CN103349354A - Sage extract, preparation method thereof and application of sage extract taken as tobacco product additive - Google Patents
Sage extract, preparation method thereof and application of sage extract taken as tobacco product additive Download PDFInfo
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- CN103349354A CN103349354A CN2013102684716A CN201310268471A CN103349354A CN 103349354 A CN103349354 A CN 103349354A CN 2013102684716 A CN2013102684716 A CN 2013102684716A CN 201310268471 A CN201310268471 A CN 201310268471A CN 103349354 A CN103349354 A CN 103349354A
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- Prior art keywords
- extract
- sage
- sage extract
- weight
- pipe tobacco
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- 235000020752 sage extract Nutrition 0.000 title claims abstract description 59
- 229940112950 sage extract Drugs 0.000 title claims abstract description 56
- 235000019505 tobacco product Nutrition 0.000 title claims abstract description 13
- 239000000654 additive Substances 0.000 title claims abstract description 12
- 230000000996 additive effect Effects 0.000 title claims abstract description 12
- 238000002360 preparation method Methods 0.000 title claims abstract description 11
- 239000000284 extract Substances 0.000 claims abstract description 38
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 29
- 238000006243 chemical reaction Methods 0.000 claims abstract description 10
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 9
- 239000008103 glucose Substances 0.000 claims abstract description 9
- 239000002798 polar solvent Substances 0.000 claims abstract description 9
- 150000001413 amino acids Chemical class 0.000 claims abstract description 7
- 239000002994 raw material Substances 0.000 claims abstract description 5
- 241000208125 Nicotiana Species 0.000 claims description 33
- 235000002637 Nicotiana tabacum Nutrition 0.000 claims description 33
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 14
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 13
- 244000143590 Salvia chinensis Species 0.000 claims description 11
- 235000007154 Salvia chinensis Nutrition 0.000 claims description 11
- 235000005794 Salvia japonica Nutrition 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 8
- DHMQDGOQFOQNFH-UHFFFAOYSA-N Glycine Chemical compound NCC(O)=O DHMQDGOQFOQNFH-UHFFFAOYSA-N 0.000 claims description 6
- 235000001014 amino acid Nutrition 0.000 claims description 6
- COLNVLDHVKWLRT-QMMMGPOBSA-N L-phenylalanine Chemical compound OC(=O)[C@@H](N)CC1=CC=CC=C1 COLNVLDHVKWLRT-QMMMGPOBSA-N 0.000 claims description 4
- 238000000605 extraction Methods 0.000 claims description 4
- COLNVLDHVKWLRT-UHFFFAOYSA-N phenylalanine Natural products OC(=O)C(N)CC1=CC=CC=C1 COLNVLDHVKWLRT-UHFFFAOYSA-N 0.000 claims description 4
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 claims description 3
- 239000004471 Glycine Substances 0.000 claims description 3
- 235000013922 glutamic acid Nutrition 0.000 claims description 3
- 239000004220 glutamic acid Substances 0.000 claims description 3
- 238000004519 manufacturing process Methods 0.000 claims description 3
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 claims description 2
- 239000003205 fragrance Substances 0.000 abstract description 4
- 239000000779 smoke Substances 0.000 abstract description 4
- 238000011161 development Methods 0.000 abstract description 2
- 230000000638 stimulation Effects 0.000 abstract description 2
- 235000019645 odor Nutrition 0.000 abstract 1
- 235000002020 sage Nutrition 0.000 abstract 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 6
- 230000000694 effects Effects 0.000 description 5
- 239000007788 liquid Substances 0.000 description 4
- 230000001105 regulatory effect Effects 0.000 description 4
- 235000013599 spices Nutrition 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- 239000003546 flue gas Substances 0.000 description 3
- 125000003118 aryl group Chemical group 0.000 description 2
- 238000004939 coking Methods 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 238000011160 research Methods 0.000 description 2
- 230000000391 smoking effect Effects 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 241000196324 Embryophyta Species 0.000 description 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 1
- 229930182558 Sterol Natural products 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000011285 coke tar Substances 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000004069 differentiation Effects 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000796 flavoring agent Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 235000013355 food flavoring agent Nutrition 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 241000411851 herbal medicine Species 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 150000007524 organic acids Chemical class 0.000 description 1
- 239000002304 perfume Substances 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 238000001556 precipitation Methods 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 150000003432 sterols Chemical class 0.000 description 1
- 235000003702 sterols Nutrition 0.000 description 1
- 238000000194 supercritical-fluid extraction Methods 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Abstract
The invention discloses a sage extract which takes sage as a raw material. The extract is extracted with a polar solvent with the weight of 1-5 times of that of the extract and a pH value of 7.5-9.5, an extracting solution is concentrated into an extractum, glucose with the weight of 20%-40% of that of the extractum and an amino acid with the weight of 5%-10% of that of the extractum are added to the extractum, an reaction is performed at a temperature of 50-120 GDEG C for 0.5-2 hours. The invention further discloses a preparation method of the sage extract and an application of the sage extract taken as a tobacco product additive. When a tobacco product made of the sage extract is smoked, fragrance can be enhanced effectively and is abundant, the thickness of the smoke is enhanced, offensive odors are covered, and stimulation is reduced remarkably. The sage extract, the preparation method and the application have a good application prospect in development of 'Chinese style cigarette' products with unique styles.
Description
Technical field
The present invention relates to the product that a kind of natural plant extracts obtains by Maillard reaction, a kind of Sage extract specifically the invention still further relates to the preparation method of Sage extract and as the purposes of additive of tobacco product.
Background technology
" Chinese-style cigarette " core competitiveness is to form the selling point style, embodies personalization and differentiation, adapts to sucking of Chinese consumers in general and is accustomed to and consumer need.The Chinese style essence spice for cigarette is Chinese-style cigarette product " soul ", is the secret place that " Chinese-style cigarette " style characteristic forms.Flavoring and casing scientifically in cigarette, the just important means of the personalized style of outstanding cigarette product.Simultaneously, in order to improve the security of smoking, lowering harm and decreasing coking becomes an important component part of " Chinese-style cigarette ".When reducing coke tar in cigarette, promote and raising flue gas concentration and fragrance, also only by means of the flavoring and casing technology.Along with going deep into of Chinese-style cigarette lowering harm and decreasing coking work, reinforced its importance that further demonstrates of tobacco flavoring.
Construct Chinese style essence spice for cigarette and the new technology of independent intellectual property right, from the natural herbal plant, extract essence and flavoring agent, succession Chinese herbal medicine in thousand is used for cigarette, allow the refined perfume (or spice) of healthy theory along with cigarette, moving towards together the consumer, is one of basic research of development " Chinese-style cigarette ".
Salvia japonica has the aromatic style of self uniqueness, contains multiple organic acid, sterol, has the prospect as essence spice for cigarette.But only have Salvia japonica and the extract thereof that see at present report are used to Chinese medicine, food etc., and extraction process is simple water extraction or CO
2Supercritical extraction process extracts wherein certain or certain several target component, has no the bibliographical information that Sage extract is used to cigarette additive.And in our research process, find the simple resulting Sage extract of extraction process by water extract-alcohol precipitation or alcohol extracting-water precipitating, have larger negative effect, can't satisfy the instructions for use as cigarette additive.
Summary of the invention
Purpose of the present invention is exactly the defective for prior art, provides a kind of Sage extract and preparation method thereof and as the purposes of additive of tobacco product.
Technical scheme of the present invention is:
A kind of Sage extract, it is as raw material take Salvia japonica, be that 7.5 ~ 9.5 polar solvent extracts with the pH value of 1 ~ 5 times of weight, extract is condensed into relative density (with respect to the density of water, lower with) be 1.15 ~ 1.25 medicinal extract, in medicinal extract, add the glucose of medicinal extract weight 20 ~ 40% and 5 ~ 10% amino acid again, made in 0.5 ~ 2 hour 50 ~ 120 ℃ of lower reactions.
Wherein said polar solvent is 0 ~ 15%(mass concentration, lower with) ethanol water.
The present invention further provides the preparation method of Sage extract, it may further comprise the steps: take Salvia japonica as raw material, be that 7.5 ~ 9.5 polar solvent extracts with the pH value of 1 ~ 5 times of weight, it is 1.15 ~ 1.25 medicinal extract that extract is condensed into relative density, in medicinal extract, add the glucose of medicinal extract weight 20 ~ 40% and 5 ~ 10% amino acid again, 50 ~ 120 ℃ of lower reactions 0.5 ~ 2 hour.
Wherein said polar solvent is 0 ~ 15% ethanol water.
The temperature of wherein said extraction is 50 ~ 90 ℃, and the time is 1 ~ 5 hour.
Wherein said amino acid is glutamic acid or glycine or phenylalanine.
The present invention further provides the purposes of Sage extract as additive of tobacco product again, and it is that Sage extract is added in the pipe tobacco of cigarette, and the Sage extract that is added in the pipe tobacco accounts for 0.01% ~ 0.05% of pipe tobacco weight.
Preferably, the Sage extract that wherein is added in the pipe tobacco accounts for 0.02% ~ 0.04% of pipe tobacco weight.
Technical scheme is that Sage extract is soluble in water preferably, the water that is dissolved with Sage extract is rolled at the pipe tobacco of production of cigarettes be sprayed in the process on the pipe tobacco, then flings to water.
One tobacco articles contains claim 1 or 2 described Sage extracts, and described Sage extract accounts for 0.01% ~ 0.05% of pipe tobacco weight, is preferably Sage extract and accounts for 0.02% ~ 0.04% of pipe tobacco weight.
A series of experimental studies of smokeing panel test show, the tobacco product that adds Sage extract flavouring effectively when suction, and fragrance is abundant, the solid sense of flue gas increases, assorted be so incensed that to cover, excitant obviously reduces.
The present invention is that Sage extract has been opened up a new application, has increased new effect and the effect of Salvia japonica.Sage extract is as additive of tobacco product, and successful has good application prospect to " Chinese-style cigarette " goods of developing characteristic style.
The specific embodiment
The present invention is described further below by embodiment.
Embodiment 1
A kind of Sage extract, it prepares as follows:
NaOH is joined in 5% ethanol water first, regulating ethanol water pH value is 9.5, ethanol water and Salvia japonica weight ratio are 3, extracted 3 hours at 90 ℃, isolate feed liquid after, be concentrated into the medicinal extract shape, relative density is 1.15, in medicinal extract, add the glucose of medicinal extract weight 20% and 5% glutamic acid, at 120 ℃ of lower reaction 0.5h, namely obtain Sage extract of the present invention.
Extract rolled in the pipe tobacco of production of cigarettes add pipe tobacco in the process.Be added into the Sage extract in the pipe tobacco, account for 0.03% of pipe tobacco weight.Concrete grammar is first soluble in water Sage extract, and the aqueous solution that is dissolved with Sage extract evenly is sprayed on the pipe tobacco, and water evaporates subsequently.Pipe tobacco rolls into test sample cigarette through cigarette machine.
Embodiment 2
A kind of Sage extract, it prepares as follows:
Potassium hydroxide is joined in 15% ethanol water first, regulating ethanol water pH value is 8.5, ethanol water and Salvia japonica weight ratio are 5, extracted 4 hours at 50 ℃, isolate feed liquid after, be concentrated into the medicinal extract shape, relative density is 1.25, in medicinal extract, add the glucose of medicinal extract weight 30% and 10% glycine, at 80 ℃ of lower reaction 1.5h, namely obtain Sage extract of the present invention.
Application process is identical with embodiment 1, difference be Sage extract account for pipe tobacco weight 0.05%.
Embodiment 3
A kind of Sage extract, it prepares as follows:
First ammoniacal liquor is joined in the pure water, regulating the pH value is 7.5, water and Salvia japonica weight ratio are 1, extracted 1 hour at 60 ℃, isolate feed liquid after, be concentrated into the medicinal extract shape, relative density is 1.2, in medicinal extract, add the glucose of medicinal extract weight 40% and 8% phenylalanine, at 50 ℃ of lower reaction 2h, namely obtain Sage extract of the present invention.
Application process is identical with embodiment 1, difference be Sage extract account for pipe tobacco weight 0.02%.
Embodiment 4
A kind of Sage extract, it prepares as follows:
NaOH is joined in 10% ethanol water first, regulating ethanol water pH value is 9.0, ethanol water and Salvia japonica weight ratio are 4, extracted 5 hours at 80 ℃, isolate feed liquid after, be concentrated into the medicinal extract shape, relative density is 1.2, in medicinal extract, add the glucose of medicinal extract weight 25% and 5% phenylalanine, at 100 ℃ of lower reaction 1h, namely obtain Sage extract of the present invention.
Application process is identical with embodiment 1, difference be Sage extract account for pipe tobacco weight 0.04%.
Embodiment 5
Effect experiment in the cigarette smoke:
Be taken at two parts of the good finished cut tobacco of 22 ℃ ± 1 ℃ of temperature and 60% ± 2% time balance of relative humidity (RH) 40 grams, take by weighing Sage extract by 0.04% of its quality, behind the dilute with water, be sprayed on equably on the pipe tobacco with the larynx jet pipe, perfuming and not the aromatic tobacco sample be placed in the climatic chamber of 22 ℃ ± 1 ℃ of temperature and RH60% ± 2% balance 48 hours, with fill out the cigarette device respectively with perfuming and not the pipe tobacco of perfuming make cigarette, 22 ℃ ± 1 ℃ and RH60% ± 2% time balance 48 hours, please cigarette sensory evaluating smoking group smoke panel test again.
The personnel that smoke panel test unanimously think the Sage extract that adds flavouring effectively when tobacco product aspirate, and fragrance is abundant, the solid sense of increase flue gas; And has the effect of covering assorted gas, reducing stimulation.
Claims (10)
1. Sage extract, it is as raw material take Salvia japonica, be that 7.5 ~ 9.5 polar solvent extracts with the pH value of 1 ~ 5 times of weight, it is 1.15 ~ 1.25 medicinal extract that extract is condensed into relative density, in medicinal extract, add the glucose of medicinal extract weight 20 ~ 40% and 5 ~ 10% amino acid again, made in 0.5 ~ 2 hour 50 ~ 120 ℃ of lower reactions.
2. Sage extract according to claim 1, wherein said polar solvent is that mass concentration is 0 ~ 15% ethanol water.
3. the preparation method of a Sage extract, it may further comprise the steps: take Salvia japonica as raw material, be that 7.5 ~ 9.5 polar solvent extracts with the pH value of 1 ~ 5 times of weight, it is 1.15 ~ 1.25 medicinal extract that extract is condensed into relative density, in medicinal extract, add the glucose of medicinal extract weight 20 ~ 40% and 5 ~ 10% amino acid again, 50 ~ 120 ℃ of lower reactions 0.5 ~ 2 hour.
4. the preparation method of Sage extract according to claim 1, wherein said polar solvent is that mass concentration is 0 ~ 15% ethanol water.
5. the preparation method of Sage extract according to claim 1, the temperature of wherein said extraction is 50 ~ 90 ℃, the time is 1 ~ 5 hour.
6. the preparation method of Sage extract according to claim 1, wherein said amino acid is glutamic acid or glycine or phenylalanine.
7. claim 1 or 2 described Sage extracts are as the purposes of additive of tobacco product, and it is that Sage extract is added in the pipe tobacco of cigarette, and the Sage extract that is added in the pipe tobacco accounts for 0.01% ~ 0.05% of pipe tobacco weight.
8. Sage extract according to claim 7 is as the purposes of additive of tobacco product, and the Sage extract that wherein is added in the pipe tobacco accounts for 0.02% ~ 0.04% of pipe tobacco weight.
9. Sage extract according to claim 6 is as the purposes of additive of tobacco product, and is wherein that Sage extract is soluble in water, the water that is dissolved with Sage extract rolled at the pipe tobacco of production of cigarettes be sprayed in the process on the pipe tobacco, then flings to water.
10. a tobacco articles contains claim 1 or 2 described Sage extracts, and described Sage extract accounts for 0.01% ~ 0.05% of pipe tobacco weight.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310268471.6A CN103349354B (en) | 2013-06-28 | 2013-06-28 | Sage extract and preparation method thereof and the purposes as additive of tobacco product |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201310268471.6A CN103349354B (en) | 2013-06-28 | 2013-06-28 | Sage extract and preparation method thereof and the purposes as additive of tobacco product |
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| Publication Number | Publication Date |
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| CN103349354A true CN103349354A (en) | 2013-10-16 |
| CN103349354B CN103349354B (en) | 2015-11-18 |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103750545A (en) * | 2014-01-15 | 2014-04-30 | 红云红河烟草(集团)有限责任公司 | Tobacco ageing method by blending tobacco with rosemary and sage |
| CN105238564A (en) * | 2015-06-18 | 2016-01-13 | 湖北中烟工业有限责任公司 | Preparation method and application of Maillard reaction product of Rhodiola rosea extract |
| CN108142985A (en) * | 2017-12-25 | 2018-06-12 | 江西中烟工业有限责任公司 | A kind of delicate fragrance type tobacco extract and preparation method thereof |
| CN108634362A (en) * | 2018-04-12 | 2018-10-12 | 江西中烟工业有限责任公司 | A kind of preparation method and applications of compound cigarette fumet |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103750545A (en) * | 2014-01-15 | 2014-04-30 | 红云红河烟草(集团)有限责任公司 | Tobacco ageing method by blending tobacco with rosemary and sage |
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| CN108142985A (en) * | 2017-12-25 | 2018-06-12 | 江西中烟工业有限责任公司 | A kind of delicate fragrance type tobacco extract and preparation method thereof |
| CN108142985B (en) * | 2017-12-25 | 2020-04-10 | 江西中烟工业有限责任公司 | Faint scent type tobacco extract |
| CN108634362A (en) * | 2018-04-12 | 2018-10-12 | 江西中烟工业有限责任公司 | A kind of preparation method and applications of compound cigarette fumet |
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| Publication number | Publication date |
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| CN103349354B (en) | 2015-11-18 |
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