
8. tobacco product according to claim 7 is characterized in that containing the seabuckthorn seeds extract in the described cigarette filter tip, accounts for 0.02% of mouth rod weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007100623271A CN101103841A (en) | 2007-07-14 | 2007-07-14 | Tobacco product |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNA2007100623271A CN101103841A (en) | 2007-07-14 | 2007-07-14 | Tobacco product |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN101103841A true CN101103841A (en) | 2008-01-16 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNA2007100623271A Pending CN101103841A (en) | 2007-07-14 | 2007-07-14 | Tobacco product |
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102499451A (en) * | 2011-10-11 | 2012-06-20 | 中国烟草总公司郑州烟草研究院 | Refreshing tablet smokeless tobacco product added with sea-buckthorn preparation |
| CN101843363B (en) * | 2010-05-13 | 2013-05-22 | 云南烟草科学研究院 | Application of seabuckthorn in preparing cigarette and application method |
| CN104031163A (en) * | 2014-06-26 | 2014-09-10 | 河南中烟工业有限责任公司 | Sea buckthorn polysaccharide and extraction and purification method thereof, and application of sea buckthorn polysaccharide as tobacco humectant |
| CN104921289A (en) * | 2015-06-17 | 2015-09-23 | 云南中烟工业有限责任公司 | Honeysuckle glyceryl triacetate extract and application thereof in cigarette |
| CN105919154A (en) * | 2016-06-28 | 2016-09-07 | 云南瑞升烟草技术（集团）有限公司 | Blasting bead filter rod for reducing free radical in cigarette smoke |
| CN107467709A (en) * | 2017-08-25 | 2017-12-15 | 四川中烟工业有限责任公司 | Chinese style style pipe tobacco process for making |
| CN107586615A (en) * | 2017-11-01 | 2018-01-16 | 广东长利香精香料有限公司 | A kind of abundant essence of cigarette perfume |
-
2007
- 2007-07-14 CN CNA2007100623271A patent/CN101103841A/en active Pending
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101843363B (en) * | 2010-05-13 | 2013-05-22 | 云南烟草科学研究院 | Application of seabuckthorn in preparing cigarette and application method |
| CN102499451A (en) * | 2011-10-11 | 2012-06-20 | 中国烟草总公司郑州烟草研究院 | Refreshing tablet smokeless tobacco product added with sea-buckthorn preparation |
| CN102499451B (en) * | 2011-10-11 | 2013-05-08 | 中国烟草总公司郑州烟草研究院 | Refreshing tablet smokeless tobacco product added with sea-buckthorn preparation |
| CN104031163A (en) * | 2014-06-26 | 2014-09-10 | 河南中烟工业有限责任公司 | Sea buckthorn polysaccharide and extraction and purification method thereof, and application of sea buckthorn polysaccharide as tobacco humectant |
| CN104921289A (en) * | 2015-06-17 | 2015-09-23 | 云南中烟工业有限责任公司 | Honeysuckle glyceryl triacetate extract and application thereof in cigarette |
| CN105919154A (en) * | 2016-06-28 | 2016-09-07 | 云南瑞升烟草技术（集团）有限公司 | Blasting bead filter rod for reducing free radical in cigarette smoke |
| CN107467709A (en) * | 2017-08-25 | 2017-12-15 | 四川中烟工业有限责任公司 | Chinese style style pipe tobacco process for making |
| CN107467709B (en) * | 2017-08-25 | 2019-03-22 | 四川中烟工业有限责任公司 | Chinese style style pipe tobacco process for making |
| CN107586615A (en) * | 2017-11-01 | 2018-01-16 | 广东长利香精香料有限公司 | A kind of abundant essence of cigarette perfume |
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Open date: 20080116 |