CN104887563A - Snow chrysanthemum tea anti-allergy mask cream and preparing method thereof - Google Patents
Snow chrysanthemum tea anti-allergy mask cream and preparing method thereof Download PDFInfo
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Abstract
The invention discloses a snow chrysanthemum tea anti-allergy mask cream and a preparing method thereof. The snow chrysanthemum tea anti-allergy mask cream comprises oil phase components such as cetostearyl alcohol, isohexadecanoic alkane and isononanoic acid acetate and aqueous phase components such as glycerol, seaweed polysaccharide rock, tremella isopolysaccharides and a medicine liquor solution in snow chrysanthemum tea, and then fermented concentrated solutions such as a co-emulsifier, the snow chrysanthemum tea, green tea and traditional Chinese medicines are added. A safe, reliable and novel snow chrysanthemum tea anti-allergy mask cream product which is obvious in effect can be prepared through balanced matching of the pure-natural snow chrysanthemum tea, the green tea, the traditional Chinese medicines, such as the liquorice, lotus and oat, which have the anti-allergy recovery effect, active matter fermented through probiotics cryytococcus neoformans and brady yeast pedigree and other effective constituents
Description
Technical field
The invention belongs to cosmetics and skincare product field, be specifically related to a kind of novel anti-allergy facial mask frost containing snowy chrysanthemum tea extract and manufacture method thereof.
Background technology
The fast development of beauty industry, makes many women liked to be beautiful achieve the dream of beautiful appearance.But beauty industry is as an emerging rising industry, and also occurred some discordant problems in the process of fast development, such as some practitioners are quick-acting in order to the cosmetic result that covets, produce the cosmetics and skincare product containing forbidden amphetamine and hormone.Though the women allowing some like to be beautiful temporarily obtains the effect of " beauty treatment ", also bury the hidden danger of skin health, made much original normal skin become more and more fragile and responsive.Therefore in the last few years, the anti-anaphylaxis of skin and reparation problem are the emphasis that people pay close attention to always.Many cosmetics and skincare products with antiallergic repair function also arise at the historic moment, and the utilization and the natural Chinese medicine anti-anaphylaxis that mainly focus on biochemical antiallergic composition and somatomedin are repaired in the utilization of composition.But the product design of this two aspect still has many limitation, the such as utilization of biochemical antiallergic composition and somatomedin, although effect is very fast sometimes, is difficult to toxin problem and the hormone Dependence Problem of fundamentally alleviating skin long term accumulation.And although the utilization of natural Chinese medicine is safe and reliable, due to external application Chinese medicine class skin care item ubiquitous " effective ingredient difficulty absorbs " problem, also makes this kind of antiallergic reparation series products seem and " effect is too slow " not easily accepted by vast client.Therefore need to develop further and be beneficial to the new type of safe that skin absorbs and have acting type anti-anaphylaxis to repair series products.
Summary of the invention
Technical problem to be solved by this invention is the defect for existing in prior art, a kind of snow chrysanthemum tea anti-allergy facial mask frost and preparation method thereof is provided, the method that snow chrysanthemum tea and Chinese medicine ferment in advance is adopted to strengthen the effective ingredient avenged in chrysanthemum tea and Chinese medicine, to reach the object being beneficial to skin and absorbing, promote anti-anaphylaxis effect.
For solving the problems of the technologies described above, the present invention by the following technical solutions:
A snow chrysanthemum tea anti-allergy facial mask frost, is prepared from by the component of following weight parts:
(1) oil phase component: 16 mixed alcohol 1-2 parts, 16 stearyl alcohol and 16 octadecyl glucoside copolymer 2-4 parts, tristerin and PEG-100 stearate copolymer 2-3 part, isomery hexadecane hydrocarbon 4-6 part, isononyl isononanoate 2-4 part, cocoanut oil alcohol caprylate caprate 2-4 part, dimethicone 2-4 part, methyl hydroxybenzoate 0.2-0.3 part, propylparaben 0.1-0.15 part, ditertbutylparacresol 0.03-0.05 part;
(2) water phase components: glycerol 6-8 part, amino acid humectant 2-4 part, Sargassum rock polysaccharide 2-4 part, the different poly-polysaccharide 0.01-0.05 part of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract 50-60 part; Described snow chrysanthemum tea Chinese medicine aqueous extract is made up of the raw material of following masses part: snow chrysanthemum tea 10-15 part, green tea 8-10 part, Radix Glycyrrhizae, oat kernel, Herba Portulacae, snow amass careless each 5-10 part, Sakura leaf, polymerization blade of grass, chinaberry leaf, polygoni cuspidati,radix, scutellariae,radix, Flos Nelumbinis, Radix Ophiopogonis grass, root of Paeonia suffruticosa Ardr., Herba Arctii leaf, elm endothelium, Magnolia bark, arnica montana, Folium Mori, each 3-5 part of Salix alba bark;
(3) component is added after: the concentrated solution 10-15 part after snow chrysanthemum tea herb fermenting;
(4) co-emulsifier component: hydroxy acrylic acid brine and sodium acryloyldimethyl taurate copolymers 0.5-1 part;
(5) antiseptic: mixture 0.1-0.15 part of MIT and 3-iodo-2-propynyl butyl carbamate;
(6) essence: Green tea essence 0.01-0.02 part.
Avenge a preparation method for chrysanthemum tea anti-allergy facial mask frost, comprise the steps:
(1) preparation of oil phase component: 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucoside copolymers, glyceryl stearate and PEG-100 stearate copolymer, different n-nonanoic acid fat in the different ninth of the ten Heavenly Stems, isomery hexadecane hydrocarbon, cocoanut oil alcohol caprylate caprate, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol are added in the rustless steel still of band stirring after taking in proportion, under the stirring of rotating speed 20-30 rev/min, heating for dissolving is complete, and constant temperature disinfection 20 minutes is stand-by at 80-85 DEG C;
(2) preparation of water phase components: the glycerol of formula ratio, amino acid humectant, Sargassum rock polysaccharide wetting agent, the different poly-polysaccharide of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract are taken rear elder generation heating for dissolving in rustless steel still in proportion, be extracted in rustless steel homogenizing still afterwards, under the stirring of 20-30 rev/min, 80-85 DEG C when continuing to be heated to, and constant temperature disinfection 20 minutes is stand-by;
(3) by oil phase slowly suction aqueous phase, and scrape wall stirring, rotating speed is increased to 40-50 rev/min, stir after 2-3 minute, start high speed homogenization device homogenizing 3-5 minute under the high speed of 3000-5000 rev/min, wall rotating speed will be scraped afterwards and drop to 30-40 rev/min, and be cooled to 45-50 DEG C under this rotating speed;
(4) concentrated solution after the snow chrysanthemum tea herb fermenting of formula ratio and co-emulsifier is added, 20-30 minute is stirred under the rotating speed of 20-30 rev/min, continue afterwards to cool to 40 DEG C, add the antiseptic of formula ratio, essence, continuation stir 15-20 minute under same rotating speed, get final product discharging.
Described step (2) snow chrysanthemum tea Chinese medicine aqueous extract prepares by the following method:
(a) weighing: take Radix Glycyrrhizae, oat kernel, Herba Portulacae, snow amasss careless each 5-10 part, Sakura leaf, polymerization blade of grass, chinaberry leaf, polygoni cuspidati,radix, scutellariae,radix, Flos Nelumbinis, Radix Ophiopogonis grass, root of Paeonia suffruticosa Ardr., Herba Arctii leaf, elm endothelium, Magnolia bark, arnica montana, Folium Mori, each 3-5 part of Salix alba bark adds in rustless steel still, take avenge chrysanthemum tea 10-15 part and green tea 8-10 part for subsequent use;
B () once extracts: when first time boils, take deionized water 700-800 part, ethanol 3-4 part, propylene glycol 3-4 part, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.0-1.2 hour, namely obtain snow chrysanthemum tea Chinese medicine aqueous extract 1. with 600 order filter-cloth filterings afterwards;
(c) second extraction: the propylene glycol adding the deionized water of 500-600 part and the ethanol of 1-3 part and 1-3 part in filtering residue, use little fire after big fire is boiled instead and boil 0.8-1.0 hour, add snow chrysanthemum tea and green tea immersion 0.5-1.0 hour afterwards, use 600 order filter-cloth filterings afterwards, chrysanthemum tea Chinese medicine aqueous extract must be avenged 2.;
D () mixes: by snow chrysanthemum tea Chinese medicine aqueous extract 1., 2. snow chrysanthemum tea Chinese medicine aqueous extract must avenge chrysanthemum tea Chinese medicine aqueous extract after mix homogeneously, its total amount should control about the half of interpolation total Water;
After described step (4) moderate snow chrysanthemum tea herb fermenting, the preparation technology of concentrated solution is as follows:
A the snow chrysanthemum tea Chinese medicine aqueous extract of the snow chrysanthemum tea Chinese medicine slag after extracted twice and 1/3rd joins in enamel fermentation tank by (), add Lemon fruit 2-4 part, brown sugar 3-5 part, edible Aloe 2-3 part, water 500-600 part, after system is heated to boiling, low baking temperature constant temperature disinfection 20 minutes, is then cooled to 25-30 DEG C;
B () adds geotrichum candidum strain by the 2-4% of fermented product total amount (strain is purchased from Chinese industrial Culture Collection, bacterium numbering: CICC32873), fermentation 2-3 days, then system temperature is raised to 30-35 DEG C, add the cloth Laplace yeast seeds (strain reaches pharmaceutical factory purchased from French encyclopaedia) of 1-3% again, then carry out fermentation 2-3 days;
Thalline sum in (c) inspection system, if be greater than 500CFU ∕ ML, then continue fermentation 1-5 days, until viable bacteria body approach exhaustion in system, thalline sum is less than 500CFU ∕ ML, when there is no living contaminants, filter out fermentation liquid, below 50 DEG C, carry out vacuum concentration, treat filtrate total amount be original cumulative volume three/for the moment, the concentrated solution after chrysanthemum tea herb fermenting must be avenged.
Beneficial effect of the present invention: the present invention adopts first by the high mountain of pure natural snow chrysanthemum tea, free of contamination green tea and Radix Glycyrrhizae, the long-pending grass of snow, Herba Portulacae, Sakura leaf, polymerization blade of grass, chinaberry leaf, polygoni cuspidati,radix, scutellariae,radix, oat kernel, Flos Nelumbinis, Flos Lonicerae, root of Paeonia suffruticosa Ardr., Herba Arctii leaf, elm endothelium, Magnolia bark, arnica montana, Folium Mori, after Salix alba bark etc. boils, again with Lemon fruit and edible Aloe, the new technologies such as probiotics fermention process are carried out in the cooperation such as brown sugar, by above-mentioned snow chrysanthemum tea, green tea, effective ingredient in Radix Glycyrrhizae and Flos Nelumbinis etc. carries out activation processing, further fermentation culture, decompose, the activated active component being more beneficial to skin and absorbing, then can reach the not only safe and reliable but also effect of improving product effect.Snow chrysanthemum tea has another name called Herba Coreopsis tinctoria tea, is the rare teas of pure natural grown in the corner of the snow mountain of Xinjiang Tianshan height above sea level more than 2600 meters and eastern Pamir mountain range.After modern science is analyzed, find in snow chrysanthemum tea, containing more than 300 kind, human body is all had to the natural component of very good effect, especially the effect such as anti-inflammation and sterilization, heat-clearing and toxic substances removing, discharging garbage from body toxin especially general Flos Chrysanthemi teas cannot reach.But because the growth of snow chrysanthemum tea is in high and cold mountain region, long-term " shrinkage " effect, not easily lixiviate is out at short notice to make to avenge effective ingredient in chrysanthemum tea, and together with Chinese medicine and probiotic bacteria, after a couple of days fermentation process, effective ingredient in snow chrysanthemum tea, green tea and Chinese medicine can be discharged, macromole is converted into the micromolecule being beneficial to skin and absorbing, and this just will inevitably improve the product efficacy of final products of the present invention-snow chrysanthemum tea anti-allergy facial mask frost greatly.
Detailed description of the invention
Embodiment 1
(1) preparation process of the present embodiment special ratios Chinese medicine snow chrysanthemum tea extracting solution is as follows:
(a) weighing: take 5 parts, Radix Glycyrrhizae, oat kernel 6 parts, Herba Portulacae part 6 parts, the long-pending grass 6 parts of snow, Sakura leaf 3 parts, polymerization 5 parts, blade of grass, 5 parts, chinaberry leaf, polygoni cuspidati,radix 4 parts, scutellariae,radix 5 parts, 3 parts, Flos Nelumbinis, careless 5 parts of Radix Ophiopogonis, root of Paeonia suffruticosa Ardr. 3 parts, Herba Arctii leaf 4 parts, elm endothelium 5 parts, Magnolia bark 4 parts, arnica montana 3 parts, 5 parts, Folium Mori, 5 parts, Salix alba bark, adds in rustless steel still, takes snow chrysanthemum tea 10 parts for subsequent use with green tea 8 parts;
B () once extracts: when first time boils, take deionized water 800 parts, ethanol 3 parts, propylene glycol 3 parts, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.0 hours, namely obtain snow chrysanthemum tea Chinese medicine aqueous extract 1. with 600 order filter-cloth filterings afterwards;
(c) second extraction: the propylene glycol adding the deionized water of 500 parts and the ethanol of 1 part and 1 part in filtering residue, use little fire after big fire is boiled instead and boil 0.8 hour again, add afterwards snow chrysanthemum tea and green tea soak 0.8 hour, use 600 order filter-cloth filterings afterwards, chrysanthemum tea Chinese medicine aqueous extract must be avenged 2.;
(d) by snow chrysanthemum tea Chinese medicine aqueous extract 1., namely 2. snow chrysanthemum tea Chinese medicine aqueous extract obtain most last snow chrysanthemum tea Chinese medicine aqueous extract after mix homogeneously, its total amount should control about the half of adding total Water.
(2) preparation technology of the concentrated solution after the present embodiment special ratios snow chrysanthemum tea herb fermenting is as follows:
A the water extraction herb liquid of the snow chrysanthemum tea Chinese medicine slag after above-mentioned water extraction and 1/3rd joins in enamel fermentation tank by (), add Lemon fruit 2 parts, 5 parts, brown sugar, edible Aloe 2 parts, 500 parts, water, after being heated to boiling by system, low baking temperature constant temperature disinfection 20 minutes, is then cooled to 25 DEG C
B () adds geotrichum candidum strain by 4% of fermented product total amount (strain is purchased from Chinese industrial Culture Collection, bacterium numbering: CICC32873), ferment 3 days, then system temperature is raised to 30 DEG C, add the cloth Laplace yeast seeds (strain reaches pharmaceutical factory purchased from French encyclopaedia) of 3% again, carry out fermentation 3 days again
Thalline sum in (c) inspection system, if be greater than 500CFU ∕ ML, then continue fermentation 4 days, until viable bacteria body approach exhaustion in system, thalline sum is less than 500CFU ∕ ML, when there is no living contaminants, filter out fermentation liquid, below 50 DEG C, carry out vacuum concentration, treat filtrate total amount be original cumulative volume three/for the moment, obtain most last snow chrysanthemum tea herb fermenting concentrated solution.
(3) the present embodiment substitutes the pure water component in snow chrysanthemum tea anti-allergy facial mask frost with obtained snow chrysanthemum tea Chinese medicine aqueous extract, and the prescription of snow chrysanthemum tea anti-allergy facial mask frost is as follows:
(1) oil phase component: 16 mixed alcohols 1 part, 16 stearyl alcohol and 16 octadecyl glucosides 3 parts, glyceryl stearate and PEG-100 stearate 2 parts, 2 parts, different n-nonanoic acid fat in the different ninth of the ten Heavenly Stems, isomery hexadecane hydrocarbon 5 parts, cocoanut oil alcohol caprylate caprate 3 parts, dimethicone 3 parts, methyl hydroxybenzoate 0.2 part, propylparaben 0.1 part, ditertbutylparacresol 0.03 part;
(2) water phase components: glycerol 6 parts, amino acid humectant 3 parts, Sargassum rock polysaccharide wetting agent 2 parts, the different poly-polysaccharide 0.05 part of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract 59 parts;
(3) later stage adds component: the concentrated solution 10 parts after snow chrysanthemum tea herb fermenting;
(4) co-emulsifier: hydroxyethylacrylate/sodium acryloyldimethyl taurate copolymers 0.5 part;
(5) antiseptic: 0.1 part, the mixture of MIT and 3-iodo-2-propynyl butyl carbamate;
(6) essence: Green tea essence 0.02 part.
(4) preparation method of the present embodiment snow chrysanthemum tea anti-allergy facial mask frost, comprises the steps:
(1) preparation of oil phase component: 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucoside copolymers, glyceryl stearate and PEG-100 stearate copolymer, different n-nonanoic acid fat in the different ninth of the ten Heavenly Stems, isomery hexadecane hydrocarbon, cocoanut oil alcohol caprylate caprate, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol are added in the rustless steel still of band stirring after taking in proportion, under the stirring of rotating speed 20 revs/min, heating for dissolving is complete, and constant temperature disinfection 20 minutes is stand-by at 80 DEG C;
(2) preparation of water phase components: the glycerol of formula ratio, amino acid humectant, Sargassum rock polysaccharide wetting agent, the different poly-polysaccharide of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract are taken rear elder generation heating for dissolving in rustless steel still in proportion, be extracted in rustless steel homogenizing still afterwards, under the stirring of 20 revs/min, when continuing to be heated to 80 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3) by oil phase slowly suction aqueous phase, and scrape wall stirring, rotating speed is increased to 40 revs/min, stir after 2 minutes, start high speed homogenization device homogenizing 3 minutes under the high speed of 3000 revs/min, wall rotating speed will be scraped afterwards and drop to 30 revs/min, and be cooled to 45 DEG C under this rotating speed;
(4) concentrated solution after the snow chrysanthemum tea herb fermenting of formula ratio and co-emulsifier is added, stir 20 minutes under the rotating speed of 20 revs/min, continue afterwards to cool to 40 DEG C, add the antiseptic of formula ratio, essence, continuation and stir 15 minutes under same rotating speed, get final product discharging.
Embodiment 2
(1) preparation process of the present embodiment special ratios Chinese medicine snow chrysanthemum tea extracting solution is as follows:
(a) weighing: take 6 parts, Radix Glycyrrhizae, oat kernel 5 parts, Herba Portulacae 5 parts, the long-pending grass 5 parts of snow, Sakura leaf 5 parts, polymerization 3 parts, blade of grass, 3 parts, chinaberry leaf, polygoni cuspidati,radix 3 parts, scutellariae,radix 4 parts, 5 parts, Flos Nelumbinis, careless 4 parts of Radix Ophiopogonis, root of Paeonia suffruticosa Ardr. 5 parts, Herba Arctii leaf 3 parts, elm endothelium 4 parts, Magnolia bark 5 parts, arnica montana 5 parts, 3 parts, Folium Mori, 4 parts, Salix alba bark, adds in rustless steel still, takes snow chrysanthemum tea 15 parts for subsequent use with green tea 9 parts;
B () once extracts: when first time boils, take deionized water 800 parts, ethanol 3 parts, propylene glycol 3 parts, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.0 hours, namely obtain snow chrysanthemum tea Chinese medicine aqueous extract 1. with 600 order filter-cloth filterings afterwards;
(c) second extraction: the propylene glycol adding the deionized water of 500 parts and the ethanol of 1 part and 1 part in filtering residue, use little fire after big fire is boiled instead and boil 0.8 hour again, add afterwards snow chrysanthemum tea and green tea soak 0.5 hour, use 600 order filter-cloth filterings afterwards, chrysanthemum tea Chinese medicine aqueous extract must be avenged 2.;
(d) by snow chrysanthemum tea Chinese medicine aqueous extract 1., namely 2. snow chrysanthemum tea Chinese medicine aqueous extract obtain most last snow chrysanthemum tea Chinese medicine aqueous extract after mix homogeneously, its total amount should control about the half of adding total Water.
(2) preparation technology of the concentrated solution after the snow chrysanthemum tea herb fermenting of the present embodiment special ratios is as follows:
A the water extraction herb liquid of the snow chrysanthemum tea Chinese medicine slag after above-mentioned water extraction and 1/3rd joins in enamel fermentation tank by (), add Lemon fruit 4 parts, 3 parts, brown sugar, edible Aloe 3 parts, 600 parts, water, after being heated to boiling by system, low baking temperature constant temperature disinfection 20 minutes, is then cooled to 30 DEG C;
B () adds geotrichum candidum strain by 4% of fermented product total amount (strain is purchased from Chinese industrial Culture Collection, bacterium numbering: CICC32873), ferment 3 days, then system temperature is raised to 35 DEG C, add the cloth Laplace yeast seeds (strain reaches pharmaceutical factory purchased from French encyclopaedia) of 2% again, then carry out fermentation 3 days;
Thalline sum in (c) inspection system, if be greater than 500CFU ∕ ML, then continue fermentation 5 days, until viable bacteria body approach exhaustion in system, thalline sum is less than 500CFU ∕ ML, when there is no living contaminants, filter out fermentation liquid, below 50 DEG C, carry out vacuum concentration, treat filtrate total amount be original cumulative volume three/for the moment, obtain most last snow chrysanthemum tea herb fermenting concentrated solution.
(3) the present embodiment substitutes the pure water component in snow chrysanthemum tea anti-allergy facial mask frost with obtained snow chrysanthemum tea Chinese medicine aqueous extract, and the prescription of snow chrysanthemum tea anti-allergy facial mask frost is as follows:
(1) oil phase component: 16 mixed alcohols 2 parts, 16 stearyl alcohol and 16 octadecyl glucosides 4 parts, glyceryl stearate and PEG-100 stearate 2 parts, 3 parts, different n-nonanoic acid fat in the different ninth of the ten Heavenly Stems, isomery hexadecane hydrocarbon 6 parts, cocoanut oil alcohol caprylate caprate 4 parts, dimethicone 4 parts, methyl hydroxybenzoate 0.2 part, propylparaben 0.1 part, ditertbutylparacresol 0.05 part;
(2) water phase components: glycerol 7 parts, amino acid humectant 2 parts, Sargassum rock polysaccharide wetting agent 4 parts, the different poly-polysaccharide 0.01 part of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract 47.9 parts;
(3) later stage adds component: the concentrated solution 13 parts after snow chrysanthemum tea herb fermenting;
(4) co-emulsifier: hydroxyethylacrylate/sodium acryloyldimethyl taurate copolymers 0.6 part;
(5) antiseptic: 0.1 part, the mixture of MIT and 3-iodo-2-propynyl butyl carbamate;
(6) essence: Green tea essence 0.01 part.
(4) preparation method of the present embodiment snow chrysanthemum tea anti-allergy facial mask frost, comprises the steps:
(1) preparation of oil phase component: 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucoside copolymers, glyceryl stearate and PEG-100 stearate copolymer, different n-nonanoic acid fat in the different ninth of the ten Heavenly Stems, isomery hexadecane hydrocarbon, cocoanut oil alcohol caprylate caprate, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol are added in the rustless steel still of band stirring after taking in proportion, under the stirring of rotating speed 30 revs/min, heating for dissolving is complete, and constant temperature disinfection 20 minutes is stand-by at 80 DEG C;
(2) preparation of water phase components: the glycerol of formula ratio, amino acid humectant, Sargassum rock polysaccharide wetting agent, the different poly-polysaccharide of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract are taken rear elder generation heating for dissolving in rustless steel still in proportion, be extracted in rustless steel homogenizing still afterwards, under the stirring of 30 revs/min, when continuing to be heated to 85 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3) by oil phase slowly suction aqueous phase, and scrape wall stirring, rotating speed is increased to 45 revs/min, stir after 3 minutes, start high speed homogenization device homogenizing 4 minutes under the high speed of 5000 revs/min, wall rotating speed will be scraped afterwards and drop to 40 revs/min, and be cooled to 50 DEG C under this rotating speed;
(4) concentrated solution after the snow chrysanthemum tea herb fermenting of formula ratio and co-emulsifier is added, stir 25 minutes under the rotating speed of 30 revs/min, continue afterwards to cool to 40 DEG C, add the antiseptic of formula ratio, essence, continuation and stir 18 minutes under same rotating speed, get final product discharging.
Embodiment 3
(1) preparation process of the present embodiment special ratios Chinese medicine snow chrysanthemum tea extracting solution is as follows:
(a) weighing: take 7 parts, Radix Glycyrrhizae, oat kernel 7 parts, Herba Portulacae 5 parts, the long-pending grass 6 parts of snow, Sakura leaf 4 parts, polymerization 3 parts, blade of grass, 4 parts, chinaberry leaf, polygoni cuspidati,radix 5 parts, scutellariae,radix 3 parts, 4 parts, Flos Nelumbinis, careless 3 parts of Radix Ophiopogonis, root of Paeonia suffruticosa Ardr. 4 parts, Herba Arctii leaf 5 parts, elm endothelium 3 parts, Magnolia bark 3 parts, arnica montana 4 parts, 4 parts, Folium Mori, 3 parts, Salix alba bark, adds in rustless steel still, takes snow chrysanthemum tea 13 parts for subsequent use with green tea 10 parts;
B () once extracts: when first time boils, take deionized water 800 parts, ethanol 3 parts, propylene glycol 3 parts, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.0 hours, namely obtain snow chrysanthemum tea Chinese medicine aqueous extract 1. with 600 order filter-cloth filterings afterwards;
(c) second extraction: the propylene glycol adding the deionized water of 500 parts and the ethanol of 1 part and 1 part in filtering residue, use little fire after big fire is boiled instead and boil 0.8 hour again, add afterwards snow chrysanthemum tea and green tea soak 0.5 hour, use 600 order filter-cloth filterings afterwards, chrysanthemum tea Chinese medicine aqueous extract must be avenged 2.;
D () mixes: by snow chrysanthemum tea Chinese medicine aqueous extract 1., namely 2. snow chrysanthemum tea Chinese medicine aqueous extract obtain most last snow chrysanthemum tea Chinese medicine aqueous extract after mix homogeneously, its total amount should control about the half of interpolation total Water.
(2) preparation technology of the concentrated solution after the present embodiment special ratios snow chrysanthemum tea herb fermenting is as follows:
A the water extraction herb liquid of the snow chrysanthemum tea Chinese medicine slag after above-mentioned water extraction and 1/3rd joins in enamel fermentation tank by (), add Lemon fruit 3 parts, 4 parts, brown sugar, edible Aloe 3 parts, 600 parts, water, after being heated to boiling by system, low baking temperature constant temperature disinfection 20 minutes, is then cooled to 25 DEG C;
B () adds geotrichum candidum strain by 2% of fermented product total amount (strain is purchased from Chinese industrial Culture Collection, bacterium numbering: CICC32873), ferment 2 days, then system temperature is raised to 30 DEG C, add the cloth Laplace yeast seeds (strain reaches pharmaceutical factory purchased from French encyclopaedia) of 2% again, then carry out fermentation 2 days;
Thalline sum in (c) inspection system, if be greater than 500CFU ∕ ML, then continue fermentation 4 days, until viable bacteria body approach exhaustion in system, thalline sum is less than 500CFU ∕ ML, when there is no living contaminants, filter out fermentation liquid, below 50 DEG C, carry out vacuum concentration, treat filtrate total amount be original cumulative volume three/for the moment, obtain most last snow chrysanthemum tea herb fermenting concentrated solution.
(3) the present embodiment substitutes the pure water component in snow chrysanthemum tea anti-allergy facial mask frost with obtained snow chrysanthemum tea Chinese medicine aqueous extract, and the prescription of snow chrysanthemum tea anti-allergy facial mask frost is as follows:
(1) oil phase component: 16 mixed alcohols 1 part, 16 stearyl alcohol and 16 octadecyl glucoside copolymers 2 parts, glyceryl stearate and PEG-100 stearate copolymer 3 parts, 4 parts, different n-nonanoic acid fat in the different ninth of the ten Heavenly Stems, isomery hexadecane hydrocarbon 4 parts, cocoanut oil alcohol caprylate caprate 2 parts, dimethicone 2 parts, methyl hydroxybenzoate 0.2 part, propylparaben 0.1 part, ditertbutylparacresol 0.04 part;
(2) water phase components: glycerol 8 parts, amino acid humectant 4 parts, Sargassum rock polysaccharide wetting agent 3 parts, the different poly-polysaccharide 0.05 part of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract 50.7 parts;
(3) later stage adds component: the concentrated solution 15 parts after snow chrysanthemum tea herb fermenting;
(4) co-emulsifier: hydroxyethylacrylate/sodium acryloyldimethyl taurate copolymers 0.8 part;
(5) antiseptic: 0.1 part, the mixture of MIT and 3-iodo-2-propynyl butyl carbamate;
(6) essence: Green tea essence 0.01 part.
(4) preparation method of the present embodiment snow chrysanthemum tea anti-allergy facial mask frost, comprises the steps:
(1) preparation of oil phase component: 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucosides, glyceryl stearate and PEG-100 stearate, different n-nonanoic acid fat in the different ninth of the ten Heavenly Stems, isomery hexadecane hydrocarbon, cocoanut oil alcohol caprylate caprate, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol are added in the rustless steel still of band stirring after taking in proportion, under the stirring of rotating speed 20 revs/min, heating for dissolving is complete, and constant temperature disinfection 20 minutes is stand-by at 85 DEG C;
(2) preparation of water phase components: the glycerol of formula ratio, amino acid humectant, Sargassum rock polysaccharide wetting agent, the different poly-polysaccharide of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract are taken rear elder generation heating for dissolving in rustless steel still in proportion, be extracted in rustless steel homogenizing still afterwards, under the stirring of 20 revs/min, when continuing to be heated to 80 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3) by oil phase slowly suction aqueous phase, and scrape wall stirring, rotating speed is increased to 50 revs/min, stir after 2 minutes, start high speed homogenization device homogenizing 5 minutes under the high speed of 4000 revs/min, wall rotating speed will be scraped afterwards and drop to 35 revs/min, and be cooled to 45 DEG C under this rotating speed;
(4) the concentrated solution co-emulsifier after the snow chrysanthemum tea herb fermenting of formula ratio is added, stir 30 minutes under the rotating speed of 25 revs/min, continue afterwards to cool to 40 DEG C, add the antiseptic of formula ratio, essence, continuation and stir 20 minutes under same rotating speed, get final product discharging.
Embodiment 4
(1) preparation process of the present embodiment special ratios Chinese medicine snow chrysanthemum tea extracting solution is as follows:
(a) weighing: take Radix Glycyrrhizae, oat kernel, Herba Portulacae, long-pending each 5 parts of the grass of snow, Sakura leaf, polymerization blade of grass, chinaberry leaf, polygoni cuspidati,radix, scutellariae,radix, Flos Nelumbinis, Radix Ophiopogonis grass, root of Paeonia suffruticosa Ardr., Herba Arctii leaf, elm endothelium, Magnolia bark, arnica montana, Folium Mori, each 3 parts of Salix alba bark add in rustless steel still, takes snow chrysanthemum tea 10 parts for subsequent use with green tea 8;
B () once extracts: when first time boils, take deionized water 700 parts, ethanol 3 parts, propylene glycol 3 parts, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.0 hours, namely obtain snow chrysanthemum tea Chinese medicine aqueous extract 1. with 600 order filter-cloth filterings afterwards;
(c) second extraction: the propylene glycol adding the deionized water of 500 parts and the ethanol of 1 part and 1 part in filtering residue, use little fire after big fire is boiled instead and boil 0.8 hour, add afterwards snow chrysanthemum tea and green tea soak 0.5 hour, use 600 order filter-cloth filterings afterwards, chrysanthemum tea Chinese medicine aqueous extract must be avenged 2.;
D () mixes: by snow chrysanthemum tea Chinese medicine aqueous extract 1., 2. snow chrysanthemum tea Chinese medicine aqueous extract must avenge chrysanthemum tea Chinese medicine aqueous extract after mix homogeneously, its total amount should control about the half of interpolation total Water;
(2) preparation technology of the concentrated solution after the present embodiment special ratios snow chrysanthemum tea herb fermenting is as follows:
A the snow chrysanthemum tea Chinese medicine aqueous extract of the snow chrysanthemum tea Chinese medicine slag after extracted twice and 1/3rd joins in enamel fermentation tank by (), add Lemon fruit 2 parts, 3 parts, brown sugar, edible Aloe 2 parts, 500 parts, water, after system is heated to boiling, low baking temperature constant temperature disinfection 20 minutes, is then cooled to 25 DEG C;
B () adds geotrichum candidum strain by 2% of fermented product total amount (strain is purchased from Chinese industrial Culture Collection, bacterium numbering: CICC32873), ferment 2 days, then system temperature is raised to 30 DEG C, add the cloth Laplace yeast seeds (strain reaches pharmaceutical factory purchased from French encyclopaedia) of 1% again, then carry out fermentation 2 days;
Thalline sum in (c) inspection system, if be greater than 500CFU ∕ ML, then continue fermentation 1-5 days, until viable bacteria body approach exhaustion in system, thalline sum is less than 500CFU ∕ ML, when there is no living contaminants, filter out fermentation liquid, below 50 DEG C, carry out vacuum concentration, treat filtrate total amount be original cumulative volume three/for the moment, the concentrated solution after chrysanthemum tea herb fermenting must be avenged.
(3) the present embodiment substitutes the pure water component in snow chrysanthemum tea anti-allergy facial mask frost with obtained snow chrysanthemum tea Chinese medicine aqueous extract, and the prescription of snow chrysanthemum tea anti-allergy facial mask frost is as follows:
(1) oil phase component: 16 mixed alcohol 1-2 parts, 16 stearyl alcohol and 16 octadecyl glucoside copolymers 2 parts, tristerin and PEG-100 stearate copolymer 2 parts, isomery hexadecane hydrocarbon 4 parts, isononyl isononanoate 2 parts, cocoanut oil alcohol caprylate caprate 2 parts, dimethicone 2 parts, methyl hydroxybenzoate 0.2 part, propylparaben 0.1 part, ditertbutylparacresol 0.03 part;
(2) water phase components: glycerol 6 parts, amino acid humectant 2 parts, trehalose rock polysaccharide 2 parts, the different poly-polysaccharide 0.01 part of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract 40.8 parts, described snow chrysanthemum tea Chinese medicine aqueous extract has the raw material of following masses part to make: snow chrysanthemum tea 10 parts, green tea 8 parts, Radix Glycyrrhizae, oat kernel, Herba Portulacae, long-pending each 5 parts of the grass of snow, Sakura leaf, polymerization blade of grass, chinaberry leaf, polygoni cuspidati,radix, scutellariae,radix, Flos Nelumbinis, Radix Ophiopogonis grass, root of Paeonia suffruticosa Ardr., Herba Arctii leaf, elm endothelium, Magnolia bark, arnica montana, Folium Mori, each 3 parts of Salix alba bark;
(3) component is added after: the concentrated solution 10 parts after snow chrysanthemum tea herb fermenting;
(4) co-emulsifier component: hydroxy acrylic acid brine and sodium acryloyldimethyl taurate copolymers 0.7 part;
(5) antiseptic: 0.1 part, the mixture of MIT and 3-iodo-2-propynyl butyl carbamate;
(6) essence: Green tea essence 0.01 part.
(4) preparation method of the present embodiment snow chrysanthemum tea anti-allergy facial mask frost, comprises the steps:
(1) preparation of oil phase component: 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucoside copolymers, glyceryl stearate and PEG-100 stearate copolymer, different n-nonanoic acid fat in the different ninth of the ten Heavenly Stems, isomery hexadecane hydrocarbon, cocoanut oil alcohol caprylate caprate, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol are added in the rustless steel still of band stirring after taking in proportion, under the stirring of rotating speed 20 revs/min, heating for dissolving is complete, and constant temperature disinfection 20 minutes is stand-by at 80 DEG C;
(2) preparation of water phase components: the glycerol of formula ratio, amino acid humectant, Sargassum rock polysaccharide wetting agent, the different poly-polysaccharide of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract are taken rear elder generation heating for dissolving in rustless steel still in proportion, be extracted in rustless steel homogenizing still afterwards, under the stirring of 20 revs/min, when continuing to be heated to 80 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3) by oil phase slowly suction aqueous phase, and scrape wall stirring, rotating speed is increased to 40 revs/min, stir after 3 minutes, start high speed homogenization device homogenizing 5 minutes under the high speed of 3000 revs/min, wall rotating speed will be scraped afterwards and drop to 30 revs/min, and be cooled to 45 DEG C under this rotating speed;
(4) concentrated solution after the snow chrysanthemum tea herb fermenting of formula ratio and co-emulsifier is added, stir 30 minutes under the rotating speed of 20 revs/min, continue afterwards to cool to 40 DEG C, add the antiseptic of formula ratio, essence, continuation and stir 15 minutes under same rotating speed, get final product discharging.
Embodiment 5
(1) preparation process of the present embodiment special ratios Chinese medicine snow chrysanthemum tea extracting solution is as follows:
(a) weighing: take Radix Glycyrrhizae, oat kernel, Herba Portulacae, long-pending each 10 parts of the grass of snow, Sakura leaf, polymerization blade of grass, chinaberry leaf, polygoni cuspidati,radix, scutellariae,radix, Flos Nelumbinis, Radix Ophiopogonis grass, root of Paeonia suffruticosa Ardr., Herba Arctii leaf, elm endothelium, Magnolia bark, arnica montana, Folium Mori, each 5 parts of Salix alba bark add in rustless steel still, takes snow chrysanthemum tea 15 parts for subsequent use with green tea 10;
B () once extracts: when first time boils, take deionized water 800 parts, ethanol 4 parts, propylene glycol 4 parts, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.2 hours, namely obtain snow chrysanthemum tea Chinese medicine aqueous extract 1. with 600 order filter-cloth filterings afterwards;
(c) second extraction: the propylene glycol adding the deionized water of 600 parts and the ethanol of 3 parts and 3 parts in filtering residue, use little fire after big fire is boiled instead and boil 1.0 hours, add afterwards snow chrysanthemum tea and green tea soak 1.0 hours, use 600 order filter-cloth filterings afterwards, chrysanthemum tea Chinese medicine aqueous extract must be avenged 2.;
D () mixes: by snow chrysanthemum tea Chinese medicine aqueous extract 1., 2. snow chrysanthemum tea Chinese medicine aqueous extract must avenge chrysanthemum tea Chinese medicine aqueous extract after mix homogeneously, its total amount should control about the half of interpolation total Water;
(2) preparation technology of the concentrated solution after the present embodiment special ratios snow chrysanthemum tea herb fermenting is as follows:
A the snow chrysanthemum tea Chinese medicine aqueous extract of the snow chrysanthemum tea Chinese medicine slag after extracted twice and 1/3rd joins in enamel fermentation tank by (), add Lemon fruit 4 parts, 5 parts, brown sugar, edible Aloe 3 parts, 600 parts, water, after system is heated to boiling, low baking temperature constant temperature disinfection 20 minutes, is then cooled to 30 DEG C;
B () adds geotrichum candidum strain by 4% of fermented product total amount (strain is purchased from Chinese industrial Culture Collection, bacterium numbering: CICC32873), ferment 3 days, then system temperature is raised to 35 DEG C, add the cloth Laplace yeast seeds (strain reaches pharmaceutical factory purchased from French encyclopaedia) of 3% again, then carry out fermentation 3 days;
Thalline sum in (c) inspection system, if be greater than 500CFU ∕ ML, then continue fermentation 1-5 days, until viable bacteria body approach exhaustion in system, thalline sum is less than 500CFU ∕ ML, when there is no living contaminants, filter out fermentation liquid, below 50 DEG C, carry out vacuum concentration, treat filtrate total amount be original cumulative volume three/for the moment, the concentrated solution after chrysanthemum tea herb fermenting must be avenged.
(3) the present embodiment substitutes the pure water component in snow chrysanthemum tea anti-allergy facial mask frost with obtained snow chrysanthemum tea Chinese medicine aqueous extract, and the prescription of snow chrysanthemum tea anti-allergy facial mask frost is as follows:
(1) oil phase component: 16 mixed alcohols 2 parts, 16 stearyl alcohol and 16 octadecyl glucoside copolymers 2 parts, tristerin and PEG-100 stearate copolymer 3 parts, isomery hexadecane hydrocarbon 6 parts, isononyl isononanoate 4 parts, cocoanut oil alcohol caprylate caprate 4 parts, dimethicone 4 parts, methyl hydroxybenzoate 0.3 part, propylparaben 0.15 part, ditertbutylparacresol 0.05 part;
(2) water phase components: glycerol 8 parts, amino acid humectant 4 parts, trehalose rock polysaccharide 4 parts, the different poly-polysaccharide 0.05 part of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract 60 parts; Described snow chrysanthemum tea Chinese medicine aqueous extract has the raw material of following masses part to make: snow chrysanthemum tea 15 parts, green tea 10 parts, Radix Glycyrrhizae, oat kernel, Herba Portulacae, long-pending each 10 parts of the grass of snow, Sakura leaf, polymerization blade of grass, chinaberry leaf, polygoni cuspidati,radix, scutellariae,radix, Flos Nelumbinis, Radix Ophiopogonis grass, root of Paeonia suffruticosa Ardr., Herba Arctii leaf, elm endothelium, Magnolia bark, arnica montana, Folium Mori, each 5 parts of Salix alba bark;
(3) component is added after: the concentrated solution 15 parts after snow chrysanthemum tea herb fermenting;
(4) co-emulsifier component: hydroxy acrylic acid brine and sodium acryloyldimethyl taurate copolymers 1 part;
(5) antiseptic: 0.15 part, the mixture of MIT and 3-iodo-2-propynyl butyl carbamate;
(6) essence: Green tea essence 0.02 part.
(4) preparation method of the present embodiment snow chrysanthemum tea anti-allergy facial mask frost, comprises the steps:
(1) preparation of oil phase component: 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucoside copolymers, glyceryl stearate and PEG-100 stearate copolymer, different n-nonanoic acid fat in the different ninth of the ten Heavenly Stems, isomery hexadecane hydrocarbon, cocoanut oil alcohol caprylate caprate, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol are added in the rustless steel still of band stirring after taking in proportion, under the stirring of rotating speed 30 revs/min, heating for dissolving is complete, and constant temperature disinfection 20 minutes is stand-by at 85 DEG C;
(2) preparation of water phase components: the glycerol of formula ratio, amino acid humectant, Sargassum rock polysaccharide wetting agent, the different poly-polysaccharide of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract are taken rear elder generation heating for dissolving in rustless steel still in proportion, be extracted in rustless steel homogenizing still afterwards, under the stirring of 30 revs/min, when continuing to be heated to 85 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3) by oil phase slowly suction aqueous phase, and scrape wall stirring, rotating speed is increased to 50 revs/min, stir after 3 minutes, start high speed homogenization device homogenizing 3 minutes under the high speed of 5000 revs/min, wall rotating speed will be scraped afterwards and drop to 40 revs/min, and be cooled to 50 DEG C under this rotating speed;
(4) concentrated solution after the snow chrysanthemum tea herb fermenting of formula ratio and co-emulsifier is added, stir 20 minutes under the rotating speed of 30 revs/min, continue afterwards to cool to 40 DEG C, add the antiseptic of formula ratio, essence, continuation and stir 20 minutes under same rotating speed, get final product discharging.
Embodiment 6
(1) preparation process of the present embodiment special ratios Chinese medicine snow chrysanthemum tea extracting solution is as follows:
(a) weighing: take Radix Glycyrrhizae, oat kernel, Herba Portulacae, long-pending each 8 parts of the grass of snow, Sakura leaf, polymerization blade of grass, chinaberry leaf, polygoni cuspidati,radix, scutellariae,radix, Flos Nelumbinis, Radix Ophiopogonis grass, root of Paeonia suffruticosa Ardr., Herba Arctii leaf, elm endothelium, Magnolia bark, arnica montana, Folium Mori, each 4 parts of Salix alba bark add in rustless steel still, takes snow chrysanthemum tea 12 parts for subsequent use with green tea 9 parts;
B () once extracts: when first time boils, take deionized water 750 parts, ethanol 3.5 parts, propylene glycol 3.5 parts, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.1 hours, namely obtain snow chrysanthemum tea Chinese medicine aqueous extract 1. with 600 order filter-cloth filterings afterwards;
(c) second extraction: the propylene glycol adding the deionized water of 550 parts and the ethanol of 2 parts and 2 parts in filtering residue, use little fire after big fire is boiled instead and boil 0.9 hour, add afterwards snow chrysanthemum tea and green tea soak 0.8 hour, use 600 order filter-cloth filterings afterwards, chrysanthemum tea Chinese medicine aqueous extract must be avenged 2.;
D () mixes: by snow chrysanthemum tea Chinese medicine aqueous extract 1., 2. snow chrysanthemum tea Chinese medicine aqueous extract must avenge chrysanthemum tea Chinese medicine aqueous extract after mix homogeneously, its total amount should control about the half of interpolation total Water;
(2) preparation technology of the concentrated solution after the present embodiment special ratios snow chrysanthemum tea herb fermenting is as follows:
A the snow chrysanthemum tea Chinese medicine aqueous extract of the snow chrysanthemum tea Chinese medicine slag after extracted twice and 1/3rd joins in enamel fermentation tank by (), add Lemon fruit 3 parts, 4 parts, brown sugar, edible Aloe 2.5 parts, 550 parts, water, after system is heated to boiling, low baking temperature constant temperature disinfection 20 minutes, is then cooled to 28 DEG C;
B () adds geotrichum candidum strain by the 2-4% of fermented product total amount (strain is purchased from Chinese industrial Culture Collection, bacterium numbering: CICC32873), ferment 3 days, then system temperature is raised to 33 DEG C, add the cloth Laplace yeast seeds (strain reaches pharmaceutical factory purchased from French encyclopaedia) of 2% again, then carry out fermentation 2 days;
Thalline sum in (c) inspection system, if be greater than 500CFU ∕ ML, then continue fermentation 1-5 days, until viable bacteria body approach exhaustion in system, thalline sum is less than 500CFU ∕ ML, when there is no living contaminants, filter out fermentation liquid, below 50 DEG C, carry out vacuum concentration, treat filtrate total amount be original cumulative volume three/for the moment, the concentrated solution after chrysanthemum tea herb fermenting must be avenged.
(3) the present embodiment substitutes the pure water component in snow chrysanthemum tea anti-allergy facial mask frost with obtained snow chrysanthemum tea Chinese medicine aqueous extract, and the prescription of snow chrysanthemum tea anti-allergy facial mask frost is as follows:
(1) oil phase component: 16 mixed alcohol 1-2 parts, 16 stearyl alcohol and 16 octadecyl glucoside copolymers 3 parts, tristerin and PEG-100 stearate copolymer 2.5 parts, isomery hexadecane hydrocarbon 5 parts, isononyl isononanoate 3 parts, cocoanut oil alcohol caprylate caprate 3 parts, dimethicone 3 parts, methyl hydroxybenzoate 0.25 part, propylparaben 0.12 part, ditertbutylparacresol 0.04 part;
(2) water phase components: glycerol 7 parts, amino acid humectant 3 parts, trehalose rock polysaccharide 3 parts, the different poly-polysaccharide 0.03 part of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract 54.9 parts; Described snow chrysanthemum tea Chinese medicine aqueous extract has the raw material of following masses part to make: snow chrysanthemum tea 12 parts, green tea 9 parts, Radix Glycyrrhizae, oat kernel, Herba Portulacae, long-pending each 8 parts of the grass of snow, Sakura leaf, polymerization blade of grass, chinaberry leaf, polygoni cuspidati,radix, scutellariae,radix, Flos Nelumbinis, Radix Ophiopogonis grass, root of Paeonia suffruticosa Ardr., Herba Arctii leaf, elm endothelium, Magnolia bark, arnica montana, Folium Mori, each 4 parts of Salix alba bark;
(3) component is added after: the concentrated solution 12 parts after snow chrysanthemum tea herb fermenting;
(4) co-emulsifier component: hydroxy acrylic acid brine and sodium acryloyldimethyl taurate copolymers 0.9 part;
(5) antiseptic: 0.12 part, the mixture of MIT and 3-iodo-2-propynyl butyl carbamate;
(6) essence: Green tea essence 0.015 part.
(4) preparation method of the present embodiment snow chrysanthemum tea anti-allergy facial mask frost, comprises the steps:
(1) preparation of oil phase component: 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucoside copolymers, glyceryl stearate and PEG-100 stearate copolymer, different n-nonanoic acid fat in the different ninth of the ten Heavenly Stems, isomery hexadecane hydrocarbon, cocoanut oil alcohol caprylate caprate, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol are added in the rustless steel still of band stirring after taking in proportion, under the stirring of rotating speed 20-30 rev/min, heating for dissolving is complete, and constant temperature disinfection 20 minutes is stand-by at 82 DEG C;
(2) preparation of water phase components: the glycerol of formula ratio, amino acid humectant, Sargassum rock polysaccharide wetting agent, the different poly-polysaccharide of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract are taken rear elder generation heating for dissolving in rustless steel still in proportion, be extracted in rustless steel homogenizing still afterwards, under the stirring of 25 revs/min, when continuing to be heated to 83 DEG C, and constant temperature disinfection 20 minutes is stand-by;
(3) by oil phase slowly suction aqueous phase, and scrape wall stirring, rotating speed is increased to 45 revs/min, stir after 3 minutes, start high speed homogenization device homogenizing 4 minutes under the high speed of 4000 revs/min, wall rotating speed will be scraped afterwards and drop to 35 revs/min, and be cooled to 48 DEG C under this rotating speed;
(4) concentrated solution after the snow chrysanthemum tea herb fermenting of formula ratio and co-emulsifier is added, stir 25 minutes under the rotating speed of 25 revs/min, continue afterwards to cool to 40 DEG C, add the antiseptic of formula ratio, essence, continuation and stir 18 minutes under same rotating speed, get final product discharging.
Part in above-described embodiment is kilogram.
Claims (2)
1. a snow chrysanthemum tea anti-allergy facial mask frost, is characterized in that being prepared from by the component of following weight parts:
(1) oil phase component: 16 mixed alcohol 1-2 parts, 16 stearyl alcohol and 16 octadecyl glucoside copolymer 2-4 parts, tristerin and PEG-100 stearate copolymer 2-3 part, isomery hexadecane hydrocarbon 4-6 part, isononyl isononanoate 2-4 part, cocoanut oil alcohol caprylate caprate 2-4 part, dimethicone 2-4 part, methyl hydroxybenzoate 0.2-0.3 part, propylparaben 0.1-0.15 part, ditertbutylparacresol 0.03-0.05 part;
(2) water phase components: glycerol 6-8 part, amino acid humectant 2-4 part, Sargassum rock polysaccharide 2-4 part, the different poly-polysaccharide 0.01-0.05 part of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract 50-60 part; Described snow chrysanthemum tea Chinese medicine aqueous extract is made up of the raw material of following weight portion: snow chrysanthemum tea 10-15 part, green tea 8-10 part, Radix Glycyrrhizae, oat kernel, Herba Portulacae, snow amass careless each 5-10 part, Sakura leaf, polymerization blade of grass, chinaberry leaf, polygoni cuspidati,radix, scutellariae,radix, Flos Nelumbinis, Radix Ophiopogonis grass, root of Paeonia suffruticosa Ardr., Herba Arctii leaf, elm endothelium, Magnolia bark, arnica montana, Folium Mori, each 3-5 part of Salix alba bark;
(3) component is added after: the concentrated solution 10-15 part after snow chrysanthemum tea herb fermenting;
(4) co-emulsifier component: hydroxy acrylic acid brine and sodium acryloyldimethyl taurate copolymers 0.5-1 part;
(5) antiseptic: mixture 0.1-0.15 part of MIT and 3-iodo-2-propynyl butyl carbamate;
(6) essence: Green tea essence 0.01-0.02 part.
2. a preparation method for snow chrysanthemum tea anti-allergy facial mask frost according to claim 1, is characterized in that comprising the steps:
(1) preparation of oil phase component: 16 mixed alcohols of formula ratio, 16 stearyl alcohol and 16 octadecyl glucoside copolymers, glyceryl stearate and PEG-100 stearate copolymer, different n-nonanoic acid fat in the different ninth of the ten Heavenly Stems, isomery hexadecane hydrocarbon, cocoanut oil alcohol caprylate caprate, dimethicone, methyl hydroxybenzoate, propylparaben, ditertbutylparacresol are added in the rustless steel still of band stirring after taking in proportion, under the stirring of rotating speed 20-30 rev/min, heating for dissolving is complete, and constant temperature disinfection 20 minutes is stand-by at 80-85 DEG C;
(2) preparation of water phase components: the glycerol of formula ratio, amino acid humectant, Sargassum rock polysaccharide wetting agent, the different poly-polysaccharide of Tremella, snow chrysanthemum tea Chinese medicine aqueous extract are taken rear elder generation heating for dissolving in rustless steel still in proportion, be extracted in rustless steel homogenizing still afterwards, under the stirring of 20-30 rev/min, 80-85 DEG C when continuing to be heated to, and constant temperature disinfection 20 minutes is stand-by;
(3) by oil phase slowly suction aqueous phase, and scrape wall stirring, rotating speed is increased to 40-50 rev/min, stir after 2-3 minute, start high speed homogenization device homogenizing 3-5 minute under the high speed of 3000-5000 rev/min, wall rotating speed will be scraped afterwards and drop to 30-40 rev/min, and be cooled to 45-50 DEG C under this rotating speed;
(4) concentrated solution after the snow chrysanthemum tea herb fermenting of formula ratio and co-emulsifier is added, under the rotating speed of 20-30 rev/min, stir 20-30 minute, continue afterwards to cool to 40 DEG C, add the antiseptic of formula ratio, essence, continue to stir 15-20 minute under same rotating speed, get final product discharging;
3. the preparation method of snow chrysanthemum tea anti-allergy facial mask frost according to claim 2, is characterized in that: described step (2) moderate snow chrysanthemum tea Chinese medicine aqueous extract is prepared by following method:
(a) weighing: take Radix Glycyrrhizae, oat kernel, Herba Portulacae, snow amasss careless each 5-10 part, Sakura leaf, polymerization blade of grass, chinaberry leaf, polygoni cuspidati,radix, scutellariae,radix, Flos Nelumbinis, Radix Ophiopogonis grass, root of Paeonia suffruticosa Ardr., Herba Arctii leaf, elm endothelium, Magnolia bark, arnica montana, Folium Mori, each 3-5 part of Salix alba bark adds in rustless steel still, take avenge chrysanthemum tea 10-15 part and green tea 8-10 part for subsequent use;
B () once extracts: when first time boils, take deionized water 700-800 part, ethanol 3-4 part, propylene glycol 3-4 part, first soaks 30 minutes before boiling, and then uses big fire boiled, after use little fire instead and boil 1.0-1.2 hour, namely obtain snow chrysanthemum tea Chinese medicine aqueous extract 1. with 600 order filter-cloth filterings afterwards;
(c) second extraction: the propylene glycol adding the deionized water of 500-600 part and the ethanol of 1-3 part and 1-3 part in filtering residue, use little fire after big fire is boiled instead and boil 0.8-1.0 hour, add snow chrysanthemum tea and green tea immersion 0.5-1.0 hour afterwards, use 600 order filter-cloth filterings afterwards, chrysanthemum tea Chinese medicine aqueous extract must be avenged 2.;
D () mixes: by snow chrysanthemum tea Chinese medicine aqueous extract 1., 2. snow chrysanthemum tea Chinese medicine aqueous extract must avenge chrysanthemum tea Chinese medicine aqueous extract after mix homogeneously, its total amount should control about the half of interpolation total Water;
After described step (4) moderate snow chrysanthemum tea herb fermenting, the preparation technology of concentrated solution is as follows:
A the snow chrysanthemum tea Chinese medicine aqueous extract of the snow chrysanthemum tea Chinese medicine slag after extracted twice and 1/3rd joins in enamel fermentation tank by (), add Lemon fruit 2-4 part, brown sugar 3-5 part, edible Aloe 2-3 part, water 500-600 part, after system is heated to boiling, low baking temperature constant temperature disinfection 20 minutes, is then cooled to 25-30 DEG C;
B () adds geotrichum candidum strain by the 2-4% of fermented product total amount, fermentation 2-3 days, is then raised to 30-35 DEG C by system temperature, then adds the cloth Laplace yeast seeds of 1-3%, then carry out fermentation 2-3 days;
Thalline sum in (c) inspection system, if be greater than 500CFU ∕ ML, then continue fermentation 1-5 days, until viable bacteria body approach exhaustion in system, thalline sum is less than 500CFU ∕ ML, when there is no living contaminants, filter out fermentation liquid, below 50 DEG C, carry out vacuum concentration, treat filtrate total amount be original cumulative volume three/for the moment, the concentrated solution after chrysanthemum tea herb fermenting must be avenged.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN106860214A (en) * | 2017-01-17 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment moisture saver mask |
| CN106860383A (en) * | 2017-02-24 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment anti-acne day cream |
| CN106860045A (en) * | 2017-02-24 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment anti-acne day cream |
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| CN106860214A (en) * | 2017-01-17 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment moisture saver mask |
| CN106860383A (en) * | 2017-02-24 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment anti-acne day cream |
| CN106860045A (en) * | 2017-02-24 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment anti-acne day cream |
| CN106860170A (en) * | 2017-02-24 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment anti-acne day cream |
| CN106860382A (en) * | 2017-02-24 | 2017-06-20 | 长沙协浩吉生物工程有限公司 | A kind of compound method of ferment anti-acne day cream |
| CN107669593A (en) * | 2017-11-06 | 2018-02-09 | 苏州菲博特环保科技有限公司 | Multiple-effect skin rejuvenating facial mask |
| WO2019084984A1 (en) * | 2017-11-06 | 2019-05-09 | 苏州菲博特环保科技有限公司 | Multi-functional skin rejuvenating facial mask |
| CN111973540A (en) * | 2020-08-26 | 2020-11-24 | 荣鼎(广东)生物科技有限公司 | Production method of cosmetic oil |
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