CN102499465A - Preparation method of tobacco essence - Google Patents
Preparation method of tobacco essence Download PDFInfo
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- CN102499465A CN102499465A CN2011103714457A CN201110371445A CN102499465A CN 102499465 A CN102499465 A CN 102499465A CN 2011103714457 A CN2011103714457 A CN 2011103714457A CN 201110371445 A CN201110371445 A CN 201110371445A CN 102499465 A CN102499465 A CN 102499465A
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- essential oil
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Abstract
The invention provides a preparation method of tobacco essence. Tobacco is used as raw material; the tobacco raw material is added to a distillation vessel; polyol cosolvents of which the weight is 5 to 15 times of that of the tobacco raw material is taken and added into the distillation vessel, and then carrying solvents of which the weight is 2 to 8 times of that of the tobacco raw material is taken; carrying solvents of which the weight is 0.5 to 2 times of that of the tobacco raw material is firstly added to the distillation vessel, evenly mixed with the tobacco raw material and the polyol cosolvents, and then heated to conduct distillation; when a fraction flows out, an operator begins to drip the rest carrying solvents into the distillation vessel; after all the carrying solvents are dripped, the mixture is continuously distilled until no fraction flows out; and a collected transparent fraction is the tobacco essence. By adopting the preparation method, tobacco perfume, namely the tobacco essence which achieves a unique aroma-increasing effect, can be prepared.
Description
Technical field
The tobacco spice that the present invention relates to have the flavouring effect is a tobacco essential oil preparing technical field.
Background technology
In order to improve the security of smoking, the requirement of the cigarette low tar being hanged down harmfulness is improving constantly.At present, reduce the important topic that tar content has become production of cigarettes, and the many fragrance matters in the tobacco are present among the tar; Be accompanied by the reduction of tar content, smoke is thin out, and fragrance weakens; Cigarette product loses original style, is difficult to accepted by the consumer.So in the cigarette lowering harm and decreasing coking, promote and improve flue gas concentration and fragrance, be a urgent problem that solves, the mode through flavoring and casing can remedy the insufficient fragrance part on the cigarette tobacco leaf formulation.But the essence spice for cigarette there be limited evidence currently of with individual style, therefore developing the essence spice for cigarette with peat-reek becomes trend.
Summary of the invention
The objective of the invention is to solve the deficiency of prior art, a kind of method that the tobacco spice with unique flavouring effect is the tobacco essential oil for preparing is provided.
The object of the invention is realized through following technical scheme.
One grow tobacco essential oil the preparation method, be to be raw material with the tobacco, tobacco material is added distil container; The polyalcohols cosolvent of getting 5～15 times of tobacco material weight adds distil container, gets the solvent that carries of 2～8 times of tobacco material weight again, and the solvent that carries with 0.5～2 times of tobacco material weight adds distil container earlier; Mixing, heating is distilled then, when having treated that cut flows out; Beginning drips the remaining solvent that carries in distil container; Carry after solvent drips, continue to be distilled to no cut again and flow out, the transparence cut of collection is the tobacco essential oil.
Tobacco material of the present invention is one or more in flue-cured tobacco, airing cigarette, Turkish tobaccos, the burley tobaccos.Described polyalcohols cosolvent is one or more in propane diols, glycerine, the butanediol.The described solvent that carries is the alcohol type goods.Said alcohol type goods are one or more in liquor, yellow rice wine, fruit wine, beer, medicinal liquor and the edible alcohol.
The present invention is directed to the characteristic of heterogeneity tobacco, is raw material with the tobacco, utilizes the method for distillation to prepare essential oil.This distil process is different with traditional water steam distillation technology, is to adopt high boiling polyol class organic solvent as cosolvent, adds low boiling alcohol type solvent as carrying solvent; Heating is distilled, and its technology is simple, easily operation; Cost is low, and the cut that distills is a transparence, need not carry out post processing; Shortened manufacturing cycle, and the used raw material of the present invention is within the cigarette additive raw material range.
The present invention makes full use of the tobacco resource, and exploitation tobacco endogenous essence spice for cigarette gives cigarette unique style and features, to developing unique essence spice for cigarette space and using value widely is provided.
The specific embodiment
Further set forth content of the present invention below in conjunction with embodiment.
One grow tobacco essential oil the preparation method, be to be raw material with the tobacco, tobacco material is added distil container; The polyalcohols cosolvent of getting 5～15 times of tobacco material weight adds distil container, gets the solvent that carries of 2～8 times of tobacco material weight again, and the solvent that carries with 0.5～2 times of tobacco material weight adds distil container earlier; Mixing, heating is distilled then, when having treated that cut flows out; Beginning drips the remaining solvent that carries in distil container; Carry after solvent drips, continue to be distilled to no cut again and flow out, the transparence cut of collection is the tobacco essential oil.
Tobacco material of the present invention is one or more in flue-cured tobacco, airing cigarette, Turkish tobaccos, the burley tobaccos.Described polyalcohols cosolvent is one or more in propane diols, glycerine, the butanediol.The described solvent that carries is the alcohol type goods, comprises in liquor, yellow rice wine, fruit wine, beer, medicinal liquor and the edible alcohol one or more.
Embodiment 1:
Get 200g flue-cured tobacco raw material, place distil container, press raw material weight and in distil container, add 5 times of propane diols.Select liquor as carrying solvent, the interpolation total amount is 6 times of material quantity.Before beginning distillation, the liquor that adds 1 times of weight of raw material earlier shakes up in distil container; Heating is distilled then, has treated to pick up counting when cut flows out, and drips remaining liquor; After treating that liquor is added dropwise to complete; Continue to be distilled to no cut and flow out, stop distillation, collected transparence cut is the tobacco essential oil.
Embodiment 2:
Get 200g airing cigarette, place distil container, add 10 times of cosolvents in the raw material weight ratio, cosolvent is in propane diols: glycerine: butanediol is the ratio compatibility of 2:1:1.Carrying solvent is yellow rice wine, and addition is 8 times of material quantity.Before beginning distillation, add 2 times earlier and carry solvent in distil container, shake up; Heating is distilled, and has treated to pick up counting when cut flows out, and drips the remaining solvent that carries; After solvent to be carried is added dropwise to complete; Continue to be distilled to no cut and flow out, stop distillation, collected transparence cut is the tobacco essential oil.
Embodiment 3
Get 200g mixing tobacco leaf, this mixing tobacco leaf, will be mixed tobacco leaf and place distil container according to the 1:1:2:1 compatibility by airing cigarette, flue-cured tobacco, burley tobaccos, Turkish tobaccos, add 12 times of glycerine in the raw material weight ratio; Carrying solvent is rice wine, and addition is 2 times of material quantity, before beginning distillation; Add 0.5 times earlier and carry solvent in distil container, shake up, heating is distilled; Treated to pick up counting when cut flows out, dripped the remaining solvent that carries, after solvent to be carried is added dropwise to complete; Continue to be distilled to no cut and flow out, stop distillation, collected cut is the tobacco essential oil.
Embodiment 4
Get 200g Turkish tobaccos raw material, place distil container, add 15 times of butanediols in the material quantity ratio, carrying solvent is that fruit wine, yellow rice wine are in 1:1 ratio compatibility; Addition is 5 times of material quantity, before beginning distillation, adds 1 times earlier and carries solvent in distil container, shakes up; Heating is distilled, and has treated to pick up counting when cut flows out, and drips the remaining solvent that carries, after solvent to be carried is added dropwise to complete; Continue to be distilled to no cut and flow out, stop distillation, collected cut is the tobacco essential oil.
Embodiment 5
Get 200g burley tobaccos raw material, place distil container, add 8 times of glycerine in the raw material weight ratio, carrying solvent is fruit wine; Addition is 6 times, before beginning distillation, adds 0.5 times earlier and carries solvent in distil container, shakes up; Heating is distilled, and has treated to pick up counting when cut flows out, and drips the remaining solvent that carries, after solvent to be carried is added dropwise to complete; Continue to be distilled to no cut and flow out, stop distillation, collected cut is the tobacco essential oil.
Embodiment 6
Get 200g airing cigarette, place distil container, add 10 times of butanediols in the raw material weight ratio; Carry solvent and be medicinal liquor, liquor, beer, yellow rice wine, fruit wine in 1:1:1:1:1 ratio compatibility, addition is 8 times, before beginning distillation; Add 2 times earlier and carry solvent in distil container, shake up, heating is distilled; Treated to pick up counting when cut flows out, dripped the remaining solvent that carries, after solvent to be carried is added dropwise to complete; Continue to be distilled to no cut and flow out, stop distillation, collected transparence cut is the tobacco essential oil.
Claims (5)
- One grow tobacco essential oil the preparation method, it is characterized in that, be raw material with the tobacco; Tobacco material is added distil container, and the polyalcohols cosolvent of getting 5～15 times of tobacco material weight adds distil container, gets the solvent that carries of 2～8 times of tobacco material weight again; The solvent that carries with 0.5～2 times of tobacco material weight adds distil container earlier, mixing, and heating is distilled then; When having treated that cut flows out, beginning remaining solvent that carries of dropping in the distil container carries after solvent drips; Continue to be distilled to no cut again and flow out, the transparence cut of collection is the tobacco essential oil.
- 2. according to claim 1 one grow tobacco essential oil the preparation method, it is characterized in that described tobacco material is one or more in flue-cured tobacco, airing cigarette, Turkish tobaccos, the burley tobaccos.
- 3. according to claim 1 one grow tobacco essential oil the preparation method, it is characterized in that described polyalcohols cosolvent is one or more in propane diols, glycerine, the butanediol.
- 4. according to claim 1 one grow tobacco essential oil the preparation method, it is characterized in that the described solvent that carries is the alcohol type goods.
- 5. according to claim 4 one grow tobacco essential oil the preparation method, it is characterized in that described alcohol type goods are one or more in liquor, yellow rice wine, fruit wine, beer, medicinal liquor and the edible alcohol.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110371445 CN102499465B (en) | 2011-11-21 | 2011-11-21 | Preparation method of tobacco essence |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201110371445 CN102499465B (en) | 2011-11-21 | 2011-11-21 | Preparation method of tobacco essence |
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| CN102499465A true CN102499465A (en) | 2012-06-20 |
| CN102499465B CN102499465B (en) | 2013-09-25 |
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| CN 201110371445 Active CN102499465B (en) | 2011-11-21 | 2011-11-21 | Preparation method of tobacco essence |
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Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103242959A (en) * | 2013-05-15 | 2013-08-14 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of tobacco chrysanthemum absolute oil |
| CN103387875A (en) * | 2013-07-31 | 2013-11-13 | 浙江中烟工业有限责任公司 | Aromatic tobacco propylene glycol aqueous solution extract, and preparation method and application thereof |
| CN103484252A (en) * | 2013-09-11 | 2014-01-01 | 上海聚华科技股份有限公司 | Zimbabwe tobacco essential oil preparation method |
| CN103525553A (en) * | 2013-10-23 | 2014-01-22 | 红云红河烟草(集团)有限责任公司 | Mixed essential oil of tobacco and spice plants and application thereof |
| CN103627525A (en) * | 2013-09-11 | 2014-03-12 | 上海聚华科技股份有限公司 | Method for preparing tobacco essential oil by reduced pressure distillation |
| CN104026728A (en) * | 2014-06-25 | 2014-09-10 | 湖南中烟工业有限责任公司 | Electronic tobacco juice with baking aroma |
| CN104068469A (en) * | 2014-06-25 | 2014-10-01 | 湖南中烟工业有限责任公司 | Nicotine liquid with smoky aromas |
| CN105146739A (en) * | 2015-07-28 | 2015-12-16 | 中国烟草总公司郑州烟草研究院 | Preparation method and application of Jin Tang tobacco essential oil |
| CN105199848A (en) * | 2015-09-07 | 2015-12-30 | 郑小柏 | Method for preparing flavor substance |
| CN106085603A (en) * | 2016-07-21 | 2016-11-09 | 武汉黄鹤楼香精香料有限公司 | A kind of cigarette paper colourless tobacco extract and preparation method thereof |
| CN108347993A (en) * | 2015-11-27 | 2018-07-31 | 菲利普莫里斯生产公司 | Method and apparatus for obtaining tobacco spice extract |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103242959A (en) * | 2013-05-15 | 2013-08-14 | 云南瑞升烟草技术（集团）有限公司 | Preparation method of tobacco chrysanthemum absolute oil |
| CN103387875B (en) * | 2013-07-31 | 2014-10-29 | 浙江中烟工业有限责任公司 | Aromatic tobacco propylene glycol aqueous solution extract, and preparation method and application thereof |
| CN103387875A (en) * | 2013-07-31 | 2013-11-13 | 浙江中烟工业有限责任公司 | Aromatic tobacco propylene glycol aqueous solution extract, and preparation method and application thereof |
| CN103484252A (en) * | 2013-09-11 | 2014-01-01 | 上海聚华科技股份有限公司 | Zimbabwe tobacco essential oil preparation method |
| CN103627525A (en) * | 2013-09-11 | 2014-03-12 | 上海聚华科技股份有限公司 | Method for preparing tobacco essential oil by reduced pressure distillation |
| CN103525553A (en) * | 2013-10-23 | 2014-01-22 | 红云红河烟草(集团)有限责任公司 | Mixed essential oil of tobacco and spice plants and application thereof |
| CN104068469B (en) * | 2014-06-25 | 2016-07-27 | 湖南中烟工业有限责任公司 | A kind of electronic cigarette liquid with sootiness fragrance |
| CN104068469A (en) * | 2014-06-25 | 2014-10-01 | 湖南中烟工业有限责任公司 | Nicotine liquid with smoky aromas |
| CN104026728B (en) * | 2014-06-25 | 2016-02-10 | 湖南中烟工业有限责任公司 | A kind of electronic cigarette liquid with baking fragrance |
| CN104026728A (en) * | 2014-06-25 | 2014-09-10 | 湖南中烟工业有限责任公司 | Electronic tobacco juice with baking aroma |
| CN105146739A (en) * | 2015-07-28 | 2015-12-16 | 中国烟草总公司郑州烟草研究院 | Preparation method and application of Jin Tang tobacco essential oil |
| CN105146739B (en) * | 2015-07-28 | 2016-07-20 | 中国烟草总公司郑州烟草研究院 | The preparation method of a kind of mao of cigarette quintessence oil and application thereof |
| CN105199848A (en) * | 2015-09-07 | 2015-12-30 | 郑小柏 | Method for preparing flavor substance |
| CN108347993A (en) * | 2015-11-27 | 2018-07-31 | 菲利普莫里斯生产公司 | Method and apparatus for obtaining tobacco spice extract |
| US11044938B2 (en) | 2015-11-27 | 2021-06-29 | Philip Morris Products S.A. | Process and apparatus to obtain tobacco flavor extracts |
| CN108347993B (en) * | 2015-11-27 | 2022-03-25 | 菲利普莫里斯生产公司 | Method and apparatus for obtaining a tobacco flavor extract |
| CN106085603A (en) * | 2016-07-21 | 2016-11-09 | 武汉黄鹤楼香精香料有限公司 | A kind of cigarette paper colourless tobacco extract and preparation method thereof |
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