CN115005490A - Electronic mint tobacco atomized liquid without nicotine and preparation method thereof - Google Patents
Electronic mint tobacco atomized liquid without nicotine and preparation method thereof Download PDFInfo
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- CN115005490A CN115005490A CN202210748943.7A CN202210748943A CN115005490A CN 115005490 A CN115005490 A CN 115005490A CN 202210748943 A CN202210748943 A CN 202210748943A CN 115005490 A CN115005490 A CN 115005490A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
- A24B15/303—Plant extracts other than tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24F—SMOKERS' REQUISITES; MATCH BOXES; SIMULATED SMOKING DEVICES
- A24F40/00—Electrically operated smoking devices; Component parts thereof; Manufacture thereof; Maintenance or testing thereof; Charging means specially adapted therefor
- A24F40/10—Devices using liquid inhalable precursors
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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Abstract
The invention discloses nicotine-free mint tobacco electronic atomized liquid and a preparation method thereof, wherein the nicotine-free mint tobacco electronic atomized liquid comprises the following raw materials in parts by weight: 3-5 parts of tobacco essence, 1-3 parts of D, L-menthol, 1-3 parts of peppermint oil, 0.3-1 part of cooling agent, 0.2-1 part of sweetening agent, 2-5 parts of ethyl maltol, 1-5 parts of vanillin, 30-55 parts of propylene glycol and 30-45 parts of glycerol. The mint tobacco electronic atomized liquid without added nicotine provided by the invention has the advantages of refreshing, fragrant and sweet taste through the synergistic effect of the raw materials, has good reduction feeling, pure mint flavor, strong tobacco flavor, comfortable and natural cool flavor, moderate cool degree, good smoke amount and mild and comfortable mouthfeel, ensures the satisfaction similar to cigarette smoking, simultaneously achieves the effects of relieving fatigue and refreshing, enables the electronic cigarette to become a leisure hobby, and has great significance for improving the safety, the working efficiency and the health function of consumers.
Description
Technical Field
The invention relates to the technical field of electronic atomized liquid, in particular to mint tobacco electronic atomized liquid without nicotine and a preparation method thereof.
Background
The cigarette is widely used as a hobby product and is popular among people, especially men. However, tar in cigarettes is harmful to human health, and some of them contain dozens of carcinogens, and secondary smoking is extremely harmful to non-smokers. The electronic cigarette is an electronic product simulating a cigarette, and has the same smoking experience as the cigarette. Because the electronic cigarette does not contain harmful substances such as tar, carbon monoxide and the like and reduces the harm to the health of users, the electronic cigarette is gradually accepted and loved by wide consumers.
With the pressure of modern urban living becoming more and giving attention to health, more and more people choose to smoke the electronic cigarette to replace the traditional cigarette, on the one hand can alleviate the pressure and fatigue of work and life, on the other hand reduces the harmfulness of traditional cigarette to the health. With the rise of the concept of big health and the trend of health care for consumption, higher requirements are put on the formula of the electronic atomized liquid.
The electronic atomization liquid is used as an important raw material of the electronic cigarette, and has direct feeling and experience for consumers. The mint is always a popular spice and gives a cool and comfortable feeling, and the fragrance of the mint and the fragrance of the electronic cigarette oil atomized liquid complement each other and are popular with consumers. However, the mint has single taste, is not rich, smooth and natural in fragrance, and is easy to generate bitter taste, so that the mint cannot meet the market demand.
Therefore, the electronic peppermint tobacco atomized liquid without nicotine and the preparation method thereof are needed to solve the problems.
Disclosure of Invention
Aiming at the defects in the prior art, the invention aims to provide the mint tobacco electronic atomized liquid without nicotine, which can truly replace cigarettes through inhalation type atomization, can meet the smoking addiction and is beneficial to body health, and atomized smoke does not contain acrolein, carbon monoxide, arsenic and other harmful substances, so that the harm of 'second-hand smoke' to other people is avoided, and the health of people around the body is protected.
In order to achieve the purpose, the invention provides the following technical scheme:
the electronic mint tobacco atomized liquid without nicotine comprises the following raw materials in parts by weight:
3-5 parts of tobacco essence base, 1-3 parts of D, L-menthol, 1-3 parts of peppermint oil, 0.3-1 part of cooling agent (WS-23), 0.2-1 part of sweetener (neotame), 2-5 parts of ethyl maltol, 1-5 parts of vanillin, 30-55 parts of propylene glycol and 30-45 parts of glycerol.
As a further scheme of the invention, the feed additive comprises the following raw materials in parts by weight: 4 parts of tobacco essence, 1.5 parts of D, L-menthol, 1.5 parts of peppermint oil, 0.65 part of cooling agent (WS-23), 0.6 part of sweetener (neotame), 3.5 parts of ethyl maltol, 3 parts of vanillin, 42.5 parts of propylene glycol and 40.5 parts of glycerol.
As a further scheme of the invention, the tobacco essence base comprises the following raw materials in parts by weight: 1-2 parts of 2, 3-dimethylpyrazine, 1-6 parts of 2, 5-dimethylpyrazine, 2,3, 5-trimethylpyrazine 2-5 parts, 5-15 parts of 2-acetylpyrazine, 1-2 parts of 2-acetylthiazole, 1-2 parts of 2-acetylfuran, 1-2 parts of alpha-angelica lactone, 2-5 parts of 2-acetylpyridine, 5-10 parts of gamma-octalactone, 1-5 parts of gamma-dodecalactone, 1-2 parts of dihydroactinidiolide, 5-10 parts of 3-hydroxy-4, 5-dimethyl-2 (5H) furanone, 5-10 parts of furanone, 4-10 parts of cocoa extract, 4-10 parts of vanilla bean tincture, 5-10 parts of flue-cured tobacco volatile extract, 5-10 parts of tobacco extract, 3-8 parts of Yunyan essential oil and 40-80 parts of propylene glycol.
As a further scheme of the invention, the tobacco essence base comprises the following raw materials in parts by weight: 1.5 parts of 2, 3-dimethyl pyrazine, 3.5 parts of 2, 5-dimethyl pyrazine, 3.5 parts of 2,3, 5-trimethyl pyrazine, 10 parts of 2-acetyl pyrazine, 1.5 parts of 2-acetyl thiazole, 1.5 parts of 2-acetyl furan, 1.5 parts of alpha-angelica lactone, 3.5 parts of 2-acetyl pyridine, 7.5 parts of gamma-octalactone, 3 parts of gamma-dodecalactone, 1.5 parts of dihydroactinidiolide, 7.5 parts of 3-hydroxy-4, 5-dimethyl-2 (5H) furanone, 7.5 parts of furanone, 7 parts of cocoa extract, 7 parts of vanilla bean tincture, 7.5 parts of flue-cured tobacco volatile extract, 7.5 parts of tobacco extract, 5.5 parts of Yunyan essential oil and 60 parts of propylene glycol.
As a still further aspect of the present invention, the sweetener is neotame sweetener.
By adopting the technical scheme, the neotame (N- [ N- (3, 3-dimethylbutyl) -L-alpha-aspartyl ] -L-phenylalanine 1-methyl ester) has pure sweet taste, is fresh and natural, has synergistic sweet taste and higher safety, and does not have the bitter taste and metal taste which are often brought by other strong sweeteners. The neotame sweetener is added into the mint tobacco electronic cigarette tobacco tar atomized liquid, so that the bitter taste of the menthol can be effectively covered, and the tobacco sweetness of the mint tobacco electronic atomized liquid is improved.
As a still further aspect of the present invention, the cooling agent is WS-23.
By adopting the technical scheme, the cooling agent WS-23 is N,2, 3-trimethyl-2-isopropyl butanamide, not only has light mint fragrance, but also has strong cooling feeling, and more importantly, has no bitter and astringent feeling of menthol and no irritating side effect. Through the synergistic effect of the cooling agent WS-23 and the menthol, the fragrance and the cooling feeling of the mint can be effectively increased.
As a further scheme of the invention, by adopting the technical scheme, the vanillin has vanilla bean fragrance and strong milk fragrance and can play roles in increasing and fixing fragrance, the ethyl maltol is a fragrance synergist and has good improvement and enhancement effects, and the mouthfeel and aftertaste of the mint tobacco electronic atomized liquid are improved by combining the synergistic effect of the vanillin.
As a further scheme of the invention, the peppermint oil has the effects of refreshing, cooling and refreshing, and simultaneously has a natural excitation function, so that the breath is smooth, and the mind is clear.
As a further aspect of the present invention, menthol has the effects of cooling, refreshing, and moistening the throat, but menthol also has a bitter and astringent feeling.
As a further scheme of the invention, the cooling agent has strong cooling feeling and no bitterness, and can effectively cover the bitterness of menthol by combining the sweetening agent, the glycerol and the ethyl maltol, so that the peppermint tobacco electronic cigarette tobacco oil atomized liquid has good sweetness.
As a further scheme of the invention, the propylene glycol has no obvious smell, has the characteristics of smooth oil and wide solubility of tobacco oil, but has less smoke amount, and the addition of the glycerol can effectively increase the smoke amount, has sweet taste, increases the sweet taste of the mint tobacco electronic atomized liquid and improves the mouthfeel of the mint tobacco electronic atomized liquid.
As a further scheme of the invention, the vanilla bean tincture is a natural vanilla bean tincture spice, is prepared from the fruit of vanilla of the family Orchidaceae, has fresh and sweet bean fragrance and good vanilla butter smell. Can improve the aroma of tobacco.
As a further scheme of the invention, the cocoa extract is composed of xanthine molecules (theobromine) and procyanidine, and the like, and the theobromine can make people sharp in thinking and concentrate energy so as to relieve fatigue and improve the working efficiency. Meanwhile, the taste of the electronic atomized liquid can be improved.
As a further scheme of the invention, the flue-cured tobacco volatile extract, the tobacco extract and the Yunyan essential oil are all effective components extracted from tobacco leaves; the throat irritation feeling of the smoke can be improved; when being smoked, the cigarette can be close to the cigarette like the fragrance of the cigarette.
As a further scheme of the invention, by adopting the technical scheme, the proportion of the mint tobacco electronic atomized liquid is further limited, and the performance of the mint tobacco electronic atomized liquid is improved.
A preparation method of mint tobacco electronic atomized liquid without nicotine comprises the following steps:
1) weighing tobacco essence, D, L-menthol, peppermint oil, cooling agent, sweetening agent, ethyl maltol, vanillin, propylene glycol and glycerol according to the weight parts for later use;
2) putting the tobacco base, the sweetening agent, the ethyl maltol and the vanillin into a mixing tank, and uniformly stirring and mixing to obtain tobacco base liquid;
3) sequentially adding D, L-menthol, peppermint oil and cooling agent into the tobacco fragrance base liquid, and stirring until the D, L-menthol, the peppermint oil and the cooling agent are completely dissolved to obtain a mint tobacco liquid precursor;
4) and adding propylene glycol and glycerol into the mint tobacco liquid precursor, and uniformly stirring to obtain the mint tobacco electronic atomized liquid without nicotine.
As a further scheme of the invention, the mixing temperature in the preparation process of the mint tobacco electronic atomized liquid without nicotine is 20-40 ℃, and the stirring speed is 150-220 r/min.
As a further aspect of the present invention, the preparation method of the electronic peppermint tobacco atomized liquid without adding nicotine further includes the preparation of a tobacco flavor base, and the preparation of the tobacco flavor base includes the following steps:
11) weighing 2, 3-dimethyl pyrazine, 2, 5-dimethyl pyrazine, 2,3, 5-trimethyl pyrazine, 2-acetyl thiazole, 2-acetyl furan, alpha-angelica lactone, 2-acetyl pyridine, gamma-octalactone, gamma-dodecalactone, dihydroactinidiolide, 3-hydroxy-4, 5-dimethyl-2 (5H) furanone, cocoa extract, vanilla bean tincture, flue-cured tobacco volatile extract, tobacco extract, Yunyan essential oil and propylene glycol according to the weight parts for later use;
12) mixing the tobacco extract, the yunyan essential oil and propylene glycol to obtain a mixture A;
13) sequentially adding 2, 3-dimethylpyrazine, 2, 5-dimethylpyrazine, 2,3, 5-trimethylpyrazine, 2-acetylpyrazine, 2-acetylthiazole, 2-acetylfuran, alpha-angelica lactone, 2-acetylpyridine, gamma-octalactone, gamma-dodecalactone, dihydroactinidiolide, 3-hydroxy-4, 5-dimethyl-2 (5H) furanone and furanone serving as food additives into the mixture A, and stirring until the materials are completely dissolved to obtain a mixture B;
14) adding cocoa extract, vanilla bean tincture and flue-cured tobacco volatile extract into the mixture B, and stirring to obtain tobacco essence base.
As a further scheme of the invention, the tobacco extract is high-quality pure natural tobacco, and the plant extract which is harmless to human bodies and shows the special fragrance of the tobacco is extracted and separated from the tobacco leaves by adopting an extraction technology.
Compared with the prior art, the invention has the beneficial effects that:
the mint tobacco electronic atomized liquid without added nicotine provided by the invention has the advantages of refreshing, fragrant and sweet taste through the synergistic effect of the raw materials, has good reduction feeling, pure mint flavor, strong tobacco flavor, comfortable and natural cool flavor, moderate cool degree, good smoke amount and mild and comfortable mouthfeel, ensures the satisfaction similar to cigarette smoking, simultaneously achieves the effects of relieving fatigue and refreshing, enables the electronic cigarette to become a leisure hobby, and has great significance for improving the safety, the working efficiency and the health function of consumers.
Detailed Description
The technical solution of the present invention will be described in further detail with reference to specific embodiments.
The purpose of the invention is realized by the following technical scheme:
the embodiment of the invention provides mint tobacco electronic atomized liquid without nicotine, which is prepared by selecting high-quality pure natural tobacco, extracting and separating plant essence which is harmless to human bodies and can embody the special fragrance of the tobacco from tobacco leaves by adopting an extraction technology, and adding a food additive.
The electronic atomization liquid mainly comprises the following components: 3-5 parts of tobacco essence, 1-3 parts of D, L-menthol, 1-3 parts of peppermint oil, 0.3-1 part of cooling agent (WS-23), 0.2-1 part of sweetener (neotame), 2-5 parts of ethyl maltol, 1-5 parts of vanillin, 30-55 parts of propylene glycol and 30-45 parts of glycerol.
In the embodiment of the application, the tobacco base comprises the following raw materials in parts by weight: 1 part of 2, 3-dimethyl pyrazine, 3 parts of 2, 5-dimethyl pyrazine, 4 parts of 2,3, 5-trimethyl pyrazine, 5.5 parts of 2-acetyl pyrazine, 1 part of 2-acetyl thiazole, 1 part of 2-acetyl furan, 1.5 parts of alpha-angelica lactone, 3.5 parts of 2-acetyl pyridine, 6.5 parts of gamma-octalactone, 3.5 parts of gamma-dodecalactone, 1 part of dihydroactinidiolide, 3-hydroxy-4, 5-dimethyl-2 (5H) furanone, 8.5 parts of furanone, 4 parts of cocoa extract, 3.5 parts of vanilla bean tincture, 6.5 parts of flue-cured tobacco volatile extract, 8 parts of tobacco extract, 5.5 parts of Yunyan essential oil and 29.5 parts of propylene glycol.
And (3) mixing and stirring the raw materials uniformly at room temperature to obtain the tobacco flavor base mixed solution.
In an embodiment of the application, the preparation method of the nicotine-free electronic mint tobacco atomized liquid further comprises the preparation of a tobacco flavor base, wherein the preparation of the tobacco flavor base comprises the following steps:
11) weighing 2, 3-dimethyl pyrazine, 2, 5-dimethyl pyrazine, 2,3, 5-trimethyl pyrazine, 2-acetyl thiazole, 2-acetyl furan, alpha-angelica lactone, 2-acetyl pyridine, gamma-octalactone, gamma-dodecalactone, dihydroactinidiolide, 3-hydroxy-4, 5-dimethyl-2 (5H) furanone, cocoa extract, vanilla bean tincture, flue-cured tobacco volatile extract, tobacco extract, Yunyan essential oil and propylene glycol according to the weight parts for later use;
12) mixing the tobacco extract, the yunyan essential oil and propylene glycol to obtain a mixture A;
13) sequentially adding 2, 3-dimethylpyrazine, 2, 5-dimethylpyrazine, 2,3, 5-trimethylpyrazine, 2-acetylpyrazine, 2-acetylthiazole, 2-acetylfuran, alpha-angelica lactone, 2-acetylpyridine, gamma-octalactone, gamma-dodecalactone, dihydroactinidiolide, 3-hydroxy-4, 5-dimethyl-2 (5H) furanone and furanone serving as food additives into the mixture A, and stirring until the materials are completely dissolved to obtain a mixture B;
14) adding cocoa extract, vanilla bean tincture and flue-cured tobacco volatile extract into the mixture B, and stirring to obtain tobacco essence base.
In the embodiment of the application, the tobacco extract is high-quality pure natural tobacco, and the plant extract which is harmless to human bodies and shows the special fragrance of the tobacco is extracted and separated from the tobacco leaves by adopting an extraction technology.
By adopting the technical scheme, the vanillin has vanilla bean fragrance and strong milk fragrance, can play the roles of increasing and fixing fragrance, the ethyl maltol is a fragrance synergist, has good improving and enhancing effects, and combines the synergistic effect of the vanillin, so that the taste and aftertaste of the mint tobacco electronic atomized liquid are improved.
The peppermint oil has refreshing effect, and also has natural exciting effect, and can promote breath circulation and improve brain. The menthol has the effects of cooling, refreshing and moistening the throat, but the menthol also has bitter taste, and the cooling agent has strong cool feeling and no bitter taste, and can effectively cover the bitter taste of the menthol by combining the sweetening agent, the glycerol and the ethyl maltol and enable the mint tobacco electronic cigarette oil atomized liquid to have good sweet taste. The propylene glycol has no obvious smell, has the characteristics of smooth oil and wide solubility of tobacco oil, but has less smoke amount, and the addition of the glycerol can effectively increase the smoke amount, has sweet taste, increases the sweet taste of the mint tobacco electronic atomized liquid and improves the mouthfeel of the mint tobacco electronic atomized liquid.
Vanilla tincture is a natural vanilla tincture spice, which is prepared from the fruit of Vanilla planifolia of Orchidaceae, and has sweet bean fragrance and good vanilla butter smell. Can improve the aroma of tobacco.
The cocoa extract is composed of xanthine molecules (theobromine) and procyanidins, and the theobromine can make people sharp in thinking and concentrate energy so as to relieve fatigue and improve work efficiency. Meanwhile, the taste of the electronic atomized liquid can be improved.
The flue-cured tobacco volatile extract, the tobacco extract and the Yunyan essential oil are effective components extracted from tobacco leaves; the throat irritation feeling of the smoke can be improved; when being smoked, the cigarette can be close to the cigarette like the cigarette.
The technical solution of the present invention will be described in further detail with reference to specific examples in the following embodiments.
The present application includes the preparation of the electronic atomized liquid of mint tobacco of examples 1 to 6. The electronic mint tobacco atomized liquid prepared in examples 1 to 6 is prepared by mixing and stirring the above raw materials uniformly according to the following table.
TABLE 1 example the content (unit: g) of each raw material in the electronic atomized liquid of peppermint tobacco
In the examples of the present application, the sweetener, the cooling agent and ethyl maltol were added to propylene glycol and dissolved in a constant temperature water bath at 40-50 ℃ for further use in each of the examples in Table 1. Then the mint tobacco electronic atomized liquid is mixed with other raw materials and stirred evenly to obtain the mint tobacco electronic atomized liquid without adding nicotine.
Specifically, example 1
The electronic mint tobacco atomized liquid without nicotine comprises the following raw materials in parts by weight:
3 parts of tobacco essence, 2 parts of D, L-menthol, 1 part of peppermint oil, 0.3 part of cooling agent (WS-23), 0.2 part of sweetener (neotame), 2 parts of ethyl maltol, 1 part of vanillin, 50.5 parts of propylene glycol and 40 parts of glycerol.
In the examples of the application, the sweetener is neotame sweetener, and neotame (N- [ N- (3, 3-dimethylbutyl) -L-alpha-aspartyl ] -L-phenylalanine 1-methyl ester) has pure sweetness, is fresh and natural, synergistic in sweetness and higher in safety, and does not have the bitter taste and metallic taste which are usually associated with other intense sweeteners. The neotame sweetener is added into the mint tobacco electronic cigarette tobacco tar atomized liquid, so that the bitter taste of the menthol can be effectively covered, and the tobacco sweetness of the mint tobacco electronic atomized liquid is improved.
In the examples of the application, the cooling agent is WS-23, and the cooling agent WS-23 is N,2, 3-trimethyl-2-isopropyl butanamide, so that the cooling agent has not only a light mint fragrance, but also a strong cooling feeling, more importantly, the cooling agent has no bitter and astringent feeling of menthol and no irritating side effect. Through the synergistic effect of the cooling agent WS-23 and the menthol, the mint aroma and the cooling feeling can be effectively increased.
A preparation method of mint tobacco electronic atomized liquid without nicotine comprises the following steps:
1) weighing tobacco essence, D, L-menthol, peppermint oil, cooling agent, sweetening agent, ethyl maltol, vanillin, propylene glycol and glycerol according to the weight parts for later use;
2) putting the tobacco essence base, the sweetening agent, the ethyl maltol and the vanillin into a mixing tank, and uniformly stirring and mixing to obtain tobacco essence base liquid;
3) sequentially adding D, L-menthol, peppermint oil and cooling agent into the tobacco fragrance base liquid, and stirring until the D, L-menthol, the peppermint oil and the cooling agent are completely dissolved to obtain a mint tobacco liquid precursor;
4) and adding propylene glycol and glycerol into the mint tobacco liquid precursor, and uniformly stirring to obtain the mint tobacco electronic atomized liquid without nicotine.
In the embodiment of the application, the mixing temperature is 25 ℃ and the stirring speed is 200r/min in the preparation process of the mint tobacco electronic atomized liquid without nicotine.
Example 2
The electronic mint tobacco atomized liquid without nicotine comprises the following raw materials in parts by weight:
3.5 parts of tobacco essence, 1.5 parts of D, L-menthol, 2 parts of peppermint oil, 0.5 part of cooling agent (WS-23), 0.3 part of sweetener (neotame), 3 parts of ethyl maltol, 2 parts of vanillin, 46.2 parts of propylene glycol and 41 parts of glycerol.
In the examples of the application, the sweetener is neotame sweetener, and neotame (N- [ N- (3, 3-dimethylbutyl) -L-alpha-aspartyl ] -L-phenylalanine 1-methyl ester) has pure sweetness, is fresh and natural, synergistic in sweetness and higher in safety, and does not have the bitter taste and metallic taste which are usually associated with other intense sweeteners. The neotame sweetener is added into the mint tobacco electronic cigarette tobacco tar atomized liquid, so that the bitter taste of the menthol can be effectively covered, and the tobacco sweetness of the mint tobacco electronic atomized liquid is improved.
In the examples of the application, the cooling agent is WS-23, and the cooling agent WS-23 is N,2, 3-trimethyl-2-isopropyl butanamide, so that the cooling agent has not only a light mint fragrance, but also a strong cooling feeling, more importantly, the cooling agent has no bitter and astringent feeling of menthol and no irritating side effect. Through the synergistic effect of the cooling agent WS-23 and the menthol, the mint aroma and the cooling feeling can be effectively increased.
A preparation method of mint tobacco electronic atomized liquid without nicotine comprises the following steps:
1) weighing tobacco essence, D, L-menthol, peppermint oil, cooling agent, sweetening agent, ethyl maltol, vanillin, propylene glycol and glycerol according to the weight parts for later use;
2) putting the tobacco base, the sweetening agent, the ethyl maltol and the vanillin into a mixing tank, and uniformly stirring and mixing to obtain tobacco base liquid;
3) sequentially adding D, L-menthol, peppermint oil and cooling agent into the tobacco fragrance base liquid, and stirring until the D, L-menthol, the peppermint oil and the cooling agent are completely dissolved to obtain a mint tobacco liquid precursor;
4) and adding propylene glycol and glycerol into the mint tobacco liquid precursor, and uniformly stirring to obtain the mint tobacco electronic atomized liquid without nicotine.
In the embodiment of the application, the mixing temperature in the preparation process of the electronic mint tobacco atomized liquid without nicotine is 25 ℃, and the stirring speed is 200/min.
Example 3
The electronic mint tobacco atomized liquid without nicotine comprises the following raw materials in parts by weight:
4 parts of tobacco essence, 2 parts of D, L-menthol, 2 parts of peppermint oil, 0.8 part of cooling agent (WS-23), 0.5 part of sweetener (neotame), 4 parts of ethyl maltol, 3.5 parts of vanillin, 43.2 parts of propylene glycol and 40 parts of glycerol.
In the examples of the present application, the sweetener is neotame, and neotame (N- [ N- (3, 3-dimethylbutyl) -L- α -aspartyl ] -L-phenylalanine 1-methyl ester) has a pure sweetness, is fresh and natural, synergistic in sweetness, and is safe and free of the bitter and metallic tastes often associated with other intense sweeteners. The neotame sweetener is added into the mint tobacco electronic cigarette tobacco tar atomized liquid, so that the bitter taste of the menthol can be effectively covered, and the tobacco sweetness of the mint tobacco electronic atomized liquid is improved.
In the examples of the application, the cooling agent is WS-23, and the cooling agent WS-23 is N,2, 3-trimethyl-2-isopropyl butanamide, so that the cooling agent has not only a light mint fragrance, but also a strong cooling feeling, more importantly, the cooling agent has no bitter and astringent feeling of menthol and no irritating side effect. Through the synergistic effect of the cooling agent WS-23 and the menthol, the mint aroma and the cooling feeling can be effectively increased.
A preparation method of mint tobacco electronic atomized liquid without nicotine comprises the following steps:
1) weighing tobacco essence, D, L-menthol, peppermint oil, cooling agent, sweetening agent, ethyl maltol, vanillin, propylene glycol and glycerol according to the weight parts for later use;
2) putting the tobacco essence base, the sweetening agent, the ethyl maltol and the vanillin into a mixing tank, and uniformly stirring and mixing to obtain tobacco essence base liquid;
3) sequentially adding D, L-menthol, peppermint oil and cooling agent into the tobacco fragrance base liquid, and stirring until the D, L-menthol, the peppermint oil and the cooling agent are completely dissolved to obtain a mint tobacco liquid precursor;
4) and adding propylene glycol and glycerol into the mint tobacco liquid precursor, and uniformly stirring to obtain the mint tobacco electronic atomized liquid without nicotine.
In the embodiment of the application, the mixing temperature in the preparation process of the electronic mint tobacco atomized liquid without nicotine is 25 ℃, and the stirring speed is 200 r/min.
Example 4
The electronic mint tobacco atomized liquid without nicotine comprises the following raw materials in parts by weight:
4.5 parts of tobacco essence, 1.5 parts of D, L-menthol, 3 parts of peppermint oil, 0.8 part of cooling agent (WS-23), 0.3 part of sweetener (neotame), 4 parts of ethyl maltol, 4 parts of vanillin, 41.4 parts of propylene glycol and 41 parts of glycerol.
In the examples of the present application, the sweetener is neotame, and neotame (N- [ N- (3, 3-dimethylbutyl) -L- α -aspartyl ] -L-phenylalanine 1-methyl ester) has a pure sweetness, is fresh and natural, synergistic in sweetness, and is safe and free of the bitter and metallic tastes often associated with other intense sweeteners. The neotame sweetener is added into the mint tobacco electronic cigarette tobacco tar atomized liquid, so that the bitter taste of the menthol can be effectively covered, and the tobacco sweetness of the mint tobacco electronic atomized liquid is improved.
In the examples of the application, the cooling agent is WS-23, and the cooling agent WS-23 is N,2, 3-trimethyl-2-isopropyl butanamide, so that the cooling agent has not only a light mint fragrance, but also a strong cooling feeling, more importantly, the cooling agent has no bitter and astringent feeling of menthol and no irritating side effect. Through the synergistic effect of the cooling agent WS-23 and the menthol, the mint aroma and the cooling feeling can be effectively increased.
A preparation method of mint tobacco electronic atomized liquid without nicotine comprises the following steps:
1) weighing tobacco essence, D, L-menthol, peppermint oil, cooling agent, sweetening agent, ethyl maltol, vanillin, propylene glycol and glycerol according to the weight parts for later use;
2) putting the tobacco essence base, the sweetening agent, the ethyl maltol and the vanillin into a mixing tank, and uniformly stirring and mixing to obtain tobacco essence base liquid;
3) sequentially adding D, L-menthol, peppermint oil and cooling agent into the tobacco fragrance base liquid, and stirring until the D, L-menthol, the peppermint oil and the cooling agent are completely dissolved to obtain a mint tobacco liquid precursor;
4) and adding propylene glycol and glycerol into the mint tobacco liquid precursor, and uniformly stirring to obtain the mint tobacco electronic atomized liquid without nicotine.
In the embodiment of the application, the mixing temperature in the preparation process of the electronic mint tobacco atomized liquid without nicotine is 25 ℃, and the stirring speed is 200 r/min.
Example 5
The electronic mint tobacco atomized liquid without nicotine comprises the following raw materials in parts by weight:
4.5 parts of tobacco essence, 2 parts of D, L-menthol, 2.5 parts of peppermint oil, 0.8 part of cooling agent (WS-23), 0.3 part of sweetener (neotame), 4 parts of ethyl maltol, 4 parts of vanillin, 40.9 parts of propylene glycol and 41 parts of glycerol.
In the examples of the present application, the sweetener is neotame, and neotame (N- [ N- (3, 3-dimethylbutyl) -L- α -aspartyl ] -L-phenylalanine 1-methyl ester) has a pure sweetness, is fresh and natural, synergistic in sweetness, and is safe and free of the bitter and metallic tastes often associated with other intense sweeteners. The neotame sweetener is added into the mint tobacco electronic cigarette tobacco tar atomized liquid, so that the bitter taste of the menthol can be effectively covered, and the tobacco sweetness of the mint tobacco electronic atomized liquid is improved.
In the examples of the application, the cooling agent is WS-23, and the cooling agent WS-23 is N,2, 3-trimethyl-2-isopropyl butanamide, so that the cooling agent has not only a light mint fragrance, but also a strong cooling feeling, more importantly, the cooling agent has no bitter and astringent feeling of menthol and no irritating side effect. Through the synergistic effect of the cooling agent WS-23 and the menthol, the mint aroma and the cooling feeling can be effectively increased.
A preparation method of mint tobacco electronic atomized liquid without nicotine comprises the following steps:
1) weighing tobacco essence, D, L-menthol, peppermint oil, cooling agent, sweetening agent, ethyl maltol, vanillin, propylene glycol and glycerol according to the weight parts for later use;
2) putting the tobacco base, the sweetening agent, the ethyl maltol and the vanillin into a mixing tank, and uniformly stirring and mixing to obtain tobacco base liquid;
3) sequentially adding D, L-menthol, peppermint oil and cooling agent into the tobacco fragrance base liquid, and stirring until the D, L-menthol, the peppermint oil and the cooling agent are completely dissolved to obtain a mint tobacco liquid precursor;
4) and adding propylene glycol and glycerol into the mint tobacco liquid precursor, and uniformly stirring to obtain the mint tobacco electronic atomized liquid without nicotine.
In the embodiment of the application, the mixing temperature in the preparation process of the electronic mint tobacco atomized liquid without nicotine is 25 ℃, and the stirring speed is 200/min.
Example 6
The electronic mint tobacco atomized liquid without nicotine comprises the following raw materials in parts by weight:
5 parts of tobacco essence base, 1.5 parts of D, L-menthol, 3 parts of peppermint oil, 0.5 part of cooling agent (WS-23), 0.5 part of sweetening agent (neotame), 4 parts of ethyl maltol, 3.5 parts of vanillin, 40 parts of propylene glycol and 40 parts of glycerol.
In the examples of the present application, the sweetener is neotame, and neotame (N- [ N- (3, 3-dimethylbutyl) -L- α -aspartyl ] -L-phenylalanine 1-methyl ester) has a pure sweetness, is fresh and natural, synergistic in sweetness, and is safe and free of the bitter and metallic tastes often associated with other intense sweeteners. The neotame sweetener is added into the mint tobacco electronic cigarette tobacco tar atomized liquid, so that the bitter taste of the menthol can be effectively covered, and the tobacco sweetness of the mint tobacco electronic atomized liquid is improved.
In the examples of the application, the cooling agent is WS-23, and the cooling agent WS-23 is N,2, 3-trimethyl-2-isopropyl butanamide, so that the cooling agent has not only a light mint fragrance, but also a strong cooling feeling, more importantly, the cooling agent has no bitter and astringent feeling of menthol and no irritating side effect. Through the synergistic effect of the cooling agent WS-23 and the menthol, the fragrance and the cooling feeling of the mint can be effectively increased.
A preparation method of mint tobacco electronic atomized liquid without nicotine comprises the following steps:
1) weighing tobacco essence, D, L-menthol, peppermint oil, cooling agent, sweetening agent, ethyl maltol, vanillin, propylene glycol and glycerol according to the weight parts for later use;
2) putting the tobacco essence base, the sweetening agent, the ethyl maltol and the vanillin into a mixing tank, and uniformly stirring and mixing to obtain tobacco essence base liquid;
3) sequentially adding D, L-menthol, peppermint oil and cooling agent into the tobacco fragrance base liquid, and stirring until the D, L-menthol, the peppermint oil and the cooling agent are completely dissolved to obtain a mint tobacco liquid precursor;
4) and adding propylene glycol and glycerol into the mint tobacco liquid precursor, and uniformly stirring to obtain the mint tobacco electronic atomized liquid without nicotine.
In the embodiment of the application, the mixing temperature is 25 ℃ and the stirring speed is 200r/min in the preparation process of the mint tobacco electronic atomized liquid without nicotine.
In the embodiment of the application, the tobacco extract is high-quality pure natural tobacco, and the plant extract which is harmless to human bodies and shows the special fragrance of the tobacco is extracted and separated from the tobacco leaves by adopting an extraction technology.
For the tobacco mint electronic aerosol samples obtained in examples 1 to 6, 70 male smokers aged 25 to 35 were selected, and the smokers were randomly divided into 7 groups of 10 persons, and the flavor and appearance were evaluated. Then, each group of smokers took the sample with the electronic cigarette, and evaluated the cooling sensation, the sweetness sensation, the reduction sensation, the smoke amount, the taste and the aftertaste of the sample after use, and the evaluation results are shown in table 2:
TABLE 2 evaluation results (unit: g) of each of the electronic peppermint tobacco spray solutions in examples
As can be seen from the table 2, the mint tobacco electronic atomized liquid has the advantages of refreshing, fragrant and sweet through the synergistic effect of the raw materials, and also has the advantages of good reduction feeling, pure mint flavor, comfortable and natural cool flavor, moderate cool degree, good smoke amount, natural and comfortable aftertaste and good smoking taste, and meets the market demand.
While the preferred embodiments of the present invention have been described in detail, the present invention is not limited to the above embodiments, and various changes can be made without departing from the spirit of the present invention within the knowledge of those skilled in the art.
Claims (10)
1. The electronic mint tobacco atomized liquid without nicotine is characterized by comprising the following raw materials in parts by weight:
3-5 parts of tobacco essence base, 1-3 parts of D, L-menthol, 1-3 parts of peppermint oil, 0.3-1 part of cooling agent, 0.2-1 part of sweetening agent, 2-5 parts of ethyl maltol, 1-5 parts of vanillin, 30-55 parts of propylene glycol and 30-45 parts of glycerol.
2. The electronic mint tobacco atomized liquid without added nicotine of claim 1, comprising the following raw materials in parts by weight: 4 parts of tobacco essence, 1.5 parts of D, L-menthol, 1.5 parts of peppermint oil, 0.65 part of cooling agent, 0.6 part of sweetening agent, 3.5 parts of ethyl maltol, 3 parts of vanillin, 42.5 parts of propylene glycol and 40.5 parts of glycerol.
3. The electronic mint tobacco atomized liquid without added nicotine of claim 2, wherein the tobacco base comprises the following raw materials in parts by weight: 1-2 parts of 2, 3-dimethylpyrazine, 1-6 parts of 2, 5-dimethylpyrazine, 2,3, 5-trimethylpyrazine 2-5 parts, 5-15 parts of 2-acetylpyrazine, 1-2 parts of 2-acetylthiazole, 1-2 parts of 2-acetylfuran, 1-2 parts of alpha-angelica lactone, 2-5 parts of 2-acetylpyridine, 5-10 parts of gamma-octalactone, 1-5 parts of gamma-dodecalactone, 1-2 parts of dihydroactinidiolide, 5-10 parts of 3-hydroxy-4, 5-dimethyl-2 (5H) furanone, 5-10 parts of furanone, 4-10 parts of cocoa extract, 4-10 parts of vanilla bean tincture, 5-10 parts of flue-cured tobacco volatile extract, 5-10 parts of tobacco extract, 3-8 parts of Yunyan essential oil and 40-80 parts of propylene glycol.
4. The electronic mint tobacco atomized liquid without added nicotine of claim 3, wherein the tobacco base comprises the following raw materials in parts by weight: 1.5 parts of 2, 3-dimethyl pyrazine, 3.5 parts of 2, 5-dimethyl pyrazine, 3.5 parts of 2,3, 5-trimethyl pyrazine, 10 parts of 2-acetyl pyrazine, 1.5 parts of 2-acetyl thiazole, 1.5 parts of 2-acetyl furan, 1.5 parts of alpha-angelica lactone, 3.5 parts of 2-acetyl pyridine, 7.5 parts of gamma-octalactone, 3 parts of gamma-dodecalactone, 1.5 parts of dihydroactinidiolide, 7.5 parts of 3-hydroxy-4, 5-dimethyl-2 (5H) furanone, 7.5 parts of furanone, 7 parts of cocoa extract, 7 parts of vanilla bean tincture, 7.5 parts of flue-cured tobacco volatile extract, 7.5 parts of tobacco extract, 5.5 parts of Yunyan essential oil and 60 parts of propylene glycol.
5. The nicotine-free electronic atomized liquid of mint tobacco, as claimed in claim 2, wherein the sweetener is neotame.
6. The nicotine-free electronic atomized liquid of mint tobacco, as claimed in claim 2, wherein the cooling agent is WS-23.
7. The method for preparing the electronic atomized liquid of the mint tobacco without adding nicotine according to any one of claims 1 to 6, comprising the following steps:
1) weighing tobacco essence, D, L-menthol, peppermint oil, cooling agent, sweetening agent, ethyl maltol, vanillin, propylene glycol and glycerol according to the weight parts for later use;
2) putting the tobacco base, the sweetening agent, the ethyl maltol and the vanillin into a mixing tank, and uniformly stirring and mixing to obtain tobacco base liquid;
3) sequentially adding D, L-menthol, peppermint oil and cooling agent into the tobacco fragrance base liquid, and stirring until the D, L-menthol, the peppermint oil and the cooling agent are completely dissolved to obtain a mint tobacco liquid precursor;
4) and adding propylene glycol and glycerol into the mint tobacco liquid precursor, and uniformly stirring to obtain the mint tobacco electronic atomized liquid without nicotine.
8. The method for preparing the electronic atomized liquid of mint tobacco without adding nicotine as claimed in claim 7, wherein the mixing temperature is 20-40 ℃ and the stirring speed is 150-220 r/min during the preparation process of the electronic atomized liquid of mint tobacco without adding nicotine.
9. The method for preparing the nicotine-free electronic atomized liquid of mint tobacco according to claim 7, further comprising the step of preparing a tobacco flavor base, wherein the preparation of the tobacco flavor base comprises the following steps:
11) weighing 2, 3-dimethylpyrazine, 2, 5-dimethylpyrazine, 2,3, 5-trimethylpyrazine, 2-acetylpyrazine, 2-acetylthiazole, 2-acetylfuran, alpha-angelica lactone, 2-acetylpyridine, gamma-octalactone, gamma-dodecalactone, dihydroactinidiolide, 3-hydroxy-4, 5-dimethyl-2 (5H) furanone, cocoa extract, vanilla bean tincture, flue-cured tobacco volatile extract, tobacco extract, yunyan essential oil and propylene glycol according to the weight parts for later use;
12) mixing the tobacco extract, the yunyan essential oil and propylene glycol to obtain a mixture A;
13) sequentially adding 2, 3-dimethylpyrazine, 2, 5-dimethylpyrazine, 2,3, 5-trimethylpyrazine, 2-acetylpyrazine, 2-acetylthiazole, 2-acetylfuran, alpha-angelica lactone, 2-acetylpyridine, gamma-octalactone, gamma-dodecalactone, dihydroactinidiolide, 3-hydroxy-4, 5-dimethyl-2 (5H) furanone and furanone serving as food additives into the mixture A, and stirring until the materials are completely dissolved to obtain a mixture B;
14) adding cocoa extract, vanilla bean tincture and flue-cured tobacco volatile extract into the mixture B, and stirring to obtain tobacco essence base.
10. The method for preparing the electronic atomized liquid of mint tobacco without added nicotine according to claim 9, wherein the tobacco extract is obtained by extracting and separating plant extracts which are harmless to human bodies and represent the special fragrance of tobacco from tobacco leaves by using an extraction technology.
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