CN102920008B - Preparation method of burley tobacco shreds for cigarettes - Google Patents
Preparation method of burley tobacco shreds for cigarettes Download PDFInfo
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- CN102920008B CN102920008B CN201210388836.4A CN201210388836A CN102920008B CN 102920008 B CN102920008 B CN 102920008B CN 201210388836 A CN201210388836 A CN 201210388836A CN 102920008 B CN102920008 B CN 102920008B
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- 241000208125 Nicotiana Species 0.000 title claims abstract description 68
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 68
- 235000019504 cigarettes Nutrition 0.000 title claims abstract description 24
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 238000000034 method Methods 0.000 claims abstract description 12
- 241000167854 Bourreria succulenta Species 0.000 claims abstract description 8
- 235000019693 cherries Nutrition 0.000 claims abstract description 8
- 238000000605 extraction Methods 0.000 claims description 28
- 239000000284 extract Substances 0.000 claims description 16
- WHUUTDBJXJRKMK-UHFFFAOYSA-N Glutamic acid Natural products OC(=O)C(N)CCC(O)=O WHUUTDBJXJRKMK-UHFFFAOYSA-N 0.000 claims description 14
- 235000013922 glutamic acid Nutrition 0.000 claims description 14
- 239000004220 glutamic acid Substances 0.000 claims description 14
- 235000009754 Vitis X bourquina Nutrition 0.000 claims description 6
- 235000012333 Vitis X labruscana Nutrition 0.000 claims description 6
- 235000014787 Vitis vinifera Nutrition 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 6
- 238000010992 reflux Methods 0.000 claims description 6
- 239000003643 water by type Substances 0.000 claims description 6
- 241000220225 Malus Species 0.000 claims description 4
- 235000011430 Malus pumila Nutrition 0.000 claims description 4
- 235000015103 Malus silvestris Nutrition 0.000 claims description 4
- 230000001476 alcoholic effect Effects 0.000 claims description 3
- 240000006365 Vitis vinifera Species 0.000 claims 1
- 238000007654 immersion Methods 0.000 claims 1
- 150000001413 amino acids Chemical class 0.000 abstract description 17
- 241000196324 Embryophyta Species 0.000 abstract description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 abstract description 10
- 235000013399 edible fruits Nutrition 0.000 abstract description 7
- 210000000214 mouth Anatomy 0.000 abstract description 3
- 230000000391 smoking effect Effects 0.000 abstract description 3
- 241000219094 Vitaceae Species 0.000 abstract description 2
- 235000021021 grapes Nutrition 0.000 abstract description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 2
- 238000002791 soaking Methods 0.000 abstract 3
- 238000001035 drying Methods 0.000 abstract 2
- 244000141359 Malus pumila Species 0.000 abstract 1
- 235000021016 apples Nutrition 0.000 abstract 1
- 238000007865 diluting Methods 0.000 abstract 1
- 230000007794 irritation Effects 0.000 abstract 1
- 230000001007 puffing effect Effects 0.000 abstract 1
- 235000001014 amino acid Nutrition 0.000 description 15
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- KDXKERNSBIXSRK-UHFFFAOYSA-N Lysine Natural products NCCCCC(N)C(O)=O KDXKERNSBIXSRK-UHFFFAOYSA-N 0.000 description 8
- 239000004472 Lysine Substances 0.000 description 8
- 239000003205 fragrance Substances 0.000 description 8
- 241000227425 Pieris rapae crucivora Species 0.000 description 6
- 241000219095 Vitis Species 0.000 description 5
- OWEGMIWEEQEYGQ-UHFFFAOYSA-N 100676-05-9 Natural products OC1C(O)C(O)C(CO)OC1OCC1C(O)C(O)C(O)C(OC2C(OC(O)C(O)C2O)CO)O1 OWEGMIWEEQEYGQ-UHFFFAOYSA-N 0.000 description 4
- GUBGYTABKSRVRQ-PICCSMPSSA-N Maltose Natural products O[C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@@H]1O[C@@H]1[C@@H](CO)OC(O)[C@H](O)[C@H]1O GUBGYTABKSRVRQ-PICCSMPSSA-N 0.000 description 4
- 239000007789 gas Substances 0.000 description 4
- 239000000203 mixture Substances 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 description 3
- WHUUTDBJXJRKMK-VKHMYHEASA-N L-glutamic acid Chemical compound OC(=O)[C@@H](N)CCC(O)=O WHUUTDBJXJRKMK-VKHMYHEASA-N 0.000 description 3
- GUBGYTABKSRVRQ-QUYVBRFLSA-N beta-maltose Chemical compound OC[C@H]1O[C@H](O[C@H]2[C@H](O)[C@@H](O)[C@H](O)O[C@@H]2CO)[C@H](O)[C@@H](O)[C@@H]1O GUBGYTABKSRVRQ-QUYVBRFLSA-N 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- 229960002715 nicotine Drugs 0.000 description 3
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 description 3
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 2
- 239000000796 flavoring agent Substances 0.000 description 2
- 235000019634 flavors Nutrition 0.000 description 2
- 239000003546 flue gas Substances 0.000 description 2
- 229940068517 fruit extracts Drugs 0.000 description 2
- 239000002304 perfume Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 244000131316 Panax pseudoginseng Species 0.000 description 1
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 description 1
- 235000003140 Panax quinquefolius Nutrition 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000004075 alteration Effects 0.000 description 1
- -1 amino class organic compound Chemical class 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000011156 evaluation Methods 0.000 description 1
- 238000011049 filling Methods 0.000 description 1
- 235000008434 ginseng Nutrition 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 210000000867 larynx Anatomy 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000003672 processing method Methods 0.000 description 1
- 150000003216 pyrazines Chemical class 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 230000001953 sensory effect Effects 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 210000003462 vein Anatomy 0.000 description 1
Abstract
The invention discloses a preparation method of burley tobacco shreds for cigarettes. The preparation method comprises the following steps of: firstly soaking the burley tobacco shreds by using a soaking solution, then removing the solution, drying, cutting the burley tobacco shreds into slices, and finally drying and puffing. The soaking solution is prepared from natural plant fruit and amino acids by adopting the following steps of: extracting the natural plant fruit by using 5-10 times by weight of edible alcohol with the mass concentration of 55-65%, then concentrating the extracting solution into extractum with the relative density of 1.1-1.5, adding the amino acids according to 0.5-3% of the weight of the extractum, and finally diluting with water into 5-20 times. The natural plant fruit is selected from one or more of grapes, cherries and apples. The burley tobacco shreds prepared by the method have high smoking quality reflected in the terms that offensive odor and irritation are reduced and oral cavity is clean; and the burley tobacco shreds can be used for various cigarettes and have wide application range.
Description
Technical field
The invention belongs to tobacco industry burley tobaccos silk processing technique field, be specifically related to the preparation method of a kind of cigarette burley tobaccos silk.
Background technology
Burley tobaccos are by the sudden change of Maryland dark sun-cured tobacco kind, and stem and vein are creamy white, and are different from other tobacco.Its cultural method is similar to flue-cured tobacco, after ripe harvesting, hangs in dry in the air canopy or the room that dries in the air and dries.Burley tobaccos moisture is higher, and blade is thin and light, institutional framework is loosened and not coarse, and elasticity is strong, and filling value is high, absorbs fragrance performance good, and nicotine and total nitrogen content are higher than flue-cured tobacco, and flue gas strength is large, and sugar content is low, has very strong absorbability.Burley tobaccos have the fragrance of mediation and jealous effect, are the important source material of blended type cigarette, are also pipe tobacco raw materials.Simple and elegant fragrant category cigarette is the new category cigarette of one taking Yellow Crane Tower brand as representative, realized alcohol and the one integrated mass of this perfume of tobacco and simple and elegant natural herbal plant flavour, there is the principal character of " fragrance is elegant, thoroughly good, the low evil of the property the sent out larynx that relaxes ".Because the nitrogen content of burley tobaccos is high, sugar content is low, therefore burley tobaccos bitter taste in combustion process is heavier, assorted gas is heavy, it is large to stimulate, has affected the quality of cigarette, has limited the use of burley tobaccos silk in simple and elegant fragrant category cigarette product.
Summary of the invention
The object of the present invention is to provide the preparation method of a kind of cigarette burley tobaccos silk, to overcome the poor defect of existing cigarette burley tobaccos silk suction quality, expand the range of application of burley tobaccos silk in simple and elegant fragrant category cigarette product.
Above-mentioned purpose is achieved through the following technical solutions:
The preparation method of burley tobaccos silk for a kind of cigarette, comprise burley tobaccos are first soaked with soak, then dry, the section of de-liquid, throwing, finally dry expanded step, described soak adopts following methods to make by natural plants fruit and amino acid: after the edible alcohol that is 55-65% by the mass concentration of 5-10 times of weight of natural plants fruit extracts, extract is condensed into the medicinal extract that relative density is 1.1-1.5, add amino acid by the 0.5-3% of medicinal extract weight, last dilute with water 5-12 doubly
Described natural plants fruit is selected from one or more in grape, cherry, apple.
Preferred soak preparation method is: after the edible alcohol that is 60% by the mass concentration of 8 times of weight of natural plants fruit extracts, it is 1.25 medicinal extract that extract is condensed into relative density, adds amino acid, finally 10 times of dilute with waters by 1% of medicinal extract weight.
Preferred natural plants fruit is the combination of three kinds of grapes, cherry, apple, and the weight ratio of described grape, cherry, apple is followed successively by 5:4:1.The burley tobaccos silk fragrance that adopts this formula to make is the denseest, and assorted gas is minimum, excitant minimum.
Preferably, by described burley tobaccos under 40-60 DEG C of condition, with soak soak 25-35 minute.Can make sugar and amino acid in soak be absorbed more fully by burley tobaccos.
Preferably, be also included in section and add sugar and amino acid whose step after throwing, described sugar and amino acid whose weight ratio are 1-3:1, and described sugar and amino acid whose gross weight account for the 4-8% of burley tobaccos weight.After section throwing, can strengthen Maillard reaction with the expanded front interpolation sugar of oven dry and amino acid, generate more fragrance matter, further improve the quality of burley tobaccos silk.
Further preferred scheme is: described sugar and amino acid whose weight ratio are 2:1, and described sugar and amino acid whose gross weight account for 4.5% of burley tobaccos weight.
Amino acid is the general name that contains the amino class organic compound with an acid carboxyl of alkalescence, and can be used for amino acid of the present invention is in glutamic acid or lysine or its mixture.
Galactolipin or maltose or its mixture for sugar of the present invention.
Because the extraction solvent of natural plants fruit is to hold volatile edible alcohol, therefore the mode of extracting is conventional refluxing extraction, this is extracted in airtight container and carries out, after heating, the alcohol of volatilization flow back into again in extraction vessel after condensation, iterative cycles, the method has not only been avoided the volatilization of alcohol, and has higher extraction efficiency.The temperature that reflow of alcohol is extracted is generally 50-80 DEG C; the time of extracting is generally 1-3 hour; the number of times extracting is generally 1-3 time, and these parameters are that those of ordinary skill in the art can both grasp on the basis of limited number of times test, therefore do not include the claimed scope of patent in.
In soak of the present invention, be rich in multiple reducing sugar and amino acid, burley tobaccos are soaked with it, reducing sugar and amino acid are absorbed by burley tobaccos, when expanded, can there is Maillard reaction in amino acid and reducing sugar, generate a large amount of pyrazine class fragrance matters, and reactant color is dark-brown under hot conditions, be conducive to improve the quality of burley tobaccos silk, avoided pipe tobacco disastrously to join problem in process, the problem includes: aberration problem simultaneously.
The invention has the beneficial effects as follows: the cigarette burley tobaccos silk suction quality that the present invention makes is good, is embodied in: assorted gas reduces, and excitant reduces, and oral cavity is cleaner, and pleasant impression is few.The burley tobaccos silk that the present invention makes can be used for various cigarette, applied range.
Detailed description of the invention
Embodiment 1
A preparation method for burley tobaccos silks for cigarette, first by burley tobaccos under 45 DEG C of conditions, soak 30 minutes with soak, then dry, the section throwing of de-liquid, finally dry expanded.Described soak adopts following methods to make: by after the edible alcohol extraction of 5 times of amount (weight) 65% of grape, be condensed into relative density and be 1.1 medicinal extract, add glutamic acid, finally 5 times of dilute with waters by 0.5% of medicinal extract weight.Described extraction is refluxing extraction, and extracting temperature is 70 DEG C, and extraction time is 2 hours, and extraction time is 2 times.After described section throwing, add in addition the step of maltose and glutamic acid, the weight ratio of maltose and glutamic acid is 2:1, and the total amount of maltose and glutamic acid accounts for 4.5% of section white rib cigarette sheet weight.
Embodiment 2
A preparation method for burley tobaccos silks for cigarette, first by burley tobaccos under 60 DEG C of conditions, soak 25 minutes with soak, then dry, the section throwing of de-liquid, finally dry expanded.Described soak adopts following methods to make: after the edible alcohol of 10 times of amount (weight) 55% of cherry is extracted, being condensed into relative density is 1.5 medicinal extract, adds lysine by 3% of medicinal extract weight, 12 times of last dilute with waters.Described extraction is refluxing extraction, and extracting temperature is 80 DEG C, and extraction time is 3 hours, and extraction time is 1 time.After described section throwing, add in addition the step of galactolipin and lysine, the weight ratio of galactolipin and lysine is 1:1, and the total amount of galactolipin and lysine accounts for 4% of the rear white rib cigarette sheet weight of section.
Embodiment 3
A preparation method for burley tobaccos silks for cigarette, first by burley tobaccos under 40 DEG C of conditions, soak 35 minutes with soak, then dry, the section throwing of de-liquid, finally dry expanded.Described soak adopts following methods to make: by after grape, the alcoholic extraction of cherry (weight ratio is 1:1) by 8 times of amount (weight) 60%, be condensed into relative density and be 1.25 medicinal extract, add glutamic acid by 1% of medicinal extract weight, 10 times of last dilute with waters.Described extraction is refluxing extraction, and extracting temperature is 60 DEG C, and extraction time is 1 hour, and extraction time is 3 times.After described section throwing, add in addition the step of galactolipin and lysine, the weight ratio of galactolipin and lysine is 1.5:1, and the total amount of galactolipin and lysine accounts for 4.5% of the rear white rib cigarette sheet weight of section.
Embodiment 4
A preparation method for burley tobaccos silks for cigarette, first by burley tobaccos under 30 DEG C of conditions, soak 40 minutes with soak, then dry, the section throwing of de-liquid, finally dry expanded.Described soak adopts following methods to make: by after grape, cherry, the alcoholic extraction of apple (weight ratio is 5:4:1) by 10 times of amount (weight) 60%, be condensed into relative density and be 1.25 medicinal extract, add glutamic acid by 3% of medicinal extract weight, 10 times of last dilute with waters.Described extraction is refluxing extraction, and extracting temperature is 80 DEG C, and extraction time is 1 hour, and extraction time is 3 times.After described section throwing, add in addition the step of galactolipin and glutamic acid, the weight ratio of galactolipin and glutamic acid is 3:1, the total amount of galactolipin and glutamic acid account for section throwing after burley tobaccos silk weight 5%.
Burley tobaccos silk prepared by embodiment and common white rib pipe tobacco carry out chemical composition contrast, the results are shown in Table 1.Total reducing sugar, the content of reducing sugar of the burley tobaccos silk that the present invention makes are higher than common white rib pipe tobacco, and total nitrogen, nicotine content are low, are conducive to the improvement of interior quality.Sugared ginseng and Maillard reaction synthesize flavor matter, are conducive to increase feature perfume (or spice).
Burley tobaccos silk and common white rib pipe tobacco chemical analysis comparing result that table 1 adopts the present invention to prepare
Processing method | Total reducing sugar % | Reduced sugar % | Total nitrogen % | Nicotine % |
Common white rib pipe tobacco | 5.37 | 3.87 | 3.91 | 2.38 |
Embodiment 1 burley tobaccos silk | 7.67 | 6.12 | 3.89 | 2.15 |
Embodiment 2 burley tobaccos silks | 7.61 | 6.05 | 3.84 | 2.21 |
Embodiment 3 burley tobaccos silks | 7.50 | 6.11 | 3.77 | 2.26 |
Embodiment 4 burley tobaccos silks | 7.69 | 6.15 | 3.65 | 2.12 |
The burley tobaccos silk and the common white rib pipe tobacco that adopt the present invention to prepare, mix to fit in certain flue-cured tobacco group according to 8% ratio and aspirate, and the fragrance while comparing smoking by method of comparison and jealous, carries out sensory evaluation by the special personnel that smoke panel test, and comparing result is in table 2.Found that, burley tobaccos silk comparison common white rib pipe tobacco prepared by the present invention, fragrance increases, and flue gas is smooth and easy soft, and assorted gas reduces, and oral cavity is clean, and overall assessment is better than the latter.
Table 2 is mixed the smoking result after burley tobaccos silk
Claims (1)
1. the preparation method of a cigarette use burley tobaccos silk, it is characterized in that: first by burley tobaccos under 30 DEG C of conditions, with soak immersion 40 minutes, then dry, the section throwing of de-liquid, finally dry expandedly, described soak adopts following methods to make: get grape, cherry, apple by weight the ratio for 5:4:1, after the alcoholic extraction by 10 times of weight 60%, be condensed into relative density and be 1.25 medicinal extract, add glutamic acid by 3% of medicinal extract weight, 10 times of last dilute with waters
Described extraction is refluxing extraction, and extracting temperature is 80 DEG C, and extraction time is 1 hour, and extraction time is 3 times,
After described section throwing, add in addition the step of galactolipin and glutamic acid, the weight ratio of described galactolipin and glutamic acid is 3:1, the total amount of galactolipin and glutamic acid account for section throwing after burley tobaccos silk weight 5%.
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Families Citing this family (5)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104188089A (en) * | 2014-08-20 | 2014-12-10 | 云南中烟工业有限责任公司 | Application of green plum extractives in cigarettes |
CN104432460A (en) * | 2014-08-20 | 2015-03-25 | 云南中烟工业有限责任公司 | Application of preserved plum extractives in cigarettes |
CN104687241B (en) * | 2015-01-21 | 2017-02-22 | 中国烟草总公司郑州烟草研究院 | Preparation method of tobacco sauce additive capable of improving smoking quality of cut tobacco stems as well as application of tobacco sauce additive |
CN109757782A (en) * | 2019-03-05 | 2019-05-17 | 铂德(深圳)科技有限公司 | Grape extract solution, grape electronics tobacco tar and preparation method thereof |
CN111418884B (en) * | 2020-05-20 | 2021-12-21 | 云南如茨生物科技有限公司 | Cigarette spice |
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US3920026A (en) * | 1972-03-07 | 1975-11-18 | Liggett & Myers Inc | Tobacco with flavor enhancer |
CN1175623A (en) * | 1995-09-05 | 1998-03-11 | 云南省烟草工业研究所 | Method for preparing tobacco reacting substance perfume and its use |
CN101268857B (en) * | 2008-06-02 | 2010-06-02 | 厦门烟草工业有限责任公司 | Process technique for burley tobacco in blend type cigarette |
CN101608145B (en) * | 2008-06-16 | 2012-08-29 | 湖北中烟工业有限责任公司 | Method for producing flavor for tobacco by using plant hydrolyzed extract and fruit extract as raw materials |
CN101999753B (en) * | 2010-11-19 | 2013-01-02 | 湖北中烟工业有限责任公司 | Method for processing burley tobacco and application thereof to cigarette |
CN102100397B (en) * | 2010-12-22 | 2013-04-10 | 湖南中烟工业有限责任公司 | Flavoring essence for tobacco and preparation method thereof |
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