CN103451020B - Preparation and application of natural cabo flavor-correcting synergist - Google Patents
Preparation and application of natural cabo flavor-correcting synergist Download PDFInfo
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- CN103451020B CN103451020B CN201310427560.0A CN201310427560A CN103451020B CN 103451020 B CN103451020 B CN 103451020B CN 201310427560 A CN201310427560 A CN 201310427560A CN 103451020 B CN103451020 B CN 103451020B
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Abstract
The invention relates to a preparation and application of a natural cabo flavor-correcting synergist. According to the preparation method, the natural cabo flavor-correcting synergist is finally obtained through solvent soaking, extraction and concentration processes by using magnolia flowers as raw materials. The flavor-correcting synergist is not remarkable in effect of reducing wood flavor and irritation of cut cabo or reconstituted tobacco, but the effect of reducing wood flavor and irritation of cut cabo or reconstituted tobacco by an astragalus extract can be remarkably improved by adding the flavor-correcting synergist together with the cabo flavor-correcting synergist astragalus extract into cut cabo or reconstituted tobacco, so that the doping rate of treated cut cabo or reconstituted tobacco in medium and high-grade cigarette formulae reaches over 10% without bringing adverse effect to smoke quality of cigarettes.
Description
Technical field
The present invention relates to tobacco additive agent field, specifically a kind of methods for making and using same of natural offal flavoring synergist, utilize the present invention can prepare a kind of natural offal flavoring synergist newly.This flavoring synergist adds in stalk filaments of tobacco stalks or reconstituted tobacco together with offal correctives, offal correctives can be significantly improved and reduce the xylon gas of stem or reconstituted tobacco and irritating effect, process stem or the reconstituted tobacco rate of mixing in cigarette composition can be made to reach more than 10%, and bring detrimentally affect can not to the flue gas quality of cigarette.
Background technology
Offal account for tobacco leaf heavy 25% ~ 30%.The flue gas xylon gas that offal burning produces is heavy, and assorted gas is large, and pungency is strong, inhale taste choke cough, puckery mouth, perfume quantity is few, seriously affects the smoking quality of cigarette.Therefore, the application percentage of offal in cigarette composition is extremely low, and this just causes a large amount of offal and discards, and both wastes natural resources, again contaminate environment, simultaneously the also corresponding production cost increasing cigarette.For improving the application percentage of offal in cigarette composition, domestic and international tobacco has carried out large quantity research to the utilization of offal.The technology that current cigarette industry adopts mainly contains expansion technique, reconstituted tobacco technology and additive treating technology etc.The major objective applying these technical finesses reduces xylon gas and the pungency of offal or reconstituted tobacco; process offal or reconstituted tobacco are added in medium-to-high grade cigarette composition pipe tobacco with larger proportion as stopping composition, and brings detrimentally affect can not to the suction taste of cigarette.But; only adopt a kind of technology will improve offal significantly or the blending proportion of reconstituted tobacco in medium-to-high grade cigarette composition pipe tobacco is impossible; it must be the comprehensive action of multiple technologies; all that compound is the same as the prescription that the traditional Chinese medical science is cured the disease; the i.e. organic assembling of multi-medicament, the treatment technology of offal or reconstituted tobacco is also like this.For example; Radix Astragali extract; although individual curing obviously can reduce xylon gas and the pungency (see Chinese patent 201210440473.4) of offal or reconstituted tobacco; if but its process offal or the blending proportion of reconstituted tobacco in medium-to-high grade cigarette composition pipe tobacco are more than 8%, will have a strong impact on the smoking quality of cigarette.Can improve the mixture proportion of offal or reconstituted tobacco further, find and a kind ofly can produce the new flavoring synergist of collaborative compatibility effect with Radix Astragali extract correctives, this problem have caused the concern about insider.
Flos Magnoliae, has another name called flos magnoliae, Flos Magnoliae, Yulan Magnolia, is the bud of the Magnoliaceae defoliation bush plant flower bud of lily magnolia.Taste warm in nature is pungent, attaches to the lung and stomach meridians.The pungent loose temperature of Flos Magnoliae is led to, and fragrance is walked to alter, up women's head-ornaments, kind relieving stuffy nose, is the key medicine for the treatment of nasosinusitis headache.As long as compatibility is proper, partially cold partial heat all can be applied, and oral administration and externally has good curative effect.Flos Magnoliae is a kind of conventional Chinese medicine, but, the preparation of relevant Flos Magnoliae extract and the application in cigarette, particularly Flos Magnoliae extract work in coordination with Radix Astragali extract together with the still rarely seen report of application in offal or reconstituted tobacco flavoring.
Summary of the invention
Object of the present invention is just for processing offal or the reconstituted tobacco problem that blending proportion is lower in medium-to-high grade cigarette composition pipe tobacco in above-mentioned existing offal or reconstituted tobacco treatment technology and developing, prepare a kind of Flos Magnoliae extract flavoring synergist; and add in stalk filaments of tobacco stalks or reconstituted tobacco as the natural flavoring synergist of one together with offal correctives Radix Astragali extract; significantly to reduce xylon gas and the pungency of offal or reconstituted tobacco; significantly improve stem or reconstituted tobacco and mix rate in cigarette composition, and do not affect the smoking quality of cigarette.
The object of the invention is to be achieved through the following technical solutions:
The preparation method of natural offal flavoring synergist of the present invention take Flos Magnoliae as raw material, through solvent soaking → extraction → filtration → concentrated, obtains natural offal flavoring synergist.
Described Flos Magnoliae is on medicinal material market or the Flos Magnoliae bud of the traditional Chinese medicine drying of medicinal material Company.
At solvent extracting process, described solvent is any one or its mixed solution in water, ethanol, propylene glycol.
At solvent extracting process, described extracting mode is that left at room temperature soak extraction extracts in conjunction with reflux.
Described concentration process is that under normal pressure, distillation and concentration or underpressure distillation concentrate, and is preferably underpressure distillation and concentrates.
Natural flavoring synergist of the present invention is added in stalk filaments of tobacco stalks or reconstituted tobacco together with offal correctives Radix Astragali extract; Radix Astragali extract can be significantly improved and reduce the xylon gas of offal or reconstituted tobacco and irritating effect; stem or the reconstituted tobacco rate of mixing in cigarette composition pipe tobacco can be made to reach more than 10%, and do not affect the suction taste of cigarette.The consumption of natural offal flavoring synergist of the present invention is 0.01% ~ 1% of stem or reconstituted tobacco quality, be preferably 0.1% ~ 0.5%, during use, natural offal flavoring synergist of the present invention first mixes with offal correctives Radix Astragali extract, the mass mixing ratio of Radix Astragali extract and natural offal flavoring synergist of the present invention is 1 ~ 10: 1, be preferably 2 ~ 5: 1 dilute with the mixed solution of water, ethanol or ethanol and water again after spray and be added in offal compressing tablet, stem or reconstituted tobacco.Described alcohol concn is 50% ~ 70%.
Outstanding feature of the present invention is: the novelty teabag developing a kind of Flos Magnoliae with the extracting method that conventional solvent is common, is proposed a kind of natural offal flavoring synergist newly.This flavoring synergist adds in stem or reconstituted tobacco together with offal correctives Radix Astragali extract; Radix Astragali extract can be significantly improved and reduce the xylon gas of offal or reconstituted tobacco and irritating effect; stem or the blending proportion of reconstituted tobacco in medium-to-high grade cigarette composition pipe tobacco can be made to reach more than 10%, and detrimentally affect can not be brought to cigarette odor-absorbing.
Specific embodiments
The present invention is described in further detail below with reference to example, but does not limit the present invention.
Example
Get the Flos Magnoliae of 50 g dryings, add 500 mL water (also can with ethanol or propylene glycol), 1 h is soaked under room temperature, heated and boiled 1 h under normal pressure, filter, the water of filter residue with amount repeats extraction 2 times under similarity condition, merges No. 3 extracting solutions, distillation and concentration under normal pressure, obtains natural offal flavoring synergist I.
Reference example (preparation of Radix Astragali extract offal correctives)
Get the astragalus root section of 50 g dryings, add 500 mL 95% ethanol, under room temperature, soak 1 h, microwave heating refluxes 0.5 h, filters, and 95% ethanol of filter residue with amount repeats extraction 2 times under similarity condition, merge No. 3 extracting solutions, distillation and concentration under normal pressure, obtain natural offal correctives I.
Application comparison example
Get 10,9,8,7,6,5,4,3,2, the natural offal correctives I of 1g, offal flavoring synergist I natural in 1g mixes respectively, then uses 10 g 50% alcohol dilutions respectively, diluent is sprayed in 1kg expanded cut stem respectively equably, the sealing of process stem, and ambient temperatare puts 6h, respectively by 3%, 5%, 8%, 10%, 15%(massfraction) ratio uniform mix during certain middle-grade Virginian-type cigarette cuts filler, contrast as interpolation 0,3%, 5%, the Virginian-type cigarette of the same race of 8%, 10%, 15% untreated expanded cut stem of the same race cuts filler.Cigarette is rolled into by ordinary method.Cigarette regulates 48 h in temperature (22 ± 1) DEG C and relative humidity (60 ± 2) % environment, and take out, by cigarette, the group of smokeing panel test smokes panel test.
Result shows, for the cigarette of interpolation 3% expanded cut stem, compared with the cigarette of the untreated expanded cut stem of interpolation 3%, add 10: 1,9: 1,8: 1,7: 1,6: 1,5: 1,4: 1,3: 1,2: 1, the cigarette smoke xylon gas that 1: 1 correctives I and flavoring synergist I process expanded cut stem all obviously alleviates, pungency obviously reduces, and inhales taste consistent with the cigarette not adding expanded cut stem, and the suction taste adding 3% untreated expanded cut stem cigarette is basically identical with the cigarette not adding expanded cut stem.
For the cigarette of interpolation 5% expanded cut stem, compared with the cigarette of the untreated expanded cut stem of interpolation 5%, add 8: 1,7: 1,6: 1,5: 1, the cigarette smoke xylon gas that 4: 1,3: 1,2: 1 correctivess I and flavoring synergist I process expanded cut stem all obviously alleviates, pungency obviously reduces, and inhales taste consistent with the cigarette not adding expanded cut stem; Add 10: 1, the cigarette smoke xylon gas that 9: 1,1: 1 correctives I and flavoring synergist I process expanded cut stem alleviates, and pungency reduces, inhale taste basically identical with the cigarette not adding expanded cut stem, the suction taste adding 5% untreated expanded cut stem cigarette is slightly poorer than the cigarette not adding expanded cut stem.
For the cigarette of interpolation 8% expanded cut stem, compared with the cigarette of the untreated expanded cut stem of interpolation 8%, add 7: 1,6: 1,5: Isosorbide-5-Nitrae: 1,3: 1, the cigarette smoke xylon gas that 2: 1 correctivess I and flavoring synergist I process expanded cut stem all obviously alleviates, and pungency obviously reduces, and inhales taste consistent with the cigarette not adding expanded cut stem; Add 10: 1,9: 1,8: 1,1: 1, the cigarette smoke xylon gas that correctives I and flavoring synergist I process expanded cut stem alleviates, and pungency reduces.Wherein, adding 9: 1,8: 1 correctivess I and flavoring synergist I, to process the cigarette odor-absorbing of expanded cut stem basically identical with the cigarette not adding expanded cut stem; The cigarette odor-absorbing that interpolation 10: 1,1: 1 correctives I and flavoring synergist I process expanded cut stem is poorer than the cigarette not adding expanded cut stem; The cigarette smoke xylon gas adding 8% untreated expanded cut stem is heavy, and assorted gas is large, and pungency is large, and it inhales taste obviously than the difference of not adding expanded cut stem cigarette.
For the cigarette of interpolation 10% expanded cut stem, compared with the cigarette of the untreated expanded cut stem of interpolation 10%, add 5: 1,4: 1,3: 1, the cigarette smoke xylon gas that 2: 1 correctivess I and flavoring synergist I process expanded cut stem obviously alleviates, and pungency obviously reduces, and inhales taste consistent with the cigarette not adding expanded cut stem; The cigarette smoke xylon gas that interpolation 7: 1,6: 1 correctivess I and flavoring synergist I process expanded cut stem alleviates, and pungency reduces, and inhales taste basically identical with the cigarette not adding expanded cut stem; The cigarette smoke xylon gas that interpolation 10: 1,9: 1,8: 1,1: 1 correctives I and flavoring synergist I process expanded cut stem and interpolation 10% untreated expanded cut stem is heavy, and greatly, pungency is large for assorted gas, and its suction taste is obviously than the difference of not adding expanded cut stem cigarette.
For the cigarette of interpolation 15% expanded cut stem, compared with the cigarette of the untreated expanded cut stem of interpolation 15%, the cigarette smoke xylon gas that interpolation 4: 1,3: 1 correctivess I and flavoring synergist I process expanded cut stem alleviates, pungency reduces, and inhales taste basically identical with the cigarette not adding expanded cut stem; Add 10: 1,9: 1,8: 1,7: 1, the cigarette smoke xylon gas that 6: 1,5: 1,2: 1,1: 1 correctives I and flavoring synergist I process expanded cut stem and interpolation 15% untreated expanded cut stem is heavy, assorted gas is large, and pungency is large, and it inhales taste obviously than the difference of not adding expanded cut stem cigarette.
Claims (6)
1. the application of a natural offal flavoring synergist in stem or reconstituted tobacco, it is characterized in that: this flavoring synergist and offal correctives are together added in stalk filaments of tobacco stalks or reconstituted tobacco, offal correctives can be significantly improved and reduce the xylon gas of stem or reconstituted tobacco and irritating effect, process stem or the reconstituted tobacco rate of mixing in medium-to-high grade cigarette composition is made to reach more than 10%, and bring detrimentally affect can not to the flue gas quality of cigarette, the preparation method of described natural offal flavoring synergist is as follows: take Flos Magnoliae as raw material, pass through solvent soaking, extract, concentration technology, finally obtain a kind of natural offal flavoring synergist, described offal correctives is Radix Astragali extract, and the mass mixing ratio of Radix Astragali extract and natural offal flavoring synergist is 2 ~ 5: 1.
2. the application of natural offal flavoring synergist according to claim 1 in stem or reconstituted tobacco, is characterized in that: described Flos Magnoliae is on medicinal material market or the Flos Magnoliae bud of the drying of medicinal material Company.
3. the application of natural offal flavoring synergist according to claim 1 in stem or reconstituted tobacco, is characterized in that: described solvent is any one or its mixed solution in water, ethanol, propylene glycol.
4. the application of natural offal flavoring synergist according to claim 1 in stem or reconstituted tobacco, is characterized in that: described extraction process is that left at room temperature soaks and reflux extraction combines.
5. the application of natural offal flavoring synergist according to claim 1 in stem or reconstituted tobacco, is characterized in that: described concentration technology is that underpressure distillation concentrates.
6. the application of natural offal flavoring synergist according to claim 1 in stem or reconstituted tobacco, it is characterized in that: the consumption of natural offal flavoring synergist is 0.3% ~ 0.8% of stem or reconstituted tobacco quality, first by a certain percentage this synergist is mixed with offal correctives during use, then dilute to spray afterwards with the mixed solution of water, ethanol or ethanol and water and be added in stalk filaments of tobacco stalks or reconstituted tobacco cut tobacco.
7.the application of natural offal flavoring synergist according to claim 6 in stem or reconstituted tobacco, is characterized in that: the concentration of described ethanol is 50% ~ 70%.
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| CN104774693B (en) * | 2015-03-31 | 2017-10-31 | 四川中烟工业有限责任公司 | The fireworks essential oil and its application and preparation method prepared using tobacco waste |
| CN110432536B (en) * | 2019-06-25 | 2021-10-29 | 内蒙古昆明卷烟有限责任公司 | Sweet and fragrant sauce type heating non-combustion tobacco product and preparation method thereof |
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| CN1094264A (en) * | 1993-04-21 | 1994-11-02 | 安徽省烟草公司蚌埠公司 | Tobacco agent health article |
| CN1244572A (en) * | 1999-07-28 | 2000-02-16 | 张桂忠 | Fragrance increasing agent containing natural perfume |
| CN102793264B (en) * | 2012-08-31 | 2014-10-29 | 中国烟草总公司郑州烟草研究院 | Preparation method of magnolia fruit extract and application thereof in cigarette |
| CN102885397B (en) * | 2012-11-07 | 2015-06-03 | 中国烟草总公司郑州烟草研究院 | Application of astragalus extract in stem strings or reproduced tobaccos |
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