CN103525553A - Tobacco and spice plant mixing essence and application thereof - Google Patents
Tobacco and spice plant mixing essence and application thereof Download PDFInfo
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- CN103525553A CN103525553A CN201310503696.5A CN201310503696A CN103525553A CN 103525553 A CN103525553 A CN 103525553A CN 201310503696 A CN201310503696 A CN 201310503696A CN 103525553 A CN103525553 A CN 103525553A
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- spice berry
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Abstract
The invention discloses tobacco and spice plant mixing essence and application thereof. The mixing essence is prepared from tobacco and spice plants and is prepared by the steps of extracting by an organic solvent, decompressing and concentrating to remove the organic solvent, performing deresination on a crude extract, and performing molecular distillation treatment on the extract in a molecular distillation evaporator. The essence can not only overcome shortcomings that the spice plants are excessive in aroma and suppress the intrinsic fragrance of tobacco in flavoring of cigarettes, but also enhance the intrinsic fragrance of the tobacco and aroma richness of the cigarettes as well as provide harmonious natural plant aroma to the cigarettes.
Description
Technical field
The invention belongs to essence spice for cigarette technical field, specifically relate to a kind of mixed essential oil that can coordinate this perfume of tobacco and spice berry note.Meanwhile, the invention still further relates to the concrete application of this mixed essential oil in production of cigarettes.
Background technology
Current, along with scientific and technical progress, people more and more pay close attention to the harm that smoking brings, and low tar content has become one of important indicator of safety cigarette.Yet along with the reduction of cigarette tar content, this perfume (or spice) of tobacco of cigarette is thin out, the rich and sophistication of fragrance also weakens, and is difficult to meet human consumer's quality demand.Therefore, flavouring becomes the important topic that low-coke tar cigarette is produced.
Essence spice for cigarette is as the basic raw material of cigarette flavouring, natural perfume plant essential oil, as rose, Flos Pelargonii, lavandula angustifolia, Rosmarinus officinalis, peppermint, lemongrass, chrysanthemum, jasmine, cloves, Verbascum, Stigma Croci essential oil be all the natural perfumes in " tobacco additive agent license register ", although these essential oils can be given the note of the different plants of cigarette, increase the rich of cigarette flavor.But, when these spice berry essential oils are applied in cigarette, be easy to cause the note of spice berry too outstanding, suppress this perfume (or spice) of tobacco.
At present, relevant essential oil of tobaccos or the spice berry essential oil report of flavouring in cigarette is more, as patent CN102559388A, CN102499465A, document " molecular distillation of rosemary ethereal oil refining and application in cigarette ", but yet there are no after tobacco is mixed with spice berry, prepare tobacco aromatics using, and can coordinate preferably the technology report of this perfume of tobacco and spice berry note.
Summary of the invention
The object of the invention is to for the deficiencies in the prior art, provide one to grow tobacco and spice berry mixed essential oil, this mixed essential oil can be coordinated the note of this perfume of tobacco and spice berry preferably, thereby promotes the suction quality of cigarette.
The present invention also aims to provide the concrete application of described mixed essential oil in cigarette.
Object of the present invention is achieved by following technical proposals.
One grows tobacco and spice berry mixed essential oil, by following methods, is prepared:
After tobacco material and spice berry raw material are mixed by the mass ratio of 10:1～200:1, the organic solvent extraction that adds 3～15 times of raw materials quality, concentrating under reduced pressure is removed organic solvent, obtain the crude extract of tobacco-spice berry mixed essential oil, crude extract is carried out after deresination processing, send in the vaporizer of molecular distillation, under the distillation pressure of 0.1～100Pa, the distillation temperature of 60～200 ℃, carry out molecular distillation processing, collect front-end volatiles and obtain required tobacco and spice berry mixed essential oil.
Described tobacco material is preferably one or more in flue-cured tobacco, Turkish tobaccos, burley tobaccos.
Described spice berry raw material be preferably rose, Flos Pelargonii, lavandula angustifolia, Rosmarinus officinalis, one or more in peppermint, lemongrass, chrysanthemum, jasmine, cloves, Verbascum, Stigma Croci.
Described organic solvent is preferably a kind of in sherwood oil, normal hexane, ether, methylene dichloride, ethyl acetate, dehydrated alcohol.
Described tobacco and the application of spice berry mixed essential oil in cigarette: described mixed essential oil and dehydrated alcohol or concentration mass percent 95% ethanol are dissolved and are mixed with perfuming solution by the mass ratio of 1:100, and then be evenly sprayed onto on pipe tobacco in the mode of feeding in raw material by the addition of 1～20mg/kg pipe tobacco.
Compared with prior art, the present invention has following beneficial effect:
1, tobacco of the present invention and spice berry mixed essential oil, can this perfume of harmony tobacco and spice berry note, solve preferably spice berry essential oil note in perfuming cigarette and too given prominence to, easily suppressed this fragrant shortcoming of tobacco, increase cigarette tobacco this fragrant in, give the spice berry note of cigarette harmony, increase the rich of cigarette flavor.
2, the present invention makes full use of tobacco and spice berry resource, develops natural, safe plant mixed essential oil, to developing unique essence spice for cigarette, provides space and using value widely.
Embodiment
In order to make object of the present invention, technical scheme and advantage clearer, below in conjunction with embodiment, the present invention is described in further detail.Should be appreciated that specific embodiment described herein is only in order to explain the present invention, the protection domain being not intended to limit the present invention.
Embodiment 1:
By 100kg flue-cured tobacco raw material and 10kg spice berry, spice berry is by lavandula angustifolia: after rose=1:1 compatibility mixes, add 330kg Petroleum ether extraction, concentrating under reduced pressure is removed sherwood oil, obtain the crude extract of tobacco-lavandula angustifolia-rose mixed essential oil, crude extract is carried out after deresination processing, send in the vaporizer of molecular distillation, under the distillation pressure of 0.1Pa, the distillation temperature of 60 ℃, carry out molecular distillation processing, collect front-end volatiles and be tobacco rose mixed essential oil.
Tobacco-lavandula angustifolia-rose mixed essential oil is dissolved and is mixed with perfuming solution by the mass ratio of 1:100 with dehydrated alcohol, then by the addition of 20mg/kg pipe tobacco, be evenly sprayed onto on pipe tobacco, and press the same manner preparation contrast, roll into cigarette and carry out sensory evaluating smoking.
Embodiment 2:
By 100kg Turkish tobaccos raw material and 1kg peppermint raw material, after mixing, add 505kg normal hexane extraction, concentrating under reduced pressure is removed normal hexane, obtain the crude extract of Turkish tobaccos peppermint mixed essential oil, crude extract is carried out after deresination processing, send in the vaporizer of molecular distillation, under the distillation pressure of 10Pa, the distillation temperature of 100 ℃, carry out molecular distillation processing, collect front-end volatiles and be Turkish tobaccos peppermint mixed essential oil.
Turkish tobaccos peppermint mixed essential oil is dissolved and is mixed with perfuming solution by the mass ratio of 1:100 with dehydrated alcohol, by the addition of 10mg/kg pipe tobacco, be evenly sprayed onto on pipe tobacco, and press the same manner preparation contrast, roll into cigarette and carry out sensory evaluating smoking.
Embodiment 3:
By 100kg burley tobaccos raw material and 0.5kg Stigma Croci raw material, after mixing, add 1005kg ether extraction, concentrating under reduced pressure is removed ether, obtain the crude extract of burley tobaccos Stigma Croci mixed essential oil, crude extract is carried out after deresination processing, send in the vaporizer of molecular distillation, under the distillation pressure of 50Pa, the distillation temperature of 150 ℃, carry out molecular distillation processing, collect front-end volatiles and be burley tobaccos Stigma Croci mixed essential oil.
Burley tobaccos Stigma Croci mixed essential oil is dissolved and is mixed with perfuming solution by the mass ratio of 1:100 with dehydrated alcohol, by the addition of 6mg/kg pipe tobacco, be evenly sprayed onto on pipe tobacco, and press the same manner preparation contrast, roll into cigarette and carry out sensory evaluating smoking.
Embodiment 4
By 100kg tobacco material and 4kg spice berry raw material, tobacco material is pressed flue-cured tobacco: Turkish tobaccos=1:1 compatibility, spice berry is pressed Flos Pelargonii: lemongrass=3:1 compatibility, after mixing, add 1560kg dichloromethane extraction, concentrating under reduced pressure is removed methylene dichloride, obtain the crude extract of tobacco-Flos Pelargonii-lemongrass mixed essential oil, crude extract is carried out after deresination processing, send in the vaporizer of molecular distillation, under the distillation pressure of 100Pa, the distillation temperature of 200 ℃, carry out molecular distillation processing, collect front-end volatiles and be tobacco-Flos Pelargonii-lemongrass mixed essential oil.
Tobacco-Flos Pelargonii-lemongrass mixed essential oil is dissolved and is mixed with perfuming solution by the mass ratio of 1:100 with 95% ethanol, by the addition of 4mg/kg pipe tobacco, be evenly sprayed onto on pipe tobacco, and press the same manner preparation contrast, roll into cigarette and carry out sensory evaluating smoking.
Embodiment 5
By 100kg tobacco material and 2kg spice berry raw material, tobacco material is pressed flue-cured tobacco: Turkish tobaccos: burley tobaccos=1:1:1 compatibility, spice berry is pressed Rosmarinus officinalis: lavandula angustifolia: jasmine=1:1:3 compatibility, after mixing, add 1020kg ethyl acetate to extract, concentrating under reduced pressure is removed ethyl acetate, obtain the crude extract of tobacco-Rosmarinus officinalis-lavandula angustifolia-jasmine mixed essential oil, crude extract is carried out after deresination processing, send in the vaporizer of molecular distillation, distillation pressure at 20Pa, under the distillation temperature of 120 ℃, carry out molecular distillation processing, collect front-end volatiles and be tobacco-Rosmarinus officinalis-lavandula angustifolia-jasmine mixed essential oil.
Tobacco-Rosmarinus officinalis-lavandula angustifolia-jasmine mixed essential oil is dissolved and is mixed with perfuming solution by the mass ratio of 1:100 with 95% ethanol, by the addition of 2mg/kg pipe tobacco, be evenly sprayed onto on pipe tobacco, after baking, roll into cigarette.And press the same manner preparation contrast, roll into cigarette and carry out sensory evaluating smoking.
Embodiment 6
By 100kg tobacco material and 1kg spice berry raw material, tobacco material is pressed flue-cured tobacco: Turkish tobaccos: burley tobaccos=2:1:1 compatibility, spice berry is pressed rose: chrysanthemum: cloves: Verbascum=3:1:1:1 compatibility, after mixing, add 1020kg dehydrated alcohol extraction, concentrating under reduced pressure is removed ethanol, obtain the crude extract of tobacco-rose-chrysanthemum-cloves-Verbascum mixed essential oil, crude extract is carried out after deresination processing, send in the vaporizer of molecular distillation, distillation pressure at 70Pa, under the distillation temperature of 180 ℃, carry out molecular distillation processing, collect front-end volatiles and be tobacco-rose-chrysanthemum-cloves-Verbascum mixed essential oil.
Tobacco-rose-chrysanthemum-cloves-Verbascum mixed essential oil is dissolved and is mixed with perfuming solution by the mass ratio of 1:100 with 95% ethanol, by the addition of 1mg/kg pipe tobacco, be evenly sprayed onto on pipe tobacco and by the same manner preparation contrast, roll into cigarette and carry out sensory evaluating smoking.
The foregoing is only preferred embodiment of the present invention, not in order to limit the present invention, all any modifications of doing within the spirit and principles in the present invention, be equal to and replace and improvement etc., within all should being included in protection scope of the present invention.
Claims (5)
1. one grow tobacco and spice berry mixed essential oil, by following methods, prepared:
After tobacco material and spice berry raw material are mixed by the mass ratio of 10:1～200:1, the organic solvent extraction that adds 3～15 times of raw materials quality, concentrating under reduced pressure is removed organic solvent, obtain the crude extract of tobacco-spice berry mixed essential oil, crude extract is carried out after deresination processing, send in the vaporizer of molecular distillation, under the distillation pressure of 0.1～100Pa, the distillation temperature of 60～200 ℃, carry out molecular distillation processing, collect front-end volatiles and obtain required tobacco and spice berry mixed essential oil.
2. tobacco according to claim 1 and spice berry mixed essential oil, is characterized in that: described tobacco material is preferably one or more in flue-cured tobacco, Turkish tobaccos, burley tobaccos.
3. tobacco according to claim 1 and spice berry mixed essential oil, is characterized in that: described spice berry raw material be preferably rose, Flos Pelargonii, lavandula angustifolia, Rosmarinus officinalis, one or more in peppermint, lemongrass, chrysanthemum, jasmine, cloves, Verbascum, Stigma Croci.
4. tobacco according to claim 1 and spice berry mixed essential oil, is characterized in that: described organic solvent is preferably a kind of in sherwood oil, normal hexane, ether, methylene dichloride, ethyl acetate, dehydrated alcohol.
5. tobacco claimed in claim 1 and the application of spice berry mixed essential oil in cigarette, be specially: described mixed essential oil and dehydrated alcohol or concentration mass percent 95% ethanol are dissolved and are mixed with perfuming solution by 1:100 mass ratio, and then be evenly sprayed onto on pipe tobacco in the mode of feeding in raw material by the addition of 1～20mg/kg pipe tobacco.
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| CN201310503696.5A CN103525553A (en) | 2013-10-23 | 2013-10-23 | Tobacco and spice plant mixing essence and application thereof |
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| CN201310503696.5A CN103525553A (en) | 2013-10-23 | 2013-10-23 | Tobacco and spice plant mixing essence and application thereof |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104939291A (en) * | 2015-05-08 | 2015-09-30 | 湖北中烟工业有限责任公司 | Method for enhancing inherent aroma of tobaccos by aid of natural plants |
| CN105268211A (en) * | 2015-11-30 | 2016-01-27 | 湖南省广林农业科技开发有限公司 | Method for extracting lipid-soluble component of rose |
| CN105542962A (en) * | 2015-12-25 | 2016-05-04 | 华宝食用香精香料（上海）有限公司 | Mixed essential oil as well as extraction method and application of mixed essential oil |
| CN105733960A (en) * | 2016-04-18 | 2016-07-06 | 云南中烟工业有限责任公司 | Trichoderma aureoviride strain and method for preparing luculia pinceana tobacco flavor from same |
| CN110527594A (en) * | 2019-09-06 | 2019-12-03 | 河北瑞龙生物科技有限公司 | A kind of plant extract essence and preparation method thereof |
| CN110663982A (en) * | 2019-11-12 | 2020-01-10 | 湖北中烟工业有限责任公司 | Preparation method and application of composite spice for cigarettes |
| CN110684599A (en) * | 2019-10-24 | 2020-01-14 | 江西中烟工业有限责任公司 | Preparation method of azalea absolute oil suitable for cigarettes |
| CN110693076A (en) * | 2019-08-07 | 2020-01-17 | 常德华馥生物技术有限公司 | Method for reducing Pb and As content in tobacco extract |
| CN110804497A (en) * | 2019-11-18 | 2020-02-18 | 湖北中烟工业有限责任公司 | Preparation method of saffron extract for tobacco bead blasting |
| CN111040876A (en) * | 2019-12-19 | 2020-04-21 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of natural spice suitable for cigarette bead blasting |
| CN112342086A (en) * | 2020-10-23 | 2021-02-09 | 新晃县华森科技有限责任公司 | Plant essential oil aroma enhancement refining method |
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| EP0822247A2 (en) * | 1996-07-29 | 1998-02-04 | Müller Extract Company GmbH | Tobacco aromatic oil substantially free of nicotine and method of preparation |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104939291A (en) * | 2015-05-08 | 2015-09-30 | 湖北中烟工业有限责任公司 | Method for enhancing inherent aroma of tobaccos by aid of natural plants |
| CN105268211A (en) * | 2015-11-30 | 2016-01-27 | 湖南省广林农业科技开发有限公司 | Method for extracting lipid-soluble component of rose |
| CN105542962A (en) * | 2015-12-25 | 2016-05-04 | 华宝食用香精香料（上海）有限公司 | Mixed essential oil as well as extraction method and application of mixed essential oil |
| CN105733960A (en) * | 2016-04-18 | 2016-07-06 | 云南中烟工业有限责任公司 | Trichoderma aureoviride strain and method for preparing luculia pinceana tobacco flavor from same |
| CN105733960B (en) * | 2016-04-18 | 2019-01-15 | 云南中烟工业有限责任公司 | A kind of trichoderma aureoviride bacterial strain and the method for preparing Dian clove tobacco aromaticss with it |
| CN110693076A (en) * | 2019-08-07 | 2020-01-17 | 常德华馥生物技术有限公司 | Method for reducing Pb and As content in tobacco extract |
| CN110527594A (en) * | 2019-09-06 | 2019-12-03 | 河北瑞龙生物科技有限公司 | A kind of plant extract essence and preparation method thereof |
| CN110684599A (en) * | 2019-10-24 | 2020-01-14 | 江西中烟工业有限责任公司 | Preparation method of azalea absolute oil suitable for cigarettes |
| CN110663982A (en) * | 2019-11-12 | 2020-01-10 | 湖北中烟工业有限责任公司 | Preparation method and application of composite spice for cigarettes |
| CN110804497A (en) * | 2019-11-18 | 2020-02-18 | 湖北中烟工业有限责任公司 | Preparation method of saffron extract for tobacco bead blasting |
| CN111040876A (en) * | 2019-12-19 | 2020-04-21 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of natural spice suitable for cigarette bead blasting |
| CN112342086A (en) * | 2020-10-23 | 2021-02-09 | 新晃县华森科技有限责任公司 | Plant essential oil aroma enhancement refining method |
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Application publication date: 20140122 |