CN112980576A - Floral-scented fruit-flavored essence and preparation method and application thereof - Google Patents
Floral-scented fruit-flavored essence and preparation method and application thereof Download PDFInfo
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- CN112980576A CN112980576A CN202110231279.4A CN202110231279A CN112980576A CN 112980576 A CN112980576 A CN 112980576A CN 202110231279 A CN202110231279 A CN 202110231279A CN 112980576 A CN112980576 A CN 112980576A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
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Abstract
The application relates to the field of essence, and particularly discloses a floral-scented fruit essence and a preparation method and application thereof. The floral fragrant fruit essence comprises the following components: (ii) albuterol; a poly santalol; tetrahydrogeraniol; marsdenia longipes alcohol; methyl dihydrojasmonate; ambrotone; cis-jasmone; muscenone; a petrolatum; privet ketone; convalanone; grapefruit methane; hydroxy vanillyl alcohol; vetiveryl acetate; laurel leaf oil; a fragrance fixative; a modifying agent; and a mixture; a solvent. The preparation method comprises the following steps: weighing the components in proportion, mixing the components, refluxing and stirring, and standing for 24-48h to obtain the floral fragrant fruit essence. The flower, fruit and fragrance blending essence can be used in perfume, shampoo, shower gel and laundry detergent, and has the advantages of high coordination degree of fragrance and comfortable fragrance; in addition, the preparation method has the advantages of simplicity and convenience.
Description
Technical Field
The application relates to the field of essence, in particular to a floral-scented fruit essence and a preparation method and application thereof.
Background
The essence belongs to volatile substances and is a mixture with certain fragrance prepared manually. In order to obtain a specific fragrance, a perfumer generally needs to blend several or several tens of fragrances at a certain ratio.
The flower fragrance and fruit fragrance flavor is one of essence flavors, and the flower fragrance and fruit fragrance flavor has the softness and beauty of flower fragrance and the freshness of fruit fragrance, so that the flower fragrance and fruit fragrance flavor is rich in natural smell. When the flower, fruit and spice essence is added into daily chemical products such as perfume, shampoo, shower gel and the like, the flower, fruit and spice essence can enable the daily chemical products to emit lasting and attractive fragrance, so that elegant and comfortable feeling is brought to people, and the life of people is more colorful.
The fragrance of the essence is the key of the quality of the essence, the fragrance of the fragrance blending essence of the flower and fruit fragrance is usually generated by mixing a plurality of spices, and meanwhile, the fragrance of the essence also has unique front, middle and back blending changes, so that the blending of the plurality of spices has important influence on the fragrance of the essence and the fragrance change, and after the blending of the plurality of spices, the phenomenon of discomfort symptoms such as disfavor, bias and even vertigo is caused easily exists, so that the improvement space is provided.
Disclosure of Invention
In order to improve the coordination degree of the fragrance of the essence and enable the essence to generate comfortable fragrance, the application provides the floral-scented fruit essence and the preparation method and the application thereof.
The application provides a fragrant fruit essence of flowers adopts following technical scheme:
the floral fragrant fruit essence comprises the following components in percentage by mass:
2% -3% of white flower alcohol;
1.2 to 1.8 percent of poly santalol;
0.1 to 0.15 percent of tetrahydrogeraniol;
2.5 to 3.4 percent of crescent moon orchid alcohol;
18-21% of methyl dihydrojasmonate;
28% -31% of ambrotone;
cis-jasmone 0.14-0.2%;
1.2 to 1.7 percent of musk ketene;
0.1 to 0.3 percent of vaseline;
0.1 to 0.3 percent of privet ketone;
4% -5.5% of convallaria majalis ketone;
0.15 to 0.25 percent of grapefruit methane;
3% -3.5% of hydroxyl vanillyl alcohol;
0.3 to 0.4 percent of vetiveryl acetate;
0.05% -0.15% of bay leaf oil;
23.4% -26.75% of a fixative;
0.66 to 1.36 percent of mixture
0.547% -1.079% of modifier;
the balance being solvent.
By adopting the technical scheme, the components are matched in a specific proportion, so that the layering sense of the floral fruity essence is obvious, the former is blackberry and grapefruit, the middle is lily of the valley and bay leaf, the latter is musk, ambergris and wood, the fragrance of the blackberry and the grapefruit is combined to enable the essence to firstly emit slightly sour fruity, the fresh and cool fragrance of a field is rich, a fresh and striking sense is given to people, the addition of the bay leaf fragrance and the boll flower fragrance neutralizes the sour taste in the former, the fresh, sweet and soft fragrance is brought at the same time, the layering sense of the fragrance is richer, the later-adjusted musk and ambergris are rich in ' vital ' fresh fragrance ' and have wooden faint scent, the warm and agile sense is given to people, the fragrance of the essence is warm and rich in emotion, the fragrance harmony of the floral fruity essence is high, the transition is natural, and people feel comfortable.
Preferably, the blending agent comprises oil of cloth withered leaves, and the mass percentage of the oil of cloth withered leaves in the essence for blending the fragrance of the flower and fruit is 0.08-0.12%.
By adopting the technical scheme, the fragrance of the essence can be better modified after the oil of the blanc leaf is added, so that the sour taste in the front adjustment is regulated and controlled in a comfortable range, and the comfort level of the fragrance of the essence is further improved.
Preferably, the modifier also comprises passionflower thioether, and the passionflower thioether accounts for 0.03-0.06% of the mass of the flower and fruit fragrant essence.
By adopting the technical scheme, the lily of the valley and laurel mixed fragrance in the essence can be better modified after the passionflower thioether is added, so that the fragrance in the essence is fresh and cool without stuffiness, the comfort level of the fragrance is further improved, and simultaneously the irritation of the essence to the skin can be obviously reduced after the bruised leaves, the passionflower thioether and the laurel leaf oil are added into the essence, so that after the essence is used as a daily additive, comfortable and pleasant feeling is brought to people, and discomfort is not easily brought to the skin of the human body.
Preferably, the mixture also comprises dynamite, and the modifier comprises alpha-damascone, wherein the alpha-damascone accounts for 0.01-0.03% of the fragrant and fruity essence by mass, and the dynamite accounts for 0.01-0.03% of the fragrant and fruity essence by mass.
By adopting the technical scheme, the royal ketone, the methyl damascone, the paraquat leaf oil and the bruised leaf oil are added into the essence in specific content, so that the fruit fragrance of the blackberry in the fragrance of the essence is converged relatively when being dispersed, the blackberry fragrance is more fresh and natural, the natural sense of the smell of the blackberry is enhanced, and the comfort level of the fragrance of the essence is further improved.
Preferably, the modifier comprises the following components in percentage by mass:
0.005% -0.012% of leaf alcohol;
benzyl acetate 0.01-0.03%;
0.001 to 0.005 percent of methyl anthranilate;
0.001 to 0.005 percent of allyl caproate;
0.01 to 0.05 percent of sunflower aldehyde;
0.005% -0.012% of dodecanal;
0.01 to 0.03 percent of diphenyl ether;
ethyl maltol 0.01-0.03%;
0.05% -0.1% of green flower fragrance;
blackcurrant essence 0.005-0.015%;
0.4 to 0.7 percent of limonene.
By adopting the technical scheme, the components have better modification effects on the blackberry and grapefruit of the former seasoning, the lily of the valley and the laurel leaf of the middle seasoning, and the musk, ambergris and wood fragrance of the latter seasoning, so that the sharp odor in the perfume can be better covered up, the fragrance is more fresh and soft, and the fragrance of the essence is more comfortable and charming.
Preferably, the blending agent also comprises the following components in percentage by mass:
0.2% -0.3% of linalool:
0.03% -0.05% of dihydromyrcenol;
0.01 to 0.05 percent of citronellol;
0.1 to 0.2 percent of methyl terpineol;
0.01 to 0.05 percent of phenethyl alcohol;
0.05 to 0.15 percent of nerolidol;
geranyl acetate 0.01% -0.05%;
vanillyl acetate 0.03% -0.1%;
0.05 to 0.1 percent of terpinyl acetate;
0.05 to 0.08 percent of rose oxide;
0.03-0.08% of vetiver oil.
By adopting the technical scheme, the blending effect of the fragrance of the raw materials is better, so that the blackberry and grapefruit of the former blend, the lily of the valley and the laurel leaf of the middle blend, and the musk, ambergris and woody fragrance of the latter blend are more prominent, and the layering of the essence is more obvious.
Preferably, the perfume fixative comprises the following components in percentage by mass:
0.3 to 0.6 percent of abelmoschus manihot lactone;
musk T23% -26%;
0.1 to 0.15 percent of synthetic oak moss.
By adopting the technical scheme, the abelmoschus manihot lactone, the musk T and the synthetic oak moss are added, so that the abelmoschus manihot lactone, the musk T and the synthetic oak moss are not easy to volatilize, and the volatilization speed of other spices can be inhibited, so that the volatilization speed of the floral fragrant fruit essence is reduced, the fragrance retaining time is prolonged, all spices are tightly combined together, and the lasting stability of fragrance is kept.
Preferably, the solvent is dipropylene glycol.
By adopting the technical scheme, the solvent is the dipropylene glycol, and the essence raw materials have better dissolubility in the dipropylene glycol, so that the components can be conveniently subjected to reflux mixing, the more uniform the spice is mixed, the more stable the quality of the essence is, and the more comfortable and attractive the fragrance is.
Preferably, the preparation method of the floral fragrant fruit essence comprises the following steps: weighing albuterol, poly santalol, tetrahydrogeraniol, gomphostearyl alcohol, dihydrojasmonic acid, ambergris ketone, cis-jasmone, musk ketene, vandula ketone, ligustral, lilial, grapefruit methane, hydroxyvanillyl alcohol, vetiveryl acetate, bay leaf oil, a fragrance fixing agent, a mixture and a modifier according to a proportion, mixing the components, refluxing and stirring, and standing for 24-48h to obtain the floral passion fruit fragrance essence.
Through adopting above-mentioned technical scheme, through weighing and mixing each essence raw materials for each spices dispersion is more even under the backward flow effect, makes each spices coordinate each other, and each spices mixes and produces the fragrance change, through stewing, makes essence fragrance become harmonious, mellow and soft, makes the stability of fragrance improve, and the preparation method of this application essence has simple, convenient, low in production cost's advantage.
An application of a fragrance essence is prepared by adding the fragrance essence into perfume, shampoo, bath lotion, and laundry detergent.
By adopting the technical scheme, the flower fragrance and fruit fragrance blending essence is added into perfume, shampoo, shower gel and laundry detergent, and the fragrance of the flower fragrance and fruit fragrance blending essence is high in harmony and good in quality, so that the perfume, the shampoo, the shower gel and the laundry detergent have comfortable and charming fragrance, and the pleasure feeling in consumption can be effectively improved.
In summary, the present application has the following beneficial effects:
1. according to the application, the fragrance of the flower fragrance and fruit fragrance essence is matched according to a specific proportion, so that the former fragrance of the flower fragrance and fruit fragrance essence is blackberry and grapefruit, the fragrance of the blackberry and grapefruit is combined to enable the essence to firstly give out slightly sour and astringent fruit fragrance, fresh and striking feeling is given to people, the middle fragrance is lily of the valley and bay leaves, the bay leaf fragrance and the lily of the valley fragrance bring fresh, sweet, warm and soft smell, the latter fragrance is musk, ambergris and wood, warm and agile feeling is given to people, the fragrance of the essence is warm and rich in feeling, the fragrance harmony of the flower fragrance and fruit fragrance essence is high, transition is natural, and people feel very comfortable.
2. This application is used through adding the collocation of blosson leaf oil and passionflower thioether for sour regulation and control in the preceding accent is in comparatively comfortable scope, makes the comfort level of essence fragrance further improve, and the combination of blosson leaf, passionflower thioether and laurel leaf oil can obviously reduce the irritability of essence to skin simultaneously, has reduced the stimulus that essence brought to human skin.
3. This application is through adding royal ketone, methyl damascenone, paraquat leaf oil collocation for the fragrance of blackberry is more fresh and does not sting, makes essence more fresh nature, thereby makes the comfort level of essence fragrance further improve.
4. The fragrance fixing agent is abelmoschus manihot lactone, musk T and synthetic oak moss, and the volatilization speed of other spices can be inhibited by the abelmoschus manihot lactone, the musk T and the synthetic oak moss, so that the fragrance retaining time is prolonged, the whole spices are tightly combined together, and the lasting stability of the fragrance is favorably maintained.
Detailed Description
The following examples further illustrate the present application in detail.
The raw material source information for this application is detailed in table 1.
TABLE 1
Example 1
The floral fragrant fruit essence comprises the following components: the perfume comprises albuterol, polysaltenol, tetrahydrogeraniol, goversol, dihydrojasmonic acid, ambergris ketone, cis-jasmone, musk ketene, vanolone, ligustral, lilial, methyl pomelo, hydroxyvanillyl alcohol, vetiveryl acetate, bay leaf oil, a perfume fixative, a mixture, a modifier and a solvent.
The mixture is selected from leaf alcohol, benzyl acetate, methyl anthranilate, allyl caproate, sunflower aldehyde, dodecanal, diphenyl ether, ethyl maltol, chloroflufen, blackcurrant essence, and limonene.
The modifier is linalool, dihydromyrcenol, citronellol, alpha terpineol, phenethyl alcohol, nerolidol, geranyl acetate, vanillyl acetate, terpinyl acetate, rose oxide and vetiver oil.
The perfume fixative is abelmoschus manihot lactone, Moschus T, and synthetic oak moss.
The solvent is dipropylene glycol.
In example 1, the preparation method of the floral fruit essence comprises the following steps:
weighing albuterol, polysaltol, tetrahydrogeraniol, gomisin, dihydrojasmonic acid, ambergris ketone, cis-jasmone, musk ketene, paraffine, ligustral, lilial, grapefruit aldehyde, methyl grapefruit, hydroxyvanillyl alcohol, vetiveryl acetate, bay leaf oil, leaf alcohol, benzyl acetate, methyl anthranilate, allyl caproate, sunflower aldehyde, dodecanal, diphenyl ether, ethyl maltol, patchouli, blackcurrant base, limonene, linalool, dihydromyrcenol, citronellol, methyl terpineol, phenethyl alcohol, nerolidol, geranyl acetate, vanillyl acetate, terpinyl acetate, rose ether, vetiver oil and dipropylene glycol according to a weighing quality table (detailed in table 2), adding into a stirring kettle at a rotating speed of 100r/min, stirring and refluxing for 20min, and standing at room temperature for 24h to obtain the floral bergamot essence.
Example 2
The difference from example 1 is that: in the preparation method of the floral bouquet essence, the albuterol, the polysaltanol, the tetrahydrogeraniol, the marjoram alcohol, the dihydrojasmonic acid, the ambergris ketone, the cis-jasmone, the musk ketene, the paraquat ketone, the ligustral, the lilial, the grapefruit methane, the hydroxyvanillyl alcohol, the vetiveryl acetate, the bay leaf oil, the leaf alcohol, the benzyl acetate, the methyl anthranilate and the allyl hexanoate are weighed according to a weighing mass table (detailed in table 2), sunflower aldehyde, dodecanal, diphenyl ether, ethyl maltol, patchouli, blackcurrant essence, limonene, linalool, dihydromyrcenol, citronellol, methyl terpineol, phenethyl alcohol, nerolidol, geranyl acetate, vanillyl acetate, terpinyl acetate, rose ether, vetiver oil and dipropylene glycol are added into a stirring kettle together, the rotating speed is 80r/min, stirring reflux is carried out for 25min, and standing is carried out for 24h at room temperature, so as to obtain the floral passion fruit essence.
Example 3
The difference from example 1 is that: in the preparation method of the floral bouquet essence, the albuterol, the polysaltanol, the tetrahydrogeraniol, the marjoram alcohol, the dihydrojasmonic acid, the ambergris ketone, the cis-jasmone, the musk ketene, the paraquat ketone, the ligustral, the lilial, the grapefruit methane, the hydroxyvanillyl alcohol, the vetiveryl acetate, the bay leaf oil, the leaf alcohol, the benzyl acetate, the methyl anthranilate and the allyl hexanoate are weighed according to a weighing mass table (detailed in table 2), sunflower aldehyde, dodecanal, diphenyl ether, ethyl maltol, patchouli, blackcurrant essence, limonene, linalool, dihydromyrcenol, citronellol, methyl terpineol, phenethyl alcohol, nerolidol, geranyl acetate, vanillyl acetate, terpinyl acetate, rose ether, vetiver oil and dipropylene glycol are added into a stirring kettle together, the rotating speed is 90r/min, stirring and refluxing are carried out for 30min, and standing is carried out for 48h at room temperature, so as to obtain the floral passion fruit essence.
Examples 4 to 6
A floral fruity essence is different from the essence in example 1 only in that: also comprises the following components:
passion flower thioether and Bukul leaf oil.
In examples 4 to 6, the preparation method of the bouquet essence comprises the following steps:
weighing passionflower thioether, brussel leaf oil and albuterol, poly-santalol, tetrahydrogeraniol, gomisin, dihydrojasmonic acid, ambergris ketone, cis-jasmone, musk ketene, vanketone, ligustral, lilial, methyl grapefruit, hydroxyvanillyl alcohol, vanillyl acetate, bay leaf oil, leaf alcohol, benzyl acetate, methyl anthranilate, allyl caproate, capric aldehyde, dodecanal, diphenyl ether, ethyl maltol, patchouli, blackcurrant aceryl, limonene, linalool, dihydromyrcenol, citronellol, methyl terpineol, phenethyl alcohol, nerol, geranyl acetate, vanillyl acetate, terpinyl acetate, rose ether, vetiver oil and dipropylene glycol according to a weighing quality table (detailed in table 2), adding into a stirring kettle, the rotating speed is 100r/min, stirring and refluxing are carried out for 20min, and standing is carried out for 36h at room temperature, so as to obtain the floral fragrant fruit essence.
Examples 7 to 9
A floral fruity essence is different from the essence in example 6 only in that: also comprises the following components:
methyl damascone, and royal ketone.
In examples 7 to 9, the preparation method of the bouquet essence comprises the following steps:
weighing the leaf oil of bruton, methyl damascone, royal ketone and albuterol, poly santalol, tetrahydrogeraniol, gomphostearyl alcohol, dihydrojasmonic acid, ambergris ketone, cis-jasmone, musk ketene, paraquat ketone, ligustral, lilial aldehyde, grapefruit methane, hydroxyvanillyl alcohol, vanillyl acetate, bay leaf oil, folyl alcohol, benzyl acetate, methyl anthranilate, allyl caproate, capric aldehyde, dodecanal, diphenyl ether, ethyl maltol, patchouli, blackcurrant essence, limonene, linalool, dihydromyrcenol, citronellol, methyl terpineol, phenethyl alcohol, nerolidol, geranyl acetate, vanillyl acetate, terpinyl acetate, rose oxide, vetiver oil and dipropylene glycol according to a weighing mass table (detailed in table 3) and adding into a stirring kettle together, the rotating speed is 100r/min, stirring and refluxing are carried out for 20min, and standing is carried out for 36h at room temperature, so as to obtain the floral fragrant fruit essence.
Tables 2 and 3 show the weighed mass (kg) of each component in the floral fruit essences in the respective examples.
TABLE 2
TABLE 3
Comparative example 1
The difference from example 4 is that: in the preparation method of the floral fragrant fruit essence, the lauric leaf oil is replaced by the same amount of dipropylene glycol.
Application examples 1 to 10
The perfume containing the scented fruit essence comprises the following components in parts by mass: 10kg of floral fragrant and fruity essence, 73kg of ethanol, 5kg of propylene glycol and 12kg of purified water.
Use of floral fruity essences of examples 1 to 10 the floral fruity essences prepared in examples 1 to 9 and comparative example 1 were used, respectively.
The preparation method of the perfume containing the floral fragrant and fruity essence comprises the following steps: mixing 10kg of the floral fragrant fruit essence, 73kg of ethanol, 5kg of propylene glycol and 12kg of purified water, and stirring for 5min at a stirring speed of 100r/min to obtain the perfume containing the floral fragrant fruit essence.
Experimental example 1
Evaluation test of fragrance
Cutting filter paper into pieces of distinguishing toilet paper with the size of 1 multiplied by 5cm, respectively dripping equal amount of samples of application examples 1-9 on the distinguishing toilet paper by a dropper, placing the pieces on a ventilated place, respectively carrying out fragrance retention tests 2h, 4h, 8h and 24h after dripping, wherein the test method comprises holding one end of the distinguishing toilet paper, approaching the distinguishing toilet paper to the nose and shaking the distinguishing toilet paper, and recording the fragrance 2h, 4h, 8h and 24h after dripping.
Application example 1: when dripping: the sour and astringent fresh blackberry fruit fragrance is mixed with the fresh grapefruit fruit fragrance, and after the dripping, the time is 2 hours: the light grapefruit fruity flavor is accompanied with fresh blackberry fruity flavor, the faint scent is mixed with light bitter taste, and the grapefruit fruity flavor is added after 4 hours: the fragrant bay leaf aroma is mixed with strong lily of the valley flower aroma, and the fragrance is 8 hours after the dripping: the agile musk and ambergris are mixed with mellow wood fragrance, and 24 hours after dripping: the agilawood musk and ambergris are mixed with mellow wood fragrance.
Application example 2: when dripping: the sour and astringent fresh blackberry fruit fragrance is mixed with the fresh grapefruit fruit fragrance, and after the dripping, the time is 2 hours: the light grapefruit fruity flavor is accompanied with fresh blackberry fruity flavor, the faint scent is mixed with light bitter taste, and the grapefruit fruity flavor is added after 4 hours: the fragrant bay leaf aroma is mixed with strong lily of the valley flower aroma, and the fragrance is 8 hours after the dripping: the agile musk and ambergris are mixed with mellow wood fragrance, and 24 hours after dripping: the agilawood musk and ambergris are mixed with mellow wood fragrance.
Application example 3: when dripping: the sour and astringent fresh blackberry fruit fragrance is mixed with the fresh grapefruit fruit fragrance, and after the dripping, the time is 2 hours: the light grapefruit fruity flavor is accompanied with fresh blackberry fruity flavor, the faint scent is mixed with light bitter taste, and the grapefruit fruity flavor is added after 4 hours: the fragrant bay leaf aroma is mixed with strong lily of the valley flower aroma, and the fragrance is 8 hours after the dripping: the agile musk and ambergris are mixed with mellow wood fragrance, and 24 hours after dripping: the agilawood musk and ambergris are mixed with mellow wood fragrance.
Application example 4: when dripping: the fresh blackberry fruit fragrance is mixed with the fresh grapefruit fruit fragrance, and after the dripping, the time is 2 hours: the faint grapefruit fruit fragrance is accompanied with the clear blackberry fruit fragrance, the faint bitter taste is mixed in the faint scent, and the grapefruit fruit fragrance is added 4 hours after dripping: the fragrant bay leaf aroma is mixed with fresh and sweet convallaria majalis aroma, and the fragrance is dropwise added for 8 hours: the agile musk and ambergris are mixed with mellow wood fragrance, and 24 hours after dripping: the agilawood musk and ambergris are mixed with mellow wood fragrance.
Application example 5: when dripping: the fresh blackberry fruit fragrance is mixed with the fresh grapefruit fruit fragrance, and after the dripping, the time is 2 hours: the faint grapefruit fruit fragrance is accompanied with the clear blackberry fruit fragrance, the faint bitter taste is mixed in the faint scent, and the grapefruit fruit fragrance is added 4 hours after dripping: the fragrant bay leaf aroma is mixed with fresh and sweet convallaria majalis aroma, and the fragrance is dropwise added for 8 hours: the agile musk and ambergris are mixed with mellow wood fragrance, and 24 hours after dripping: the agilawood musk and ambergris are mixed with mellow wood fragrance.
Application example 6: when dripping: the fresh blackberry fruit fragrance is mixed with the fresh grapefruit fruit fragrance, and after the dripping, the time is 2 hours: the faint grapefruit fruit fragrance is accompanied with the clear blackberry fruit fragrance, the faint bitter taste is mixed in the faint scent, and the grapefruit fruit fragrance is added 4 hours after dripping: the fragrant bay leaf aroma is mixed with fresh and sweet convallaria majalis aroma, and the fragrance is dropwise added for 8 hours: the agile musk and ambergris are mixed with mellow wood fragrance, and 24 hours after dripping: the agilawood musk and ambergris are mixed with mellow wood fragrance.
Application example 7: when dripping: mixing the sour and sweet blackberry fruit fragrance with fresh grapefruit fruit fragrance, and adding the mixture for 2h after dropwise adding: the light grapefruit fruity flavor is accompanied with the sour and sweet blackberry fruity flavor, the faint scent is mixed with light bitter taste, and the grapefruit fruity flavor is added after 4 hours: the fragrant and sweet lily of the valley flower fragrance is mixed with the fragrant and sweet lily of the valley flower fragrance, and the fragrance is 8 hours after the dripping: the agile musk and ambergris are mixed with mellow wood fragrance, and 24 hours after dripping: the agilawood musk and ambergris are mixed with mellow wood fragrance.
Application example 8: when dripping: mixing the sour and sweet blackberry fruit fragrance with fresh grapefruit fruit fragrance, and adding the mixture for 2h after dropwise adding: the light grapefruit fruity flavor is accompanied with the sour and sweet blackberry fruity flavor, the faint scent is mixed with light bitter taste, and the grapefruit fruity flavor is added after 4 hours: the fragrant and sweet lily of the valley flower fragrance is mixed with the fragrant and sweet lily of the valley flower fragrance, and the fragrance is 8 hours after the dripping: the agile musk and ambergris are mixed with mellow wood fragrance, and 24 hours after dripping: the agilawood musk and ambergris are mixed with mellow wood fragrance.
Application example 9: when dripping: mixing the sour and sweet blackberry fruit fragrance with fresh grapefruit fruit fragrance, and adding the mixture for 2h after dropwise adding: the light grapefruit fruity flavor is accompanied with the sour and sweet blackberry fruity flavor, the faint scent is mixed with light bitter taste, and the grapefruit fruity flavor is added after 4 hours: the fragrant and sweet lily of the valley flower fragrance is mixed with the fragrant and sweet lily of the valley flower fragrance, and the fragrance is 8 hours after the dripping: the agile musk and ambergris are mixed with mellow wood fragrance, and 24 hours after dripping: the agilawood musk and ambergris are mixed with mellow wood fragrance.
According to the fragrance comparison of application examples 4-6 and application examples 1-3, the addition of the passionflower thioether and the bruised leaf oil can converge the sour taste in the blackberry fragrance to a certain extent, so that the sour taste of the blackberry becomes softer and astringent, and meanwhile, the fragrance of the middle-mixed laurel and lily of the valley is more refreshing and not stuffy, so that the fragrance of the essence is more comfortable and charming.
According to the comparison of the aromas of the application examples 7-9 and the application examples 1-3, by adding the dynamite, the alpha-damascone, the paraquat leaf oil and the fresh and sweet fruity oil, the acidic odor in the blackberry aroma is obviously reduced, the smell of the blackberry is more convergent and more mellow, the aroma of the blackberry is more attractive, and the integral aroma of the floral fruit aroma essence is more coordinated.
Experiment 2
Allergy test experiment
50 adults with sensitive skin are selected and divided into 10 groups on average, 5 persons in each group are selected, the perfume samples of the corresponding application examples 1-10 are equally sprayed on the inner side of the wrist, the neck and the back of the ear of each group of testees, and the allergic conditions of the inner side of the wrist, the neck and the back of the ear of each group of testees are observed and recorded within 30min after spraying. The assay data are detailed in table 4.
TABLE 4
The comparison of the data of the application examples 4-6 and the data of the application examples 1-3 in the table 4 shows that by adding the passionflower thioether and the oil of the bruised leaves, the change of the fragrance is obtained, and the allergic rate of a skin sensitive person after using is obviously reduced, so that the passionflower thioether and the bruised leaves are proved to be beneficial to reducing the irritation of the essence to the skin of a human body after being added, so that the essence is more mild and not irritated, and the essence is more suitable for wide consumer groups.
The data comparison of application examples 4-6 and application examples 1-3 can show that the passion flower thioether and the bruised leaf oil are absent, and the anaphylaxis of the essence is not obviously changed, and further, the data comparison of application example 10 and application examples 4-6 in table 4 can show that the anaphylaxis of the essence is also not obviously changed when the bay leaf oil is not added, so that the synergistic cooperation effect of the bay leaf oil, the passion flower thioether and the bruised leaf oil is proved, the effect of reducing the anaphylaxis of the essence is achieved, and the essence is mild and does not irritate.
By comparing the data of application examples 7-9 and application examples 4-6 in table 4, the essence has no change in fragrance and no change in sensitivity by adding alpha damascone and royal ketone.
The specific application example is only for explaining the application, and is not limiting to the application, and a person skilled in the art can make modifications without inventive contribution to the application example as required after reading the present specification, but all of them are protected by patent laws within the scope of the claims of the present application.
Claims (10)
1. The floral fragrant fruit essence is characterized in that: the composite material comprises the following components in percentage by mass:
2% -3% of white flower alcohol;
1.2 to 1.8 percent of poly santalol;
0.1 to 0.15 percent of tetrahydrogeraniol;
2.5 to 3.4 percent of crescent moon orchid alcohol;
18-21% of methyl dihydrojasmonate;
28% -31% of ambrotone;
cis-jasmone 0.14-0.2%;
1.2 to 1.7 percent of musk ketene;
0.1 to 0.3 percent of vaseline;
0.1 to 0.3 percent of privet ketone;
4% -5.5% of convallaria majalis ketone;
0.15 to 0.25 percent of grapefruit methane;
3% -3.5% of hydroxyl vanillyl alcohol;
0.3 to 0.4 percent of vetiveryl acetate;
0.05% -0.15% of bay leaf oil;
23.4% -26.75% of a fixative;
0.66 to 1.36 percent of mixture
0.547% -1.079% of modifier;
the balance being solvent.
2. The floral bouquet essence of claim 1, characterized in that: the blending agent comprises the oil of the leaf of the cloth withered fruit, and the mass percentage of the oil of the cloth withered leaf in the essence of the flower fragrance and the fruit fragrance is 0.08-0.12%.
3. The floral bouquet essence of claim 2, characterized in that: the modifier also comprises passionflower thioether, and the mass percentage of the passionflower thioether in the flower and fruit fragrant essence is 0.03-0.06%.
4. The floral bouquet essence of claim 2, characterized in that: the mixture also comprises Dyssone, the modifier comprises alpha-damascone, the alpha-damascone accounts for 0.01-0.03% of the fragrant fruit essence by mass, and the Dyssone accounts for 0.01-0.03% of the fragrant fruit essence by mass.
5. The floral bouquet essence of claim 1, characterized in that: the modifier comprises the following components in percentage by mass:
0.005% -0.012% of leaf alcohol;
benzyl acetate 0.01-0.03%;
0.001 to 0.005 percent of methyl anthranilate;
0.001 to 0.005 percent of allyl caproate;
0.01 to 0.05 percent of sunflower aldehyde;
0.005% -0.012% of dodecanal;
0.01 to 0.03 percent of diphenyl ether;
ethyl maltol 0.01-0.03%;
0.05% -0.1% of green flower fragrance;
blackcurrant essence 0.005-0.015%;
0.4 to 0.7 percent of limonene.
6. The floral bouquet essence of claim 1, characterized in that: the blending agent also comprises the following components in percentage by mass:
linalool 0.2% -0.3%;
0.03% -0.05% of dihydromyrcenol;
0.01 to 0.05 percent of citronellol;
0.1 to 0.2 percent of methyl terpineol;
0.01 to 0.05 percent of phenethyl alcohol;
0.05 to 0.15 percent of nerolidol;
geranyl acetate 0.01% -0.05%;
vanillyl acetate 0.03% -0.1%;
0.05 to 0.1 percent of terpinyl acetate;
0.05 to 0.08 percent of rose oxide;
0.03-0.08% of vetiver oil.
7. The floral bouquet essence of claim 1, characterized in that: the fragrance fixative comprises the following components in percentage by mass:
0.3 to 0.6 percent of abelmoschus manihot lactone;
musk T23% -26%;
0.1 to 0.15 percent of synthetic oak moss.
8. The floral bouquet essence of claim 1, characterized in that: the solvent is dipropylene glycol.
9. The method for preparing a floral bouquet essence according to any one of claims 1 to 8, characterized in that: the preparation method of the floral fragrant fruit essence comprises the following steps: weighing albuterol, poly santalol, tetrahydrogeraniol, gomphostearyl alcohol, dihydrojasmonic acid, ambergris ketone, cis-jasmone, musk ketene, vandula ketone, ligustral, lilial, grapefruit methane, hydroxyvanillyl alcohol, vetiveryl acetate, bay leaf oil, a fragrance fixing agent and the rest substances according to a proportion, mixing the components, refluxing and stirring, and standing for 24-48h to obtain the floral passion fruit fragrance essence.
10. The use of the floral fruit essence of any one of claims 1 to 8, wherein: the floral bouquet essence according to any one of claims 1 to 8, to be added to perfumes, shampoos, body washes, laundry detergents.
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| CN113444591A (en) * | 2021-07-23 | 2021-09-28 | 广州芬豪香精有限公司 | Preparation method of rose-fragrance laundry soap essence |
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