CN1051001C - Fine powder of fruit of Chinese wolfberry, oil made of fruit of Chinese wolfberry and their producing methods - Google Patents
Fine powder of fruit of Chinese wolfberry, oil made of fruit of Chinese wolfberry and their producing methods Download PDFInfo
- Publication number
- CN1051001C CN1051001C CN93116265A CN93116265A CN1051001C CN 1051001 C CN1051001 C CN 1051001C CN 93116265 A CN93116265 A CN 93116265A CN 93116265 A CN93116265 A CN 93116265A CN 1051001 C CN1051001 C CN 1051001C
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- China
- Prior art keywords
- fructus lycii
- matrimony vine
- meticulous powder
- fruit
- fine powder
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- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
- Coloring Foods And Improving Nutritive Qualities (AREA)
Abstract
The present invention discloses matrimony vine fine powder and matrimony vine essential oil produced by the matrimony vine fine powder and a production method of the matrimony vine fine powder and the matrimony vine essential oil. The dry fruit or the fresh fruit of the matrimony vine are dried at the low temperature of-10 DEG C to-90 DEG C for 2 to 4 hours in the mode of evacuation, and then, the dry fruit or the fresh fruit of the matrimony vine is transferred to a disintegrator under the condition of-10 DEG C to-90 DEG C and is pulverized by the disintegrator; after the crushed dry fruit or the crushed fresh fruit of the matrimony vine is sieved, 10 to 400 meshes of matrimony vine fine powder are obtained. The obtained matrimony vine fine powder is extracted by using an organic solvent, and the matrimony vine essential oil is made after an extractant is removed. The matrimony vine fine powder and the matrimony vine essential oil made by the present invention keep the original natural nutrition ingredients and flavour, and can be directly applied to medicine, food and administration. The matrimony vine essential oil can also be made into natural pigments and cosmetic.
Description
The present invention relates to a kind of meticulous powder of Fructus Lycii that utilizes Fructus Lycii to produce reaches by the made Fructus Lycii quintessence oil of the meticulous powder of Fructus Lycii.
Fructus Lycii has existed in the books such as the earliest ancient medical book " 52 Bingfang " of China, " interior warp ", " book on Chinese herbal medicine converge speech ", Compendium of Material Medica as Chinese medicine.It is enriched blood as Chinese medicine, the function of liver heat removing and eyesight improving, the kidney invigorating is very obvious.Measuring contained multiple nutrients composition such as ascorbic acid, vitamin E, carotene etc. through modern science all is the indispensable nutrition of human body, can be used for the treatment of multiple disease.What but for many years, application of Fructus Lycii and corresponding product thereof were more is with fresh fruit and the direct pharmacy of dry fruit and edible.The Fructus Lycii of using in other food (as Fructus Lycii juice, Fructus Lycii sugar etc.) also grinds and gets by soaking the back, is difficult to give full play to the active ingredient of medicine wherein.Fructus Lycii powder is broken into superfines, can makes the intraseminal active ingredient of Fructus Lycii also can give full play to the active ingredient of its medicine, but, be difficult to obtain the meticulous powder of a large amount of Fructus Lyciis at normal temperatures because Fructus Lycii contains a large amount of sugar part and colloid.
The objective of the invention is Fructus Lycii to be made the meticulous powder of Fructus Lycii of extra small fineness and makes the Fructus Lycii quintessence oil with the meticulous powder of this Fructus Lycii in order more effectively to bring into play the active ingredient in the medicine.
The solution of the present invention is as follows: one. and the preparation of the meticulous powder of Fructus Lycii, the evacuation drying kept low temperature 2-6 hour when dried fruit of lycium barbarum or fresh fruit were refrigerated to the temperature of low temperature-10 ℃～-90 ℃ in cryogenic refrigerator.Send into the crusher for crushing under the temperature of low temperature-10 ℃～-90 ℃ then, the rotating speed of pulverizer is 600-3600 rev/min, and the fineness of the product that draws after screening is the meticulous powder of Fructus Lycii of 1.65mm-0.038mm, and color and luster is a salmon pink.
Above-mentioned pulverizer is to place the refrigerator of low temperature-10 ℃～-90 ℃ to work.
Two. prepare the Fructus Lycii quintessence oil with the meticulous powder of Fructus Lycii; meticulous powder of above-mentioned Fructus Lycii (fineness is 1.65mm-0.038mm) and 3-5 extractant (organic solvent) are doubly mixed; extract then; extraction temperature is 20-120 ℃; the extraction time is 0.5-4 hour; merge oil phase then, evaporated under reduced pressure solvent under nitrogen protection makes the Fructus Lycii quintessence oil.
As the organic solvent of extractant is in petroleum ether, ether, ethanol, ethyl acetate, the butyl acetate any, or the mixture of above-mentioned petroleum ether, ether, ethanol, ethyl acetate, butyl acetate.
Extraction can utilize the reactor paddling process, also can utilize the pipeline extraction.
The invention solves Fructus Lycii at normal temperatures and can not be processed into the problem of the meticulous powder of ultrafine, made and keep constant meticulous powder of ultrafine Fructus Lycii that its nutrition easily is absorbed by the body and the Fructus Lycii quintessence oil that contains a large amount of active substances and trace element of making again of Fructus Lycii local flavor, natural nutrition composition.Meticulous powder of this Fructus Lycii and Fructus Lycii quintessence oil can be used for pharmacy, system nutraceutical, also can directly take, and especially the Fructus Lycii quintessence oil also can be used as cosmetics and natural senior food coloring.Used processing step cost is low, and market prospect is wide.
Embodiment 1 (the meticulous powder of Fructus Lycii):
100 gram Fructus Lyciis are freezing to-40 ℃～-50 ℃ in cryogenic refrigerator, evacuation then dry 5 hours, is sent to it temperature then and is in-40 ℃～-50 ℃ the pulverizer and pulverize, through the meticulous powder 98.5g of salmon pink Fructus Lycii of screening gained, fineness is 120 orders (0.12mm);
Embodiment 2 (Fructus Lycii quintessence oil):
Get the meticulous powder 50g+4 of the Fructus Lycii that makes according to embodiment 1 method ether doubly with the extraction of reactor paddling process, extraction temperature 50-85 ℃, 4 hours extraction time, merge oil phase then, under nitrogen protection, adopt distillation under vacuum solvent evaporated → obtain Fructus Lycii quintessence oil 0.5g.
Claims (5)
1. meticulous powder of Fructus Lycii, it is characterized in that the meticulous powder of above-mentioned Fructus Lycii is dry 2-6 hour of evacuation when dried fruit of lycium barbarum or fresh fruit are refrigerated to the temperature of low temperature-10 ℃～-90 ℃ in cryogenic refrigerator, send into the crusher for crushing under the temperature of low temperature-10 ℃～-90 ℃ then, the fineness of the product that draws after screening is the meticulous powder of salmon pink Fructus Lycii of 1.65mm-0.038mm.
2. the Fructus Lycii quintessence oil that the meticulous powder of Fructus Lycii according to claim 1 is made, it is characterized in that earlier meticulous powder of above-mentioned Fructus Lycii and the 3-5 organic solvent as extractant doubly being mixed, extract then, extraction temperature is 20 ℃-120 ℃, the extraction time is 0.5-4 hour, slough organic solvent then, the henna Fructus Lycii quintessence oil of gained.
3. the Fructus Lycii quintessence oil that the meticulous powder of Fructus Lycii according to claim 2 is made is characterized in that above-mentioned organic solvent is to choose any one kind of them in petroleum ether, ether, ethanol, ethyl acetate, the butyl acetate.
4. the Fructus Lycii quintessence oil that the meticulous powder of Fructus Lycii according to claim 2 is made is characterized in that above-mentioned organic solvent is the mixture of petroleum ether, ether, ethanol, ethyl acetate, butyl acetate.
5. the Fructus Lycii quintessence oil that the meticulous powder of Fructus Lycii according to claim 2 is made; it is characterized in that earlier the meticulous powder of Fructus Lycii and 4 times of ether to the meticulous powder of Fructus Lycii being mixed; extract then; extraction temperature is 50-85 ℃; the extraction time is 0.5-4 hour; merge oil phase then, evaporated under reduced pressure solvent under protection of nitrogen gas makes the Fructus Lycii quintessence oil.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN93116265A CN1051001C (en) | 1993-08-09 | 1993-08-09 | Fine powder of fruit of Chinese wolfberry, oil made of fruit of Chinese wolfberry and their producing methods |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN93116265A CN1051001C (en) | 1993-08-09 | 1993-08-09 | Fine powder of fruit of Chinese wolfberry, oil made of fruit of Chinese wolfberry and their producing methods |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1086730A CN1086730A (en) | 1994-05-18 |
| CN1051001C true CN1051001C (en) | 2000-04-05 |
Family
ID=4991540
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN93116265A Expired - Fee Related CN1051001C (en) | 1993-08-09 | 1993-08-09 | Fine powder of fruit of Chinese wolfberry, oil made of fruit of Chinese wolfberry and their producing methods |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1051001C (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2930155B1 (en) * | 2008-04-21 | 2012-08-24 | Oreal | USE OF A BAY EXTRACT, AND ESPECIALLY WOLFBERRY, AS ANTI-POLLUTION AGENT |
| CN103080238B (en) | 2010-08-25 | 2016-01-20 | 帝斯曼知识产权资产管理有限公司 | For the manufacture of the method for the high extracting and enriching thing containing zeaxanthin and/or its ester |
| CN102132879B (en) * | 2011-03-28 | 2012-10-24 | 韩红雯 | Process for freezing and drying medlar powder in vacuum |
| CN103734741B (en) * | 2013-12-30 | 2015-11-04 | 徐州绿之野生物食品有限公司 | A kind of preparation method and application of wolfberry fruit extract |
| CN103704700A (en) * | 2013-12-30 | 2014-04-09 | 徐州绿之野生物食品有限公司 | Petroleum ether extraction type lycium barbarum extract and preparation method and application thereof |
| CN104606365B (en) * | 2015-01-07 | 2018-08-24 | 青岛大学 | A kind of wolfberry pigment medicine materical crude slice and preparation method thereof |
| CN108175720A (en) * | 2018-03-06 | 2018-06-19 | 宁夏医科大学 | A kind of skin care item |
-
1993
- 1993-08-09 CN CN93116265A patent/CN1051001C/en not_active Expired - Fee Related
Non-Patent Citations (4)
| Title |
|---|
| 《中草药》23,(6) 1992. 6. 1 刘书堂等,强力宁片提取工艺的改进" * |
| 《医药工程设计》1986,(4) 1986. 4. 1 周黎,"超低温粉碎装置LINREX粉碎系统" * |
| 《特产研究》1989,(3) 1989. 3. 1 李树殿等,"活性人参有效成分的分析" * |
| 《特产研究》1989,(3) 1989. 3. 1 李树殿等,"活性人参有效成分的分析";《医药工程设计》1986,(4) 1986. 4. 1 周黎,"超低温粉碎装置LINREX粉碎系统";《中草药》23,(6) 1992. 6. 1 刘书堂等,强力宁片提取工艺的改进" * |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1086730A (en) | 1994-05-18 |
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