CN108142985A - A kind of delicate fragrance type tobacco extract and preparation method thereof - Google Patents
A kind of delicate fragrance type tobacco extract and preparation method thereof Download PDFInfo
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- CN108142985A CN108142985A CN201711416575.1A CN201711416575A CN108142985A CN 108142985 A CN108142985 A CN 108142985A CN 201711416575 A CN201711416575 A CN 201711416575A CN 108142985 A CN108142985 A CN 108142985A
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- extraction
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- cigarette
- propylene glycol
- pasty masses
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
- Tea And Coffee (AREA)
Abstract
The invention discloses a kind of delicate fragrance type tobacco extracts, are made from the following raw materials in parts by weight：Tea tree young leaves 45~52, salvia officianlis 9~15, flores aurantii 2~5 and appropriate propylene glycol, preparation method include the following steps：(1) tea tree young leaves blended, steam beating, cooling, drying, the separation of stalk leaf, remove sandstone, sterilization, rapid draing grinding, extraction, filtering, concentration, obtain pasty masses A；(2) it by salvia officianlis ultrasound interval extraction reflux, collection extracting solution, is concentrated under reduced pressure, obtains pasty masses B；(3) flores aurantii is subjected to supercritical CO2Extraction, adds honey after separation, stirs evenly, obtain pasty masses C；(4) by pasty masses A, B, C and mixed with propylene glycol；(5) paste mixture is taken to be sprayed on pipe tobacco, cigarette is made in pipe tobacco with Cigarette making device.The present invention has special faint scent, the effect of giving full play to natural plant extracts, can play the role of reducing oral cavity and dry throat sense, anti-oxidant and refresh oneself, loosen.
Description
Technical field
The present invention relates to cigarette technical field, a kind of particularly delicate fragrance type tobacco extract and preparation method thereof.
Background technology
In the prior art, " Chinese-style cigarette " core competitiveness is to form selling point style, embodies personalized and differentiation,
Adapt to Chinese consumers in general sucks custom and consumer need.Chinese style essence spice for cigarette is the " spirit of Chinese-style cigarette product
Soul " is the secret place that " Chinese-style cigarette " style characteristic is formed.Scientifically flavoring and casing, exactly prominent cigarette produce in cigarette
The important means of the personalized style of product.Meanwhile for the safety for improving smoking, lowering harm and decreasing coking has become " Chinese-style cigarette "
One important component.While coke tar in cigarette is reduced, also promote and improve flue gas concentration and fragrance, only by means of adding
Fragrant feeding technique.With going deep into for Chinese-style cigarette lowering harm and decreasing coking work, tobacco flavoring charging shows its importance further.
The Chinese style essence spice for cigarette and new technology of independent intellectual property right are constructed, it is fragrant that essence is extracted from natural herbal plant
Material allows the theory of health to move towards consumer together with the refined perfume (or spice) of cigarette, be one of basic research for developing " Chinese-style cigarette ".
Tea tree young leaves have pleasant faint scent, add in cigarette, can assign cigarette special aromatic style.And containing abundant
Nutritional ingredient and trace element, mainly have tea polyphenols, caffeine, free amino acid, chlorophyll, protein, aromatic substance, fibre
Dimension element, multivitamin and various trace elements.
Tea polyphenols have very strong inoxidizability and physiological activity, are the scavengers of human free radical, help to delay to decline
Always；Tea polyphenols can also block the synthesis of a variety of carcinogen in vivo such as ammonium nilrite, and with direct killing cancer cell and
The effect of improving human body immunocompetence；Tea polyphenols have stronger astriction, have apparent inhibition to pathogen, virus and kill
Effect, has positive effect to anti-inflammatory antidiarrheal.
Caffeine can promote human central nervous excited, enhance corticocerebral excited process, play benefit of refreshing oneself and think, clear away heart-fire
Effect, contribute to arousing brain, raising spirit；Caffeine can also stimulate kidney, and urine is promoted to excrete rapidly, improve filtering out for kidney
Rate reduces harmful substance residence time in kidney.Caffeine can also exclude excessive lactic acid, help human body is made to eliminate as early as possible tired
Labor contributes to diuresis to recover from fatigue.
Salvia officianlis complete stool has strong cooling fragrance, special herbaceous aroma, and blade gives out light pineapple fragrance,
It is fresh, simple and elegant.
Flores aurantii is the white petal of bigarabe, originates in South of France, Morocco, Egypt, Italy.There are bitter taste, flavour of a drug
Lily flowery odour, flores aurantii have the function of surprising to pacify soul.
Invention content
The present invention mesh be to provide a kind of delicate fragrance type tobacco extract, it using tea tree young leaves, salvia officianlis, flores aurantii as raw material,
Obtain a kind of cigarette additive with delicate fragrance type special favor, and as additive of tobacco product among cigarette,
Quality to improve Chinese-style cigarette is made contributions.
The invention discloses a kind of delicate fragrance type tobacco extracts, are made from the following raw materials in parts by weight：Tea tree young leaves 45~52,
Salvia officianlis 9~15, flores aurantii 2~5 and appropriate propylene glycol.
Preferred embodiment is made from the following raw materials in parts by weight：Tea tree young leaves 50, salvia officianlis 12, flores aurantii 3 and appropriate the third two
Alcohol.
The preparation method of above-mentioned delicate fragrance type tobacco extract, includes the following steps：
(1) tea tree young leaves of the parts by weight are blended, steam beating, cooling, drying, the separation of stalk leaf, removal sandstone, killed
Bacterium, rapid draing are ground to 500~800 mesh, add in 3~5 times of 50~80% ethyl alcohol, are then soaked under the conditions of 30~50 DEG C of temperature
1~3h is steeped, is 50~100KHz in supersonic frequency, ultrasound adverse current 30~90min of extraction, mistake under the conditions of temperature is 30~50 DEG C
Filter is collected extracting solution and is concentrated under reduced pressure, obtains pasty masses A；
(2) the salvia officianlis complete stool of the parts by weight is added in into 2~3 times of water ultrasound interval extraction 1~2h, then 75~95 DEG C
3~5h is heated to reflux, then 2~3h is extracted at 75~90 DEG C with 50% ethyl alcohol, reflux extracting liquid is collected, is concentrated under reduced pressure, obtains cream
Shape substance B；
(3) it is 12~30MPa in extracting pressure by the flores aurantii of the parts by weight, extraction temperature is 35~60 DEG C, during extraction
Between be 45~240min, CO2Gas flow carries out supercritical CO under the conditions of being 6~50Kg/H2Extraction, obtains extract；Then exist
Separating pressure is 3~7MPa, under the conditions of separation temperature is 30~60 DEG C, the extract is detached, obtains isolate；Its
In, extraction entrainer is that percentage by volume is 90~95% ethyl alcohol, and dosage is the 1~15% of flores aurantii total weight；To described point
From appropriate propylene glycol is added in object, mixed liquor is obtained, honey is added into the mixed liquor, stirs evenly, obtain pasty masses
C；
(4) by pasty masses A, B, C and propylene glycol with mass ratio 3.0~5.0:1.0~2.0:0.5~1.0:0.5~1.0
Mixing；
(5) paste mixture 0.5g is taken, after being diluted according to 0.01-0.1 ‰, is uniformly sprayed on pipe tobacco, naturally dry, in
60% time 22 DEG C of temperature, humidity balance more than 10h, cigarette is made with Cigarette making device by pipe tobacco.
Compared with prior art, advantages of the present invention and generation good effect are：
The present invention uses pure natural raw material, is made according to natural perfume material compatibility theory and using compounded technology, not addition
The effect of learning additive, having special faint scent, give full play to natural plant extracts can play and reduce oral cavity and dry throat
Sense, mitigates flue gas irritation, the anti-oxidant and effect refreshing oneself, loosen, meanwhile, water resistant moisture resistance is excellent, make cigarette in suction not
Viscous lip.The present invention is as additive of tobacco product, and with obvious effects, " Chinese-style cigarette " product to developing with distinctive style has
Good application prospect.
Specific embodiment
Technical scheme of the present invention is described in detail with reference to embodiment：
Embodiment 1
A kind of delicate fragrance type tobacco extract, is made from the following raw materials in parts by weight：Tea tree young leaves 52, salvia officianlis 9,3 and of flores aurantii
Appropriate propylene glycol.
The preparation method of above-mentioned delicate fragrance type tobacco extract, which is characterized in that include the following steps：
(1) tea tree young leaves of the parts by weight are blended, steam beating, cooling, drying, the separation of stalk leaf, removal sandstone, killed
Bacterium, rapid draing are ground to 500~800 mesh, add in 3~5 times of 50~80% ethyl alcohol, are then soaked under the conditions of 30~50 DEG C of temperature
1~3h is steeped, is 50~100KHz in supersonic frequency, ultrasound adverse current 30~90min of extraction, mistake under the conditions of temperature is 30~50 DEG C
Filter is collected extracting solution and is concentrated under reduced pressure, obtains pasty masses A；
(2) the salvia officianlis complete stool of the parts by weight is added in into 2~3 times of water ultrasound interval extraction 1~2h, then 75~95 DEG C
3~5h is heated to reflux, then 2~3h is extracted at 75~90 DEG C with 50% ethyl alcohol, reflux extracting liquid is collected, is concentrated under reduced pressure, obtains cream
Shape substance B；
(3) it is 12~30MPa in extracting pressure by the flores aurantii of the parts by weight, extraction temperature is 35~60 DEG C, during extraction
Between be 45~240min, CO2Gas flow carries out supercritical CO under the conditions of being 6~50Kg/H2Extraction, obtains extract；Then exist
Separating pressure is 3~7MPa, under the conditions of separation temperature is 30~60 DEG C, the extract is detached, obtains isolate；Its
In, extraction entrainer is that percentage by volume is 90~95% ethyl alcohol, and dosage is the 1~15% of flores aurantii total weight；To described point
From appropriate propylene glycol is added in object, mixed liquor is obtained, honey is added into the mixed liquor, stirs evenly, obtain pasty masses
C；
(4) by pasty masses A, B, C and propylene glycol with mass ratio 5.0:1.2:0.6:0.5 mixing；
(5) paste mixture 0.5g is taken, after being diluted according to 0.01-0.1 ‰, is uniformly sprayed on pipe tobacco, naturally dry, in
60% time 22 DEG C of temperature, humidity balance more than 10h, cigarette is made with Cigarette making device by pipe tobacco.
Embodiment 2
A kind of delicate fragrance type tobacco extract, which is characterized in that be made from the following raw materials in parts by weight：Tea tree young leaves 50, ocean Soviet Union
Grass 12, flores aurantii 3 and appropriate propylene glycol.
The preparation method of above-mentioned delicate fragrance type tobacco extract, which is characterized in that include the following steps：
(1) tea tree young leaves of the parts by weight are blended, steam beating, cooling, drying, the separation of stalk leaf, removal sandstone, killed
Bacterium, rapid draing are ground to 500~800 mesh, add in 3~5 times of 50~80% ethyl alcohol, are then soaked under the conditions of 30~50 DEG C of temperature
1~3h is steeped, is 50~100KHz in supersonic frequency, ultrasound adverse current 30~90min of extraction, mistake under the conditions of temperature is 30~50 DEG C
Filter is collected extracting solution and is concentrated under reduced pressure, obtains pasty masses A；
(2) the salvia officianlis complete stool of the parts by weight is added in into 2~3 times of water ultrasound interval extraction 1~2h, then 75~95 DEG C
3~5h is heated to reflux, then 2~3h is extracted at 75~90 DEG C with 50% ethyl alcohol, reflux extracting liquid is collected, is concentrated under reduced pressure, obtains cream
Shape substance B；
(3) it is 12~30MPa in extracting pressure by the flores aurantii of the parts by weight, extraction temperature is 35~60 DEG C, during extraction
Between be 45~240min, CO2Gas flow carries out supercritical CO under the conditions of being 6~50Kg/H2Extraction, obtains extract；Then exist
Separating pressure is 3~7MPa, under the conditions of separation temperature is 30~60 DEG C, the extract is detached, obtains isolate；Its
In, extraction entrainer is that percentage by volume is 90~95% ethyl alcohol, and dosage is the 1~15% of flores aurantii total weight；To described point
From appropriate propylene glycol is added in object, mixed liquor is obtained, honey is added into the mixed liquor, stirs evenly, obtain pasty masses
C；
(4) by pasty masses A, B, C and propylene glycol with mass ratio 3.0:2.0:0.5:1.0 mixing；
(5) paste mixture 0.5g is taken, after being diluted according to 0.01-0.1 ‰, is uniformly sprayed on pipe tobacco, naturally dry, in
60% time 22 DEG C of temperature, humidity balance more than 10h, cigarette is made with Cigarette making device by pipe tobacco.
Embodiment 3
A kind of delicate fragrance type tobacco extract, is made from the following raw materials in parts by weight：Tea tree young leaves 45, salvia officianlis 15,4 and of flores aurantii
Appropriate propylene glycol.
The preparation method of above-mentioned delicate fragrance type tobacco extract, which is characterized in that include the following steps：
(1) tea tree young leaves of the parts by weight are blended, steam beating, cooling, drying, the separation of stalk leaf, removal sandstone, killed
Bacterium, rapid draing are ground to 500~800 mesh, add in 3~5 times of 50~80% ethyl alcohol, are then soaked under the conditions of 30~50 DEG C of temperature
1~3h is steeped, is 50~100KHz in supersonic frequency, ultrasound adverse current 30~90min of extraction, mistake under the conditions of temperature is 30~50 DEG C
Filter is collected extracting solution and is concentrated under reduced pressure, obtains pasty masses A；
(2) the salvia officianlis complete stool of the parts by weight is added in into 2~3 times of water ultrasound interval extraction 1~2h, then 75~95 DEG C
3~5h is heated to reflux, then 2~3h is extracted at 75~90 DEG C with 50% ethyl alcohol, reflux extracting liquid is collected, is concentrated under reduced pressure, obtains cream
Shape substance B；
(3) it is 12~30MPa in extracting pressure by the flores aurantii of the parts by weight, extraction temperature is 35~60 DEG C, during extraction
Between be 45~240min, CO2Gas flow carries out supercritical CO under the conditions of being 6~50Kg/H2Extraction, obtains extract；Then exist
Separating pressure is 3~7MPa, under the conditions of separation temperature is 30~60 DEG C, the extract is detached, obtains isolate；Its
In, extraction entrainer is that percentage by volume is 90~95% ethyl alcohol, and dosage is the 1~15% of flores aurantii total weight；To described point
From appropriate propylene glycol is added in object, mixed liquor is obtained, honey is added into the mixed liquor, stirs evenly, obtain pasty masses
C；
(4) by pasty masses A, B, C and propylene glycol with mass ratio 3.0:1.5:0.8:0.6 mixing；
(5) paste mixture 0.5g is taken, after being diluted according to 0.01-0.1 ‰, is uniformly sprayed on pipe tobacco, naturally dry, in
60% time 22 DEG C of temperature, humidity balance more than 10h, cigarette is made with Cigarette making device by pipe tobacco.
Test example
With reference to GB5606.4-2005《The 4th part of cigarette：The requirement of sense organ technology》With YC/T 497-2014《Cigarette Chinese style is rolled up
Cigarette style sensory evaluation method》The cigarette of delicate fragrance type tobacco extract to being added with 1-3 of the embodiment of the present invention carries out sensory evaluation,
As a result it is as shown in table 1 below：
1 cigarette sensory evaluation of table
The Analyses Methods for Sensory Evaluation Results of table 1 shows the cigarette of the delicate fragrance type tobacco extract added with 1-3 of the embodiment of the present invention,
The fragrant of flue gas is pleasant, and sweet sense is apparent, can play reduce oral cavity and dry throat sense during the smoking process, mitigates
The effect of flue gas stimulation, is suitble to high-quality cigarette.
Above-described embodiment is only the more excellent embodiment of the present invention, and every technical spirit according to the present invention to implementing above
Any simple modification, modification and the alternate variation that example is made, belong in the range of technical solution of the present invention.
Claims (3)
1. a kind of delicate fragrance type tobacco extract, which is characterized in that be made from the following raw materials in parts by weight：Tea tree young leaves 45~52, ocean
Soviet Union's grass 9~15, flores aurantii 2~5 and appropriate propylene glycol.
2. a kind of delicate fragrance type tobacco extract according to claim 1, which is characterized in that by the raw material system of following parts by weight
Into：Tea tree young leaves 50, salvia officianlis 12, flores aurantii 3 and appropriate propylene glycol.
3. a kind of preparation method of delicate fragrance type tobacco extract as claimed in claim 1 or 2, which is characterized in that including walking as follows
Suddenly：
(1) tea tree young leaves of the parts by weight are blended, steam beating, cooling, drying, stalk leaf separation, removal sandstone, sterilization,
Rapid draing is ground to 500~800 mesh, adds in 3~5 times of 50~80% ethyl alcohol, then impregnates 1 under the conditions of 30~50 DEG C of temperature
~3h is 50~100KHz in supersonic frequency, and ultrasound adverse current 30~90min of extraction, is filtered under the conditions of temperature is 30~50 DEG C, is received
Collect extracting solution to be concentrated under reduced pressure, obtain pasty masses A；
(2) the salvia officianlis complete stool of the parts by weight is added in into 2~3 times of water ultrasound interval 1~2h of extraction, then 75~95 DEG C of heating
Flow back 3~5h, then extracts 2~3h at 75~90 DEG C with 50% ethyl alcohol, collects reflux extracting liquid, is concentrated under reduced pressure, obtains paste
Matter B；
(3) it is 12~30MPa in extracting pressure by the flores aurantii of the parts by weight, extraction temperature is 35~60 DEG C, and extraction time is
45~240min, CO2Gas flow carries out supercritical CO under the conditions of being 6~50Kg/H2Extraction, obtains extract；Then it is detaching
Pressure is 3~7MPa, under the conditions of separation temperature is 30~60 DEG C, the extract is detached, obtains isolate；Wherein,
Extraction entrainer is that percentage by volume is 90~95% ethyl alcohol, and dosage is the 1~15% of flores aurantii total weight；To the isolate
It is middle to add in appropriate propylene glycol, mixed liquor is obtained, honey is added into the mixed liquor, stirs evenly, obtains pasty masses C；
(4) by pasty masses A, B, C and propylene glycol with mass ratio 3.0~5.0:1.0~2.0:0.5~1.0:0.5~1.0 is mixed
It closes；
(5) paste mixture 0.5g is taken, after being diluted according to 0.01-0.1 ‰, is uniformly sprayed on pipe tobacco, naturally dry, in temperature
60% time 22 DEG C, humidity balance more than 10h, cigarette is made with Cigarette making device by pipe tobacco.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711416575.1A CN108142985B (en) | 2017-12-25 | 2017-12-25 | Faint scent type tobacco extract |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201711416575.1A CN108142985B (en) | 2017-12-25 | 2017-12-25 | Faint scent type tobacco extract |
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| Publication Number | Publication Date |
|---|---|
| CN108142985A true CN108142985A (en) | 2018-06-12 |
| CN108142985B CN108142985B (en) | 2020-04-10 |
Family
ID=62464442
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201711416575.1A Active CN108142985B (en) | 2017-12-25 | 2017-12-25 | Faint scent type tobacco extract |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112210439A (en) * | 2020-07-30 | 2021-01-12 | 常德华馥生物技术有限公司 | Preparation method of physalis pubescens tobacco flavor and application of compound of physalis pubescens tobacco flavor in cigarettes |
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| GB2173985A (en) * | 1985-04-24 | 1986-10-29 | Pauls Flavours & Fragrances Lt | Extraction of aroma materials |
| CN101156711A (en) * | 2007-10-18 | 2008-04-09 | 广西中烟工业公司 | Additive for tea odor type tobacco and method for making same |
| CN102125300A (en) * | 2010-12-13 | 2011-07-20 | 云南瑞升烟草技术（集团）有限公司 | Preparation and adding methods of additive capable of reducing HCN and CO content of cigarettes |
| CN102687901A (en) * | 2011-03-22 | 2012-09-26 | 湖北中烟工业有限责任公司 | A faint scent-type special cigarette flavor and application thereof in cigarettes |
| CN103349354A (en) * | 2013-06-28 | 2013-10-16 | 湖北中烟工业有限责任公司 | Sage extract, preparation method thereof and application of sage extract taken as tobacco product additive |
| CN105969524A (en) * | 2016-07-29 | 2016-09-28 | 福建中烟工业有限责任公司 | Composition and application of composition in cigarettes |
-
2017
- 2017-12-25 CN CN201711416575.1A patent/CN108142985B/en active Active
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2173985A (en) * | 1985-04-24 | 1986-10-29 | Pauls Flavours & Fragrances Lt | Extraction of aroma materials |
| CN101156711A (en) * | 2007-10-18 | 2008-04-09 | 广西中烟工业公司 | Additive for tea odor type tobacco and method for making same |
| CN102125300A (en) * | 2010-12-13 | 2011-07-20 | 云南瑞升烟草技术（集团）有限公司 | Preparation and adding methods of additive capable of reducing HCN and CO content of cigarettes |
| CN102687901A (en) * | 2011-03-22 | 2012-09-26 | 湖北中烟工业有限责任公司 | A faint scent-type special cigarette flavor and application thereof in cigarettes |
| CN103349354A (en) * | 2013-06-28 | 2013-10-16 | 湖北中烟工业有限责任公司 | Sage extract, preparation method thereof and application of sage extract taken as tobacco product additive |
| CN105969524A (en) * | 2016-07-29 | 2016-09-28 | 福建中烟工业有限责任公司 | Composition and application of composition in cigarettes |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN112210439A (en) * | 2020-07-30 | 2021-01-12 | 常德华馥生物技术有限公司 | Preparation method of physalis pubescens tobacco flavor and application of compound of physalis pubescens tobacco flavor in cigarettes |
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| CN108142985B (en) | 2020-04-10 |
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