CN114587004B - Essence for improving tobacco quality of Indonesia cigar and preparation method thereof - Google Patents
Essence for improving tobacco quality of Indonesia cigar and preparation method thereof Download PDFInfo
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- CN114587004B CN114587004B CN202210323965.9A CN202210323965A CN114587004B CN 114587004 B CN114587004 B CN 114587004B CN 202210323965 A CN202210323965 A CN 202210323965A CN 114587004 B CN114587004 B CN 114587004B
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- 239000002243 precursor Substances 0.000 description 2
- 239000008213 purified water Substances 0.000 description 2
- UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 2
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- 239000004480 active ingredient Substances 0.000 description 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 description 1
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Images
Classifications
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B3/00—Preparing tobacco in the factory
- A24B3/12—Steaming, curing, or flavouring tobacco
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0026—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring
- C11B9/0034—Essential oils; Perfumes compounds containing an alicyclic ring not condensed with another ring the ring containing six carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0092—Heterocyclic compounds containing only N as heteroatom
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention discloses an essence for improving the quality of Indonesia cigar tobacco and a preparation method thereof, wherein the essence is prepared from the following raw materials in parts by weight: 0.6-6.5 parts of natural plant spice, 0.2-2 parts of tobacco extract, 0.2-3 parts of preservative, 0.3-3 parts of fixative, 0.2-1.5 parts of flavor compensator, 1-5 parts of red date Maillard reactant, 10-20 parts of diluent and 59-87.5 parts of solvent. The essence added into cigar leaves can coordinate the characteristic fragrance of various raw materials, improve the problem of bitter taste, and improve the overall quality of cigar.
Description
Technical Field
The invention relates to the field of tobacco essence, in particular to essence for improving the quality of Indonesia cigar tobacco and a preparation method thereof.
Background
Cigar leaves are distinguished from other types of tobacco leaves by their unique cigar-type aroma, and can be divided into 3 types of cores, coats and covers according to their uses. The eggplant sleeve and the eggplant coat, namely the inner wrapper cigarette and the outer wrapper cigarette, are all air-cured cigarettes; the cigar core can be high-quality sun-cured tobacco or air-cured tobacco, and is required to have typical cigar fragrance, good taste with certain strength, good combustibility and good smoldering fire-holding power. The eggplant coat requires bright and uniform luster of leaves, sufficient combustion, moderate to fast combustion speed, no special requirements on aroma and taste, and is suitable for not influencing or contributing to the aroma style of the cigars. The eggplant sheath is required to be similar to the outer wrapping leaves in appearance, is not heavy in color, and has better tobacco leaf elasticity, toughness and combustibility as main quality requirements. From the aspect of supply of cigar raw materials, at present, the cigar raw materials mainly come from Caribbean regions, indonesia and China, are influenced by trade environment, the supply of the cigar raw materials is limited abroad, and the development of the cigar raw materials made in China just starts, so that large-scale supply is not formed yet. From the quality of cigar raw materials, the maturity of cigar tobacco leaves in the Caribbean region is high, the cigar style characteristics are obvious, the industrial availability is high, but the supply cannot be guaranteed at present, the Indonesia cigar raw material aroma is mainly characterized by green grass aroma and bitter taste, while the Chinese cigar raw material aroma level and aftertaste comfort level are poor, which is mainly reflected in the defects of characteristic aroma, insufficient aroma concentration, large strength, obvious miscellaneous gas, heavy bitter taste and astringent taste and the like.
The tobacco essence is a tobacco flavor mixture prepared from two or more flavors and certain auxiliary materials (a carrier, a solvent, a pigment, an antioxidant, a preservative, a humectant, a flavoring agent and the like) according to a certain proportion and a blending process. At present, the production of tobacco essence and spice in the world is mainly artificially synthesized and extracted from natural animals and plants. The artificial synthetic essence and spice for cigarette has limited application because people have debate on the safety problem. Along with the trend of returning to nature of human beings, people increasingly demand safe tobacco essence and spice, the plant extracted spice is pure natural essence and has the original fragrance of plants, but the plant extracted spice is used for tobacco tar and has poor solubility, and effective active ingredients in the plant extracted spice are easy to oxidize, volatilize, decompose and the like in the storage and transportation process, so that the effect is removed, and the plant extracted spice has a plurality of defects when being directly added into tobacco leaves.
For example, the application number is (CN 202110695675.2) the strawberry-flavored electronic cigarette tobacco tar with lasting fragrance and the preparation method thereof. The strawberry-flavor electronic cigarette tobacco tar with lasting fragrance is prepared from the following raw materials in parts by weight: 10-50 parts of 1, 2-propylene glycol, 5-45 parts of glycerol, 5-35 parts of tobacco leaf extract, 2-4 parts of 2-acetylpyridine tobacco essence, 1-5 parts of strawberry flavor substances and 4-8 parts of a fixative; the preparation method comprises the following steps: mixing 1, 2-propylene glycol, glycerol, tobacco leaf extract and 2-acetylpyridine tobacco essence, uniformly stirring to obtain base tobacco tar, adding strawberry flavor substance and fixative into the base tobacco tar, mixing, and uniformly stirring to obtain the electronic cigarette tobacco tar.
The electronic cigarette tobacco tar has the advantages of lasting fragrance and enhancement of satisfaction of smokers through the synergistic effect of the raw materials. However, the electronic cigarette oil can only be used in electronic cigarettes, and the diffusion of flavor components in the cigarette oil is completed by heating, so that the electronic cigarette oil is not suitable for long-term storage in tobacco leaves.
Disclosure of Invention
In order to solve the problems, the invention provides the essence for improving the quality of Indonesia cigar tobacco leaves and the preparation method thereof.
In order to achieve the purpose, the invention is realized by the following technical scheme: on one hand, the invention provides an essence for improving the quality of Indonesia cigar tobacco, which is prepared from the following raw materials in parts by weight: 0.6-6.5 parts of natural plant spice, 0.2-2 parts of tobacco extract, 0.2-3 parts of preservative, 0.3-3 parts of fixative, 0.2-1.5 parts of flavor compensator, 1-5 parts of red date Maillard reactant, 10-20 parts of diluent and 59-87.5 parts of solvent.
In the invention, the natural plant spice is used as a main spice in the essence, is the basis for forming the main body note of the essence, is a basic raw material for forming the fragrance of the essence and represents the real style of the essence.
The tobacco extract can increase the nicotine content of the cigar tobacco leaves, cover up miscellaneous gas, improve smoking satisfaction, and promote the volatilization of natural plant spices, so that the spices can enter the oral cavity of smokers more easily.
The perfume fixative is the most basic and important component of the essence and has the function of making various components in the essence volatilize uniformly.
The fragrance compensating agent has a supplementing effect on the fragrance of the main fragrance, and can make the fragrance in the essence fresh, elegant, rich and not monotonous.
The red date Maillard reaction product contains rich nutrient components such as protein, saccharides, organic acid, vitamin A, vitamin C, various trace calcium, amino acid and the like. Amino acids in red dates can synthesize proteins and nicotine. And has dual functions in endowing the flavor of the flue-cured tobacco, on one hand, the combustion of amino acid can generate nitrogen-containing compounds such as NH which affect the smoke quality 3 (ii) a On the other hand, during the preparation, alcoholization and fermentation of tobacco leaves, the free amino acids and reducing sugars undergo slow non-enzymatic browning to generate various aldehydes and ketones and heterocyclic compounds with roasting flavor such as pyran, pyrrole, pyrazine and pyridine, wherein some amino acids such as phenylalanine are precursors of benzyl alcohol and phenethyl alcohol, and can be decomposed into flavor compounds under proper conditions. Therefore, in the preparation process of adding the red dates into the essence, the tobacco leaves can be greatly improvedAmount of fragrance and type of fragrance.
In the process of synthesizing the red date Maillard reactants, maillard reaction base liquid contains dozens of free amino acids and monosaccharides, a proper reaction environment is provided, and the amino acids and the sugars in the base liquid undergo complex Maillard reaction to generate a large amount of flavor substances. Sufficient exogenous amino acid can be provided after the red date extract is added, the concentration of free amino acid in the reaction base liquid is increased at the moment, the Maillard reaction is promoted, the generation of flavor substances is further promoted, and the Maillard reaction liquid with the characteristic style of red date amino acid is generated by the self degradation and the competition of the additional amino acid with other types of amino acid.
In addition, the invention adopts alanine to carry out Maillard reaction, can generate aldehyde, ketone and other reducing substances, has better oxidation resistance, and particularly has obvious effect on preventing the oxidation of grease, and the addition of the red date Maillard reactant into the essence not only can obviously enhance the tobacco fragrance, reduce the miscellaneous gas and improve the smoking taste, but also can prevent the oxidation deterioration of the effective components in the essence and prolong the service life of the essence.
The thinner can adjust the concentration of the essence to avoid over-strong or over-weak fragrance components.
Preferably, the natural plant perfume comprises, by weight, 0.5-5 parts of labdanum extract and 0.1-1.5 parts of benzoin paste.
Labdanum, commonly known as cistus, is a perennial evergreen shrub of the genus cistus of the family of the semifloridae. The labdanum extract added with spice has warm ambergris and amber paste fragrance, long fragrance retention time and good fragrance fixing effect. The benzoin cream is rich in fruit aroma and herbal medicine aroma, and belongs to traditional Chinese medicinal materials. The invention uses the labdanum extract and the benzoin extract in a composite way as the main flavor of the flavor, and the flavor is added into the tobacco leaves, so that the tobacco leaves have functional effects and can treat angry fishing, internal fishing, insect pain, external hernia, cardialgia, and the like.
Preferably, the tobacco extract is at least one of a flue-cured tobacco extract and an air-cured tobacco extract.
Preferably, the fixative comprises 0.1-1 part of benzyl benzoate, 0.1-1 part of benzyl alcohol and 0.1-1 part of cinnamyl alcohol in parts by weight.
Preferably, the fragrance compensating agent comprises 0.1-1 part of ethyl laurate and 0.1-0.5 part of 2-acetylpyrazine in parts by weight.
Preferably, the solvent is propylene glycol, the diluent is alcohol with the mass concentration of 95%, and the preservative is lactic acid.
According to the invention, the lactic acid is added into the essence, so that the essence not only can play a role of corrosion prevention, but also can reduce stimulation due to unique sour taste, so that smoke is soft and smooth, and the lactic acid can neutralize nicotine and nicotine, so that harmful ingredients to human bodies are reduced, and the quality of tobacco leaves is improved.
On the other hand, the invention provides a preparation method of the essence for improving the quality of Indonesia cigar tobacco leaves, which comprises the following steps:
s1, adding 0.5-5 parts of natural plant spice, 0.1-1 part of cinnamyl alcohol, 0.2-2 parts of tobacco extract, 0.1-1.5 parts of benzoin paste, 0.2-3 parts of lactic acid, 0.2-2 parts of fixative, 0.1-1 part of fragrance compensator, 0.1-0.5 part of 2-acetylpyrazine, 1-5 parts of red date Maillard reactant, 10-20 parts of 95% alcohol and 59-87.5 parts of solvent into a stirring tank, stirring and mixing uniformly to obtain a mixture, and standing for later use;
and S2, filtering the mixture obtained in the step S1 by using a 80-100-mesh screen, and filling to obtain the essence. In a preferred embodiment of the method of the invention,
preferably, the stirring tank in S1 is stirred for 20-30min under the condition that the rotating speed is 300-500 r/min.
Preferably, the preparation method of the red date Maillard reactant is as follows: adding the red date extract, vanillin, alanine and water into a reaction tank in sequence, stirring, heating to 48-52 ℃ until the red date extract is dissolved, then adding catalyst ascorbic acid and ammonia water, heating to 93-97 ℃, reacting for 5 hours, cooling to 30-40 ℃ after the reaction is finished, and finally filtering and filling by using a 80-100 mesh screen to obtain the red date Maillard reaction product.
Preferably, the mass ratio of the red date extract to the vanillin to the alanine to the water to the ascorbic acid to the ammonia water is (1-5): (1-10): (1-2): (2-3): (50-60): (1-5): (5-10).
Compared with the prior art, the invention has the following beneficial effects:
1. the essence for improving the quality of Indonesia cigar tobacco provided by the invention can coordinate the characteristic aromas of various raw materials, can improve the smoke quality by adding the essence into cigar tobacco, can improve the problem of bitter taste, can soften and refine smoke, and can improve aftertaste.
2. The essence for improving the quality of Indonesia cigar tobacco provided by the invention is simple in preparation method, the preparation raw materials comprise natural plant spices, red date Maillard reactants and other green beneficial substances, and the essence is non-toxic and harmless and conforms to the environment-friendly development concept.
Drawings
Fig. 1 is a flow chart of a method for preparing a flavor for improving the quality of indonesia cigar tobacco in an embodiment of the present invention.
Detailed Description
In order to more clearly illustrate the embodiments of the present invention and the technical solutions in the prior art, the following will describe the specific embodiments of the present invention with reference to the accompanying drawings.
It is obvious that the drawings in the following description are only some embodiments of the invention, and that for a person skilled in the art, without inventive effort, other drawings and embodiments can be derived from them, and the invention is not limited to this embodiment.
The specific embodiment of the invention is as follows:
example 1
The essence for improving the quality of Indonesia cigar tobacco is prepared from the following raw materials in parts by weight: 0.5 part of labdanum extract, 0.1 part of cinnamyl alcohol, 0.2 part of flue-cured tobacco extract, 0.1 part of benzoin paste, 0.2 part of lactic acid, 0.1 part of benzyl benzoate, 0.1 part of benzyl alcohol, 0.1 part of ethyl laurate, 0.1 part of 2-acetylpyrazine, 1 part of red date Maillard reactant, 10 parts of 95% alcohol and 87.5 parts of propylene glycol.
In this example:
the preparation method of the essence comprises the following steps:
s1, adding 0.5 part of labdane extract, 0.1 part of cinnamyl alcohol, 0.2 part of flue-cured tobacco extract, 0.1 part of benzoin paste, 0.2 part of lactic acid, 0.1 part of benzyl benzoate, 0.1 part of benzyl alcohol, 0.1 part of ethyl laurate, 0.1 part of 2-acetylpyrazine, 1 part of red date Maillard reactant, 10 parts of 95% alcohol and 87.5 parts of propylene glycol into a stirring tank, stirring for 20min under the condition that the rotation speed is 300r/min, uniformly mixing to obtain a mixture, and standing for later use;
and S2, filtering the mixture obtained in the step S1 by using an 80-mesh screen, and filling to obtain the essence.
The preparation method of the red date Maillard reaction product comprises the following steps: adding red date extract, vanillin, alanine and water into a reaction tank in sequence, stirring, heating to 48 ℃ until the red date extract is dissolved, then adding catalyst ascorbic acid and ammonia water, heating to 93 ℃, reacting for 5 hours, cooling to 30 ℃ after the reaction is finished, and finally filtering and filling by using a 80-mesh screen to obtain the red date Maillard reaction product.
The mass ratio of the red date extract to the vanillin to the alanine to the water to the ascorbic acid to the ammonia water is 5:1:2:50:1:10.
example 2
The essence for improving the quality of Indonesia cigar tobacco is prepared from the following raw materials in parts by weight: 1 part of labdanum extract, 0.2 part of cinnamyl alcohol, 0.5 part of tobacco extract, 0.5 part of benzoin paste, 0.5 part of lactic acid, 0.2 part of benzyl benzoate, 0.2 part of benzyl alcohol, 0.2 part of ethyl laurate, 0.2 part of 2-acetylpyrazine, 2 parts of red date Maillard reactant, 12 parts of 95 parts of alcohol and 62 parts of propylene glycol.
In this example:
the preparation method of the essence comprises the following steps:
s1, adding 1 part of labdanum extract, 0.2 part of cinnamyl alcohol, 0.5 part of tobacco extract, 0.5 part of benzoin paste, 0.5 part of lactic acid, 0.2 part of benzyl benzoate, 0.2 part of benzyl alcohol, 0.2 part of ethyl laurate, 0.2 part of 2-acetylpyrazine, 2 parts of red date Maillard reactant, 12 parts of alcohol and 62 parts of propylene glycol into a stirring tank, stirring for 22min under the condition that the rotating speed is 350r/min, uniformly mixing to obtain a mixture, and standing for later use;
and S2, filtering the mixture obtained in the S1 through a 80-mesh screen, and filling to obtain the essence.
The preparation method of the red date Maillard reactant comprises the following steps: adding red date extract, vanillin, alanine and water into a reaction tank in sequence, stirring, heating to 49 ℃ until the red date extract is dissolved, then adding catalyst ascorbic acid and ammonia water, heating to 94 ℃, reacting for 5 hours, cooling to 32 ℃ after the reaction is finished, and finally filtering and filling by using a 80-mesh screen to obtain the red date Maillard reaction product.
The mass ratio of the red date extract to the vanillin to the alanine to the water to the ascorbic acid to the ammonia water is 6:2:2:52:2:12.
example 3
The essence for improving the quality of Indonesia cigar tobacco is prepared from the following raw materials in parts by weight: 2 parts of labdanum extract, 0.4 part of cinnamyl alcohol, 1 part of tobacco extract, 0.8 part of benzoin paste, 1 part of lactic acid, 0.5 part of benzyl benzoate, 0.5 part of benzyl alcohol, 0.5 part of ethyl laurate, 0.3 part of 2-acetylpyrazine, 3 parts of red date Maillard reactant, 15 parts of 95 parts of alcohol and 70 parts of propylene glycol.
In this example:
the preparation method of the essence comprises the following steps:
s1, adding 2 parts of labdane extract, 0.4 part of cinnamyl alcohol, 1 part of tobacco extract, 0.8 part of benzoin paste, 1 part of lactic acid, 0.5 part of benzyl benzoate, 0.5 part of benzyl alcohol, 0.5 part of ethyl laurate, 0.3 part of 2-acetylpyrazine, 3 parts of red date Maillard reactant, 15 parts of alcohol and 70 parts of propylene glycol into a stirring tank, stirring for 25min under the condition that the rotating speed is 400r/min, uniformly mixing to obtain a mixture, and standing for later use;
and S2, filtering the mixture obtained in the step S1 by using an 80-mesh screen, and filling to obtain the essence.
The preparation method of the red date Maillard reaction product comprises the following steps: adding red date extract, vanillin, alanine and water into a reaction tank in sequence, stirring, heating to 50 ℃ until the red date extract is dissolved, then adding catalyst ascorbic acid and ammonia water, heating to 95 ℃, reacting for 5 hours, cooling to 35 ℃ after the reaction is finished, and finally filtering and filling by using a 80-mesh screen to obtain the red date Maillard reaction product.
Wherein the mass ratio of the red date extract to the vanillin to the alanine to the water to the ascorbic acid to the ammonia water is 8:3:3:55:3:15.
example 4
The essence for improving the quality of Indonesia cigar tobacco is prepared from the following raw materials in parts by weight: 4 parts of Liberbant extract, 0.7 part of cinnamyl alcohol, 1.5 parts of tobacco extract, 1.3 parts of benzoin paste, 2.5 parts of lactic acid, 0.8 part of benzyl benzoate, 0.8 part of benzyl alcohol, 0.8 part of ethyl laurate, 0.4 part of 2-acetylpyrazine, 4 parts of red date Maillard reactant, 18 parts of 95 parts of alcohol and 80 parts of propylene glycol.
In this example:
the preparation method of the essence comprises the following steps:
s1, adding 4 parts of labdane extract, 0.7 part of cinnamyl alcohol, 1.5 parts of tobacco extract, 1.3 parts of benzoin paste, 2.5 parts of lactic acid, 0.8 part of benzyl benzoate, 0.8 part of benzyl alcohol, 0.8 part of ethyl laurate, 0.4 part of 2-acetylpyrazine, 4 parts of red date Maillard reactant, 18 parts of alcohol and 80 parts of propylene glycol into a stirring tank, stirring for 25min under the condition that the rotation speed is 450r/min, uniformly mixing to obtain a mixture, and standing for later use;
and S2, filtering the mixture obtained in the step S1 by using a 100-mesh screen, and filling to obtain the essence.
The preparation method of the red date Maillard reactant comprises the following steps: adding the red date extract, vanillin, alanine and water into a reaction tank in sequence, stirring, heating to 51 ℃ until the red date extract is dissolved, adding catalyst ascorbic acid and ammonia water, heating to 96 ℃, reacting for 5 hours, cooling to 38 ℃ after the reaction is finished, and finally filtering and filling by using a 100-mesh screen to obtain the red date Maillard reactant.
Wherein the mass ratio of the red date extract to the vanillin to the alanine to the water to the ascorbic acid to the ammonia water is 9:3:3:58:4:18.
example 5
The essence for improving the quality of Indonesia cigar tobacco is prepared from the following raw materials in parts by weight: 5 parts of labdanum extract, 1 part of cinnamyl alcohol, 2 parts of tobacco extract, 1.5 parts of benzoin paste, 3 parts of lactic acid, 1 part of benzyl benzoate, 1 part of benzyl alcohol, 1 part of ethyl laurate, 0.5 part of 2-acetylpyrazine, 5 parts of red date Maillard reactant, 20 parts of 95 parts of alcohol and 87.5 parts of propylene glycol.
In this example:
the preparation method of the essence comprises the following steps:
s1, adding 5 parts of Liberbant extract, 1 part of cinnamyl alcohol, 2 parts of tobacco extract, 1.5 parts of benzoin paste, 3 parts of lactic acid, 1 part of benzyl benzoate, 1 part of benzyl alcohol, 1 part of ethyl laurate, 0.5 part of 2-acetylpyrazine, 5 parts of red date Maillard reactant, 20 parts of 95 parts of alcohol and 87.5 parts of propylene glycol into a stirring tank, stirring for 30min under the condition that the rotating speed is 500r/min, uniformly mixing to obtain a mixture, and standing for later use;
and S2, filtering the mixture obtained in the step S1 by using a 100-mesh screen, and filling to obtain the essence.
The preparation method of the red date Maillard reactant comprises the following steps: adding the red date extract, vanillin, alanine and water into a reaction tank in sequence, stirring, heating to 52 ℃ until the red date extract is dissolved, adding catalyst ascorbic acid and ammonia water, heating to 97 ℃, reacting for 5 hours, cooling to 40 ℃ after the reaction is finished, and finally filtering and filling by using a 100-mesh screen to obtain the red date Maillard reactant.
Wherein the mass ratio of the red date extract to the vanillin to the alanine to the water to the ascorbic acid to the ammonia water is 10:3:3:60:5:20.
comparative example 1
On the basis of example 1, the Maillard reaction product of red dates is not added as the condition of comparative example 1, and the concrete conditions are as follows:
the essence for improving the quality of Indonesia cigar tobacco is prepared from the following raw materials in parts by weight: 0.5 part of labdanum extract, 0.1 part of cinnamyl alcohol, 0.2 part of flue-cured tobacco extract, 0.1 part of benzoin extract, 0.2 part of lactic acid, 0.1 part of benzyl benzoate, 0.1 part of benzyl alcohol, 0.1 part of ethyl laurate, 0.1 part of 2-acetylpyrazine, 10 parts of 95% alcohol and 88.5 parts of propylene glycol.
In this example:
the preparation method of the essence comprises the following steps:
s1, adding 0.5 part of labdanum extract, 0.1 part of cinnamyl alcohol, 0.2 part of flue-cured tobacco extract, 0.1 part of benzoin paste, 0.2 part of lactic acid, 0.1 part of benzyl benzoate, 0.1 part of benzyl alcohol, 0.1 part of ethyl laurate, 0.1 part of 2-acetylpyrazine, 10 parts of 95% alcohol and 88.5 parts of propylene glycol into a stirring tank, stirring for 20min under the condition that the rotation speed is 300r/min, uniformly mixing to obtain a mixture, and standing for later use;
and S2, filtering the mixture obtained in the step S1 by using an 80-mesh screen, and filling to obtain the essence.
The essences prepared in examples 1 to 5 and comparative example 1 were grouped and added to the corresponding tobacco leaves, respectively, and the smoking experience of the tobacco leaves was evaluated. The specific process is as follows:
taking 20 complete Indonesia cigar leaves, weighing essence products in a small beaker according to one thousandth of the weight of the leaves, adding a proper amount of purified water, uniformly spraying the purified water on the leaves, balancing for 48 hours in a natural environment, rolling into cigars, and smoking evaluation and recording.
Test example 1
The essences prepared in examples 1 to 5 and comparative example 1 were added to tobacco leaves and subjected to smoking evaluation, and the results of the note characteristics in the smoke are shown in table 1 below.
TABLE 1 results of charm characteristics
From the results in table 1, it can be seen that the tobacco leaf smoking quality can be improved to various degrees and the fragrance amount of the tobacco leaf can be enriched by adding the essences prepared in examples 1 to 5 and comparative example 1 into the indonesia cigar tobacco leaf. Wherein the tobacco leaves of the Indonesia cigar added with the essence prepared in the comparative example 1 have less smoke lifting amount and less newly added smoke taste. This is probably due to the fact that no red date maillard reactant was added during the preparation of the flavour in comparative example 1. In the synthesis process of the red date Maillard reactant, because the Maillard reaction base solution contains more than ten free amino acids and monosaccharides, the amino acids and the sugars in the base solution undergo complex Maillard reaction, and a large amount of flavor substances are generated. Sufficient exogenous amino acid can be provided after the red date extract is added, the concentration of free amino acid in the reaction base liquid is increased at the moment, the Maillard reaction is promoted, the generation of flavor substances is further promoted, and the Maillard reaction liquid with the characteristic style of red date amino acid is generated by the self degradation and the competition of the additional amino acid with other types of amino acid. Therefore, the red date Maillard reactant is added into the essence, so that the smoking quality of the tobacco leaves is improved, and the aroma quantity of the tobacco leaves is enriched.
Test example 2
The essences prepared in examples 1 to 5 and comparative example 1 were added to tobacco leaves and evaluated by smoking, and the sensory quality results of smoking are shown in table 2 below.
TABLE 2 sensory quality results of puffs
From the results in table 2, it can be seen that the addition of the essences prepared in examples 1 to 5 and comparative example 1 to indonesia cigar leaves can improve the elegance and richness of the aroma of the tobacco leaves, soften and smooth the smoke, improve the aftertaste, and reduce the bitterness. Wherein the essence prepared in comparative example 1 is added into Indonesia cigar leaves, and has poor smoke characteristics and light sweet and moist feeling. This is probably due to the fact that no red date maillard reactant was added during the preparation of the flavour in comparative example 1.
The amino acid in the red dates can synthesize protein and nicotine. And has a dual role in imparting flavor to flue-cured tobacco, on the one hand, amino acid combustion can produce nitrogen-containing compounds such as NH that affect smoke quality 3 (ii) a On the other hand, during the preparation, alcoholization and fermentation of tobacco leaves, the free amino acids and reducing sugars undergo slow non-enzymatic browning to generate various aldehydes and ketones and pyran, pyrrole, pyrazine, pyridine and other heterocyclic compounds with baking flavor, wherein some amino acids such as phenylalanine are precursors of benzyl alcohol and phenethyl alcohol, and the heterocyclic compounds are subjected to proper treatmentCan itself decompose into aroma compounds under the conditions of (1).
In the invention, the red date Maillard reactant is added into the essence, so that the sweet smoking feeling of the tobacco leaves can be effectively improved, and the smoke characteristics of the tobacco leaves are improved.
The above-described aspects may be implemented individually or in various combinations, and such variations are within the scope of the present invention.
It is noted that, herein, relational terms such as first and second, and the like may be used solely to distinguish one entity or action from another entity or action without necessarily requiring or implying any actual such relationship or order between such entities or actions. Also, the terms "comprises," "comprising," or any other variation thereof, are intended to cover a non-exclusive inclusion, such that a process, method, article, or apparatus that comprises a list of elements does not include only those elements but may include other elements not expressly listed or inherent to such process, method, article, or apparatus. Without further limitation, an element defined by the phrase "comprising a component of 8230means that the element does not exclude the presence of another like element in a process, method, article, or apparatus that comprises the element.
The foregoing is a more detailed description of the invention in connection with specific preferred embodiments and it is not intended that the specific embodiments of the invention be limited to these descriptions. For those skilled in the art to which the invention pertains, several simple deductions or substitutions can be made without departing from the spirit of the invention, and all shall be considered as belonging to the protection scope of the invention.
Claims (4)
1. The essence for improving the quality of Indonesia cigar tobacco is characterized by being prepared from the following raw materials in parts by weight: 0.6-6.5 parts of natural plant spice, 0.2-2 parts of tobacco extract, 0.2-3 parts of preservative, 0.3-3 parts of fixative, 0.2-1.5 parts of flavor compensator, 1-5 parts of red date Maillard reactant, 10-20 parts of diluent and 59-87.5 parts of solvent;
the natural plant spice comprises 0.5-5 parts of labdanum extract and 0.1-1.5 parts of benzoin cream by weight;
the fixative comprises 0.1-1 part of benzyl benzoate, 0.1-1 part of benzyl alcohol and 0.1-1 part of cinnamyl alcohol in parts by weight;
the fragrance compensating agent comprises 0.1-1 part by weight of ethyl laurate and 0.1-0.5 part by weight of 2-acetylpyrazine;
the solvent is propylene glycol, the diluent is alcohol with the mass concentration of 95%, and the preservative is lactic acid;
the preparation method of the red date Maillard reactant comprises the following steps: adding red date extract, vanillin, alanine and water into a reaction tank in sequence, stirring, heating to 48-52 ℃ until the red date extract is dissolved, then adding catalyst ascorbic acid and ammonia water, heating to 93-97 ℃, reacting for 5 hours, cooling to 30-40 ℃ after the reaction is finished, and finally filtering and filling by using a 80-100 mesh screen to obtain a red date Maillard reactant;
the mass ratio of the red date extract to the vanillin to the alanine to the water to the ascorbic acid to the ammonia water is (5-10): (1-3): (2-3): (50-60): (1-5): (10-20).
2. The essence for improving the quality of Indonesia cigar tobacco according to claim 1, wherein the tobacco extract is at least one of a flue-cured tobacco extract and an air-cured tobacco extract.
3. A process for the preparation of a flavour for improving the quality of indonesian cigar tobacco leaves according to any one of claims 1-2, comprising the steps of:
s1, adding 0.5-5 parts of labdanum extract, 0.1-1 part of cinnamyl alcohol, 0.2-2 parts of tobacco extract, 0.1-1.5 parts of benzoin paste, 0.2-3 parts of lactic acid, 0.1-1 part of benzyl benzoate, 0.1-1 part of benzyl alcohol, 0.1-1 part of ethyl laurate, 0.1-0.5 part of 2-acetylpyrazine, 1-5 parts of red date Maillard reactant, 10-20 parts of 95% alcohol and 59-87.5 parts of solvent into a stirring tank, stirring and mixing uniformly to obtain a mixture, and standing for later use;
and S2, filtering the mixture obtained in the step S1 by using a 80-100-mesh screen, and filling to obtain the essence.
4. The preparation method of the essence for improving the quality of Indonesia cigar tobacco leaves as claimed in claim 3, wherein the stirring tank in S1 is stirred for 20-30min at a rotation speed of 300-500 r/min.
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| US6298858B1 (en) * | 1998-11-18 | 2001-10-09 | R. J. Reynolds Tobacco Company | Tobacco flavoring components of enhanced aromatic content and method of providing same |
| CN101497845B (en) * | 2008-01-30 | 2012-10-03 | 湖北中烟工业有限责任公司 | Method for producing cigarette flavor by maillard reaction with red date extract as raw material |
| CN102206548B (en) * | 2011-01-29 | 2013-06-05 | 广州市澳键丰泽生物科技有限公司 | Formula of tobacco essence additive containing maple extract |
| CN104479869A (en) * | 2014-12-03 | 2015-04-01 | 湖北中烟工业有限责任公司 | Casing essence for quietly elegant fragrance style cigarette |
| CN107164094B (en) * | 2017-07-07 | 2021-03-16 | 湖北中烟工业有限责任公司 | Preparation method and application of Maillard reactant for increasing color and increasing aroma of proline |
| CN110699181A (en) * | 2019-09-28 | 2020-01-17 | 重庆中烟工业有限责任公司 | Tobacco essence based on tobacco leaves and preparation method and application thereof |
| CN113667536A (en) * | 2021-07-19 | 2021-11-19 | 河南中烟工业有限责任公司 | Cigar-flavor essence and application thereof |
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