CN105581253A - Extract oatmeal and preparation method thereof - Google Patents
Extract oatmeal and preparation method thereof Download PDFInfo
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- CN105581253A CN105581253A CN201511022028.6A CN201511022028A CN105581253A CN 105581253 A CN105581253 A CN 105581253A CN 201511022028 A CN201511022028 A CN 201511022028A CN 105581253 A CN105581253 A CN 105581253A
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- 241000334160 Isatis Species 0.000 claims abstract description 18
- 239000000706 filtrate Substances 0.000 claims description 84
- 238000000498 ball milling Methods 0.000 claims description 69
- 238000000605 extraction Methods 0.000 claims description 22
- 238000004140 cleaning Methods 0.000 claims description 12
- 238000004108 freeze drying Methods 0.000 claims description 12
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- 238000010438 heat treatment Methods 0.000 claims description 6
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- 239000007788 liquid Substances 0.000 claims description 3
- 229910052708 sodium Inorganic materials 0.000 claims description 3
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- 208000001953 Hypotension Diseases 0.000 description 2
- 229920002752 Konjac Polymers 0.000 description 2
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- 241000699666 Mus <mouse, genus> Species 0.000 description 2
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- HVYWMOMLDIMFJA-DPAQBDIFSA-N cholesterol Chemical compound C1C=C2C[C@@H](O)CC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 HVYWMOMLDIMFJA-DPAQBDIFSA-N 0.000 description 2
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- TWNIBLMWSKIRAT-VFUOTHLCSA-N levoglucosan Chemical compound O[C@@H]1[C@@H](O)[C@H](O)[C@H]2CO[C@@H]1O2 TWNIBLMWSKIRAT-VFUOTHLCSA-N 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23V—INDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
- A23V2002/00—Food compositions, function of food ingredients or processes for food or foodstuffs
Landscapes
- Medicines Containing Plant Substances (AREA)
Abstract
The invention discloses extract oatmeal and a preparation method thereof and belongs to the technical of food processing. The extract oatmeal is prepared from components in parts by weight as follows: 85-95 parts of oatmeal, 4-6 parts of an oatmeal extract, 10-15 parts of a shinyleaf pricklyash root extract, 3-5 parts of a forsythia extract and 1-3 parts of an isatis root extract. The preparation method comprises steps including preparation of the oatmeal extract, preparation of the shinyleaf pricklyash root extract, preparation of the forsythia extract, preparation of the isatis root extract and preparation of the extract oatmeal. Shinyleaf pricklyash roots and the oatmeal are combined, the blank of preparation of oatmeal from the shinyleaf pricklyash roots is filled up, thus, beneficial components of the two substances are combined, and healthcare functions of the two substances are complementary. Meanwhile, nutritional ingredients of the oatmeal, forsythia and isatis roots are added on the basis, so that the effects of the oatmeal are more comprehensive, and requirements of different consumers are met.
Description
Technical field
The present invention relates to a kind of extract oatmeal and preparation method thereof, belong to food production process technologyField.
Background technology
Oatmeal is taking oat as primary raw material, and through boiling, oven dry, compressing tablet, the technique such as dryThe low sugar that flow process is made, high nutrition, high energy food. Along with the raising of people's living standard, oatmealLittle by little become health food salable. This is because oat has reducing blood lipid, reduces cholesterol, fallsThe multiple bioactive functions such as blood pressure, hypoglycemic and non-oxidizability. At present, grinding taking oat as raw materialStudy carefully the extraction (as avenabeta glucosan, oat polypeptide etc.) that mainly concentrates on oat major function compositionWith the oatmeal processing with oat. But along with the raising of health of people consciousness, people are to foodThe requirement of product is also more and more higher, makes the oatmeal processing with oat deeply be subject to oat research workerFavor.
In recent years, the research of oatmeal has obtained certain achievement in research, as Chinese patent CN102835629B discloses " fast food ginger juice buttermilk oatmeal and preparation method thereof ", this ginger juice buttermilk swallowOatmeal is by milk powder 40～50%, ginger 15～20%, and white granulated sugar 10～25%, maltodextrin 0～15%,Oatmeal 6～20%, coagulating agent 0.5～1.0%, instant concentrated pure ginger powder 0.3～0.8%, essence 0.2～0.5% is made, and it is mainly that in the unique taste of ginger milk curd and oat, to be of value to human body strong by havingThe dietary fiber of health combines, and improves the mouthfeel of oatmeal; CN103919051A discloses " oneThere is matrimony vine oatmeal of blood sugar reducing function and preparation method thereof ", this matrimony vine oatmeal is by oatmeal110-150 part, fruit of Chinese wolfberry 4-16 part, konjaku flour 4-16 part, duck wheat 15-40 part is made, itsBe mainly by combinations such as oatmeal and the fruit of Chinese wolfberry, konjaku flour, duck wheats, thereby produced a kind of mouthfeelUnique, have blood sugar reducing function, cheap matrimony vine oatmeal; CN103141755B discloses " toolNutrition oatmeal and the processing method thereof of hypotensive blood-fat and blood sugar health-care effect ", this nutrition oatmeal isNaked oat grain 90-110 part, celery concentrate 4-6 part of 30%, root of kudzu vine concentrate 4-6 part of 30%,Hawthorn concentrate 1.5-2.5 part of 25%, 10% Momordica grosvenori concentrate is made in right amount, and it is mainIf oat is combined with celery, the root of kudzu vine, hawthorn and Momordica grosvenori, thereby produce health-care effect stackComplementation, the nutrition oatmeal of the health care to hypotensive, blood fat and blood sugar. Technique scheme is all logicalCross and add other compositions and combine with oat, thereby obtain the oatmeal of different efficacies. Therefore, pass throughAdding other compositions, is one of effective way of improving oatmeal effect.
Radix zanthoxyli is Guangxi Special plant, and its nature and flavor are pungent, bitter, tepor, mild toxicity, have dispelling wind and removing obstruction in the meridians,The effect such as removing dampness to relieve pain, subdhing swelling and detoxicating. In addition, modern study proves, Radix zanthoxyli have swelling and pain relieving,Antibacterial isoreactivity, has significant pharmacology to do for cardiovascular system, nervous system and smooth muscle etc.With, there is exploitation to be worth at anticancer aspect again simultaneously. Although Radix zanthoxyli has so significant pharmacological action,But the product that Radix zanthoxyli and oatmeal combine be there is not yet. Therefore, in order to meet people to protectingThe different demands of strong effect, develop a kind of extract oat that Radix zanthoxyli is combined with oatmeal and formSheet is a very valuable research.
Summary of the invention
For above-mentioned the deficiencies in the prior art, technical problem to be solved by this invention is to have proposed oneExtract oatmeal and preparation method thereof.
The present invention for addressing the above problem taked technical scheme is:
A kind of extract oatmeal, is made up of each component of following weight portion proportioning: oatmeal 85～95Part, 4～6 parts of oat extracts, 10～15 parts of Radix Zanthoxyli extracts, 3～5 parts of forsythia suspense extractions,1～3 part of isatis root extract.
Preferably,
A kind of extract oatmeal, made by each component of following weight portion proportioning: 90 parts of oatmeals,5 parts of oat extracts, 12 parts of Radix Zanthoxyli extracts, 4 parts of forsythia suspense extractions, isatis root extract 2Part.
The preparation method of described extract oatmeal, comprises the following steps:
(1) oat extract preparation
S1, by oat cleaning screening, then pulverize, and cross 40 mesh sieves, and carry out microwave drying:Microwave power 30～40kW, microwave time 10～15min;
S2, first through step S1In the dry oatmeal that processing obtains, add solid-liquid ratio be 1:10～30～40 DEG C of warm water of 15, soak 3～5min, then with sodium carbonate liquor regulate pH value to 8.0～11.0, be finally the ball mill ball milling ball milling of 200～300 turn/min with rotating speed, ball milling 20～30min,Filter, and collect filtrate 1;
S3, first will be through step S2The filtrate 1 that processing obtains regulates enzymolysis pH value to 4.0～6.0, enzymeSeparating temperature is 30～40 DEG C, and adds successively AMS, carbohydrase to carry out enzymolysis, enzyme additionBe respectively 0.08～0.18%, 0.04～0.08%, and then with rotating speed be 200～300 turn/minBall mill ball milling, ball milling 20～30min, filters, and collects filtrate 2;
S4, will be through step S3The filtrate 2 that processing obtains is placed in supersonic frequency and is 30～40KHz, ultrasonicAt 40～50 DEG C of temperature, extract, extract 20～30min, filter, collect filtrate 3;
S5, will be through step S4The filtrate 3 that processing obtains is heated to 80～90 DEG C, insulation 10～15minGo out after enzyme, be placed on 4000～5000 centrifuges that turn centrifugal 15～20 minutes, filter, collect filterLiquid 4, and concentrated, and freeze drying, obtains oat extract, for subsequent use;
(2) Radix Zanthoxyli extract preparation
S1, first by Radix zanthoxyli cleaning screening, then pulverize, and cross 80 mesh sieves, and add its weight10～15 times of amount acidic ethanols, are finally the ball mill ball milling ball milling of 200～300 turn/min with rotating speed,Ball milling 20～30min, filters, and collects filtrate 1;
S2, through step S1In the filtrate 1 that processing obtains, add 10～15 times of amount chloroforms of its weight,And be placed in the ball mill ball milling ball milling that rotating speed is 200～300 turn/min, ball milling 15～20min, mistakeFilter, and collect filtrate 2;
S3, through step S2The filtrate 2 that processing obtains is carried out heating and refluxing extraction 2 times, each 2～3H, filters, and collects filtrate 3;
S4, will be through step S3The filtrate 3 that processing obtains is placed in supersonic frequency and is 30～40KHz, ultrasonicAt 40～50 DEG C of temperature, extract, extract 20～30min, filter, collect filtrate 4;
S5, will be through step S4The filtrate 4 that processing obtains be placed on 4000～5000 centrifuges that turn fromThe heart 15～20 minutes, filters, and collects filtrate 5, and concentrated, and freeze drying, obtains Radix zanthoxyli and carryGet thing, for subsequent use;
(3) forsythia suspense extraction preparation
S1, first by Folium Forsythia cleaning screening, then pulverize, and cross 80 mesh sieves, then add it heavyMeasure the 5%Na of 10～15 times 30～40 DEG C2CO3Solution, soaks 10～15min, finally uses rotating speedBe the ball mill ball milling ball milling of 200～300 turn/min, ball milling 20～30min;
S2, first will be through step S1The mixture that processing obtains is adjusted pH to 4.0～6.0 with hydrochloric acid, thenWith warm water tune solution temperature to 30～40 DEG C, and add successively 0.3%～0.7% of mixture weightCellulase and 0.4%～0.8% pectase, be finally 200～300 turn/min with rotating speedBall mill ball milling ball milling, ball milling 20～30min filters, and collects filtrate 1;
S3, will be through step S2The filtrate 1 that processing obtains is placed in supersonic frequency and is 30～40KHz, ultrasonicAt 40～50 DEG C of temperature, extract, extract 30～40min, filter, collect filtrate 2;
S4, will be through step S3The filtrate 2 that processing obtains is heated to 80～90 DEG C, insulation 10～15minGo out after enzyme, be placed on 4000～5000 centrifuges that turn centrifugal 20～25 minutes, filter, collect filterLiquid 3, and concentrated, and freeze drying, obtains forsythia suspense extraction, for subsequent use;
(4) isatis root extract preparation
S1, first by Radix Isatidis cleaning screening, then pulverize, and cross 80 mesh sieves, then add it heavyMeasuring the distilled water of 10～15 times 30～40 DEG C, soak 10～15min, is finally 200～300 with rotating speedThe ball mill ball milling ball milling of turn/min, ball milling 20～30min, filters, and collects filtrate 1;
S2, through step S1In the filtrate 1 that processing obtains, add 10～15 times of amounts 60～70% of its weightEthanolic solution, and be placed in the ball mill ball milling ball milling that rotating speed is 200～300 turn/min, ball milling 15～20min, filters, and collects filtrate 2;
S3, through step S2The filtrate 2 that processing obtains is carried out heating and refluxing extraction 2 times, each 2～3H, filters, and collects filtrate 3;
S4, will be through step S3The filtrate 3 that processing obtains is placed in supersonic frequency and is 30～40KHz, ultrasonicAt 40～50 DEG C of temperature, extract, extract 20～30min, filter, collect filtrate 4;
S5, will be through step S4The filtrate 4 that processing obtains be placed on 4000～5000 centrifuges that turn fromThe heart 15～20 minutes, filters, and collects filtrate 5, and concentrated, and freeze drying obtains Radix Isatidis and extractsThing, for subsequent use;
(5) extract oatmeal preparation
S1, by oat extract, Radix Zanthoxyli extract, forsythia suspense extraction and isatis root extract respectivelyPulverize, and cross 200 mesh sieves;
S2, be by weight 4～6 parts of oat extracts, 10～15 parts of Radix Zanthoxyli extracts, connectStick up 3～5 parts of extracts, 1～3 portion of oatmeal being added to after microwave treatment slaking of isatis root extractIn 85～95 parts, mix, can obtain extract oatmeal.
Compared with prior art, tool of the present invention has the following advantages:
The present invention combines Radix zanthoxyli and oatmeal, has made up Radix zanthoxyli and has prepared the sky of oatmealIn vain, so both combine the beneficiating ingredient of these two kinds of materials, can make again the stack of their health-care effects complementary.Meanwhile, on this basis, add again the nutritional labeling of the capsule of weeping forsythia, Radix Isatidis, make effect of oatmeal moreAdd diversity, thereby meet different consumer demands. In addition, also added oat extract, madeEffect of oatmeal more comprehensively.
Detailed description of the invention
Below in conjunction with embodiment, the invention will be further described:
The preparation method of extract oatmeal of the present invention, comprises the following steps:
(1) oat extract preparation
S1, by oat cleaning screening, then pulverize, and cross 40 mesh sieves, and carry out microwave drying:Microwave power 30～40kW, microwave time 10～15min;
S2, first through step S1In the dry oatmeal that processing obtains, add solid-liquid ratio be 1:10～30～40 DEG C of warm water of 15, soak 3～5min, then with sodium carbonate liquor regulate pH value to 8.0～11.0, be finally the ball mill ball milling ball milling of 200～300 turn/min with rotating speed, ball milling 20～30min,Filter, and collect filtrate 1;
S3, first will be through step S2The filtrate 1 that processing obtains regulates enzymolysis pH value to 4.0～6.0, enzymeSeparating temperature is 30～40 DEG C, and adds successively AMS, carbohydrase to carry out enzymolysis, enzyme additionBe respectively 0.08～0.18%, 0.04～0.08%, and then with rotating speed be 200～300 turn/minBall mill ball milling, ball milling 20～30min, filters, and collects filtrate 2;
S4, will be through step S3The filtrate 2 that processing obtains is placed in supersonic frequency and is 30～40KHz, ultrasonicAt 40～50 DEG C of temperature, extract, extract 20～30min, filter, collect filtrate 3;
S5, will be through step S4The filtrate 3 that processing obtains is heated to 80～90 DEG C, insulation 10～15minGo out after enzyme, be placed on 4000～5000 centrifuges that turn centrifugal 15～20 minutes, filter, collect filterLiquid 4, and concentrated, and freeze drying, obtains oat extract, for subsequent use;
(2) Radix Zanthoxyli extract preparation
S1, first by Radix zanthoxyli cleaning screening, then pulverize, and cross 80 mesh sieves, and add its weight10～15 times of amount acidic ethanols, are finally the ball mill ball milling ball milling of 200～300 turn/min with rotating speed,Ball milling 20～30min, filters, and collects filtrate 1;
S2, through step S1In the filtrate 1 that processing obtains, add 10～15 times of amount chloroforms of its weight,And be placed in the ball mill ball milling ball milling that rotating speed is 200～300 turn/min, ball milling 15～20min, mistakeFilter, and collect filtrate 2;
S3, through step S2The filtrate 2 that processing obtains is carried out heating and refluxing extraction 2 times, each 2～3H, filters, and collects filtrate 3;
S4, will be through step S3The filtrate 3 that processing obtains is placed in supersonic frequency and is 30～40KHz, ultrasonicAt 40～50 DEG C of temperature, extract, extract 20～30min, filter, collect filtrate 4;
S5, will be through step S4The filtrate 4 that processing obtains be placed on 4000～5000 centrifuges that turn fromThe heart 15～20 minutes, filters, and collects filtrate 5, and concentrated, and freeze drying, obtains Radix zanthoxyli and carryGet thing, for subsequent use;
(3) forsythia suspense extraction preparation
S1, first by Folium Forsythia cleaning screening, then pulverize, and cross 80 mesh sieves, then add it heavyMeasure the 5%Na of 10～15 times 30～40 DEG C2CO3Solution, soaks 10～15min, finally uses rotating speedBe the ball mill ball milling ball milling of 200～300 turn/min, ball milling 20～30min;
S2, first will be through step S1The mixture that processing obtains is adjusted pH to 4.0～6.0 with hydrochloric acid, thenWith warm water tune solution temperature to 30～40 DEG C, and add successively 0.3%～0.7% of mixture weightCellulase and 0.4%～0.8% pectase, be finally 200～300 turn/min with rotating speedBall mill ball milling ball milling, ball milling 20～30min filters, and collects filtrate 1;
S3, will be through step S2The filtrate 1 that processing obtains is placed in supersonic frequency and is 30～40KHz, ultrasonicAt 40～50 DEG C of temperature, extract, extract 30～40min, filter, collect filtrate 2;
S4, will be through step S3The filtrate 2 that processing obtains is heated to 80～90 DEG C, insulation 10～15minGo out after enzyme, be placed on 4000～5000 centrifuges that turn centrifugal 20～25 minutes, filter, collect filterLiquid 3, and concentrated, and freeze drying, obtains forsythia suspense extraction, for subsequent use;
(4) isatis root extract preparation
S1, first by Radix Isatidis cleaning screening, then pulverize, and cross 80 mesh sieves, then add it heavyMeasuring the distilled water of 10～15 times 30～40 DEG C, soak 10～15min, is finally 200～300 with rotating speedThe ball mill ball milling ball milling of turn/min, ball milling 20～30min, filters, and collects filtrate 1;
S2, through step S1In the filtrate 1 that processing obtains, add 10～15 times of amounts 60～70% of its weightEthanolic solution, and be placed in the ball mill ball milling ball milling that rotating speed is 200～300 turn/min, ball milling 15～20min, filters, and collects filtrate 2;
S3, through step S2The filtrate 2 that processing obtains is carried out heating and refluxing extraction 2 times, each 2～3H, filters, and collects filtrate 3;
S4, will be through step S3The filtrate 3 that processing obtains is placed in supersonic frequency and is 30～40KHz, ultrasonicAt 40～50 DEG C of temperature, extract, extract 20～30min, filter, collect filtrate 4;
S5, will be through step S4The filtrate 4 that processing obtains be placed on 4000～5000 centrifuges that turn fromThe heart 15～20 minutes, filters, and collects filtrate 5, and concentrated, and freeze drying obtains Radix Isatidis and extractsThing, for subsequent use;
(5) extract oatmeal preparation
S1, by oat extract, Radix Zanthoxyli extract, forsythia suspense extraction and isatis root extract respectivelyPulverize, and cross 200 mesh sieves;
S2, be by weight 4～6 parts of oat extracts, 10～15 parts of Radix Zanthoxyli extracts, connectStick up 3～5 parts of extracts, 1～3 portion of oatmeal being added to after microwave treatment slaking of isatis root extractIn 85～95 parts, mix, can obtain extract oatmeal.
Embodiment 1
A kind of extract oatmeal, made by each component of following weight portion proportioning: 90 parts of oatmeals,5 parts of oat extracts, 12 parts of Radix Zanthoxyli extracts, 4 parts of forsythia suspense extractions, isatis root extract 2Part.
Embodiment 2
A kind of extract oatmeal, made by each component of following weight portion proportioning: 85 parts of oatmeals,4 parts of oat extracts, 10 parts of Radix Zanthoxyli extracts, 3 parts of forsythia suspense extractions, isatis root extract 1Part.
Embodiment 3
A kind of extract oatmeal, made by each component of following weight portion proportioning: 95 parts of oatmeals,6 parts of oat extracts, 15 parts of Radix Zanthoxyli extracts, 5 parts of forsythia suspense extractions, isatis root extract 3Part.
In addition, applicant has also carried out the impact test of extract oatmeal on animal blood glucose:
By 30 of the diabetes model kunming mices of body weight (20 ± 2) g, be divided at random 3 groups, every group10, i.e. A group, B group and C group; Wherein, A organizes the oatmeal for preparing with embodiment 1 and feedsFood, B organizes the oatmeal feeding preparing with embodiment 2, and C group prepares with embodiment 3Oatmeal feeding, every day three times, each 10mg, continuously feeding 30 days; Measure mouse fasting blood-glucoseValue, test result is as shown in table 1.
Table 1 mouse blood sugar concentration determination result
| Type | Blood sugar concentration (mmol/L) before test | Blood sugar concentration (mmol/L) after test |
| Embodiment 1 | 19.8±2.1 | 16.3±2.8 |
| Embodiment 2 | 19.8±2.2 | 16.6±2.6 |
| Embodiment 3 | 19.8±2.3 | 16.5±2.9 |
As known from Table 1, the oatmeal that embodiment 1, embodiment 2, embodiment 3 prepare can makeMouse blood sugar concentration reduces, and the oatmeal that this explanation the present invention prepares has the blood sugar concentration of reduction meritEffect.
Certainly, just the preferred embodiments of the disclosure is described in detail above, not with thisLimit practical range of the present invention, all equivalences of doing according to principle of the present invention, structure and structure becomeChange, all should be covered by protection scope of the present invention.
Claims (2)
1. an extract oatmeal, is characterized in that: by each component system of following weight portion proportioningBecome: 85～95 parts of oatmeals, 4～6 parts of oat extracts, 10～15 parts of Radix Zanthoxyli extracts,3～5 parts of forsythia suspense extractions, 1～3 part of isatis root extract.
2. the preparation method of extract oatmeal according to claim 1, is characterized in that:Comprise the following steps:
(1) oat extract preparation
S1, by oat cleaning screening, then pulverize, and cross 40 mesh sieves, and carry out microwave drying:Microwave power 30～40kW, microwave time 10～15min;
S2, first through step S1In the dry oatmeal that processing obtains, add solid-liquid ratio be 1:10～30～40 DEG C of warm water of 15, soak 3～5min, then with sodium carbonate liquor regulate pH value to 8.0～11.0, be finally the ball mill ball milling ball milling of 200～300 turn/min with rotating speed, ball milling 20～30min,Filter, and collect filtrate 1;
S3, first will be through step S2The filtrate 1 that processing obtains regulates enzymolysis pH value to 4.0～6.0, enzymeSeparating temperature is 30～40 DEG C, and adds successively AMS, carbohydrase to carry out enzymolysis, enzyme additionBe respectively 0.08～0.18%, 0.04～0.08%, and then with rotating speed be 200～300 turn/minBall mill ball milling, ball milling 20～30min, filters, and collects filtrate 2;
S4, will be through step S3The filtrate 2 that processing obtains is placed in supersonic frequency and is 30～40KHz, ultrasonicAt 40～50 DEG C of temperature, extract, extract 20～30min, filter, collect filtrate 3;
S5, will be through step S4The filtrate 3 that processing obtains is heated to 80～90 DEG C, insulation 10～15minGo out after enzyme, be placed on 4000～5000 centrifuges that turn centrifugal 15～20 minutes, filter, collect filterLiquid 4, and concentrated, and freeze drying, obtains oat extract, for subsequent use;
(2) Radix Zanthoxyli extract preparation
S1, first by Radix zanthoxyli cleaning screening, then pulverize, and cross 80 mesh sieves, and add its weight10～15 times of amount acidic ethanols, are finally the ball mill ball milling ball milling of 200～300 turn/min with rotating speed,Ball milling 20～30min, filters, and collects filtrate 1;
S2, through step S1In the filtrate 1 that processing obtains, add 10～15 times of amount chloroforms of its weight,And be placed in the ball mill ball milling ball milling that rotating speed is 200～300 turn/min, ball milling 15～20min, mistakeFilter, and collect filtrate 2;
S3, through step S2The filtrate 2 that processing obtains is carried out heating and refluxing extraction 2 times, each 2～3H, filters, and collects filtrate 3;
S4, will be through step S3The filtrate 3 that processing obtains is placed in supersonic frequency and is 30～40KHz, ultrasonicAt 40～50 DEG C of temperature, extract, extract 20～30min, filter, collect filtrate 4;
S5, will be through step S4The filtrate 4 that processing obtains be placed on 4000～5000 centrifuges that turn fromThe heart 15～20 minutes, filters, and collects filtrate 5, and concentrated, and freeze drying, obtains Radix zanthoxyli and carryGet thing, for subsequent use;
(3) forsythia suspense extraction preparation
S1, first by Folium Forsythia cleaning screening, then pulverize, and cross 80 mesh sieves, then add it heavyMeasure the 5%Na of 10～15 times 30～40 DEG C2CO3Solution, soaks 10～15min, finally uses rotating speedBe the ball mill ball milling ball milling of 200～300 turn/min, ball milling 20～30min;
S2, first will be through step S1The mixture that processing obtains is adjusted pH to 4.0～6.0 with hydrochloric acid, thenWith warm water tune solution temperature to 30～40 DEG C, and add successively 0.3%～0.7% of mixture weightCellulase and 0.4%～0.8% pectase, be finally 200～300 turn/min with rotating speedBall mill ball milling ball milling, ball milling 20～30min filters, and collects filtrate 1;
S3, will be through step S2The filtrate 1 that processing obtains is placed in supersonic frequency and is 30～40KHz, ultrasonicAt 40～50 DEG C of temperature, extract, extract 30～40min, filter, collect filtrate 2;
S4, will be through step S3The filtrate 2 that processing obtains is heated to 80～90 DEG C, insulation 10～15minGo out after enzyme, be placed on 4000～5000 centrifuges that turn centrifugal 20～25 minutes, filter, collect filterLiquid 3, and concentrated, and freeze drying, obtains forsythia suspense extraction, for subsequent use;
(4) isatis root extract preparation
S1, first by Radix Isatidis cleaning screening, then pulverize, and cross 80 mesh sieves, then add it heavyMeasuring the distilled water of 10～15 times 30～40 DEG C, soak 10～15min, is finally 200～300 with rotating speedThe ball mill ball milling ball milling of turn/min, ball milling 20～30min, filters, and collects filtrate 1;
S2, through step S1In the filtrate 1 that processing obtains, add 10～15 times of amounts 60～70% of its weightEthanolic solution, and be placed in the ball mill ball milling ball milling that rotating speed is 200～300 turn/min, ball milling 15～20min, filters, and collects filtrate 2;
S3, through step S2The filtrate 2 that processing obtains is carried out heating and refluxing extraction 2 times, each 2～3H, filters, and collects filtrate 3;
S4, will be through step S3The filtrate 3 that processing obtains is placed in supersonic frequency and is 30～40KHz, ultrasonicAt 40～50 DEG C of temperature, extract, extract 20～30min, filter, collect filtrate 4;
S5, will be through step S4The filtrate 4 that processing obtains be placed on 4000～5000 centrifuges that turn fromThe heart 15～20 minutes, filters, and collects filtrate 5, and concentrated, and freeze drying obtains Radix Isatidis and extractsThing, for subsequent use;
(5) extract oatmeal preparation
S1, by oat extract, Radix Zanthoxyli extract, forsythia suspense extraction and isatis root extract respectivelyPulverize, and cross 200 mesh sieves;
S2, be by weight 4～6 parts of oat extracts, 10～15 parts of Radix Zanthoxyli extracts, connectStick up 3～5 parts of extracts, 1～3 portion of oatmeal being added to after microwave treatment slaking of isatis root extractIn 85～95 parts, mix, can obtain extract oatmeal.
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| CN107981204A (en) * | 2017-11-24 | 2018-05-04 | 恭城福茂生油茶文化产业发展有限公司 | A kind of preparation method with the nutrient oatmeal of sedative health-care |
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| CN107981204A (en) * | 2017-11-24 | 2018-05-04 | 恭城福茂生油茶文化产业发展有限公司 | A kind of preparation method with the nutrient oatmeal of sedative health-care |
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